Complete assignment and conformational studies of tomatine and tomatidine
Heteronuclear correlation techniques and homonuclear E.COSY spectra were used to obtain a complete assignment of the 13C and 1H NMR spectra of the aglycone tomatidine. In addition, 1D/2D TOCSY, NOESY and ROESY spectra allowed the assignment of the sugar moiety in tomatine. The procedure used is of g...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
|---|
| Format: |
E-Artikel |
|---|---|
| Sprache: |
Englisch |
| Erschienen: |
1992 |
|---|
| Umfang: |
5 Ill. ; 3 Tab. 6 |
|---|
| Reproduktion: |
Wiley InterScience Backfile Collection 1832-2000 |
|---|---|
| Übergeordnetes Werk: |
in: Organic Magnetic Resonance - Chichester : Wiley, 30(1992) vom: Juli, Seite 645-650 |
| Übergeordnetes Werk: |
volume:30 ; year:1992 ; month:07 ; pages:645-650 ; extent:6 |
| Links: |
|---|
| Katalog-ID: |
NLEJ159327202 |
|---|
| LEADER | 01000caa a22002652 4500 | ||
|---|---|---|---|
| 001 | NLEJ159327202 | ||
| 003 | DE-627 | ||
| 005 | 20210707004014.0 | ||
| 007 | cr uuu---uuuuu | ||
| 008 | 070201s1992 xx |||||o 00| ||eng c | ||
| 035 | |a (DE-627)NLEJ159327202 | ||
| 040 | |a DE-627 |b ger |c DE-627 |e rakwb | ||
| 041 | |a eng | ||
| 245 | 1 | 0 | |a Complete assignment and conformational studies of tomatine and tomatidine |
| 264 | 1 | |c 1992 | |
| 300 | |b 5 Ill. |b 3 Tab. | ||
| 300 | |a 6 | ||
| 336 | |a nicht spezifiziert |b zzz |2 rdacontent | ||
| 337 | |a nicht spezifiziert |b z |2 rdamedia | ||
| 338 | |a nicht spezifiziert |b zu |2 rdacarrier | ||
| 520 | |a Heteronuclear correlation techniques and homonuclear E.COSY spectra were used to obtain a complete assignment of the 13C and 1H NMR spectra of the aglycone tomatidine. In addition, 1D/2D TOCSY, NOESY and ROESY spectra allowed the assignment of the sugar moiety in tomatine. The procedure used is of general applicability for the structural elucidation of sugars and glycosidic biomolecules. | ||
| 533 | |f Wiley InterScience Backfile Collection 1832-2000 | ||
| 700 | 1 | |a Willker, W. |4 oth | |
| 700 | 1 | |a Leibfritz, D. |4 oth | |
| 773 | 0 | 8 | |i in |t Organic Magnetic Resonance |d Chichester : Wiley |g 30(1992) vom: Juli, Seite 645-650 |w (DE-627)NLEJ159070503 |w (DE-600)1475029-6 |x 0030-4921 |7 nnns |
| 773 | 1 | 8 | |g volume:30 |g year:1992 |g month:07 |g pages:645-650 |g extent:6 |
| 856 | 4 | 0 | |u http://dx.doi.org/10.1002/mrc.1260300713 |q text/html |z Deutschlandweit zugänglich |
| 912 | |a GBV_USEFLAG_U | ||
| 912 | |a ZDB-1-WIS | ||
| 912 | |a GBV_NL_ARTICLE | ||
| 951 | |a AR | ||
| 952 | |d 30 |j 1992 |c 7 |h 645-650 |g 6 | ||
| matchkey_str |
article:00304921:1992----::opeesinetncnomtoasuisfoa |
|---|---|
| hierarchy_sort_str |
1992 |
| publishDate |
1992 |
| allfields |
(DE-627)NLEJ159327202 DE-627 ger DE-627 rakwb eng Complete assignment and conformational studies of tomatine and tomatidine 1992 5 Ill. 3 Tab. 6 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Heteronuclear correlation techniques and homonuclear E.COSY spectra were used to obtain a complete assignment of the 13C and 1H NMR spectra of the aglycone tomatidine. In addition, 1D/2D TOCSY, NOESY and ROESY spectra allowed the assignment of the sugar moiety in tomatine. The procedure used is of general applicability for the structural elucidation of sugars and glycosidic biomolecules. Wiley InterScience Backfile Collection 1832-2000 Willker, W. oth Leibfritz, D. oth in Organic Magnetic Resonance Chichester : Wiley 30(1992) vom: Juli, Seite 645-650 (DE-627)NLEJ159070503 (DE-600)1475029-6 0030-4921 nnns volume:30 year:1992 month:07 pages:645-650 extent:6 http://dx.doi.org/10.1002/mrc.1260300713 text/html Deutschlandweit zugänglich GBV_USEFLAG_U ZDB-1-WIS GBV_NL_ARTICLE AR 30 1992 7 645-650 6 |
| spelling |
