Efficient physical delamination of Ti 3 C 2 T x MXene under periodic and constant shear field of Taylor vortex flow

Employing Taylor vortex flow (TVF), we have devised an innovative technique for the delamination of MXene without using a chemical intercalant and demonstrated the enhanced optoelectronic characteristics of this delaminated MXene through their successful implementation in light emitting diode (LED)....
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Gespeichert in:

Autor*in:	Gupta, Kiran [verfasserIn] Heo, Jin Hyuck [verfasserIn] Im, Sang Hyuk [verfasserIn] Kim, Woo-Sik [verfasserIn]

Format:	E-Artikel
Sprache:	Englisch

Erschienen:	2024

Schlagwörter:	Delamination of MXene High productivity of MXene Taylor vortex flow, Turbulent eddy flow Light emitting diodes

Übergeordnetes Werk:	Enthalten in: The chemical engineering journal - Amsterdam : Elsevier, 1997, 481
Übergeordnetes Werk:	volume:481

DOI / URN:	10.1016/j.cej.2024.148700

Katalog-ID:	ELV066906601

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100	1		\|a Gupta, Kiran \|e verfasserin \|4 aut
245	1	0	\|a Efficient physical delamination of Ti 3 C 2 T x MXene under periodic and constant shear field of Taylor vortex flow
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520			\|a Employing Taylor vortex flow (TVF), we have devised an innovative technique for the delamination of MXene without using a chemical intercalant and demonstrated the enhanced optoelectronic characteristics of this delaminated MXene through their successful implementation in light emitting diode (LED). The pairwise toroidal fluid motion of TVF was induced by the rotation of the inner cylinder in the Couette-Taylor (CT) reactor. Due to periodic and constant shear field, TVF was highly efficient for the exfoliation of MXene. So, the continuous exfoliation process using CT reactor always showed 8.1 ∼ 12.5 times higher delaminated MXene (d-Ti3C2Tx) yield than that using a conventional mixing tank (MT) reactor which generated turbulent eddy flow (TEF) by impeller agitation. As such, 8.26 mgּ/mL (42.90 % of recovery ratio) of d-Ti3C2Tx was obtained in CT reactor at 1300 rpm of inner cylinder rotation speed and 24 min of mean residence time (MRT). In comparison, d-Ti3C2Tx in MT reactor at 3000 rpm of agitation speed and 24 min of MRT was 0.66 mgּ/mL (3.42 % of recovery ratio). In addition, d-Ti3C2Tx in TVF was thinner and wider than that in TEF. So, the d-Ti3C2Tx was homogeneously suspended without sedimentation and oxidation in aqueous suspension over 30 days. In addition, d-Ti3C2Tx in the TVF was applied to the transparent conducting electrode of inorganic CsPbBr3 perovskite light emitting diodes (PeLEDs). The transparent conducting oxide-free PeLED had 62.52 cd/A of maximum current efficiency and 14.48 % of maximum external quantum efficiency, which is comparable to the best performance of ITO-based inorganic CsPbBr3 PeLEDs.
650		4	\|a Delamination of MXene
650		4	\|a High productivity of MXene
650		4	\|a Taylor vortex flow, Turbulent eddy flow
650		4	\|a Light emitting diodes
700	1		\|a Heo, Jin Hyuck \|e verfasserin \|4 aut
700	1		\|a Im, Sang Hyuk \|e verfasserin \|4 aut
700	1		\|a Kim, Woo-Sik \|e verfasserin \|0 (orcid)0000-0001-6876-4726 \|4 aut
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936	b	k	\|a 58.10 \|j Verfahrenstechnik: Allgemeines \|q VZ
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allfields	10.1016/j.cej.2024.148700 doi (DE-627)ELV066906601 (ELSEVIER)S1385-8947(24)00185-2 DE-627 ger DE-627 rda eng 660 VZ 660 VZ 58.10 bkl Gupta, Kiran verfasserin aut Efficient physical delamination of Ti 3 C 2 T x MXene under periodic and constant shear field of Taylor vortex flow 2024 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Employing Taylor vortex flow (TVF), we have devised an innovative technique for the delamination of MXene without using a chemical intercalant and demonstrated the enhanced optoelectronic characteristics of this delaminated MXene through their successful implementation in light emitting diode (LED). The pairwise