Inverse editing of protons in two-dimensional homonuclear and heteronuclear relayed COSY spectra
Several 1D and 2D inverse proton editing pulse sequences have recently been introduced. One of these, the REPAY sequence, allows the individual editing of XH or XH2 groups. Some new 2D combinations of one- and two-dimensional REPAY experiments with a COSY or TOCSY transfer are described. These combi...
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| Autor*in: |
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| Format: |
E-Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
1991 |
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| Umfang: |
8 Ill. ; 1 Tab. 6 |
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| Reproduktion: |
Wiley InterScience Backfile Collection 1832-2000 |
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| Übergeordnetes Werk: |
in: Organic Magnetic Resonance - Chichester : Wiley, 29(1991) vom: März, Seite 238-243 |
| Übergeordnetes Werk: |
volume:29 ; year:1991 ; month:03 ; pages:238-243 ; extent:6 |
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| 520 | |a Several 1D and 2D inverse proton editing pulse sequences have recently been introduced. One of these, the REPAY sequence, allows the individual editing of XH or XH2 groups. Some new 2D combinations of one- and two-dimensional REPAY experiments with a COSY or TOCSY transfer are described. These combinations provide various possibilities for structural elucidation: the determination of heteronuclear long-range coupling constants nJ(CH) (n = 2, 3), the editing of XH or XH2 groups in two-dimensional H,H COSY spectra and the editing of XH or XH2 groups in X,H COSY spectra followed by a relayed transfer. In contrast to earlier versions of SHIPPED-COSY experiments, the spectra show improved sensitivity and offer the possibility of selecting XH2 groups only, and contain no 1J(XH) coupling because of heteronuclear X decoupling. | ||
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(DE-627)NLEJ159323789 DE-627 ger DE-627 rakwb eng Inverse editing of protons in two-dimensional homonuclear and heteronuclear relayed COSY spectra 1991 8 Ill. 1 Tab. 6 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Several 1D and 2D inverse proton editing pulse sequences have recently been introduced. One of these, the REPAY sequence, allows the individual editing of XH or XH2 groups. Some new 2D combinations of one- and two-dimensional REPAY experiments with a COSY or TOCSY transfer are described. These combinations provide various possibilities for structural elucidation: the determination of heteronuclear long-range coupling constants nJ(CH) (n = 2, 3), the editing of XH or XH2 groups in two-dimensional H,H COSY spectra and the editing of XH or XH2 groups in X,H COSY spectra followed by a relayed transfer. In contrast to earlier versions of SHIPPED-COSY experiments, the spectra show improved sensitivity and offer the possibility of selecting XH2 groups only, and contain no 1J(XH) coupling because of heteronuclear X decoupling. Wiley InterScience Backfile Collection 1832-2000 Wollborn, U. oth Leibfritz, D. oth in Organic Magnetic Resonance Chichester : Wiley 29(1991) vom: März, Seite 238-243 (DE-627)NLEJ159070503 (DE-600)1475029-6 0030-4921 nnns volume:29 year:1991 month:03 pages:238-243 extent:6 http://dx.doi.org/10.1002/mrc.1260290308 text/html Deutschlandweit zugänglich GBV_USEFLAG_U ZDB-1-WIS GBV_NL_ARTICLE AR 29 1991 3 238-243 6 |
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(DE-627)NLEJ159323789 DE-627 ger DE-627 rakwb eng Inverse editing of protons in two-dimensional homonuclear and heteronuclear relayed COSY spectra 1991 8 Ill. 1 Tab. 6 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Several 1D and 2D inverse proton editing pulse sequences have recently been introduced. One of these, the REPAY sequence, allows the individual editing of XH or XH2 groups. Some new 2D combinations of one- and two-dimensional REPAY experiments with a COSY or TOCSY transfer are described. These combinations provide various possibilities for structural elucidation: the determination of heteronuclear long-range coupling constants nJ(CH) (n = 2, 3), the editing of XH or XH2 groups in