(DE-627)NLEJ159327202 DE-627 ger DE-627 rakwb eng Complete assignment and conformational studies of tomatine and tomatidine 1992 5 Ill. 3 Tab. 6 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Heteronuclear correlation techniques and homonuclear E.COSY spectra were used to obtain a complete assignment of the 13C and 1H NMR spectra of the aglycone tomatidine. In addition, 1D/2D TOCSY, NOESY and ROESY spectra allowed the assignment of the sugar moiety in tomatine. The procedure used is of general applicability for the structural elucidation of sugars and glycosidic biomolecules. Wiley InterScience Backfile Collection 1832-2000 Willker, W. oth Leibfritz, D. oth in Organic Magnetic Resonance Chichester : Wiley 30(1992) vom: Juli, Seite 645-650 (DE-627)NLEJ159070503 (DE-600)1475029-6 0030-4921 nnns volume:30 year:1992 month:07 pages:645-650 extent:6 http://dx.doi.org/10.1002/mrc.1260300713 text/html Deutschlandweit zugänglich GBV_USEFLAG_U ZDB-1-WIS GBV_NL_ARTICLE AR 30 1992 7 645-650 6 |
| allfields_unstemmed |
(DE-627)NLEJ159327202 DE-627 ger DE-627 rakwb eng Complete assignment and conformational studies of tomatine and tomatidine 1992 5 Ill. 3 Tab. 6 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Heteronuclear correlation techniques and homonuclear E.COSY spectra were used to obtain a complete assignment of the 13C and 1H NMR spectra of the aglycone tomatidine. In addition, 1D/2D TOCSY, NOESY and ROESY spectra allowed the assignment of the sugar moiety in tomatine. The procedure used is of general applicability for the structural elucidation of sugars and glycosidic biomolecules. Wiley InterScience Backfile Collection 1832-2000 Willker, W. oth Leibfritz, D. oth in Organic Magnetic Resonance Chichester : Wiley 30(1992) vom: Juli, Seite 645-650 (DE-627)NLEJ159070503 (DE-600)1475029-6 0030-4921 nnns volume:30 year:1992 month:07 pages:645-650 extent:6 http://dx.doi.org/10.1002/mrc.1260300713 text/html Deutschlandweit zugänglich GBV_USEFLAG_U ZDB-1-WIS GBV_NL_ARTICLE AR 30 1992 7 645-650 6 |
| allfieldsGer |
(DE-627)NLEJ159327202 DE-627 ger DE-627 rakwb eng Complete assignment and conformational studies of tomatine and tomatidine 1992 5 Ill. 3 Tab. 6 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Heteronuclear correlation techniques and homonuclear E.COSY spectra were used to obtain a complete assignment of the 13C and 1H NMR spectra of the aglycone tomatidine. In addition, 1D/2D TOCSY, NOESY and ROESY spectra allowed the assignment of the sugar moiety in tomatine. The procedure used is of general applicability for the structural elucidation of sugars and glycosidic biomolecules. Wiley InterScience Backfile Collection 1832-2000 Willker, W. oth Leibfritz, D. oth in Organic Magnetic Resonance Chichester : Wiley 30(1992) vom: Juli, Seite 645-650 (DE-627)NLEJ159070503 (DE-600)1475029-6 0030-4921 nnns volume:30 year:1992 month:07 pages:645-650 extent:6 http://dx.doi.org/10.1002/mrc.1260300713 text/html Deutschlandweit zugänglich GBV_USEFLAG_U ZDB-1-WIS GBV_NL_ARTICLE AR 30 1992 7 645-650 6 |
| allfieldsSound |
(DE-627)NLEJ159327202 DE-627 ger DE-627 rakwb eng Complete assignment and conformational studies of tomatine and tomatidine 1992 5 Ill. 3 Tab. 6 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Heteronuclear correlation techniques and homonuclear E.COSY spectra were used to obtain a complete assignment of the 13C and 1H NMR spectra of the aglycone tomatidine. In addition, 1D/2D TOCSY, NOESY and ROESY spectra allowed the assignment of the sugar moiety in tomatine. The procedure used is of general applicability for the structural elucidation of sugars and glycosidic biomolecules. Wiley InterScience Backfile Collection 1832-2000 Willker, W. oth Leibfritz, D. oth in Organic Magnetic Resonance Chichester : Wiley 30(1992) vom: Juli, Seite 645-650 (DE-627)NLEJ159070503 (DE-600)1475029-6 0030-4921 nnns volume:30 year:1992 month:07 pages:645-650 extent:6 http://dx.doi.org/10.1002/mrc.1260300713 text/html Deutschlandweit zugänglich GBV_USEFLAG_U ZDB-1-WIS GBV_NL_ARTICLE AR 30 1992 7 645-650 6 |
| language |
English |
| source |
