Synthesis of catena -Poly[[di-aqua(2,2′-bipyridine)copper(II)]- μ -sulfato-κ 2 O:O'] 1D coordination polymer and [di-chloro(2,2′-bipyridine)copper(II)] complex, redetermination of their crystal structures

The title compounds [Cu(bpy)(H2O)2(SO4)] n (1) and [Cu(bpy)Cl2] (2) were successfully synthesized, and their crystal structures were redetermined as some corrections were needed. The Cu(II) centers in 1 are coordinated in elongated octahedral geometry by the two nitro...
Ausführliche Beschreibung

Gespeichert in:

Autor*in:	Yilmaz, İsmail [verfasserIn]

Format:	E-Artikel
Sprache:	Englisch

Erschienen:	2023

Schlagwörter:	Copper(II) complex Bipyridine Coordination polymer Crystal structure Redetermination

Übergeordnetes Werk:	Enthalten in: Polyhedron - Amsterdam [u.a.] : Elsevier Science, 1982, 250
Übergeordnetes Werk:	volume:250

DOI / URN:	10.1016/j.poly.2023.116816

Katalog-ID:	ELV066765471

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100	1		\|a Yilmaz, İsmail \|e verfasserin \|0 (orcid)0000-0002-0139-0122 \|4 aut
245	1	0	\|a Synthesis of catena -Poly[[di-aqua(2,2′-bipyridine)copper(II)]- μ -sulfato-κ 2 O:O'] 1D coordination polymer and [di-chloro(2,2′-bipyridine)copper(II)] complex, redetermination of their crystal structures
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520			\|a The title compounds [Cu(bpy)(H2O)2(SO4)] n (1) and [Cu(bpy)Cl2] (2) were successfully synthesized, and their crystal structures were redetermined as some corrections were needed. The Cu(II) centers in 1 are coordinated in elongated octahedral geometry by the two nitrogen atoms of a bpy ligand and four oxygen atoms belonging to aqua molecules and sulfato ligands, forming a polymeric chain by bridging the sulfato ligands. The Cu(II) center in 2 is coordinated by the two chloride ions and the two nitrogen atoms of the bipyridine ligand, forming a distorted square planar geometry. The [Cu(bpy)(H2O)2(SO4)] n complex crystallizes in the monoclinic crystal system with space group C2/c. The unit cell parameters were determined to be a = 15.154(3) Å, b = 12.477(3) Å, c = 7.0158(14) Å, α = 90°, β = 105.873(12)°, γ = 90°, V = 1276.0(5) Å3, Z = 4. The Cu–N, Cu–O(aqua) and Cu–O(sulfate) bond lengths are 2.000(3) Å, 1.978(2) Å and 2.464(2) Å, respectively. The [Cu(bpy)Cl2] complex crystallizes in the monoclinic crystal system with space group I2/a. The unit cell parameters were determined to be a = 7.306(2) Å, b = 9.016(2) Å, c = 15.879(6) Å, α = 90°, β = 92.141(15)°, γ = 90°, V = 1045.2(5) Å3, Z = 4. The Cu–N and Cu–Cl bond lengths are 2.031(5) Å and 2.2662(17) Å, respectively.