two-dimensional H,H COSY spectra and the editing of XH or XH2 groups in X,H COSY spectra followed by a relayed transfer. In contrast to earlier versions of SHIPPED-COSY experiments, the spectra show improved sensitivity and offer the possibility of selecting XH2 groups only, and contain no 1J(XH) coupling because of heteronuclear X decoupling. Wiley InterScience Backfile Collection 1832-2000 Wollborn, U. oth Leibfritz, D. oth in Organic Magnetic Resonance Chichester : Wiley 29(1991) vom: März, Seite 238-243 (DE-627)NLEJ159070503 (DE-600)1475029-6 0030-4921 nnns volume:29 year:1991 month:03 pages:238-243 extent:6 http://dx.doi.org/10.1002/mrc.1260290308 text/html Deutschlandweit zugänglich GBV_USEFLAG_U ZDB-1-WIS GBV_NL_ARTICLE AR 29 1991 3 238-243 6 |
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(DE-627)NLEJ159323789 DE-627 ger DE-627 rakwb eng Inverse editing of protons in two-dimensional homonuclear and heteronuclear relayed COSY spectra 1991 8 Ill. 1 Tab. 6 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Several 1D and 2D inverse proton editing pulse sequences have recently been introduced. One of these, the REPAY sequence, allows the individual editing of XH or XH2 groups. Some new 2D combinations of one- and two-dimensional REPAY experiments with a COSY or TOCSY transfer are described. These combinations provide various possibilities for structural elucidation: the determination of heteronuclear long-range coupling constants nJ(CH) (n = 2, 3), the editing of XH or XH2 groups in two-dimensional H,H COSY spectra and the editing of XH or XH2 groups in X,H COSY spectra followed by a relayed transfer. In contrast to earlier versions of SHIPPED-COSY experiments, the spectra show improved sensitivity and offer the possibility of selecting XH2 groups only, and contain no 1J(XH) coupling because of heteronuclear X decoupling. Wiley InterScience Backfile Collection 1832-2000 Wollborn, U. oth Leibfritz, D. oth in Organic Magnetic Resonance Chichester : Wiley 29(1991) vom: März, Seite 238-243 (DE-627)NLEJ159070503 (DE-600)1475029-6 0030-4921 nnns volume:29 year:1991 month:03 pages:238-243 extent:6 http://dx.doi.org/10.1002/mrc.1260290308 text/html Deutschlandweit zugänglich GBV_USEFLAG_U ZDB-1-WIS GBV_NL_ARTICLE AR 29 1991 3 238-243 6 |
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(DE-627)NLEJ159323789 DE-627 ger DE-627 rakwb eng Inverse editing of protons in two-dimensional homonuclear and heteronuclear relayed COSY spectra 1991 8 Ill. 1 Tab. 6 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Several 1D and 2D inverse proton editing pulse sequences have recently been introduced. One of these, the REPAY sequence, allows the individual editing of XH or XH2 groups. Some new 2D combinations of one- and two-dimensional REPAY experiments with a COSY or TOCSY transfer are described. These combinations provide various possibilities for structural elucidation: the determination of heteronuclear long-range coupling constants nJ(CH) (n = 2, 3), the editing of XH or XH2 groups in two-dimensional H,H COSY spectra and the editing of XH or XH2 groups in X,H COSY spectra followed by a relayed transfer. In contrast to earlier versions of SHIPPED-COSY experiments, the spectra show improved sensitivity and offer the possibility of selecting XH2 groups only, and contain no 1J(XH) coupling because of heteronuclear X decoupling. Wiley InterScience Backfile Collection 1832-2000 Wollborn, U. oth Leibfritz, D. oth in Organic Magnetic Resonance Chichester : Wiley 29(1991) vom: März, Seite 238-243 (DE-627)NLEJ159070503 (DE-600)1475029-6 0030-4921 nnns volume:29 year:1991 month:03 pages:238-243 extent:6 http://dx.doi.org/10.1002/mrc.1260290308 text/html Deutschlandweit zugänglich GBV_USEFLAG_U ZDB-1-WIS GBV_NL_ARTICLE AR 29 1991 3 238-243 6 |