in Organic Magnetic Resonance 30(1992) vom: Juli, Seite 645-650 volume:30 year:1992 month:07 pages:645-650 extent:6 |
| sourceStr |
in Organic Magnetic Resonance 30(1992) vom: Juli, Seite 645-650 volume:30 year:1992 month:07 pages:645-650 extent:6 |
| format_phy_str_mv |
Article |
| institution |
findex.gbv.de |
| isfreeaccess_bool |
false |
| container_title |
Organic Magnetic Resonance |
| authorswithroles_txt_mv |
Willker, W. @@oth@@ Leibfritz, D. @@oth@@ |
| publishDateDaySort_date |
1992-07-01T00:00:00Z |
| hierarchy_top_id |
NLEJ159070503 |
| id |
NLEJ159327202 |
| language_de |
englisch |
| fullrecord_marcxml |
<?xml version="1.0" encoding="UTF-8"?><collection xmlns="http://www.loc.gov/MARC21/slim"><record><leader>01000caa a22002652 4500</leader><controlfield tag="001">NLEJ159327202</controlfield><controlfield tag="003">DE-627</controlfield><controlfield tag="005">20210707004014.0</controlfield><controlfield tag="007">cr uuu---uuuuu</controlfield><controlfield tag="008">070201s1992 xx |||||o 00| ||eng c</controlfield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(DE-627)NLEJ159327202</subfield></datafield><datafield tag="040" ind1=" " ind2=" "><subfield code="a">DE-627</subfield><subfield code="b">ger</subfield><subfield code="c">DE-627</subfield><subfield code="e">rakwb</subfield></datafield><datafield tag="041" ind1=" " ind2=" "><subfield code="a">eng</subfield></datafield><datafield tag="245" ind1="1" ind2="0"><subfield code="a">Complete assignment and conformational studies of tomatine and tomatidine</subfield></datafield><datafield tag="264" ind1=" " ind2="1"><subfield code="c">1992</subfield></datafield><datafield tag="300" ind1=" " ind2=" "><subfield code="b">5 Ill.</subfield><subfield code="b">3 Tab.</subfield></datafield><datafield tag="300" ind1=" " ind2=" "><subfield code="a">6</subfield></datafield><datafield tag="336" ind1=" " ind2=" "><subfield code="a">nicht spezifiziert</subfield><subfield code="b">zzz</subfield><subfield code="2">rdacontent</subfield></datafield><datafield tag="337" ind1=" " ind2=" "><subfield code="a">nicht spezifiziert</subfield><subfield code="b">z</subfield><subfield code="2">rdamedia</subfield></datafield><datafield tag="338" ind1=" " ind2=" "><subfield code="a">nicht spezifiziert</subfield><subfield code="b">zu</subfield><subfield code="2">rdacarrier</subfield></datafield><datafield tag="520" ind1=" " ind2=" "><subfield code="a">Heteronuclear correlation techniques and homonuclear E.COSY spectra were used to obtain a complete assignment of the 13C and 1H NMR spectra of the aglycone tomatidine. In addition, 1D/2D TOCSY, NOESY and ROESY spectra allowed the assignment of the sugar moiety in tomatine. The procedure used is of general applicability for the structural elucidation of sugars and glycosidic biomolecules.</subfield></datafield><datafield tag="533" ind1=" " ind2=" "><subfield code="f">Wiley InterScience Backfile Collection 1832-2000</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Willker, W.</subfield><subfield code="4">oth</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Leibfritz, D.</subfield><subfield code="4">oth</subfield></datafield><datafield tag="773" ind1="0" ind2="8"><subfield code="i">in</subfield><subfield code="t">Organic Magnetic Resonance</subfield><subfield code="d">Chichester : Wiley</subfield><subfield code="g">30(1992) vom: Juli, Seite 645-650</subfield><subfield code="w">(DE-627)NLEJ159070503</subfield><subfield code="w">(DE-600)1475029-6</subfield><subfield code="x">0030-4921</subfield><subfield code="7">nnns</subfield></datafield><datafield tag="773" ind1="1" ind2="8"><subfield code="g">volume:30</subfield><subfield code="g">year:1992</subfield><subfield code="g">month:07</subfield><subfield code="g">pages:645-650</subfield><subfield code="g">extent:6</subfield></datafield><datafield tag="856" ind1="4" ind2="0"><subfield code="u">http://dx.doi.org/10.1002/mrc.1260300713</subfield><subfield code="q">text/html</subfield><subfield code="z">Deutschlandweit zugänglich</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_USEFLAG_U</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">ZDB-1-WIS</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_NL_ARTICLE</subfield></datafield><datafield tag="951" ind1=" " ind2=" "><subfield code="a">AR</subfield></datafield><datafield tag="952" ind1=" " ind2=" "><subfield code="d">30</subfield><subfield code="j">1992</subfield><subfield code="c">7</subfield><subfield code="h">645-650</subfield><subfield code="g">6</subfield></datafield></record></collection>