toroidal fluid motion of TVF was induced by the rotation of the inner cylinder in the Couette-Taylor (CT) reactor. Due to periodic and constant shear field, TVF was highly efficient for the exfoliation of MXene. So, the continuous exfoliation process using CT reactor always showed 8.1 ∼ 12.5 times higher delaminated MXene (d-Ti3C2Tx) yield than that using a conventional mixing tank (MT) reactor which generated turbulent eddy flow (TEF) by impeller agitation. As such, 8.26 mgּ/mL (42.90 % of recovery ratio) of d-Ti3C2Tx was obtained in CT reactor at 1300 rpm of inner cylinder rotation speed and 24 min of mean residence time (MRT). In comparison, d-Ti3C2Tx in MT reactor at 3000 rpm of agitation speed and 24 min of MRT was 0.66 mgּ/mL (3.42 % of recovery ratio). In addition, d-Ti3C2Tx in TVF was thinner and wider than that in TEF. So, the d-Ti3C2Tx was homogeneously suspended without sedimentation and oxidation in aqueous suspension over 30 days. In addition, d-Ti3C2Tx in the TVF was applied to the transparent conducting electrode of inorganic CsPbBr3 perovskite light emitting diodes (PeLEDs). The transparent conducting oxide-free PeLED had 62.52 cd/A of maximum current efficiency and 14.48 % of maximum external quantum efficiency, which is comparable to the best performance of ITO-based inorganic CsPbBr3 PeLEDs. Delamination of MXene High productivity of MXene Taylor vortex flow, Turbulent eddy flow Light emitting diodes Heo, Jin Hyuck verfasserin aut Im, Sang Hyuk verfasserin aut Kim, Woo-Sik verfasserin (orcid)0000-0001-6876-4726 aut Enthalten in The chemical engineering journal Amsterdam : Elsevier, 1997 481 Online-Ressource (DE-627)320500322 (DE-600)2012137-4 (DE-576)098330152 1873-3212 nnns volume:481 GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2088 GBV_ILN_2106 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 58.10 Verfahrenstechnik: Allgemeines VZ AR 481
spelling	10.1016/j.cej.2024.148700 doi (DE-627)ELV066906601 (ELSEVIER)S1385-8947(24)00185-2 DE-627 ger DE-627 rda eng 660 VZ 660 VZ 58.10 bkl Gupta, Kiran verfasserin aut Efficient physical delamination of Ti 3 C 2 T x MXene under periodic and constant shear field of Taylor vortex flow 2024 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Employing Taylor vortex flow (TVF), we have devised an innovative technique for the delamination of MXene without using a chemical intercalant and demonstrated the enhanced optoelectronic characteristics of this delaminated MXene through their successful implementation in light emitting diode (LED). The pairwise toroidal fluid motion of TVF was induced by the rotation of the inner cylinder in the Couette-Taylor (CT) reactor. Due to periodic and constant shear field, TVF was highly efficient for the exfoliation of MXene. So, the continuous exfoliation process using CT reactor always showed 8.1 ∼ 12.5 times higher delaminated MXene (d-Ti3C2Tx) yield than that using a conventional mixing tank (MT) reactor which generated turbulent eddy flow (TEF) by impeller agitation. As such, 8.26 mgּ/mL (42.90 % of recovery ratio) of d-Ti3C2Tx was obtained in CT reactor at 1300 rpm of inner cylinder rotation speed and 24 min of mean residence time (MRT). In comparison, d-Ti3C2Tx in MT reactor at 3000 rpm of agitation speed and 24 min of MRT was 0.66 mgּ/mL (3.42 % of recovery ratio). In addition, d-Ti3C2Tx in TVF was thinner and wider than that in TEF. So, the d-Ti3C2Tx was homogeneously suspended without sedimentation and oxidation in aqueous suspension over 30 days. In addition, d-Ti3C2Tx in the TVF was applied to the transparent conducting electrode of inorganic CsPbBr3 perovskite light emitting diodes (PeLEDs). The transparent conducting oxide-free PeLED had 62.52 cd/A of maximum current efficiency and 14.48 % of maximum external quantum efficiency, which is comparable to the best performance of ITO-based inorganic CsPbBr3 PeLEDs. Delamination of MXene High productivity of MXene Taylor vortex flow, Turbulent eddy flow Light emitting diodes Heo, Jin Hyuck verfasserin aut Im, Sang Hyuk verfasserin aut Kim, Woo-Sik verfasserin (orcid)0000-0001-6876-4726 aut Enthalten in The chemical engineering journal Amsterdam : Elsevier, 1997 481 Online-Ressource (DE-627)320500322 (DE-600)2012137-4 (DE-576)098330152 1873-3212 nnns volume:481 GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2088 GBV_ILN_2106 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 58.10 Verfahrenstechnik: Allgemeines VZ AR 481