650		4	\|a Copper(II) complex
650		4	\|a Bipyridine
650		4	\|a Coordination polymer
650		4	\|a Crystal structure
650		4	\|a Redetermination
773	0	8	\|i Enthalten in \|t Polyhedron \|d Amsterdam [u.a.] : Elsevier Science, 1982 \|g 250 \|h Online-Ressource \|w (DE-627)320402967 \|w (DE-600)2000326-2 \|w (DE-576)096704209 \|7 nnns
773	1	8	\|g volume:250
912			\|a GBV_USEFLAG_U
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912			\|a GBV_ILN_24
912			\|a GBV_ILN_31
912			\|a GBV_ILN_32
912			\|a GBV_ILN_40
912			\|a GBV_ILN_60
912			\|a GBV_ILN_62
912			\|a GBV_ILN_65
912			\|a GBV_ILN_69
912			\|a GBV_ILN_70
912			\|a GBV_ILN_73
912			\|a GBV_ILN_74
912			\|a GBV_ILN_90
912			\|a GBV_ILN_95
912			\|a GBV_ILN_100
912			\|a GBV_ILN_101
912			\|a GBV_ILN_105
912			\|a GBV_ILN_110
912			\|a GBV_ILN_150
912			\|a GBV_ILN_151
912			\|a GBV_ILN_187
912			\|a GBV_ILN_213
912			\|a GBV_ILN_224
912			\|a GBV_ILN_230
912			\|a GBV_ILN_370
912			\|a GBV_ILN_602
912			\|a GBV_ILN_702
912			\|a GBV_ILN_2001
912			\|a GBV_ILN_2003
912			\|a GBV_ILN_2004
912			\|a GBV_ILN_2005
912			\|a GBV_ILN_2007
912			\|a GBV_ILN_2008
912			\|a GBV_ILN_2009
912			\|a GBV_ILN_2010
912			\|a GBV_ILN_2011
912			\|a GBV_ILN_2014
912			\|a GBV_ILN_2015
912			\|a GBV_ILN_2020
912			\|a GBV_ILN_2021
912			\|a GBV_ILN_2025
912			\|a GBV_ILN_2026
912			\|a GBV_ILN_2027
912			\|a GBV_ILN_2034
912			\|a GBV_ILN_2044
912			\|a GBV_ILN_2048
912			\|a GBV_ILN_2049
912			\|a GBV_ILN_2050
912			\|a GBV_ILN_2055
912			\|a GBV_ILN_2056
912			\|a GBV_ILN_2059
912			\|a GBV_ILN_2061
912			\|a GBV_ILN_2064
912			\|a GBV_ILN_2088
912			\|a GBV_ILN_2106
912			\|a GBV_ILN_2110
912			\|a GBV_ILN_2111
912			\|a GBV_ILN_2112
912			\|a GBV_ILN_2122
912			\|a GBV_ILN_2129
912			\|a GBV_ILN_2143
912			\|a GBV_ILN_2152
912			\|a GBV_ILN_2153
912			\|a GBV_ILN_2190
912			\|a GBV_ILN_2232
912			\|a GBV_ILN_2336
912			\|a GBV_ILN_2470
912			\|a GBV_ILN_2507
912			\|a GBV_ILN_4035
912			\|a GBV_ILN_4037
912			\|a GBV_ILN_4112
912			\|a GBV_ILN_4125
912			\|a GBV_ILN_4242
912			\|a GBV_ILN_4249
912			\|a GBV_ILN_4251
912			\|a GBV_ILN_4305
912			\|a GBV_ILN_4306
912			\|a GBV_ILN_4307
912			\|a GBV_ILN_4313
912			\|a GBV_ILN_4322
912			\|a GBV_ILN_4323
912			\|a GBV_ILN_4324
912			\|a GBV_ILN_4325
912			\|a GBV_ILN_4326
912			\|a GBV_ILN_4333
912			\|a GBV_ILN_4334
912			\|a GBV_ILN_4338
912			\|a GBV_ILN_4393
912			\|a GBV_ILN_4700
936	b	k	\|a 35.00 \|j Chemie: Allgemeines \|q VZ
951			\|a AR
952			\|d 250

Indexfelder

author_variant	i y iy
matchkey_str	yilmazsmail:2023----:yteioctnpldau2bprdncpeislaoo1codntoplmrndclr2bprdncpeicml
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publishDate	2023
allfields	10.1016/j.poly.2023.116816 doi (DE-627)ELV066765471 (ELSEVIER)S0277-5387(23)00538-7 DE-627 ger DE-627 rda eng 540 VZ 35.00 bkl Yilmaz, İsmail verfasserin (orcid)0000-0002-0139-0122 aut Synthesis of catena -Poly[[di-aqua(2,2′-bipyridine)copper(II)]- μ -sulfato-κ 2 O:O'] 1D coordination polymer and [di-chloro(2,2′-bipyridine)copper(II)] complex, redetermination of their crystal structures 2023 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier The title compounds [Cu(bpy)(H2O)2(SO4)] n (1) and [Cu(bpy)Cl2] (2) were successfully synthesized, and their crystal structures were redetermined as some corrections were needed. The Cu(II) centers in 1 are coordinated