Auger Electron Spectroscopy Analysis of Cross-Section Surface of Oxidized Titanium Carbide Single Crystal
A TiC monocrystal was heated by three thermal cycles with isotherm at 1108 K while exposed to Ar/O2 mixtures respectively with O2 contents of 239, 1.0, and 324 ppm. The reactivity was detected with a homemade device based on two identical solid electrolyte oxygen sensors connected to a quadrupole ma...
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| Autor*in: |
Bellucci, Alessandra [verfasserIn] Gozzi, Daniele [verfasserIn] Kimura, Takashi [verfasserIn] |
|---|
| Format: |
E-Artikel |
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| Erschienen: |
Westerville, Ohio: American Ceramics Society ; 2003 |
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| Schlagwörter: |
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| Umfang: |
Online-Ressource |
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| Reproduktion: |
2004 ; Blackwell Publishing Journal Backfiles 1879-2005 |
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| Übergeordnetes Werk: |
In: Journal of the American Ceramic Society - American Ceramic Society ; GKD-ID: 6113X, Oxford [u.a.] : Wiley-Blackwell, 1918, 86(2003), 12, Seite 0 |
| Übergeordnetes Werk: |
volume:86 ; year:2003 ; number:12 ; pages:0 |
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| DOI / URN: |
10.1111/j.1151-2916.2003.tb03618.x |
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| 520 | |a A TiC monocrystal was heated by three thermal cycles with isotherm at 1108 K while exposed to Ar/O2 mixtures respectively with O2 contents of 239, 1.0, and 324 ppm. The reactivity was detected with a homemade device based on two identical solid electrolyte oxygen sensors connected to a quadrupole mass spectrometer (QMS). The oxidized sample was cleaved by impact bending under high vacuum and the cross section investigated by Auger electron spectroscopy (AES) and scanning electron microscopy (SEM) techniques. Both area and profile AES spectra were acquired by using a 70 nm diameter beam. Spectral changes have been analyzed to identify chemical species present at the TiC/TiO2 interface. A model for high-temperature oxidation of TiC has been proposed. It implies oxygen diffusion through a protective TiO2 layer and the existence of two inner interfaces: TiC/TiC1−xOx and TiC1−xOx/TiO2. | ||
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10.1111/j.1151-2916.2003.tb03618.x doi (DE-627)NLEJ243457340 DE-627 ger DE-627 rakwb Bellucci, Alessandra verfasserin aut Auger Electron Spectroscopy Analysis of Cross-Section Surface of Oxidized Titanium Carbide Single Crystal Westerville, Ohio American Ceramics Society 2003 Online-Ressource nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier A TiC monocrystal was heated by three thermal cycles with isotherm at 1108 K while exposed to Ar/O2 mixtures respectively with O2 contents of 239, 1.0, and 324 ppm. The reactivity was detected with a homemade device based on two identical solid electrolyte oxygen sensors connected to a quadrupole mass spectrometer (QMS). The oxidized sample was cleaved by impact bending under high vacuum and the cross section investigated by Auger electron spectroscopy (AES) and scanning electron microscopy (SEM) techniques. Both area and profile AES spectra were acquired by using a 70 nm diameter beam. Spectral changes have been analyzed to identify chemical species present at the TiC/TiO2 interface. A model for high-temperature oxidation of TiC has been proposed. It implies oxygen diffusion through a protective TiO2 layer and the existence of two inner interfaces: TiC/TiC1−xOx and TiC1−xOx/TiO2. 2004 Blackwell Publishing Journal Backfiles 1879-2005 |2004|||||||||| Auger electron spectroscopy Gozzi, Daniele verfasserin aut Kimura, Takashi verfasserin aut Noda, Tetsuji oth Otani, Shigeki oth In American Ceramic Society ; GKD-ID: 6113X Journal of the American Ceramic Society Oxford [u.a.] : Wiley-Blackwell, 1918 86(2003), 12, Seite 0 Online-Ressource (DE-627)NLEJ243927835 (DE-600)2008170-4 1551-2916 nnns volume:86 year:2003 number:12 pages:0 http://dx.doi.org/10.1111/j.1151-2916.2003.tb03618.x text/html Verlag Deutschlandweit zugänglich Volltext GBV_USEFLAG_U ZDB-1-DJB GBV_NL_ARTICLE AR 86 2003 12 0 |
