Reaction of Trimethylsilyl Enol Ethers with 2-Mercaptoethanol
We wish to report that the acid catalyzed reaction of trimethylsilyl enol ethers with 2-mercaptoethanol gives hemithio ketals in moderate to good yield (eq 1).1 The reaction is analogous to the recently reported reaction of trimethylsilyl enol ethers with diols.2 The reaction is exothermic and rapid...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Larson, Gerald [verfasserIn] Hernandez, Antonio [verfasserIn] |
|---|
| Format: |
E-Artikel |
|---|---|
| Sprache: |
Englisch |
| Erschienen: |
2011 |
|---|
| Übergeordnetes Werk: |
Enthalten in: Synthetic communications - Philadelphia, Pa. : Taylor & Francis, 1971, 4(1974), 1, Seite 61-62 |
|---|---|
| Übergeordnetes Werk: |
number:1 ; volume:4 ; year:1974 ; pages:61-62 |
| Links: |
|---|
| DOI / URN: |
10.1080/00397917408062056 |
|---|
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NLEJ252392019 |
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| 520 | |a We wish to report that the acid catalyzed reaction of trimethylsilyl enol ethers with 2-mercaptoethanol gives hemithio ketals in moderate to good yield (eq 1).1 The reaction is analogous to the recently reported reaction of trimethylsilyl enol ethers with diols.2 The reaction is exothermic and rapid, requiring from 10 to 30 minutes for completion. A number of organic solvents were employed with essentially no change in t the results.3 The intermediate carbonium ion, I, is proposed to account for this reaction. The results of the reaction are shown in Table I. | ||
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10.1080/00397917408062056 doi (DE-627)NLEJ252392019 (TFO)762525593 DE-627 ger DE-627 rda eng Larson, Gerald verfasserin aut Reaction of Trimethylsilyl Enol Ethers with 2-Mercaptoethanol 2011 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier We wish to report that the acid catalyzed reaction of trimethylsilyl enol ethers with 2-mercaptoethanol gives hemithio ketals in moderate to good yield (eq 1).1 The reaction is analogous to the recently reported reaction of trimethylsilyl enol ethers with diols.2 The reaction is exothermic and rapid, requiring from 10 to 30 minutes for completion. A number of organic solvents were employed with essentially no change in t the results.3 The intermediate carbonium ion, I, is proposed to account for this reaction. The results of the reaction are shown in Table I. Hernandez, Antonio verfasserin aut Enthalten in Synthetic communications Philadelphia, Pa. : Taylor & Francis, 1971 4(1974), 1, Seite 61-62 Online-Ressource (DE-627)NLEJ252311264 (DE-600)2043259-8 (DE-576)117544086 1532-2432 nnns number:1 volume:4 year:1974 pages:61-62 https://www.tib.eu/de/suchen/id/tandf%3A95ce53832dc31901621a77f0c3efcf3d2c682418 Digitalisierung Deutschlandweit zugänglich ZDB-1-TFO GBV_NL_ARTICLE AR 1 4 1974 61-62 |
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10.1080/00397917408062056 doi (DE-627)NLEJ252392019 (TFO)762525593 DE-627 ger DE-627 rda eng Larson, Gerald verfasserin aut Reaction of Trimethylsilyl Enol Ethers with 2-Mercaptoethanol 2011 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier We wish to report that the acid catalyzed reaction of trimethylsilyl enol ethers with 2-mercaptoethanol gives hemithio ketals in moderate to good yield (eq 1).1 The reaction is analogous to the recently reported reaction of trimethylsilyl enol ethers with diols.2 The reaction is exothermic and rapid, requiring from 10 to 30 minutes for completion. A number of organic solvents were employed with essentially no change in t the results.3 The intermediate carbonium ion, I, is proposed to account for this reaction. The results of the reaction are shown in Table I. Hernandez, Antonio verfasserin aut Enthalten in Synthetic communications Philadelphia, Pa. : Taylor & Francis, 1971 4(1974), 1, Seite 61-62 Online-Ressource (DE-627)NLEJ252311264 (DE-600)2043259-8 (DE-576)117544086 1532-2432 nnns number:1 volume:4 year:1974 pages:61-62 https://www.tib.eu/de/suchen/id/tandf%3A95ce53832dc31901621a77f0c3efcf3d2c682418 Digitalisierung Deutschlandweit zugänglich ZDB-1-TFO GBV_NL_ARTICLE AR 1 4 1974 61-62 |