in elongated octahedral geometry by the two nitrogen atoms of a bpy ligand and four oxygen atoms belonging to aqua molecules and sulfato ligands, forming a polymeric chain by bridging the sulfato ligands. The Cu(II) center in 2 is coordinated by the two chloride ions and the two nitrogen atoms of the bipyridine ligand, forming a distorted square planar geometry. The [Cu(bpy)(H2O)2(SO4)] n complex crystallizes in the monoclinic crystal system with space group C2/c. The unit cell parameters were determined to be a = 15.154(3) Å, b = 12.477(3) Å, c = 7.0158(14) Å, α = 90°, β = 105.873(12)°, γ = 90°, V = 1276.0(5) Å3, Z = 4. The Cu–N, Cu–O(aqua) and Cu–O(sulfate) bond lengths are 2.000(3) Å, 1.978(2) Å and 2.464(2) Å, respectively. The [Cu(bpy)Cl2] complex crystallizes in the monoclinic crystal system with space group I2/a. The unit cell parameters were determined to be a = 7.306(2) Å, b = 9.016(2) Å, c = 15.879(6) Å, α = 90°, β = 92.141(15)°, γ = 90°, V = 1045.2(5) Å3, Z = 4. The Cu–N and Cu–Cl bond lengths are 2.031(5) Å and 2.2662(17) Å, respectively. Copper(II) complex Bipyridine Coordination polymer Crystal structure Redetermination Enthalten in Polyhedron Amsterdam [u.a.] : Elsevier Science, 1982 250 Online-Ressource (DE-627)320402967 (DE-600)2000326-2 (DE-576)096704209 nnns volume:250 GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2088 GBV_ILN_2106 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 35.00 Chemie: Allgemeines VZ AR 250
spelling	10.1016/j.poly.2023.116816 doi (DE-627)ELV066765471 (ELSEVIER)S0277-5387(23)00538-7 DE-627 ger DE-627 rda eng 540 VZ 35.00 bkl Yilmaz, İsmail verfasserin (orcid)0000-0002-0139-0122 aut Synthesis of catena -Poly[[di-aqua(2,2′-bipyridine)copper(II)]- μ -sulfato-κ 2 O:O'] 1D coordination polymer and [di-chloro(2,2′-bipyridine)copper(II)] complex, redetermination of their crystal structures 2023 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier The title compounds [Cu(bpy)(H2O)2(SO4)] n (1) and [Cu(bpy)Cl2] (2) were successfully synthesized, and their crystal structures were redetermined as some corrections were needed. The Cu(II) centers in 1 are coordinated in elongated octahedral geometry by the two nitrogen atoms of a bpy ligand and four oxygen atoms belonging to aqua molecules and sulfato ligands, forming a polymeric chain by bridging the sulfato ligands. The Cu(II) center in 2 is coordinated by the two chloride ions and the two nitrogen atoms of the bipyridine ligand, forming a distorted square planar geometry. The [Cu(bpy)(H2O)2(SO4)] n complex crystallizes in the monoclinic crystal system with space group C2/c. The unit cell parameters were determined to be a = 15.154(3) Å, b = 12.477(3) Å, c = 7.0158(14) Å, α = 90°, β = 105.873(12)°, γ = 90°, V = 1276.0(5) Å3, Z = 4. The Cu–N, Cu–O(aqua) and Cu–O(sulfate) bond lengths are 2.000(3) Å, 1.978(2) Å and 2.464(2) Å, respectively. The [Cu(bpy)Cl2] complex crystallizes in the monoclinic crystal system with space group I2/a. The unit cell parameters were determined to be a = 7.306(2) Å, b = 9.016(2) Å, c = 15.879(6) Å, α = 90°, β = 92.141(15)°, γ = 90°, V = 1045.2(5) Å3, Z = 4. The Cu–N and Cu–Cl bond lengths are 2.031(5) Å and 2.2662(17) Å, respectively. Copper(II) complex Bipyridine Coordination polymer Crystal structure Redetermination Enthalten in Polyhedron Amsterdam [u.a.] : Elsevier Science, 1982 250 Online-Ressource (DE-627)320402967 (DE-600)2000326-2 (DE-576)096704209 nnns volume:250 GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2088 GBV_ILN_2106 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 35.00 Chemie: Allgemeines VZ AR 250