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10.1111/j.1151-2916.2003.tb03618.x doi (DE-627)NLEJ243457340 DE-627 ger DE-627 rakwb Bellucci, Alessandra verfasserin aut Auger Electron Spectroscopy Analysis of Cross-Section Surface of Oxidized Titanium Carbide Single Crystal Westerville, Ohio American Ceramics Society 2003 Online-Ressource nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier A TiC monocrystal was heated by three thermal cycles with isotherm at 1108 K while exposed to Ar/O2 mixtures respectively with O2 contents of 239, 1.0, and 324 ppm. The reactivity was detected with a homemade device based on two identical solid electrolyte oxygen sensors connected to a quadrupole mass spectrometer (QMS). The oxidized sample was cleaved by impact bending under high vacuum and the cross section investigated by Auger electron spectroscopy (AES) and scanning electron microscopy (SEM) techniques. Both area and profile AES spectra were acquired by using a 70 nm diameter beam. Spectral changes have been analyzed to identify chemical species present at the TiC/TiO2 interface. A model for high-temperature oxidation of TiC has been proposed. It implies oxygen diffusion through a protective TiO2 layer and the existence of two inner interfaces: TiC/TiC1−xOx and TiC1−xOx/TiO2. 2004 Blackwell Publishing Journal Backfiles 1879-2005 |2004|||||||||| Auger electron spectroscopy Gozzi, Daniele verfasserin aut Kimura, Takashi verfasserin aut Noda, Tetsuji oth Otani, Shigeki oth In American Ceramic Society ; GKD-ID: 6113X Journal of the American Ceramic Society Oxford [u.a.] : Wiley-Blackwell, 1918 86(2003), 12, Seite 0 Online-Ressource (DE-627)NLEJ243927835 (DE-600)2008170-4 1551-2916 nnns volume:86 year:2003 number:12 pages:0 http://dx.doi.org/10.1111/j.1151-2916.2003.tb03618.x text/html Verlag Deutschlandweit zugänglich Volltext GBV_USEFLAG_U ZDB-1-DJB GBV_NL_ARTICLE AR 86 2003 12 0 |
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10.1111/j.1151-2916.2003.tb03618.x doi (DE-627)NLEJ243457340 DE-627 ger DE-627 rakwb Bellucci, Alessandra verfasserin aut Auger Electron Spectroscopy Analysis of Cross-Section Surface of Oxidized Titanium Carbide Single Crystal Westerville, Ohio American Ceramics Society 2003 Online-Ressource nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier A TiC monocrystal was heated by three thermal cycles with isotherm at 1108 K while exposed to Ar/O2 mixtures respectively with O2 contents of 239, 1.0, and 324 ppm. The reactivity was detected with a homemade device based on two identical solid electrolyte oxygen sensors connected to a quadrupole mass spectrometer (QMS). The oxidized sample was cleaved by impact bending under high vacuum and the cross section investigated by Auger electron spectroscopy (AES) and scanning electron microscopy (SEM) techniques. Both area and profile AES spectra were acquired by using a 70 nm diameter beam. Spectral changes have been analyzed to identify chemical species present at the TiC/TiO2 interface. A model for high-temperature oxidation of TiC has been proposed. It implies oxygen diffusion through a protective TiO2 layer and the existence of two inner interfaces: TiC/TiC1−xOx and TiC1−xOx/TiO2. 2004 Blackwell Publishing Journal Backfiles 1879-2005 |2004|||||||||| Auger electron spectroscopy Gozzi, Daniele verfasserin aut Kimura, Takashi verfasserin aut Noda, Tetsuji oth Otani, Shigeki oth In American Ceramic Society ; GKD-ID: 6113X Journal of the American Ceramic Society Oxford [u.a.] : Wiley-Blackwell, 1918 86(2003), 12, Seite 0 Online-Ressource (DE-627)NLEJ243927835 (DE-600)2008170-4 1551-2916 nnns volume:86 year:2003 number:12 pages:0 http://dx.doi.org/10.1111/j.1151-2916.2003.tb03618.x text/html Verlag Deutschlandweit zugänglich Volltext GBV_USEFLAG_U ZDB-1-DJB GBV_NL_ARTICLE AR 86 2003 12 0 |
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10.1111/j.1151-2916.2003.tb03618.x doi (DE-627)NLEJ243457340 DE-627 ger DE-627 rakwb Bellucci, Alessandra verfasserin aut Auger Electron Spectroscopy Analysis of Cross-Section Surface of Oxidized Titanium Carbide Single Crystal Westerville, Ohio American Ceramics Society 2003 Online-Ressource nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier A TiC monocrystal was heated by three thermal cycles with isotherm at 1108 K while exposed to Ar/O2 mixtures respectively with O2 contents of 239, 1.0, and 324 ppm. The reactivity was detected with a homemade device based on two identical solid electrolyte oxygen sensors connected to a quadrupole mass spectrometer (QMS). The oxidized sample was cleaved by impact bending under high vacuum and the cross section investigated by Auger electron spectroscopy (AES) and scanning electron microscopy (SEM) techniques. Both area and profile AES spectra were acquired by using a 70 nm diameter beam. Spectral changes have been analyzed to identify chemical species present at the TiC/TiO2 interface. A model for high-temperature oxidation of TiC has been proposed. It implies oxygen diffusion through a protective TiO2 layer and the existence of two inner interfaces: TiC/TiC1−xOx and TiC1−xOx/TiO2. 