allfields_unstemmed	10.1016/j.cej.2024.148700 doi (DE-627)ELV066906601 (ELSEVIER)S1385-8947(24)00185-2 DE-627 ger DE-627 rda eng 660 VZ 660 VZ 58.10 bkl Gupta, Kiran verfasserin aut Efficient physical delamination of Ti 3 C 2 T x MXene under periodic and constant shear field of Taylor vortex flow 2024 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Employing Taylor vortex flow (TVF), we have devised an innovative technique for the delamination of MXene without using a chemical intercalant and demonstrated the enhanced optoelectronic characteristics of this delaminated MXene through their successful implementation in light emitting diode (LED). The pairwise toroidal fluid motion of TVF was induced by the rotation of the inner cylinder in the Couette-Taylor (CT) reactor. Due to periodic and constant shear field, TVF was highly efficient for the exfoliation of MXene. So, the continuous exfoliation process using CT reactor always showed 8.1 ∼ 12.5 times higher delaminated MXene (d-Ti3C2Tx) yield than that using a conventional mixing tank (MT) reactor which generated turbulent eddy flow (TEF) by impeller agitation. As such, 8.26 mgּ/mL (42.90 % of recovery ratio) of d-Ti3C2Tx was obtained in CT reactor at 1300 rpm of inner cylinder rotation speed and 24 min of mean residence time (MRT). In comparison, d-Ti3C2Tx in MT reactor at 3000 rpm of agitation speed and 24 min of MRT was 0.66 mgּ/mL (3.42 % of recovery ratio). In addition, d-Ti3C2Tx in TVF was thinner and wider than that in TEF. So, the d-Ti3C2Tx was homogeneously suspended without sedimentation and oxidation in aqueous suspension over 30 days. In addition, d-Ti3C2Tx in the TVF was applied to the transparent conducting electrode of inorganic CsPbBr3 perovskite light emitting diodes (PeLEDs). The transparent conducting oxide-free PeLED had 62.52 cd/A of maximum current efficiency and 14.48 % of maximum external quantum efficiency, which is comparable to the best performance of ITO-based inorganic CsPbBr3 PeLEDs. Delamination of MXene High productivity of MXene Taylor vortex flow, Turbulent eddy flow Light emitting diodes Heo, Jin Hyuck verfasserin aut Im, Sang Hyuk verfasserin aut Kim, Woo-Sik verfasserin (orcid)0000-0001-6876-4726 aut Enthalten in The chemical engineering journal Amsterdam : Elsevier, 1997 481 Online-Ressource (DE-627)320500322 (DE-600)2012137-4 (DE-576)098330152 1873-3212 nnns volume:481 GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2088 GBV_ILN_2106 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 58.10 Verfahrenstechnik: Allgemeines VZ AR 481
allfieldsGer	10.1016/j.cej.2024.148700 doi (DE-627)ELV066906601 (ELSEVIER)S1385-8947(24)00185-2 DE-627 ger DE-627 rda eng 660 VZ 660 VZ 58.10 bkl Gupta, Kiran verfasserin aut Efficient physical delamination of Ti 3 C 2 T x MXene under periodic and constant shear field of Taylor vortex flow 2024 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Employing Taylor vortex flow (TVF), we have devised an innovative technique for the delamination of MXene without using a chemical intercalant and demonstrated the enhanced optoelectronic characteristics of this delaminated MXene through their successful implementation in light emitting diode (LED). The pairwise toroidal fluid motion of TVF was induced by the rotation of the inner cylinder in the Couette-Taylor (CT) reactor. Due to periodic and constant shear field, TVF was highly efficient for the exfoliation of MXene. So, the continuous exfoliation process using CT reactor always showed 8.1 ∼ 12.5 times higher delaminated MXene (d-Ti3C2Tx) yield than that using a conventional mixing tank (MT) reactor which generated turbulent eddy flow (TEF) by impeller agitation. As