allfields_unstemmed	10.1016/j.poly.2023.116816 doi (DE-627)ELV066765471 (ELSEVIER)S0277-5387(23)00538-7 DE-627 ger DE-627 rda eng 540 VZ 35.00 bkl Yilmaz, İsmail verfasserin (orcid)0000-0002-0139-0122 aut Synthesis of catena -Poly[[di-aqua(2,2′-bipyridine)copper(II)]- μ -sulfato-κ 2 O:O'] 1D coordination polymer and [di-chloro(2,2′-bipyridine)copper(II)] complex, redetermination of their crystal structures 2023 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier The title compounds [Cu(bpy)(H2O)2(SO4)] n (1) and [Cu(bpy)Cl2] (2) were successfully synthesized, and their crystal structures were redetermined as some corrections were needed. The Cu(II) centers in 1 are coordinated in elongated octahedral geometry by the two nitrogen atoms of a bpy ligand and four oxygen atoms belonging to aqua molecules and sulfato ligands, forming a polymeric chain by bridging the sulfato ligands. The Cu(II) center in 2 is coordinated by the two chloride ions and the two nitrogen atoms of the bipyridine ligand, forming a distorted square planar geometry. The [Cu(bpy)(H2O)2(SO4)] n complex crystallizes in the monoclinic crystal system with space group C2/c. The unit cell parameters were determined to be a = 15.154(3) Å, b = 12.477(3) Å, c = 7.0158(14) Å, α = 90°, β = 105.873(12)°, γ = 90°, V = 1276.0(5) Å3, Z = 4. The Cu–N, Cu–O(aqua) and Cu–O(sulfate) bond lengths are 2.000(3) Å, 1.978(2) Å and 2.464(2) Å, respectively. The [Cu(bpy)Cl2] complex crystallizes in the monoclinic crystal system with space group I2/a. The unit cell parameters were determined to be a = 7.306(2) Å, b = 9.016(2) Å, c = 15.879(6) Å, α = 90°, β = 92.141(15)°, γ = 90°, V = 1045.2(5) Å3, Z = 4. The Cu–N and Cu–Cl bond lengths are 2.031(5) Å and 2.2662(17) Å, respectively. Copper(II) complex Bipyridine Coordination polymer Crystal structure Redetermination Enthalten in Polyhedron Amsterdam [u.a.] : Elsevier Science, 1982 250 Online-Ressource (DE-627)320402967 (DE-600)2000326-2 (DE-576)096704209 nnns volume:250 GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2088 GBV_ILN_2106 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 35.00 Chemie: Allgemeines VZ AR 250
allfieldsGer	10.1016/j.poly.2023.116816 doi (DE-627)ELV066765471 (ELSEVIER)S0277-5387(23)00538-7 DE-627 ger DE-627 rda eng 540 VZ 35.00 bkl Yilmaz, İsmail verfasserin (orcid)0000-0002-0139-0122 aut Synthesis of catena -Poly[[di-aqua(2,2′-bipyridine)copper(II)]- μ -sulfato-κ 2 O:O'] 1D coordination polymer and [di-chloro(2,2′-bipyridine)copper(II)] complex, redetermination of their crystal structures 2023 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier The title compounds [Cu(bpy)(H2O)2(SO4)] n (1) and [Cu(bpy)Cl2] (2) were successfully synthesized, and their crystal structures were redetermined as some corrections were needed. The Cu(II) centers in 1 are coordinated in elongated octahedral geometry by the two nitrogen atoms of a bpy ligand and four oxygen atoms belonging to aqua molecules and sulfato ligands, forming a polymeric chain by bridging the sulfato ligands. The Cu(II) center in 2 is coordinated by the two chloride