Optimization of mechanochemical surface modification parameters on planetary mill using an I -optimal experimental design

Several micro-particle-size additives and filler minerals are added to many industrial products, especially plastic, in order to reduce cost and improve mechanical properties and appearance. Also, grinding and surface modification are two fundamental properties of the filler minerals used in plastic...
Ausführliche Beschreibung

Gespeichert in:

Autor*in:	Özdemir, Akın [verfasserIn] Uçurum, Metin [verfasserIn]

Format:	E-Artikel
Sprache:	Englisch

Erschienen:	2024

Schlagwörter:	Planetary mill Mechanochemical Surface modification Bayburt stone

Übergeordnetes Werk:	Enthalten in: Powder technology - Amsterdam [u.a.] : Elsevier Science, 1967, 436
Übergeordnetes Werk:	volume:436

DOI / URN:	10.1016/j.powtec.2024.119495

Katalog-ID:	ELV067203876

Internformat


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245	1	0	\|a Optimization of mechanochemical surface modification parameters on planetary mill using an I -optimal experimental design
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520			\|a Several micro-particle-size additives and filler minerals are added to many industrial products, especially plastic, in order to reduce cost and improve mechanical properties and appearance. Also, grinding and surface modification are two fundamental properties of the filler minerals used in plastic products. Notably, Bayburt stone (BS) used as a natural raw material from Bayburt, Türkiye contains 76% SiO2 and 15% Al2O3. In this paper, the hydrophilic surface structure of micronized Bayburt stone (MBS) was made hydrophobe by mechanochemical surface modification using calcium stearate [Ca(C17H35COO)2] in a laboratory-type planetary mill. Next, the optimum conditions of the surface modification design factors, which are (1) ball filling ratio = 30.53%, (2) powder filling ratio = 10.43%, (3) mill speed = 475.91 rpm, (4) chemical dosage = 1.99% of powder, and (5) modification time = 4.83 min., were obtained using the proposed I-optimal design-focused optimization model when predicting the model parameters. In addition, a coated micronized Bayburt stone (CMBS) product with an active ratio (AR) of 99.90% and d 10, d 50, and d 90 values of 1.32 μm, 3.48 μm and 9.55 μm were achieved. Finally, particle size distribution (PSD), thermo-gravimetric and differential thermal analyzer (TG-DTA), Fourier transform infrared (FTIR), scanning electron microscope (SEM), electron dispersive spectrum (EDS), and contact angle analyses were performed on the CMBS product.
650		4	\|a Planetary mill
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publishDate	2024
allfields	10.1016/j.powtec.2024.119495 doi (DE-627)ELV067203876 (ELSEVIER)S0032-5910(24)00137-2 DE-627 ger DE-627 rda eng 660 VZ 58.10 bkl 52.77 bkl Özdemir, Akın verfasserin aut Optimization of mechanochemical surface modification parameters on planetary mill using an I -optimal experimental design 2024 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Several micro-particle-size additives and filler minerals are added to many industrial products, especially plastic, in order to reduce cost and improve mechanical properties and appearance. Also, grinding and surface modification are two fundamental properties of the filler minerals used in plastic products. Notably, Bayburt stone (BS) used as a natural raw material from Bayburt, Türkiye contains 76% SiO2 and 15% Al2O3. In this paper, the hydrophilic surface structure of micronized Bayburt stone (MBS) was made hydrophobe by mechanochemical surface modification using calcium stearate [Ca(C17H35COO)2] in a laboratory-type planetary mill. Next, the optimum conditions of the surface modification design factors, which are (1) ball filling ratio = 30.53%, (2) powder filling ratio = 10.43%, (3) mill speed = 475.91 rpm, (4) chemical dosage = 1.99% of powder, and (5) modification time = 4.83 min., were obtained using the proposed I-optimal design-focused optimization model when predicting the model parameters. In addition, a coated micronized Bayburt stone (CMBS) product with an active ratio (AR) of 99.90% and d 10, d 50, and d 90 values of 1.32 μm, 3.48 μm and 9.55 μm were achieved. Finally, particle size