2004 Blackwell Publishing Journal Backfiles 1879-2005 |2004|||||||||| Auger electron spectroscopy Gozzi, Daniele verfasserin aut Kimura, Takashi verfasserin aut Noda, Tetsuji oth Otani, Shigeki oth In American Ceramic Society ; GKD-ID: 6113X Journal of the American Ceramic Society Oxford [u.a.] : Wiley-Blackwell, 1918 86(2003), 12, Seite 0 Online-Ressource (DE-627)NLEJ243927835 (DE-600)2008170-4 1551-2916 nnns volume:86 year:2003 number:12 pages:0 http://dx.doi.org/10.1111/j.1151-2916.2003.tb03618.x text/html Verlag Deutschlandweit zugänglich Volltext GBV_USEFLAG_U ZDB-1-DJB GBV_NL_ARTICLE AR 86 2003 12 0 |
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10.1111/j.1151-2916.2003.tb03618.x doi (DE-627)NLEJ243457340 DE-627 ger DE-627 rakwb Bellucci, Alessandra verfasserin aut Auger Electron Spectroscopy Analysis of Cross-Section Surface of Oxidized Titanium Carbide Single Crystal Westerville, Ohio American Ceramics Society 2003 Online-Ressource nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier A TiC monocrystal was heated by three thermal cycles with isotherm at 1108 K while exposed to Ar/O2 mixtures respectively with O2 contents of 239, 1.0, and 324 ppm. The reactivity was detected with a homemade device based on two identical solid electrolyte oxygen sensors connected to a quadrupole mass spectrometer (QMS). The oxidized sample was cleaved by impact bending under high vacuum and the cross section investigated by Auger electron spectroscopy (AES) and scanning electron microscopy (SEM) techniques. Both area and profile AES spectra were acquired by using a 70 nm diameter beam. Spectral changes have been analyzed to identify chemical species present at the TiC/TiO2 interface. A model for high-temperature oxidation of TiC has been proposed. It implies oxygen diffusion through a protective TiO2 layer and the existence of two inner interfaces: TiC/TiC1−xOx and TiC1−xOx/TiO2. 2004 Blackwell Publishing Journal Backfiles 1879-2005 |2004|||||||||| Auger electron spectroscopy Gozzi, Daniele verfasserin aut Kimura, Takashi verfasserin aut Noda, Tetsuji oth Otani, Shigeki oth In American Ceramic Society ; GKD-ID: 6113X Journal of the American Ceramic Society Oxford [u.a.] : Wiley-Blackwell, 1918 86(2003), 12, Seite 0 Online-Ressource (DE-627)NLEJ243927835 (DE-600)2008170-4 1551-2916 nnns volume:86 year:2003 number:12 pages:0 http://dx.doi.org/10.1111/j.1151-2916.2003.tb03618.x text/html Verlag Deutschlandweit zugänglich Volltext GBV_USEFLAG_U ZDB-1-DJB GBV_NL_ARTICLE AR 86 2003 12 0 |
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A TiC monocrystal was heated by three thermal cycles with isotherm at 1108 K while exposed to Ar/O2 mixtures respectively with O2 contents of 239, 1.0, and 324 ppm. The reactivity was detected with a homemade device based on two identical solid electrolyte oxygen sensors connected to a quadrupole mass spectrometer (QMS). The oxidized sample was cleaved by impact bending under high vacuum and the cross section investigated by Auger electron spectroscopy (AES) and scanning electron microscopy (SEM) techniques. Both area and profile AES spectra were acquired by using a 70 nm diameter beam. Spectral changes have been analyzed to identify chemical species present at the TiC/TiO2 interface. A model for high-temperature oxidation of TiC has been proposed. It implies oxygen diffusion through a protective TiO2 layer and the existence of two inner interfaces: TiC/TiC1−xOx and TiC1−xOx/TiO2. |