ions and the two nitrogen atoms of the bipyridine ligand, forming a distorted square planar geometry. The [Cu(bpy)(H2O)2(SO4)] n complex crystallizes in the monoclinic crystal system with space group C2/c. The unit cell parameters were determined to be a = 15.154(3) Å, b = 12.477(3) Å, c = 7.0158(14) Å, α = 90°, β = 105.873(12)°, γ = 90°, V = 1276.0(5) Å3, Z = 4. The Cu–N, Cu–O(aqua) and Cu–O(sulfate) bond lengths are 2.000(3) Å, 1.978(2) Å and 2.464(2) Å, respectively. The [Cu(bpy)Cl2] complex crystallizes in the monoclinic crystal system with space group I2/a. The unit cell parameters were determined to be a = 7.306(2) Å, b = 9.016(2) Å, c = 15.879(6) Å, α = 90°, β = 92.141(15)°, γ = 90°, V = 1045.2(5) Å3, Z = 4. The Cu–N and Cu–Cl bond lengths are 2.031(5) Å and 2.2662(17) Å, respectively. Copper(II) complex Bipyridine Coordination polymer Crystal structure Redetermination Enthalten in Polyhedron Amsterdam [u.a.] : Elsevier Science, 1982 250 Online-Ressource (DE-627)320402967 (DE-600)2000326-2 (DE-576)096704209 nnns volume:250 GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2088 GBV_ILN_2106 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 35.00 Chemie: Allgemeines VZ AR 250
allfieldsSound	10.1016/j.poly.2023.116816 doi (DE-627)ELV066765471 (ELSEVIER)S0277-5387(23)00538-7 DE-627 ger DE-627 rda eng 540 VZ 35.00 bkl Yilmaz, İsmail verfasserin (orcid)0000-0002-0139-0122 aut Synthesis of catena -Poly[[di-aqua(2,2′-bipyridine)copper(II)]- μ -sulfato-κ 2 O:O'] 1D coordination polymer and [di-chloro(2,2′-bipyridine)copper(II)] complex, redetermination of their crystal structures 2023 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier The title compounds [Cu(bpy)(H2O)2(SO4)] n (1) and [Cu(bpy)Cl2] (2) were successfully synthesized, and their crystal structures were redetermined as some corrections were needed. The Cu(II) centers in 1 are coordinated in elongated octahedral geometry by the two nitrogen atoms of a bpy ligand and four oxygen atoms belonging to aqua molecules and sulfato ligands, forming a polymeric chain by bridging the sulfato ligands. The Cu(II) center in 2 is coordinated by the two chloride ions and the two nitrogen atoms of the bipyridine ligand, forming a distorted square planar geometry. The [Cu(bpy)(H2O)2(SO4)] n complex crystallizes in the monoclinic crystal system with space group C2/c. The unit cell parameters were determined to be a = 15.154(3) Å, b = 12.477(3) Å, c = 7.0158(14) Å, α = 90°, β = 105.873(12)°, γ = 90°, V = 1276.0(5) Å3, Z = 4. The Cu–N, Cu–O(aqua) and Cu–O(sulfate) bond lengths are 2.000(3) Å, 1.978(2) Å and 2.464(2) Å, respectively. The [Cu(bpy)Cl2] complex crystallizes in the monoclinic crystal system with space group I2/a. The unit cell parameters were determined to be a = 7.306(2) Å, b = 9.016(2) Å, c = 15.879(6) Å, α = 90°, β = 92.141(15)°, γ = 90°, V = 1045.2(5) Å3, Z = 4. The Cu–N and Cu–Cl bond lengths are 2.031(5) Å and 2.2662(17) Å, respectively. Copper(II) complex Bipyridine Coordination polymer Crystal structure Redetermination Enthalten in Polyhedron Amsterdam [u.a.] : Elsevier Science, 1982 250 Online-Ressource (DE-627)320402967 (DE-600)2000326-2 (DE-576)096704209 nnns volume:250 GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2088 GBV_ILN_2106 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 35.00 Chemie: Allgemeines VZ AR 250