such, 8.26 mgּ/mL (42.90 % of recovery ratio) of d-Ti3C2Tx was obtained in CT reactor at 1300 rpm of inner cylinder rotation speed and 24 min of mean residence time (MRT). In comparison, d-Ti3C2Tx in MT reactor at 3000 rpm of agitation speed and 24 min of MRT was 0.66 mgּ/mL (3.42 % of recovery ratio). In addition, d-Ti3C2Tx in TVF was thinner and wider than that in TEF. So, the d-Ti3C2Tx was homogeneously suspended without sedimentation and oxidation in aqueous suspension over 30 days. In addition, d-Ti3C2Tx in the TVF was applied to the transparent conducting electrode of inorganic CsPbBr3 perovskite light emitting diodes (PeLEDs). The transparent conducting oxide-free PeLED had 62.52 cd/A of maximum current efficiency and 14.48 % of maximum external quantum efficiency, which is comparable to the best performance of ITO-based inorganic CsPbBr3 PeLEDs. Delamination of MXene High productivity of MXene Taylor vortex flow, Turbulent eddy flow Light emitting diodes Heo, Jin Hyuck verfasserin aut Im, Sang Hyuk verfasserin aut Kim, Woo-Sik verfasserin (orcid)0000-0001-6876-4726 aut Enthalten in The chemical engineering journal Amsterdam : Elsevier, 1997 481 Online-Ressource (DE-627)320500322 (DE-600)2012137-4 (DE-576)098330152 1873-3212 nnns volume:481 GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2088 GBV_ILN_2106 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 58.10 Verfahrenstechnik: Allgemeines VZ AR 481
allfieldsSound	10.1016/j.cej.2024.148700 doi (DE-627)ELV066906601 (ELSEVIER)S1385-8947(24)00185-2 DE-627 ger DE-627 rda eng 660 VZ 660 VZ 58.10 bkl Gupta, Kiran verfasserin aut Efficient physical delamination of Ti 3 C 2 T x MXene under periodic and constant shear field of Taylor vortex flow 2024 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Employing Taylor vortex flow (TVF), we have devised an innovative technique for the delamination of MXene without using a chemical intercalant and demonstrated the enhanced optoelectronic characteristics of this delaminated MXene through their successful implementation in light emitting diode (LED). The pairwise toroidal fluid motion of TVF was induced by the rotation of the inner cylinder in the Couette-Taylor (CT) reactor. Due to periodic and constant shear field, TVF was highly efficient for the exfoliation of MXene. So, the continuous exfoliation process using CT reactor always showed 8.1 ∼ 12.5 times higher delaminated MXene (d-Ti3C2Tx) yield than that using a conventional mixing tank (MT) reactor which generated turbulent eddy flow (TEF) by impeller agitation. As such, 8.26 mgּ/mL (42.90 % of recovery ratio) of d-Ti3C2Tx was obtained in CT reactor at 1300 rpm of inner cylinder rotation speed and 24 min of mean residence time (MRT). In comparison, d-Ti3C2Tx in MT reactor at 3000 rpm of agitation speed and 24 min of MRT was 0.66 mgּ/mL (3.42 % of recovery ratio). In addition, d-Ti3C2Tx in TVF was thinner and wider than that in TEF. So, the d-Ti3C2Tx was homogeneously suspended without sedimentation and oxidation in aqueous suspension over 30 days. In addition, d-Ti3C2Tx in the TVF was applied to the transparent conducting electrode of inorganic CsPbBr3 perovskite light emitting diodes (PeLEDs). The transparent conducting oxide-free PeLED had 62.52 cd/A of maximum current efficiency and 14.48 % of maximum external quantum efficiency, which is comparable to the best performance of ITO-based inorganic CsPbBr3 PeLEDs. Delamination of MXene High productivity of MXene Taylor vortex flow, Turbulent eddy flow Light emitting diodes Heo, Jin Hyuck verfasserin aut Im, Sang Hyuk verfasserin aut Kim, Woo-Sik verfasserin (orcid)0000-0001-6876-4726 aut Enthalten in The chemical engineering journal Amsterdam : Elsevier, 1997 481 Online-Ressource (DE-627)320500322 (DE-600)2012137-4 (DE-576)098330152 1873-3212 nnns volume:481 GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2088 GBV_ILN_2106 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 58.10 Verfahrenstechnik: Allgemeines VZ AR 481
language	English
source	Enthalten in The chemical engineering journal 481 volume:481