distribution (PSD), thermo-gravimetric and differential thermal analyzer (TG-DTA), Fourier transform infrared (FTIR), scanning electron microscope (SEM), electron dispersive spectrum (EDS), and contact angle analyses were performed on the CMBS product. Planetary mill Mechanochemical Surface modification Bayburt stone Uçurum, Metin verfasserin aut Enthalten in Powder technology Amsterdam [u.a.] : Elsevier Science, 1967 436 Online-Ressource (DE-627)320599019 (DE-600)2019938-7 (DE-576)098474278 0032-5910 nnns volume:436 GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2007 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2106 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 58.10 Verfahrenstechnik: Allgemeines VZ 52.77 Urformen VZ AR 436
spelling	10.1016/j.powtec.2024.119495 doi (DE-627)ELV067203876 (ELSEVIER)S0032-5910(24)00137-2 DE-627 ger DE-627 rda eng 660 VZ 58.10 bkl 52.77 bkl Özdemir, Akın verfasserin aut Optimization of mechanochemical surface modification parameters on planetary mill using an I -optimal experimental design 2024 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Several micro-particle-size additives and filler minerals are added to many industrial products, especially plastic, in order to reduce cost and improve mechanical properties and appearance. Also, grinding and surface modification are two fundamental properties of the filler minerals used in plastic products. Notably, Bayburt stone (BS) used as a natural raw material from Bayburt, Türkiye contains 76% SiO2 and 15% Al2O3. In this paper, the hydrophilic surface structure of micronized Bayburt stone (MBS) was made hydrophobe by mechanochemical surface modification using calcium stearate [Ca(C17H35COO)2] in a laboratory-type planetary mill. Next, the optimum conditions of the surface modification design factors, which are (1) ball filling ratio = 30.53%, (2) powder filling ratio = 10.43%, (3) mill speed = 475.91 rpm, (4) chemical dosage = 1.99% of powder, and (5) modification time = 4.83 min., were obtained using the proposed I-optimal design-focused optimization model when predicting the model parameters. In addition, a coated micronized Bayburt stone (CMBS) product with an active ratio (AR) of 99.90% and d 10, d 50, and d 90 values of 1.32 μm, 3.48 μm and 9.55 μm were achieved. Finally, particle size distribution (PSD), thermo-gravimetric and differential thermal analyzer (TG-DTA), Fourier transform infrared (FTIR), scanning electron microscope (SEM), electron dispersive spectrum (EDS), and contact angle analyses were performed on the CMBS product. Planetary mill Mechanochemical Surface modification Bayburt stone Uçurum, Metin verfasserin aut Enthalten in Powder technology Amsterdam [u.a.] : Elsevier Science, 1967 436 Online-Ressource (DE-627)320599019 (DE-600)2019938-7 (DE-576)098474278 0032-5910 nnns volume:436 GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2007 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2106 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 58.10 Verfahrenstechnik: Allgemeines VZ 52.77 Urformen VZ AR 436
allfields_unstemmed	10.1016/j.powtec.2024.119495 doi (DE-627)ELV067203876 (ELSEVIER)S0032-5910(24)00137-2 DE-627 ger DE-627 rda eng 660 VZ 58.10 bkl 52.77 bkl Özdemir, Akın verfasserin aut Optimization of mechanochemical surface modification parameters on planetary mill using an I -optimal experimental design 2024 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Several micro-particle-size additives and filler minerals are added to many industrial products, especially plastic, in order to reduce cost and improve mechanical properties and appearance. Also, grinding and surface modification are two fundamental properties of the filler minerals used in plastic products. Notably, Bayburt stone (BS) used as a natural raw material from Bayburt, Türkiye contains 76% SiO2 and 15% Al2O3. In this paper, the hydrophilic surface structure of micronized Bayburt stone (MBS) was made hydrophobe by mechanochemical surface modification using calcium stearate [Ca(C17H35COO)2] in a laboratory-type planetary mill. Next, the optimum conditions of the surface modification design factors, which are (1) ball filling ratio = 30.53%, (2) powder filling ratio = 10.43%, (3) mill speed = 475.91 rpm, (4) chemical