|
| fullrecord |
<?xml version="1.0" encoding="UTF-8"?><collection xmlns="http://www.loc.gov/MARC21/slim"><record><leader>01000caa a22002652 4500</leader><controlfield tag="001">NLEJ159327202</controlfield><controlfield tag="003">DE-627</controlfield><controlfield tag="005">20210707004014.0</controlfield><controlfield tag="007">cr uuu---uuuuu</controlfield><controlfield tag="008">070201s1992 xx |||||o 00| ||eng c</controlfield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(DE-627)NLEJ159327202</subfield></datafield><datafield tag="040" ind1=" " ind2=" "><subfield code="a">DE-627</subfield><subfield code="b">ger</subfield><subfield code="c">DE-627</subfield><subfield code="e">rakwb</subfield></datafield><datafield tag="041" ind1=" " ind2=" "><subfield code="a">eng</subfield></datafield><datafield tag="245" ind1="1" ind2="0"><subfield code="a">Complete assignment and conformational studies of tomatine and tomatidine</subfield></datafield><datafield tag="264" ind1=" " ind2="1"><subfield code="c">1992</subfield></datafield><datafield tag="300" ind1=" " ind2=" "><subfield code="b">5 Ill.</subfield><subfield code="b">3 Tab.</subfield></datafield><datafield tag="300" ind1=" " ind2=" "><subfield code="a">6</subfield></datafield><datafield tag="336" ind1=" " ind2=" "><subfield code="a">nicht spezifiziert</subfield><subfield code="b">zzz</subfield><subfield code="2">rdacontent</subfield></datafield><datafield tag="337" ind1=" " ind2=" "><subfield code="a">nicht spezifiziert</subfield><subfield code="b">z</subfield><subfield code="2">rdamedia</subfield></datafield><datafield tag="338" ind1=" " ind2=" "><subfield code="a">nicht spezifiziert</subfield><subfield code="b">zu</subfield><subfield code="2">rdacarrier</subfield></datafield><datafield tag="520" ind1=" " ind2=" "><subfield code="a">Heteronuclear correlation techniques and homonuclear E.COSY spectra were used to obtain a complete assignment of the 13C and 1H NMR spectra of the aglycone tomatidine. In addition, 1D/2D TOCSY, NOESY and ROESY spectra allowed the assignment of the sugar moiety in tomatine. The procedure used is of general applicability for the structural elucidation of sugars and glycosidic biomolecules.</subfield></datafield><datafield tag="533" ind1=" " ind2=" "><subfield code="f">Wiley InterScience Backfile Collection 1832-2000</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Willker, W.</subfield><subfield code="4">oth</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Leibfritz, D.</subfield><subfield code="4">oth</subfield></datafield><datafield tag="773" ind1="0" ind2="8"><subfield code="i">in</subfield><subfield code="t">Organic Magnetic Resonance</subfield><subfield code="d">Chichester : Wiley</subfield><subfield code="g">30(1992) vom: Juli, Seite 645-650</subfield><subfield code="w">(DE-627)NLEJ159070503</subfield><subfield code="w">(DE-600)1475029-6</subfield><subfield code="x">0030-4921</subfield><subfield code="7">nnns</subfield></datafield><datafield tag="773" ind1="1" ind2="8"><subfield code="g">volume:30</subfield><subfield code="g">year:1992</subfield><subfield code="g">month:07</subfield><subfield code="g">pages:645-650</subfield><subfield code="g">extent:6</subfield></datafield><datafield tag="856" ind1="4" ind2="0"><subfield code="u">http://dx.doi.org/10.1002/mrc.1260300713</subfield><subfield code="q">text/html</subfield><subfield code="z">Deutschlandweit zugänglich</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_USEFLAG_U</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">ZDB-1-WIS</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_NL_ARTICLE</subfield></datafield><datafield tag="951" ind1=" " ind2=" "><subfield code="a">AR</subfield></datafield><datafield tag="952" ind1=" " ind2=" "><subfield code="d">30</subfield><subfield code="j">1992</subfield><subfield code="c">7</subfield><subfield code="h">645-650</subfield><subfield code="g">6</subfield></datafield></record></collection>