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A TiC monocrystal was heated by three thermal cycles with isotherm at 1108 K while exposed to Ar/O2 mixtures respectively with O2 contents of 239, 1.0, and 324 ppm. The reactivity was detected with a homemade device based on two identical solid electrolyte oxygen sensors connected to a quadrupole mass spectrometer (QMS). The oxidized sample was cleaved by impact bending under high vacuum and the cross section investigated by Auger electron spectroscopy (AES) and scanning electron microscopy (SEM) techniques. Both area and profile AES spectra were acquired by using a 70 nm diameter beam. Spectral changes have been analyzed to identify chemical species present at the TiC/TiO2 interface. A model for high-temperature oxidation of TiC has been proposed. It implies oxygen diffusion through a protective TiO2 layer and the existence of two inner interfaces: TiC/TiC1−xOx and TiC1−xOx/TiO2. |
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A TiC monocrystal was heated by three thermal cycles with isotherm at 1108 K while exposed to Ar/O2 mixtures respectively with O2 contents of 239, 1.0, and 324 ppm. The reactivity was detected with a homemade device based on two identical solid electrolyte oxygen sensors connected to a quadrupole mass spectrometer (QMS). The oxidized sample was cleaved by impact bending under high vacuum and the cross section investigated by Auger electron spectroscopy (AES) and scanning electron microscopy (SEM) techniques. Both area and profile AES spectra were acquired by using a 70 nm diameter beam. Spectral changes have been analyzed to identify chemical species present at the TiC/TiO2 interface. A model for high-temperature oxidation of TiC has been proposed. It implies oxygen diffusion through a protective TiO2 layer and the existence of two inner interfaces: TiC/TiC1−xOx and TiC1−xOx/TiO2. |
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<?xml version="1.0" encoding="UTF-8"?><collection xmlns="http://www.loc.gov/MARC21/slim"><record><leader>01000caa a22002652 4500</leader><controlfield tag="001">NLEJ243457340</controlfield><controlfield tag="003">DE-627</controlfield><controlfield tag="005">20210707181343.0</controlfield><controlfield tag="007">cr uuu---uuuuu</controlfield><controlfield tag="008">120427s2003 xx |||||o 00| ||und c</controlfield><datafield tag="024" ind1="7" ind2=" "><subfield code="a">10.1111/j.1151-2916.2003.tb03618.x</subfield><subfield code="2">doi</subfield></datafield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(DE-627)NLEJ243457340</subfield></datafield><datafield tag="040" ind1=" " ind2=" "><subfield code="a">DE-627</subfield><subfield code="b">ger</subfield><subfield code="c">DE-627</subfield><subfield code="e">rakwb</subfield></datafield><datafield tag="100" ind1="1" ind2=" "><subfield code="a">Bellucci, Alessandra</subfield><subfield code="e">verfasserin</subfield><subfield code="4">aut</subfield></datafield><datafield tag="245" ind1="1" ind2="0"><subfield code="a">Auger Electron Spectroscopy Analysis of Cross-Section Surface of Oxidized Titanium Carbide Single Crystal</subfield></datafield><datafield tag="264" ind1=" " ind2="1"><subfield code="a">Westerville, Ohio</subfield><subfield code="b">American Ceramics Society</subfield><subfield code="c">2003</subfield></datafield><datafield tag="300" ind1=" " ind2=" "><subfield code="a">Online-Ressource</subfield></datafield><datafield tag="336" ind1=" " ind2=" "><subfield code="a">nicht spezifiziert</subfield><subfield code="b">zzz</subfield><subfield code="2">rdacontent</subfield></datafield><datafield tag="337" ind1=" " ind2=" "><subfield code="a">nicht spezifiziert</subfield><subfield code="b">z</subfield><subfield code="2">rdamedia</subfield></datafield><datafield tag="338" ind1=" " ind2=" "><subfield code="a">nicht spezifiziert</subfield><subfield code="b">zu</subfield><subfield code="2">rdacarrier</subfield></datafield><datafield tag="520" ind1=" " ind2=" "><subfield code="a">A TiC monocrystal was heated by three thermal cycles with isotherm at 1108 K while exposed to Ar/O2 mixtures respectively with O2 contents of 239, 1.0, and 324 ppm. The reactivity was detected with a homemade device based on two identical solid electrolyte oxygen sensors connected to a quadrupole mass spectrometer (QMS). The oxidized sample was cleaved by impact bending under high vacuum and the cross section investigated by Auger electron spectroscopy (AES) and scanning electron microscopy (SEM) techniques. Both area and profile AES spectra were acquired by using a 70 nm diameter beam. Spectral changes have been analyzed to identify chemical species present at the TiC/TiO2 interface. A model for high-temperature oxidation of TiC has been proposed. 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