dosage = 1.99% of powder, and (5) modification time = 4.83 min., were obtained using the proposed I-optimal design-focused optimization model when predicting the model parameters. In addition, a coated micronized Bayburt stone (CMBS) product with an active ratio (AR) of 99.90% and d 10, d 50, and d 90 values of 1.32 μm, 3.48 μm and 9.55 μm were achieved. Finally, particle size distribution (PSD), thermo-gravimetric and differential thermal analyzer (TG-DTA), Fourier transform infrared (FTIR), scanning electron microscope (SEM), electron dispersive spectrum (EDS), and contact angle analyses were performed on the CMBS product. Planetary mill Mechanochemical Surface modification Bayburt stone Uçurum, Metin verfasserin aut Enthalten in Powder technology Amsterdam [u.a.] : Elsevier Science, 1967 436 Online-Ressource (DE-627)320599019 (DE-600)2019938-7 (DE-576)098474278 0032-5910 nnns volume:436 GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2007 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2106 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 58.10 Verfahrenstechnik: Allgemeines VZ 52.77 Urformen VZ AR 436
allfieldsGer	10.1016/j.powtec.2024.119495 doi (DE-627)ELV067203876 (ELSEVIER)S0032-5910(24)00137-2 DE-627 ger DE-627 rda eng 660 VZ 58.10 bkl 52.77 bkl Özdemir, Akın verfasserin aut Optimization of mechanochemical surface modification parameters on planetary mill using an I -optimal experimental design 2024 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Several micro-particle-size additives and filler minerals are added to many industrial products, especially plastic, in order to reduce cost and improve mechanical properties and appearance. Also, grinding and surface modification are two fundamental properties of the filler minerals used in plastic products. Notably, Bayburt stone (BS) used as a natural raw material from Bayburt, Türkiye contains 76% SiO2 and 15% Al2O3. In this paper, the hydrophilic surface structure of micronized Bayburt stone (MBS) was made hydrophobe by mechanochemical surface modification using calcium stearate [Ca(C17H35COO)2] in a laboratory-type planetary mill. Next, the optimum conditions of the surface modification design factors, which are (1) ball filling ratio = 30.53%, (2) powder filling ratio = 10.43%, (3) mill speed = 475.91 rpm, (4) chemical dosage = 1.99% of powder, and (5) modification time = 4.83 min., were obtained using the proposed I-optimal design-focused optimization model when predicting the model parameters. In addition, a coated micronized Bayburt stone (CMBS) product with an active ratio (AR) of 99.90% and d 10, d 50, and d 90 values of 1.32 μm, 3.48 μm and 9.55 μm were achieved. Finally, particle size distribution (PSD), thermo-gravimetric and differential thermal analyzer (TG-DTA), Fourier transform infrared (FTIR), scanning electron microscope (SEM), electron dispersive spectrum (EDS), and contact angle analyses were performed on the CMBS product. Planetary mill Mechanochemical Surface modification Bayburt stone Uçurum, Metin verfasserin aut Enthalten in Powder technology Amsterdam [u.a.] : Elsevier Science, 1967 436 Online-Ressource (DE-627)320599019 (DE-600)2019938-7 (DE-576)098474278 0032-5910 nnns volume:436 GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2007 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2106 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 58.10 Verfahrenstechnik: Allgemeines VZ 52.77 Urformen VZ AR 436
allfieldsSound	10.1016/j.powtec.2024.119495 doi (DE-627)ELV067203876 (ELSEVIER)S0032-5910(24)00137-2 DE-627 ger DE-627 rda eng 660 VZ 58.10 bkl 52.77 bkl Özdemir, Akın verfasserin aut Optimization of mechanochemical surface modification parameters on planetary mill using an I -optimal experimental design 2024 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Several micro-particle-size additives and filler minerals are added to many industrial products, especially plastic, in order to reduce cost and improve mechanical properties and appearance. Also, grinding and surface modification are two fundamental properties of the filler minerals used in plastic products. Notably, Bayburt stone (BS) used as a natural raw material from Bayburt, Türkiye contains 76% SiO2 and 15% Al2O3. In this paper, the