Determination of trace vanadium in natural waters by a combined ion exchange-catalytic photometric method
A sensitive, selective and simple method is described for the determination of trace vanadium in natural waters. Vanadium is separated and concentrated by a combined cation- and anion-exchange procedure in 0.05 M HCl-0.1 % H"2O"2 media, and determined by the catalytic method based on the o...
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| Autor*in: |
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| Format: |
E-Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
1977 |
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| Reproduktion: |
Elsevier Journal Backfiles on ScienceDirect 1907 - 2002 |
|---|---|
| Übergeordnetes Werk: |
in: Analytica Chimica Acta - Amsterdam : Elsevier, 88(1977), 1, Seite 147-153 |
| Übergeordnetes Werk: |
volume:88 ; year:1977 ; number:1 ; pages:147-153 |
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| 520 | |a A sensitive, selective and simple method is described for the determination of trace vanadium in natural waters. Vanadium is separated and concentrated by a combined cation- and anion-exchange procedure in 0.05 M HCl-0.1 % H"2O"2 media, and determined by the catalytic method based on the oxidation of gallic acid by bromate. The proposed method is applied to the analysis of natural waters. The relative standard deviations are 3.9 % for 0.8 p.p.b. of vanadium in river water and 3.2 % for 1.9 p.p.b. of vanadium in lake water (surface). As little as 0.03 p.p.b. of vanadium can be determined in samples of 100 ml or less. | ||
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(DE-627)NLEJ17358893X (DE-599)GBVNLZ17358893X DE-627 ger DE-627 rakwb eng Determination of trace vanadium in natural waters by a combined ion exchange-catalytic photometric method 1977 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier A sensitive, selective and simple method is described for the determination of trace vanadium in natural waters. Vanadium is separated and concentrated by a combined cation- and anion-exchange procedure in 0.05 M HCl-0.1 % H"2O"2 media, and determined by the catalytic method based on the oxidation of gallic acid by bromate. The proposed method is applied to the analysis of natural waters. The relative standard deviations are 3.9 % for 0.8 p.p.b. of vanadium in river water and 3.2 % for 1.9 p.p.b. of vanadium in lake water (surface). As little as 0.03 p.p.b. of vanadium can be determined in samples of 100 ml or less. Elsevier Journal Backfiles on ScienceDirect 1907 - 2002 Fukasawa, T. oth Yamane, T. oth in Analytica Chimica Acta Amsterdam : Elsevier 88(1977), 1, Seite 147-153 (DE-627)NLEJ173450067 (DE-600)1483436-4 0003-2670 nnns volume:88 year:1977 number:1 pages:147-153 http://linkinghub.elsevier.com/retrieve/pii/S0003-2670(01)96059-3 GBV_USEFLAG_H ZDB-1-SDJ GBV_NL_ARTICLE AR 88 1977 1 147-153 |
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(DE-627)NLEJ17358893X (DE-599)GBVNLZ17358893X DE-627 ger DE-627 rakwb eng Determination of trace vanadium in natural waters by a combined ion exchange-catalytic photometric method 1977 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier A sensitive, selective and simple method is described for the determination of trace vanadium in natural waters. Vanadium is separated and concentrated by a combined cation- and anion-exchange procedure in 0.05 M HCl-0.1 % H"2O"2 media, and determined by the catalytic method based on the oxidation of gallic acid by bromate. The proposed method is applied to the analysis of natural waters. The relative standard deviations are 3.9 % for 0.8 p.p.b. of vanadium in river water and 3.2 % for 1.9 p.p.b. of vanadium in lake water (surface). As little as 0.03 p.p.b. of vanadium can be determined in samples of 100 ml or less. Elsevier Journal Backfiles on ScienceDirect 1907 - 2002 Fukasawa, T. oth Yamane, T. oth in Analytica Chimica Acta Amsterdam : Elsevier 88(1977), 1, Seite 147-153 (DE-627)NLEJ173450067 (DE-600)1483436-4 0003-2670 nnns volume:88 year:1977 number:1 pages:147-153 http://linkinghub.elsevier.com/retrieve/pii/S0003-2670(01)96059-3 GBV_USEFLAG_H ZDB-1-SDJ GBV_NL_ARTICLE AR 88 1977 1 147-153 |
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(DE-627)NLEJ17358893X (DE-599)GBVNLZ17358893X DE-627 ger DE-627 rakwb eng Determination of trace vanadium in natural waters by a combined ion exchange-catalytic photometric method 1977 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier A sensitive, selective and simple method is described for the determination of trace vanadium in natural waters. Vanadium is separated and concentrated by a combined cation- and anion-exchange procedure in 0.05 M HCl-0.1 % H"2O"2 media, and determined by the catalytic method based on the oxidation of gallic acid by bromate. The proposed method is applied to the analysis of natural waters. The relative standard deviations are 3.9 % for 0.8 p.p.b. of vanadium in river water and 3.2 % for 1.9 p.p.b. of vanadium in lake water (surface). As little as 0.03 p.p.b. of vanadium can be determined in samples of 100 ml or less. Elsevier Journal Backfiles on ScienceDirect 1907 - 2002 Fukasawa, T. oth Yamane, T. oth in Analytica Chimica Acta Amsterdam : Elsevier 88(1977), 1, Seite 147-153 (DE-627)NLEJ173450067 (DE-600)1483436-4 0003-2670 nnns volume:88 year:1977 number:1 pages:147-153 http://linkinghub.elsevier.com/retrieve/pii/S0003-2670(01)96059-3 GBV_USEFLAG_H ZDB-1-SDJ GBV_NL_ARTICLE AR 88 1977 1 147-153 |