language	English
source	Enthalten in Polyhedron 250 volume:250
sourceStr	Enthalten in Polyhedron 250 volume:250
format_phy_str_mv	Article
bklname	Chemie: Allgemeines
institution	findex.gbv.de
topic_facet	Copper(II) complex Bipyridine Coordination polymer Crystal structure Redetermination
dewey-raw	540
isfreeaccess_bool	false
container_title	Polyhedron
authorswithroles_txt_mv	Yilmaz, İsmail @@aut@@
publishDateDaySort_date	2023-01-01T00:00:00Z
hierarchy_top_id	320402967
dewey-sort	3540
id	ELV066765471
language_de	englisch
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The Cu(II) centers in 1 are coordinated in elongated octahedral geometry by the two nitrogen atoms of a bpy ligand and four oxygen atoms belonging to aqua molecules and sulfato ligands, forming a polymeric chain by bridging the sulfato ligands. The Cu(II) center in 2 is coordinated by the two chloride ions and the two nitrogen atoms of the bipyridine ligand, forming a distorted square planar geometry. The [Cu(bpy)(H2O)2(SO4)] n complex crystallizes in the monoclinic crystal system with space group C2/c. The unit cell parameters were determined to be a = 15.154(3) Å, b = 12.477(3) Å, c = 7.0158(14) Å, α = 90°, β = 105.873(12)°, γ = 90°, V = 1276.0(5) Å3, Z = 4. The Cu–N, Cu–O(aqua) and Cu–O(sulfate) bond lengths are 2.000(3) Å, 1.978(2) Å and 2.464(2) Å, respectively. The [Cu(bpy)Cl2] complex crystallizes in the monoclinic crystal system with space group I2/a. The unit cell parameters were determined to be a = 7.306(2) Å, b = 9.016(2) Å, c = 15.879(6) Å, α = 90°, β = 92.141(15)°, γ = 90°, V = 1045.2(5) Å3, Z = 4. 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author	Yilmaz, İsmail
spellingShingle	Yilmaz, İsmail ddc 540 bkl 35.00 misc Copper(II) complex misc Bipyridine misc Coordination polymer misc Crystal structure misc Redetermination Synthesis of catena -Poly[[di-aqua(2,2′-bipyridine)copper(II)]- μ -sulfato-κ 2 O:O'] 1D coordination polymer and [di-chloro(2,2′-bipyridine)copper(II)] complex, redetermination of their crystal structures
authorStr	Yilmaz, İsmail
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topic_title	540 VZ 35.00 bkl Synthesis of catena -Poly[[di-aqua(2,2′-bipyridine)copper(II)]- μ -sulfato-κ 2 O:O'] 1D coordination polymer and [di-chloro(2,2′-bipyridine)copper(II)] complex, redetermination of their crystal structures Copper(II) complex Bipyridine Coordination polymer Crystal structure Redetermination
topic	ddc 540 bkl 35.00 misc Copper(II) complex misc Bipyridine misc Coordination polymer misc Crystal structure misc Redetermination
topic_unstemmed	ddc 540 bkl 35.00 misc Copper(II) complex misc Bipyridine misc Coordination polymer misc Crystal structure misc Redetermination
topic_browse	ddc 540 bkl 35.00 misc Copper(II) complex misc Bipyridine misc Coordination polymer misc Crystal structure misc Redetermination
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title	Synthesis of catena -Poly[[di-aqua(2,2′-bipyridine)copper(II)]- μ -sulfato-κ 2 O:O'] 1D coordination polymer and [di-chloro(2,2′-bipyridine)copper(II)] complex, redetermination of their crystal structures
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title_full	Synthesis of catena -Poly[[di-aqua(2,2′-bipyridine)copper(II)]- μ -sulfato-κ 2 O:O'] 1D coordination polymer and [di-chloro(2,2′-bipyridine)copper(II)] complex, redetermination of their crystal structures
