Redox reactions involving rhenium and uranium hexafluorides, a convenient synthesis of β-uranium pentafluoride
Rhenium and uranium hexafluorides oxidise elemental iodine in iodine pentafluoride at ambient temperature to give the I"2^+ cation. With UF"6 an additional reaction occurs to give β-uranium pentafluoride as one product, β-UF"5 is soluble in acetonitrile without disproportionation and...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
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| Format: |
E-Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
1977 |
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| Reproduktion: |
Elsevier Journal Backfiles on ScienceDirect 1907 - 2002 |
|---|---|
| Übergeordnetes Werk: |
in: Journal of Fluorine Chemistry - Amsterdam : Elsevier, 10(1977), 3, Seite 247-254 |
| Übergeordnetes Werk: |
volume:10 ; year:1977 ; number:3 ; pages:247-254 |
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| 520 | |a Rhenium and uranium hexafluorides oxidise elemental iodine in iodine pentafluoride at ambient temperature to give the I"2^+ cation. With UF"6 an additional reaction occurs to give β-uranium pentafluoride as one product, β-UF"5 is soluble in acetonitrile without disproportionation and is also formed from the reduction of UF"6 by MeCN. Copper, cadmium, and thallium metals are oxidised by ReF"6 in MeCN giving Cu^I, Cd^I^I, and Tl^I hexafluororhenates(V) but the reactions are complicated by reaction between ReF"6 and the solvent. | ||
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(DE-627)NLEJ175526923 (DE-599)GBVNLZ175526923 DE-627 ger DE-627 rakwb eng Redox reactions involving rhenium and uranium hexafluorides, a convenient synthesis of β-uranium pentafluoride 1977 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Rhenium and uranium hexafluorides oxidise elemental iodine in iodine pentafluoride at ambient temperature to give the I"2^+ cation. With UF"6 an additional reaction occurs to give β-uranium pentafluoride as one product, β-UF"5 is soluble in acetonitrile without disproportionation and is also formed from the reduction of UF"6 by MeCN. Copper, cadmium, and thallium metals are oxidised by ReF"6 in MeCN giving Cu^I, Cd^I^I, and Tl^I hexafluororhenates(V) but the reactions are complicated by reaction between ReF"6 and the solvent. Elsevier Journal Backfiles on ScienceDirect 1907 - 2002 Berry, J.A. oth Prescott, A. oth Sharp, D.W.A. oth Winfield, J.M. oth in Journal of Fluorine Chemistry Amsterdam : Elsevier 10(1977), 3, Seite 247-254 (DE-627)NLEJ175525072 (DE-600)1491286-7 0022-1139 nnns volume:10 year:1977 number:3 pages:247-254 http://linkinghub.elsevier.com/retrieve/pii/S0022-1139(00)82138-7 GBV_USEFLAG_H ZDB-1-SDJ GBV_NL_ARTICLE AR 10 1977 3 247-254 |
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(DE-627)NLEJ175526923 (DE-599)GBVNLZ175526923 DE-627 ger DE-627 rakwb eng Redox reactions involving rhenium and uranium hexafluorides, a convenient synthesis of β-uranium pentafluoride 1977 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Rhenium and uranium hexafluorides oxidise elemental iodine in iodine pentafluoride at ambient temperature to give the I"2^+ cation. With UF"6 an additional reaction occurs to give β-uranium pentafluoride as one product, β-UF"5 is soluble in acetonitrile without disproportionation and is also formed from the reduction of UF"6 by MeCN. Copper, cadmium, and thallium metals are oxidised by ReF"6 in MeCN giving Cu^I, Cd^I^I, and Tl^I hexafluororhenates(V) but the reactions are complicated by reaction between ReF"6 and the solvent. Elsevier Journal Backfiles on ScienceDirect 1907 - 2002 Berry, J.A. oth Prescott, A. oth Sharp, D.W.A. oth Winfield, J.M. oth in Journal of Fluorine Chemistry Amsterdam : Elsevier 10(1977), 3, Seite 247-254 (DE-627)NLEJ175525072 (DE-600)1491286-7 0022-1139 nnns volume:10 year:1977 number:3 pages:247-254 http://linkinghub.elsevier.com/retrieve/pii/S0022-1139(00)82138-7 GBV_USEFLAG_H ZDB-1-SDJ GBV_NL_ARTICLE AR 10 1977 3 247-254 |
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(DE-627)NLEJ175526923 (DE-599)GBVNLZ175526923 DE-627 ger DE-627 rakwb eng Redox reactions involving rhenium and uranium hexafluorides, a convenient synthesis of β-uranium pentafluoride 1977 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Rhenium and uranium hexafluorides oxidise elemental iodine in iodine pentafluoride at ambient temperature to give the I"2^+ cation. With UF"6 an additional reaction occurs to give β-uranium pentafluoride as one product, β-UF"5 is soluble in acetonitrile without disproportionation and is also formed from the reduction of UF"6 by MeCN. Copper, cadmium, and thallium metals are oxidised by ReF"6 in MeCN giving Cu^I, Cd^I^I, and Tl^I hexafluororhenates(V) but the reactions are complicated by reaction between ReF"6 and the solvent. Elsevier Journal Backfiles on ScienceDirect 1907 - 2002 Berry, J.A. oth Prescott, A. oth Sharp, D.W.A. oth Winfield, J.M. oth in Journal of Fluorine Chemistry Amsterdam : Elsevier 10(1977), 3, Seite 247-254 (DE-627)NLEJ175525072 (DE-600)1491286-7 0022-1139 nnns volume:10 year:1977 number:3 pages:247-254 http://linkinghub.elsevier.com/retrieve/pii/S0022-1139(00)82138-7 GBV_USEFLAG_H ZDB-1-SDJ GBV_NL_ARTICLE AR 10 1977 3 247-254 |