sourceStr	Enthalten in The chemical engineering journal 481 volume:481
format_phy_str_mv	Article
bklname	Verfahrenstechnik: Allgemeines
institution	findex.gbv.de
topic_facet	Delamination of MXene High productivity of MXene Taylor vortex flow, Turbulent eddy flow Light emitting diodes
dewey-raw	660
isfreeaccess_bool	false
container_title	The chemical engineering journal
authorswithroles_txt_mv	Gupta, Kiran @@aut@@ Heo, Jin Hyuck @@aut@@ Im, Sang Hyuk @@aut@@ Kim, Woo-Sik @@aut@@
publishDateDaySort_date	2024-01-01T00:00:00Z
hierarchy_top_id	320500322
dewey-sort	3660
id	ELV066906601
language_de	englisch
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author	Gupta, Kiran
spellingShingle	Gupta, Kiran ddc 660 bkl 58.10 misc Delamination of MXene misc High productivity of MXene misc Taylor vortex flow, Turbulent eddy flow misc Light emitting diodes Efficient physical delamination of Ti 3 C 2 T x MXene under periodic and constant shear field of Taylor vortex flow
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topic_title	660 VZ 58.10 bkl Efficient physical delamination of Ti 3 C 2 T x MXene under periodic and constant shear field of Taylor vortex flow Delamination of MXene High productivity of MXene Taylor vortex flow, Turbulent eddy flow Light emitting diodes
topic	ddc 660 bkl 58.10 misc Delamination of MXene misc High productivity of MXene misc Taylor vortex flow, Turbulent eddy flow misc Light emitting diodes
topic_unstemmed	ddc 660 bkl 58.10 misc Delamination of MXene misc High productivity of MXene misc Taylor vortex flow, Turbulent eddy flow misc Light emitting diodes
topic_browse	ddc 660 bkl 58.10 misc Delamination of MXene misc High productivity of MXene misc Taylor vortex flow, Turbulent eddy flow misc Light emitting diodes
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title	Efficient physical delamination of Ti 3 C 2 T x MXene under periodic and constant shear field of Taylor vortex flow
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title_full	Efficient physical delamination of Ti 3 C 2 T x MXene under periodic and constant shear field of Taylor vortex flow
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title_sort	efficient physical delamination of ti 3 c 2 t x mxene under periodic and constant shear field of taylor vortex flow
title_auth	Efficient physical delamination of Ti 3 C 2 T x MXene under periodic and constant shear field of Taylor vortex flow
abstract	Employing Taylor vortex flow (TVF), we have devised an innovative technique for the delamination of MXene without using a chemical intercalant and demonstrated the enhanced optoelectronic characteristics of this delaminated MXene through their successful implementation in light emitting diode (LED). The pairwise toroidal fluid motion of TVF was induced by the rotation of the inner cylinder in the Couette-Taylor (CT) reactor. Due to periodic and constant shear field, TVF was highly efficient for the exfoliation of MXene. So, the continuous exfoliation process using CT reactor always showed 8.1 ∼ 12.5 times higher delaminated MXene (d-Ti3C2Tx) yield than that using a conventional mixing tank (MT) reactor which generated turbulent eddy flow (TEF) by impeller agitation. As such, 8.26 mgּ/mL (42.90 % of recovery ratio) of d-Ti3C2Tx was obtained in CT reactor at 1300 rpm of inner cylinder rotation speed and 24 min of mean residence time (MRT). In comparison, d-Ti3C2Tx in MT reactor at 3000 rpm of agitation speed and 24 min of MRT was 0.66 mgּ/mL (3.42 % of recovery ratio). In addition, d-Ti3C2Tx in TVF was thinner and wider than that in TEF. So, the d-Ti3C2Tx was homogeneously suspended without sedimentation and oxidation in aqueous suspension over 30 days. In addition, d-Ti3C2Tx in the TVF was applied to the transparent conducting electrode of inorganic CsPbBr3 perovskite light emitting diodes (PeLEDs). The transparent conducting oxide-free PeLED had 62.52 cd/A of maximum current efficiency and 14.48 % of maximum external quantum efficiency, which is comparable to the best performance of ITO-based inorganic CsPbBr3 PeLEDs.