author_sort	Yilmaz, İsmail
journal	Polyhedron
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class	540 VZ 35.00 bkl
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author-letter	Yilmaz, İsmail
doi_str_mv	10.1016/j.poly.2023.116816
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dewey-full	540
title_sort	synthesis of catena -poly[[di-aqua(2,2′-bipyridine)copper(ii)]- μ -sulfato-κ 2 o:o'] 1d coordination polymer and [di-chloro(2,2′-bipyridine)copper(ii)] complex, redetermination of their crystal structures
title_auth	Synthesis of catena -Poly[[di-aqua(2,2′-bipyridine)copper(II)]- μ -sulfato-κ 2 O:O'] 1D coordination polymer and [di-chloro(2,2′-bipyridine)copper(II)] complex, redetermination of their crystal structures
abstract	The title compounds [Cu(bpy)(H2O)2(SO4)] n (1) and [Cu(bpy)Cl2] (2) were successfully synthesized, and their crystal structures were redetermined as some corrections were needed. The Cu(II) centers in 1 are coordinated in elongated octahedral geometry by the two nitrogen atoms of a bpy ligand and four oxygen atoms belonging to aqua molecules and sulfato ligands, forming a polymeric chain by bridging the sulfato ligands. The Cu(II) center in 2 is coordinated by the two chloride ions and the two nitrogen atoms of the bipyridine ligand, forming a distorted square planar geometry. The [Cu(bpy)(H2O)2(SO4)] n complex crystallizes in the monoclinic crystal system with space group C2/c. The unit cell parameters were determined to be a = 15.154(3) Å, b = 12.477(3) Å, c = 7.0158(14) Å, α = 90°, β = 105.873(12)°, γ = 90°, V = 1276.0(5) Å3, Z = 4. The Cu–N, Cu–O(aqua) and Cu–O(sulfate) bond lengths are 2.000(3) Å, 1.978(2) Å and 2.464(2) Å, respectively. The [Cu(bpy)Cl2] complex crystallizes in the monoclinic crystal system with space group I2/a. The unit cell parameters were determined to be a = 7.306(2) Å, b = 9.016(2) Å, c = 15.879(6) Å, α = 90°, β = 92.141(15)°, γ = 90°, V = 1045.2(5) Å3, Z = 4. The Cu–N and Cu–Cl bond lengths are 2.031(5) Å and 2.2662(17) Å, respectively.
abstractGer	The title compounds [Cu(bpy)(H2O)2(SO4)] n (1) and [Cu(bpy)Cl2] (2) were successfully synthesized, and their crystal structures were redetermined as some corrections were needed. The Cu(II) centers in 1 are coordinated in elongated octahedral geometry by the two nitrogen atoms of a bpy ligand and four oxygen atoms belonging to aqua molecules and sulfato ligands, forming a polymeric chain by bridging the sulfato ligands. The Cu(II) center in 2 is coordinated by the two chloride ions and the two nitrogen atoms of the bipyridine ligand, forming a distorted square planar geometry. The [Cu(bpy)(H2O)2(SO4)] n complex crystallizes in the monoclinic crystal system with space group C2/c. The unit cell parameters were determined to be a = 15.154(3) Å, b = 12.477(3) Å, c = 7.0158(14) Å, α = 90°, β = 105.873(12)°, γ = 90°, V = 1276.0(5) Å3, Z = 4. The Cu–N, Cu–O(aqua) and Cu–O(sulfate) bond lengths are 2.000(3) Å, 1.978(2) Å and 2.464(2) Å, respectively. The [Cu(bpy)Cl2] complex crystallizes in the monoclinic crystal system with space group I2/a. The unit cell parameters were determined to be a = 7.306(2) Å, b = 9.016(2) Å, c = 15.879(6) Å, α = 90°, β = 92.141(15)°, γ = 90°, V = 1045.2(5) Å3, Z = 4. The Cu–N and Cu–Cl bond lengths are 2.031(5) Å and 2.2662(17) Å, respectively.