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(DE-627)NLEJ175526923 (DE-599)GBVNLZ175526923 DE-627 ger DE-627 rakwb eng Redox reactions involving rhenium and uranium hexafluorides, a convenient synthesis of β-uranium pentafluoride 1977 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Rhenium and uranium hexafluorides oxidise elemental iodine in iodine pentafluoride at ambient temperature to give the I"2^+ cation. With UF"6 an additional reaction occurs to give β-uranium pentafluoride as one product, β-UF"5 is soluble in acetonitrile without disproportionation and is also formed from the reduction of UF"6 by MeCN. Copper, cadmium, and thallium metals are oxidised by ReF"6 in MeCN giving Cu^I, Cd^I^I, and Tl^I hexafluororhenates(V) but the reactions are complicated by reaction between ReF"6 and the solvent. Elsevier Journal Backfiles on ScienceDirect 1907 - 2002 Berry, J.A. oth Prescott, A. oth Sharp, D.W.A. oth Winfield, J.M. oth in Journal of Fluorine Chemistry Amsterdam : Elsevier 10(1977), 3, Seite 247-254 (DE-627)NLEJ175525072 (DE-600)1491286-7 0022-1139 nnns volume:10 year:1977 number:3 pages:247-254 http://linkinghub.elsevier.com/retrieve/pii/S0022-1139(00)82138-7 GBV_USEFLAG_H ZDB-1-SDJ GBV_NL_ARTICLE AR 10 1977 3 247-254 |
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(DE-627)NLEJ175526923 (DE-599)GBVNLZ175526923 DE-627 ger DE-627 rakwb eng Redox reactions involving rhenium and uranium hexafluorides, a convenient synthesis of β-uranium pentafluoride 1977 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Rhenium and uranium hexafluorides oxidise elemental iodine in iodine pentafluoride at ambient temperature to give the I"2^+ cation. With UF"6 an additional reaction occurs to give β-uranium pentafluoride as one product, β-UF"5 is soluble in acetonitrile without disproportionation and is also formed from the reduction of UF"6 by MeCN. Copper, cadmium, and thallium metals are oxidised by ReF"6 in MeCN giving Cu^I, Cd^I^I, and Tl^I hexafluororhenates(V) but the reactions are complicated by reaction between ReF"6 and the solvent. Elsevier Journal Backfiles on ScienceDirect 1907 - 2002 Berry, J.A. oth Prescott, A. oth Sharp, D.W.A. oth Winfield, J.M. oth in Journal of Fluorine Chemistry Amsterdam : Elsevier 10(1977), 3, Seite 247-254 (DE-627)NLEJ175525072 (DE-600)1491286-7 0022-1139 nnns volume:10 year:1977 number:3 pages:247-254 http://linkinghub.elsevier.com/retrieve/pii/S0022-1139(00)82138-7 GBV_USEFLAG_H ZDB-1-SDJ GBV_NL_ARTICLE AR 10 1977 3 247-254 |
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redox reactions involving rhenium and uranium hexafluorides, a convenient synthesis of β-uranium pentafluoride |
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Redox reactions involving rhenium and uranium hexafluorides, a convenient synthesis of β-uranium pentafluoride |
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Rhenium and uranium hexafluorides oxidise elemental iodine in iodine pentafluoride at ambient temperature to give the I"2^+ cation. With UF"6 an additional reaction occurs to give β-uranium pentafluoride as one product, β-UF"5 is soluble in acetonitrile without disproportionation and is also formed from the reduction of UF"6 by MeCN. Copper, cadmium, and thallium metals are oxidised by ReF"6 in MeCN giving Cu^I, Cd^I^I, and Tl^I hexafluororhenates(V) but the reactions are complicated by reaction between ReF"6 and the solvent. |
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Rhenium and uranium hexafluorides oxidise elemental iodine in iodine pentafluoride at ambient temperature to give the I"2^+ cation. With UF"6 an additional reaction occurs to give β-uranium pentafluoride as one product, β-UF"5 is soluble in acetonitrile without disproportionation and is also formed from the reduction of UF"6 by MeCN. Copper, cadmium, and thallium metals are oxidised by ReF"6 in MeCN giving Cu^I, Cd^I^I, and Tl^I hexafluororhenates(V) but the reactions are complicated by reaction between ReF"6 and the solvent. |
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Rhenium and uranium hexafluorides oxidise elemental iodine in iodine pentafluoride at ambient temperature to give the I"2^+ cation. With UF"6 an additional reaction occurs to give β-uranium pentafluoride as one product, β-UF"5 is soluble in acetonitrile without disproportionation and is also formed from the reduction of UF"6 by MeCN. Copper, cadmium, and thallium metals are oxidised by ReF"6 in MeCN giving Cu^I, Cd^I^I, and Tl^I hexafluororhenates(V) but the reactions are complicated by reaction between ReF"6 and the solvent. |
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