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(DE-627)NLEJ159323789 DE-627 ger DE-627 rakwb eng Inverse editing of protons in two-dimensional homonuclear and heteronuclear relayed COSY spectra 1991 8 Ill. 1 Tab. 6 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Several 1D and 2D inverse proton editing pulse sequences have recently been introduced. One of these, the REPAY sequence, allows the individual editing of XH or XH2 groups. Some new 2D combinations of one- and two-dimensional REPAY experiments with a COSY or TOCSY transfer are described. These combinations provide various possibilities for structural elucidation: the determination of heteronuclear long-range coupling constants nJ(CH) (n = 2, 3), the editing of XH or XH2 groups in two-dimensional H,H COSY spectra and the editing of XH or XH2 groups in X,H COSY spectra followed by a relayed transfer. In contrast to earlier versions of SHIPPED-COSY experiments, the spectra show improved sensitivity and offer the possibility of selecting XH2 groups only, and contain no 1J(XH) coupling because of heteronuclear X decoupling. Wiley InterScience Backfile Collection 1832-2000 Wollborn, U. oth Leibfritz, D. oth in Organic Magnetic Resonance Chichester : Wiley 29(1991) vom: März, Seite 238-243 (DE-627)NLEJ159070503 (DE-600)1475029-6 0030-4921 nnns volume:29 year:1991 month:03 pages:238-243 extent:6 http://dx.doi.org/10.1002/mrc.1260290308 text/html Deutschlandweit zugänglich GBV_USEFLAG_U ZDB-1-WIS GBV_NL_ARTICLE AR 29 1991 3 238-243 6 |
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inverse editing of protons in two-dimensional homonuclear and heteronuclear relayed cosy spectra |
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Inverse editing of protons in two-dimensional homonuclear and heteronuclear relayed COSY spectra |
| abstract |
Several 1D and 2D inverse proton editing pulse sequences have recently been introduced. One of these, the REPAY sequence, allows the individual editing of XH or XH2 groups. Some new 2D combinations of one- and two-dimensional REPAY experiments with a COSY or TOCSY transfer are described. These combinations provide various possibilities for structural elucidation: the determination of heteronuclear long-range coupling constants nJ(CH) (n = 2, 3), the editing of XH or XH2 groups in two-dimensional H,H COSY spectra and the editing of XH or XH2 groups in X,H COSY spectra followed by a relayed transfer. In contrast to earlier versions of SHIPPED-COSY experiments, the spectra show improved sensitivity and offer the possibility of selecting XH2 groups only, and contain no 1J(XH) coupling because of heteronuclear X decoupling. |
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Several 1D and 2D inverse proton editing pulse sequences have recently been introduced. One of these, the REPAY sequence, allows the individual editing of XH or XH2 groups. Some new 2D combinations of one- and two-dimensional REPAY experiments with a COSY or TOCSY transfer are described. These combinations provide various possibilities for structural elucidation: the determination of heteronuclear long-range coupling constants nJ(CH) (n = 2, 3), the editing of XH or XH2 groups in two-dimensional H,H COSY spectra and the editing of XH or XH2 groups in X,H COSY spectra followed by a relayed transfer. In contrast to earlier versions of SHIPPED-COSY experiments, the spectra show improved sensitivity and offer the possibility of selecting XH2 groups only, and contain no 1J(XH) coupling because of heteronuclear X decoupling. |
| abstract_unstemmed |
Several 1D and 2D inverse proton editing pulse sequences have recently been introduced. One of these, the REPAY sequence, allows the individual editing of XH or XH2 groups. Some new 2D combinations of one- and two-dimensional REPAY experiments with a COSY or TOCSY transfer are described. These combinations provide various possibilities for structural elucidation: the determination of heteronuclear long-range coupling constants nJ(CH) (n = 2, 3), the editing of XH or XH2 groups in two-dimensional H,H COSY spectra and the editing of XH or XH2 groups in X,H COSY spectra followed by a relayed transfer. In contrast to earlier versions of SHIPPED-COSY experiments, the spectra show improved sensitivity and offer the possibility of selecting XH2 groups only, and contain no 1J(XH) coupling because of heteronuclear X decoupling. |