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(DE-627)NLEJ17358893X (DE-599)GBVNLZ17358893X DE-627 ger DE-627 rakwb eng Determination of trace vanadium in natural waters by a combined ion exchange-catalytic photometric method 1977 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier A sensitive, selective and simple method is described for the determination of trace vanadium in natural waters. Vanadium is separated and concentrated by a combined cation- and anion-exchange procedure in 0.05 M HCl-0.1 % H"2O"2 media, and determined by the catalytic method based on the oxidation of gallic acid by bromate. The proposed method is applied to the analysis of natural waters. The relative standard deviations are 3.9 % for 0.8 p.p.b. of vanadium in river water and 3.2 % for 1.9 p.p.b. of vanadium in lake water (surface). As little as 0.03 p.p.b. of vanadium can be determined in samples of 100 ml or less. Elsevier Journal Backfiles on ScienceDirect 1907 - 2002 Fukasawa, T. oth Yamane, T. oth in Analytica Chimica Acta Amsterdam : Elsevier 88(1977), 1, Seite 147-153 (DE-627)NLEJ173450067 (DE-600)1483436-4 0003-2670 nnns volume:88 year:1977 number:1 pages:147-153 http://linkinghub.elsevier.com/retrieve/pii/S0003-2670(01)96059-3 GBV_USEFLAG_H ZDB-1-SDJ GBV_NL_ARTICLE AR 88 1977 1 147-153 |
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(DE-627)NLEJ17358893X (DE-599)GBVNLZ17358893X DE-627 ger DE-627 rakwb eng Determination of trace vanadium in natural waters by a combined ion exchange-catalytic photometric method 1977 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier A sensitive, selective and simple method is described for the determination of trace vanadium in natural waters. Vanadium is separated and concentrated by a combined cation- and anion-exchange procedure in 0.05 M HCl-0.1 % H"2O"2 media, and determined by the catalytic method based on the oxidation of gallic acid by bromate. The proposed method is applied to the analysis of natural waters. The relative standard deviations are 3.9 % for 0.8 p.p.b. of vanadium in river water and 3.2 % for 1.9 p.p.b. of vanadium in lake water (surface). As little as 0.03 p.p.b. of vanadium can be determined in samples of 100 ml or less. Elsevier Journal Backfiles on ScienceDirect 1907 - 2002 Fukasawa, T. oth Yamane, T. oth in Analytica Chimica Acta Amsterdam : Elsevier 88(1977), 1, Seite 147-153 (DE-627)NLEJ173450067 (DE-600)1483436-4 0003-2670 nnns volume:88 year:1977 number:1 pages:147-153 http://linkinghub.elsevier.com/retrieve/pii/S0003-2670(01)96059-3 GBV_USEFLAG_H ZDB-1-SDJ GBV_NL_ARTICLE AR 88 1977 1 147-153 |
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determination of trace vanadium in natural waters by a combined ion exchange-catalytic photometric method |
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Determination of trace vanadium in natural waters by a combined ion exchange-catalytic photometric method |
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A sensitive, selective and simple method is described for the determination of trace vanadium in natural waters. Vanadium is separated and concentrated by a combined cation- and anion-exchange procedure in 0.05 M HCl-0.1 % H"2O"2 media, and determined by the catalytic method based on the oxidation of gallic acid by bromate. The proposed method is applied to the analysis of natural waters. The relative standard deviations are 3.9 % for 0.8 p.p.b. of vanadium in river water and 3.2 % for 1.9 p.p.b. of vanadium in lake water (surface). As little as 0.03 p.p.b. of vanadium can be determined in samples of 100 ml or less. |
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A sensitive, selective and simple method is described for the determination of trace vanadium in natural waters. Vanadium is separated and concentrated by a combined cation- and anion-exchange procedure in 0.05 M HCl-0.1 % H"2O"2 media, and determined by the catalytic method based on the oxidation of gallic acid by bromate. The proposed method is applied to the analysis of natural waters. The relative standard deviations are 3.9 % for 0.8 p.p.b. of vanadium in river water and 3.2 % for 1.9 p.p.b. of vanadium in lake water (surface). As little as 0.03 p.p.b. of vanadium can be determined in samples of 100 ml or less. |
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A sensitive, selective and simple method is described for the determination of trace vanadium in natural waters. Vanadium is separated and concentrated by a combined cation- and anion-exchange procedure in 0.05 M HCl-0.1 % H"2O"2 media, and determined by the catalytic method based on the oxidation of gallic acid by bromate. The proposed method is applied to the analysis of natural waters. The relative standard deviations are 3.9 % for 0.8 p.p.b. of vanadium in river water and 3.2 % for 1.9 p.p.b. of vanadium in lake water (surface). As little as 0.03 p.p.b. of vanadium can be determined in samples of 100 ml or less. |
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