|
| series2 |
Wiley InterScience Backfile Collection 1832-2000 |
| ppnlink_with_tag_str_mv |
@@773@@(DE-627)NLEJ159070503 |
| format |
electronic Article |
| delete_txt_mv |
keep |
| collection |
NL |
| remote_str |
true |
| illustrated |
Illustrated |
| issn |
0030-4921 |
| topic_title |
Complete assignment and conformational studies of tomatine and tomatidine |
| format_facet |
Elektronische Aufsätze Aufsätze Elektronische Ressource |
| format_main_str_mv |
Text Zeitschrift/Artikel |
| carriertype_str_mv |
zu |
| author2_variant |
w w ww d l dl |
| hierarchy_parent_title |
Organic Magnetic Resonance |
| hierarchy_parent_id |
NLEJ159070503 |
| hierarchy_top_title |
Organic Magnetic Resonance |
| isfreeaccess_txt |
false |
| familylinks_str_mv |
(DE-627)NLEJ159070503 (DE-600)1475029-6 |
| title |
Complete assignment and conformational studies of tomatine and tomatidine |
| spellingShingle |
Complete assignment and conformational studies of tomatine and tomatidine |
| ctrlnum |
(DE-627)NLEJ159327202 |
| title_full |
Complete assignment and conformational studies of tomatine and tomatidine |
| journal |
Organic Magnetic Resonance |
| journalStr |
Organic Magnetic Resonance |
| lang_code |
eng |
| isOA_bool |
false |
| recordtype |
marc |
| publishDateSort |
1992 |
| contenttype_str_mv |
zzz |
| container_start_page |
645 |
| container_volume |
30 |
| physical |
5 Ill. 3 Tab. 6 |
| format_se |
Elektronische Aufsätze |
| title_sort |
complete assignment and conformational studies of tomatine and tomatidine |
| title_auth |
Complete assignment and conformational studies of tomatine and tomatidine |
| abstract |
Heteronuclear correlation techniques and homonuclear E.COSY spectra were used to obtain a complete assignment of the 13C and 1H NMR spectra of the aglycone tomatidine. In addition, 1D/2D TOCSY, NOESY and ROESY spectra allowed the assignment of the sugar moiety in tomatine. The procedure used is of general applicability for the structural elucidation of sugars and glycosidic biomolecules. |
| abstractGer |
Heteronuclear correlation techniques and homonuclear E.COSY spectra were used to obtain a complete assignment of the 13C and 1H NMR spectra of the aglycone tomatidine. In addition, 1D/2D TOCSY, NOESY and ROESY spectra allowed the assignment of the sugar moiety in tomatine. The procedure used is of general applicability for the structural elucidation of sugars and glycosidic biomolecules. |
| abstract_unstemmed |
Heteronuclear correlation techniques and homonuclear E.COSY spectra were used to obtain a complete assignment of the 13C and 1H NMR spectra of the aglycone tomatidine. In addition, 1D/2D TOCSY, NOESY and ROESY spectra allowed the assignment of the sugar moiety in tomatine. The procedure used is of general applicability for the structural elucidation of sugars and glycosidic biomolecules. |
| collection_details |
GBV_USEFLAG_U ZDB-1-WIS GBV_NL_ARTICLE |
| title_short |
Complete assignment and conformational studies of tomatine and tomatidine |
| url |
http://dx.doi.org/10.1002/mrc.1260300713 |
| remote_bool |
true |
| author2 |
Willker, W. Leibfritz, D. |
| author2Str |
Willker, W. Leibfritz, D. |
| ppnlink |
NLEJ159070503 |
| mediatype_str_mv |
z |
| isOA_txt |
false |
| hochschulschrift_bool |
false |
| author2_role |
oth oth |
| up_date |
2024-07-06T05:41:39.180Z |
| _version_ |
1803807095972167680 |
| score |
7.3988543 |