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<?xml version="1.0" encoding="UTF-8"?><collection xmlns="http://www.loc.gov/MARC21/slim"><record><leader>01000caa a22002652 4500</leader><controlfield tag="001">NLEJ159323789</controlfield><controlfield tag="003">DE-627</controlfield><controlfield tag="005">20210707003938.0</controlfield><controlfield tag="007">cr uuu---uuuuu</controlfield><controlfield tag="008">070201s1991 xx |||||o 00| ||eng c</controlfield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(DE-627)NLEJ159323789</subfield></datafield><datafield tag="040" ind1=" " ind2=" "><subfield code="a">DE-627</subfield><subfield code="b">ger</subfield><subfield code="c">DE-627</subfield><subfield code="e">rakwb</subfield></datafield><datafield tag="041" ind1=" " ind2=" "><subfield code="a">eng</subfield></datafield><datafield tag="245" ind1="1" ind2="0"><subfield code="a">Inverse editing of protons in two-dimensional homonuclear and heteronuclear relayed COSY spectra</subfield></datafield><datafield tag="264" ind1=" " ind2="1"><subfield code="c">1991</subfield></datafield><datafield tag="300" ind1=" " ind2=" "><subfield code="b">8 Ill.</subfield><subfield code="b">1 Tab.</subfield></datafield><datafield tag="300" ind1=" " ind2=" "><subfield code="a">6</subfield></datafield><datafield tag="336" ind1=" " ind2=" "><subfield code="a">nicht spezifiziert</subfield><subfield code="b">zzz</subfield><subfield code="2">rdacontent</subfield></datafield><datafield tag="337" ind1=" " ind2=" "><subfield code="a">nicht spezifiziert</subfield><subfield code="b">z</subfield><subfield code="2">rdamedia</subfield></datafield><datafield tag="338" ind1=" " ind2=" "><subfield code="a">nicht spezifiziert</subfield><subfield code="b">zu</subfield><subfield code="2">rdacarrier</subfield></datafield><datafield tag="520" ind1=" " ind2=" "><subfield code="a">Several 1D and 2D inverse proton editing pulse sequences have recently been introduced. One of these, the REPAY sequence, allows the individual editing of XH or XH2 groups. Some new 2D combinations of one- and two-dimensional REPAY experiments with a COSY or TOCSY transfer are described. These combinations provide various possibilities for structural elucidation: the determination of heteronuclear long-range coupling constants nJ(CH) (n = 2, 3), the editing of XH or XH2 groups in two-dimensional H,H COSY spectra and the editing of XH or XH2 groups in X,H COSY spectra followed by a relayed transfer. In contrast to earlier versions of SHIPPED-COSY experiments, the spectra show improved sensitivity and offer the possibility of selecting XH2 groups only, and contain no 1J(XH) coupling because of heteronuclear X decoupling.</subfield></datafield><datafield tag="533" ind1=" " ind2=" "><subfield code="f">Wiley InterScience Backfile Collection 1832-2000</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Wollborn, U.</subfield><subfield code="4">oth</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Leibfritz, D.</subfield><subfield code="4">oth</subfield></datafield><datafield tag="773" ind1="0" ind2="8"><subfield code="i">in</subfield><subfield code="t">Organic Magnetic Resonance</subfield><subfield code="d">Chichester : Wiley</subfield><subfield code="g">29(1991) vom: März, Seite 238-243</subfield><subfield code="w">(DE-627)NLEJ159070503</subfield><subfield code="w">(DE-600)1475029-6</subfield><subfield code="x">0030-4921</subfield><subfield code="7">nnns</subfield></datafield><datafield tag="773" ind1="1" ind2="8"><subfield code="g">volume:29</subfield><subfield code="g">year:1991</subfield><subfield code="g">month:03</subfield><subfield code="g">pages:238-243</subfield><subfield code="g">extent:6</subfield></datafield><datafield tag="856" ind1="4" ind2="0"><subfield code="u">http://dx.doi.org/10.1002/mrc.1260290308</subfield><subfield code="q">text/html</subfield><subfield code="z">Deutschlandweit zugänglich</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_USEFLAG_U</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">ZDB-1-WIS</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_NL_ARTICLE</subfield></datafield><datafield tag="951" ind1=" " ind2=" "><subfield code="a">AR</subfield></datafield><datafield tag="952" ind1=" " ind2=" "><subfield code="d">29</subfield><subfield code="j">1991</subfield><subfield code="c">3</subfield><subfield code="h">238-243</subfield><subfield code="g">6</subfield></datafield></record></collection>
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