hydrophilic surface structure of micronized Bayburt stone (MBS) was made hydrophobe by mechanochemical surface modification using calcium stearate [Ca(C17H35COO)2] in a laboratory-type planetary mill. Next, the optimum conditions of the surface modification design factors, which are (1) ball filling ratio = 30.53%, (2) powder filling ratio = 10.43%, (3) mill speed = 475.91 rpm, (4) chemical dosage = 1.99% of powder, and (5) modification time = 4.83 min., were obtained using the proposed I-optimal design-focused optimization model when predicting the model parameters. In addition, a coated micronized Bayburt stone (CMBS) product with an active ratio (AR) of 99.90% and d 10, d 50, and d 90 values of 1.32 μm, 3.48 μm and 9.55 μm were achieved. Finally, particle size distribution (PSD), thermo-gravimetric and differential thermal analyzer (TG-DTA), Fourier transform infrared (FTIR), scanning electron microscope (SEM), electron dispersive spectrum (EDS), and contact angle analyses were performed on the CMBS product. Planetary mill Mechanochemical Surface modification Bayburt stone Uçurum, Metin verfasserin aut Enthalten in Powder technology Amsterdam [u.a.] : Elsevier Science, 1967 436 Online-Ressource (DE-627)320599019 (DE-600)2019938-7 (DE-576)098474278 0032-5910 nnns volume:436 GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2007 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2106 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4336 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 58.10 Verfahrenstechnik: Allgemeines VZ 52.77 Urformen VZ AR 436
language	English
source	Enthalten in Powder technology 436 volume:436
sourceStr	Enthalten in Powder technology 436 volume:436
format_phy_str_mv	Article
bklname	Verfahrenstechnik: Allgemeines Urformen
institution	findex.gbv.de
topic_facet	Planetary mill Mechanochemical Surface modification Bayburt stone
dewey-raw	660
isfreeaccess_bool	false
container_title	Powder technology
authorswithroles_txt_mv	Özdemir, Akın @@aut@@ Uçurum, Metin @@aut@@
publishDateDaySort_date	2024-01-01T00:00:00Z
hierarchy_top_id	320599019
dewey-sort	3660
id	ELV067203876
language_de	englisch
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author	Özdemir, Akın
spellingShingle	Özdemir, Akın ddc 660 bkl 58.10 bkl 52.77 misc Planetary mill misc Mechanochemical misc Surface modification misc Bayburt stone Optimization of mechanochemical surface modification parameters on planetary mill using an I -optimal experimental design
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topic_title	660 VZ 58.10 bkl 52.77 bkl Optimization of mechanochemical surface modification parameters on planetary mill using an I -optimal experimental design Planetary mill Mechanochemical Surface modification Bayburt stone
topic	ddc 660 bkl 58.10 bkl 52.77 misc Planetary mill misc Mechanochemical misc Surface modification misc Bayburt stone
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title	Optimization of mechanochemical surface modification parameters on planetary mill using an I -optimal experimental design
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title_full	Optimization of mechanochemical surface modification parameters on planetary mill using an I -optimal experimental design
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title_sort	optimization of mechanochemical surface modification parameters on planetary mill using an i -optimal experimental design
title_auth	Optimization of mechanochemical surface modification parameters on planetary mill using an I -optimal experimental design
abstract	Several micro-particle-size additives and filler minerals are added to many industrial products, especially plastic, in order to reduce cost and improve mechanical properties and appearance. Also, grinding and surface modification are two fundamental properties of the filler minerals used in plastic products. Notably, Bayburt stone (BS) used as a natural raw material from Bayburt, Türkiye contains 76% SiO2 and 15% Al2O3. In this paper, the hydrophilic surface structure of micronized Bayburt stone (MBS) was made hydrophobe by mechanochemical surface modification using calcium stearate [Ca(C17H35COO)2] in a laboratory-type planetary mill. Next, the optimum conditions of the surface