abstract_unstemmed	The title compounds [Cu(bpy)(H2O)2(SO4)] n (1) and [Cu(bpy)Cl2] (2) were successfully synthesized, and their crystal structures were redetermined as some corrections were needed. The Cu(II) centers in 1 are coordinated in elongated octahedral geometry by the two nitrogen atoms of a bpy ligand and four oxygen atoms belonging to aqua molecules and sulfato ligands, forming a polymeric chain by bridging the sulfato ligands. The Cu(II) center in 2 is coordinated by the two chloride ions and the two nitrogen atoms of the bipyridine ligand, forming a distorted square planar geometry. The [Cu(bpy)(H2O)2(SO4)] n complex crystallizes in the monoclinic crystal system with space group C2/c. The unit cell parameters were determined to be a = 15.154(3) Å, b = 12.477(3) Å, c = 7.0158(14) Å, α = 90°, β = 105.873(12)°, γ = 90°, V = 1276.0(5) Å3, Z = 4. The Cu–N, Cu–O(aqua) and Cu–O(sulfate) bond lengths are 2.000(3) Å, 1.978(2) Å and 2.464(2) Å, respectively. The [Cu(bpy)Cl2] complex crystallizes in the monoclinic crystal system with space group I2/a. The unit cell parameters were determined to be a = 7.306(2) Å, b = 9.016(2) Å, c = 15.879(6) Å, α = 90°, β = 92.141(15)°, γ = 90°, V = 1045.2(5) Å3, Z = 4. The Cu–N and Cu–Cl bond lengths are 2.031(5) Å and 2.2662(17) Å, respectively.
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title_short	Synthesis of catena -Poly[[di-aqua(2,2′-bipyridine)copper(II)]- μ -sulfato-κ 2 O:O'] 1D coordination polymer and [di-chloro(2,2′-bipyridine)copper(II)] complex, redetermination of their crystal structures
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doi_str	10.1016/j.poly.2023.116816
up_date	2024-07-06T18:55:03.322Z
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The Cu(II) centers in 1 are coordinated in elongated octahedral geometry by the two nitrogen atoms of a bpy ligand and four oxygen atoms belonging to aqua molecules and sulfato ligands, forming a polymeric chain by bridging the sulfato ligands. The Cu(II) center in 2 is coordinated by the two chloride ions and the two nitrogen atoms of the bipyridine ligand, forming a distorted square planar geometry. The [Cu(bpy)(H2O)2(SO4)] n complex crystallizes in the monoclinic crystal system with space group C2/c. The unit cell parameters were determined to be a = 15.154(3) Å, b = 12.477(3) Å, c = 7.0158(14) Å, α = 90°, β = 105.873(12)°, γ = 90°, V = 1276.0(5) Å3, Z = 4. The Cu–N, Cu–O(aqua) and Cu–O(sulfate) bond lengths are 2.000(3) Å, 1.978(2) Å and 2.464(2) Å, respectively. The [Cu(bpy)Cl2] complex crystallizes in the monoclinic crystal system with space group I2/a. The unit cell parameters were determined to be a = 7.306(2) Å, b = 9.016(2) Å, c = 15.879(6) Å, α = 90°, β = 92.141(15)°, γ = 90°, V = 1045.2(5) Å3, Z = 4. 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Synthesis of catena -Poly[[di-aqua(2,2′-bipyridine)copper(II)]- μ -sulfato-κ 2 O:O'] 1D coordination polymer and [di-chloro(2,2′-bipyridine)copper(II)] complex, redetermination of their crystal structures

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