abstractGer	Employing Taylor vortex flow (TVF), we have devised an innovative technique for the delamination of MXene without using a chemical intercalant and demonstrated the enhanced optoelectronic characteristics of this delaminated MXene through their successful implementation in light emitting diode (LED). The pairwise toroidal fluid motion of TVF was induced by the rotation of the inner cylinder in the Couette-Taylor (CT) reactor. Due to periodic and constant shear field, TVF was highly efficient for the exfoliation of MXene. So, the continuous exfoliation process using CT reactor always showed 8.1 ∼ 12.5 times higher delaminated MXene (d-Ti3C2Tx) yield than that using a conventional mixing tank (MT) reactor which generated turbulent eddy flow (TEF) by impeller agitation. As such, 8.26 mgּ/mL (42.90 % of recovery ratio) of d-Ti3C2Tx was obtained in CT reactor at 1300 rpm of inner cylinder rotation speed and 24 min of mean residence time (MRT). In comparison, d-Ti3C2Tx in MT reactor at 3000 rpm of agitation speed and 24 min of MRT was 0.66 mgּ/mL (3.42 % of recovery ratio). In addition, d-Ti3C2Tx in TVF was thinner and wider than that in TEF. So, the d-Ti3C2Tx was homogeneously suspended without sedimentation and oxidation in aqueous suspension over 30 days. In addition, d-Ti3C2Tx in the TVF was applied to the transparent conducting electrode of inorganic CsPbBr3 perovskite light emitting diodes (PeLEDs). The transparent conducting oxide-free PeLED had 62.52 cd/A of maximum current efficiency and 14.48 % of maximum external quantum efficiency, which is comparable to the best performance of ITO-based inorganic CsPbBr3 PeLEDs.
abstract_unstemmed	Employing Taylor vortex flow (TVF), we have devised an innovative technique for the delamination of MXene without using a chemical intercalant and demonstrated the enhanced optoelectronic characteristics of this delaminated MXene through their successful implementation in light emitting diode (LED). The pairwise toroidal fluid motion of TVF was induced by the rotation of the inner cylinder in the Couette-Taylor (CT) reactor. Due to periodic and constant shear field, TVF was highly efficient for the exfoliation of MXene. So, the continuous exfoliation process using CT reactor always showed 8.1 ∼ 12.5 times higher delaminated MXene (d-Ti3C2Tx) yield than that using a conventional mixing tank (MT) reactor which generated turbulent eddy flow (TEF) by impeller agitation. As such, 8.26 mgּ/mL (42.90 % of recovery ratio) of d-Ti3C2Tx was obtained in CT reactor at 1300 rpm of inner cylinder rotation speed and 24 min of mean residence time (MRT). In comparison, d-Ti3C2Tx in MT reactor at 3000 rpm of agitation speed and 24 min of MRT was 0.66 mgּ/mL (3.42 % of recovery ratio). In addition, d-Ti3C2Tx in TVF was thinner and wider than that in TEF. So, the d-Ti3C2Tx was homogeneously suspended without sedimentation and oxidation in aqueous suspension over 30 days. In addition, d-Ti3C2Tx in the TVF was applied to the transparent conducting electrode of inorganic CsPbBr3 perovskite light emitting diodes (PeLEDs). The transparent conducting oxide-free PeLED had 62.52 cd/A of maximum current efficiency and 14.48 % of maximum external quantum efficiency, which is comparable to the best performance of ITO-based inorganic CsPbBr3 PeLEDs.
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title_short	Efficient physical delamination of Ti 3 C 2 T x MXene under periodic and constant shear field of Taylor vortex flow
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author2	Heo, Jin Hyuck Im, Sang Hyuk Kim, Woo-Sik
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doi_str	10.1016/j.cej.2024.148700
up_date	2024-07-06T19:24:46.900Z
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The pairwise toroidal fluid motion of TVF was induced by the rotation of the inner cylinder in the Couette-Taylor (CT) reactor. Due to periodic and constant shear field, TVF was highly efficient for the exfoliation of MXene. So, the continuous exfoliation process using CT reactor always showed 8.1 ∼ 12.5 times higher delaminated MXene (d-Ti3C2Tx) yield than that using a conventional mixing tank (MT) reactor which generated turbulent eddy flow (TEF) by impeller agitation. As such, 8.26 mgּ/mL (42.90 % of recovery ratio) of d-Ti3C2Tx was obtained in CT reactor at 1300 rpm of inner cylinder rotation speed and 24 min of mean residence time (MRT). In comparison, d-Ti3C2Tx in MT reactor at 3000 rpm of agitation speed and 24 min of MRT was 0.66 mgּ/mL (3.42 % of recovery ratio). In addition, d-Ti3C2Tx in TVF was thinner and wider than that in TEF. So, the d-Ti3C2Tx was homogeneously suspended without sedimentation and oxidation in aqueous suspension over 30 days. In addition, d-Ti3C2Tx in the TVF was applied to the transparent conducting electrode of inorganic CsPbBr3 perovskite light emitting diodes (PeLEDs). 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Efficient physical delamination of Ti 3 C 2 T x MXene under periodic and constant shear field of Taylor vortex flow

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