modification design factors, which are (1) ball filling ratio = 30.53%, (2) powder filling ratio = 10.43%, (3) mill speed = 475.91 rpm, (4) chemical dosage = 1.99% of powder, and (5) modification time = 4.83 min., were obtained using the proposed I-optimal design-focused optimization model when predicting the model parameters. In addition, a coated micronized Bayburt stone (CMBS) product with an active ratio (AR) of 99.90% and d 10, d 50, and d 90 values of 1.32 μm, 3.48 μm and 9.55 μm were achieved. Finally, particle size distribution (PSD), thermo-gravimetric and differential thermal analyzer (TG-DTA), Fourier transform infrared (FTIR), scanning electron microscope (SEM), electron dispersive spectrum (EDS), and contact angle analyses were performed on the CMBS product.
abstractGer	Several micro-particle-size additives and filler minerals are added to many industrial products, especially plastic, in order to reduce cost and improve mechanical properties and appearance. Also, grinding and surface modification are two fundamental properties of the filler minerals used in plastic products. Notably, Bayburt stone (BS) used as a natural raw material from Bayburt, Türkiye contains 76% SiO2 and 15% Al2O3. In this paper, the hydrophilic surface structure of micronized Bayburt stone (MBS) was made hydrophobe by mechanochemical surface modification using calcium stearate [Ca(C17H35COO)2] in a laboratory-type planetary mill. Next, the optimum conditions of the surface modification design factors, which are (1) ball filling ratio = 30.53%, (2) powder filling ratio = 10.43%, (3) mill speed = 475.91 rpm, (4) chemical dosage = 1.99% of powder, and (5) modification time = 4.83 min., were obtained using the proposed I-optimal design-focused optimization model when predicting the model parameters. In addition, a coated micronized Bayburt stone (CMBS) product with an active ratio (AR) of 99.90% and d 10, d 50, and d 90 values of 1.32 μm, 3.48 μm and 9.55 μm were achieved. Finally, particle size distribution (PSD), thermo-gravimetric and differential thermal analyzer (TG-DTA), Fourier transform infrared (FTIR), scanning electron microscope (SEM), electron dispersive spectrum (EDS), and contact angle analyses were performed on the CMBS product.
abstract_unstemmed	Several micro-particle-size additives and filler minerals are added to many industrial products, especially plastic, in order to reduce cost and improve mechanical properties and appearance. Also, grinding and surface modification are two fundamental properties of the filler minerals used in plastic products. Notably, Bayburt stone (BS) used as a natural raw material from Bayburt, Türkiye contains 76% SiO2 and 15% Al2O3. In this paper, the hydrophilic surface structure of micronized Bayburt stone (MBS) was made hydrophobe by mechanochemical surface modification using calcium stearate [Ca(C17H35COO)2] in a laboratory-type planetary mill. Next, the optimum conditions of the surface modification design factors, which are (1) ball filling ratio = 30.53%, (2) powder filling ratio = 10.43%, (3) mill speed = 475.91 rpm, (4) chemical dosage = 1.99% of powder, and (5) modification time = 4.83 min., were obtained using the proposed I-optimal design-focused optimization model when predicting the model parameters. In addition, a coated micronized Bayburt stone (CMBS) product with an active ratio (AR) of 99.90% and d 10, d 50, and d 90 values of 1.32 μm, 3.48 μm and 9.55 μm were achieved. Finally, particle size distribution (PSD), thermo-gravimetric and differential thermal analyzer (TG-DTA), Fourier transform infrared (FTIR), scanning electron microscope (SEM), electron dispersive spectrum (EDS), and contact angle analyses were performed on the CMBS product.
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title_short	Optimization of mechanochemical surface modification parameters on planetary mill using an I -optimal experimental design
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doi_str	10.1016/j.powtec.2024.119495
up_date	2024-07-06T20:27:41.505Z
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Optimization of mechanochemical surface modification parameters on planetary mill using an I -optimal experimental design

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