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10.1080/00397917408062056 doi (DE-627)NLEJ252392019 (TFO)762525593 DE-627 ger DE-627 rda eng Larson, Gerald verfasserin aut Reaction of Trimethylsilyl Enol Ethers with 2-Mercaptoethanol 2011 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier We wish to report that the acid catalyzed reaction of trimethylsilyl enol ethers with 2-mercaptoethanol gives hemithio ketals in moderate to good yield (eq 1).1 The reaction is analogous to the recently reported reaction of trimethylsilyl enol ethers with diols.2 The reaction is exothermic and rapid, requiring from 10 to 30 minutes for completion. A number of organic solvents were employed with essentially no change in t the results.3 The intermediate carbonium ion, I, is proposed to account for this reaction. The results of the reaction are shown in Table I. Hernandez, Antonio verfasserin aut Enthalten in Synthetic communications Philadelphia, Pa. : Taylor & Francis, 1971 4(1974), 1, Seite 61-62 Online-Ressource (DE-627)NLEJ252311264 (DE-600)2043259-8 (DE-576)117544086 1532-2432 nnns number:1 volume:4 year:1974 pages:61-62 https://www.tib.eu/de/suchen/id/tandf%3A95ce53832dc31901621a77f0c3efcf3d2c682418 Digitalisierung Deutschlandweit zugänglich ZDB-1-TFO GBV_NL_ARTICLE AR 1 4 1974 61-62 |
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10.1080/00397917408062056 doi (DE-627)NLEJ252392019 (TFO)762525593 DE-627 ger DE-627 rda eng Larson, Gerald verfasserin aut Reaction of Trimethylsilyl Enol Ethers with 2-Mercaptoethanol 2011 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier We wish to report that the acid catalyzed reaction of trimethylsilyl enol ethers with 2-mercaptoethanol gives hemithio ketals in moderate to good yield (eq 1).1 The reaction is analogous to the recently reported reaction of trimethylsilyl enol ethers with diols.2 The reaction is exothermic and rapid, requiring from 10 to 30 minutes for completion. A number of organic solvents were employed with essentially no change in t the results.3 The intermediate carbonium ion, I, is proposed to account for this reaction. The results of the reaction are shown in Table I. Hernandez, Antonio verfasserin aut Enthalten in Synthetic communications Philadelphia, Pa. : Taylor & Francis, 1971 4(1974), 1, Seite 61-62 Online-Ressource (DE-627)NLEJ252311264 (DE-600)2043259-8 (DE-576)117544086 1532-2432 nnns number:1 volume:4 year:1974 pages:61-62 https://www.tib.eu/de/suchen/id/tandf%3A95ce53832dc31901621a77f0c3efcf3d2c682418 Digitalisierung Deutschlandweit zugänglich ZDB-1-TFO GBV_NL_ARTICLE AR 1 4 1974 61-62 |
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10.1080/00397917408062056 doi (DE-627)NLEJ252392019 (TFO)762525593 DE-627 ger DE-627 rda eng Larson, Gerald verfasserin aut Reaction of Trimethylsilyl Enol Ethers with 2-Mercaptoethanol 2011 Text txt rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier We wish to report that the acid catalyzed reaction of trimethylsilyl enol ethers with 2-mercaptoethanol gives hemithio ketals in moderate to good yield (eq 1).1 The reaction is analogous to the recently reported reaction of trimethylsilyl enol ethers with diols.2 The reaction is exothermic and rapid, requiring from 10 to 30 minutes for completion. A number of organic solvents were employed with essentially no change in t the results.3 The intermediate carbonium ion, I, is proposed to account for this reaction. The results of the reaction are shown in Table I. Hernandez, Antonio verfasserin aut Enthalten in Synthetic communications Philadelphia, Pa. : Taylor & Francis, 1971 4(1974), 1, Seite 61-62 Online-Ressource (DE-627)NLEJ252311264 (DE-600)2043259-8 (DE-576)117544086 1532-2432 nnns number:1 volume:4 year:1974 pages:61-62 https://www.tib.eu/de/suchen/id/tandf%3A95ce53832dc31901621a77f0c3efcf3d2c682418 Digitalisierung Deutschlandweit zugänglich ZDB-1-TFO GBV_NL_ARTICLE AR 1 4 1974 61-62 |
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reaction of trimethylsilyl enol ethers with 2-mercaptoethanol |
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Reaction of Trimethylsilyl Enol Ethers with 2-Mercaptoethanol |
| abstract |
We wish to report that the acid catalyzed reaction of trimethylsilyl enol ethers with 2-mercaptoethanol gives hemithio ketals in moderate to good yield (eq 1).1 The reaction is analogous to the recently reported reaction of trimethylsilyl enol ethers with diols.2 The reaction is exothermic and rapid, requiring from 10 to 30 minutes for completion. A number of organic solvents were employed with essentially no change in t the results.3 The intermediate carbonium ion, I, is proposed to account for this reaction. The results of the reaction are shown in Table I. |
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We wish to report that the acid catalyzed reaction of trimethylsilyl enol ethers with 2-mercaptoethanol gives hemithio ketals in moderate to good yield (eq 1).1 The reaction is analogous to the recently reported reaction of trimethylsilyl enol ethers with diols.2 The reaction is exothermic and rapid, requiring from 10 to 30 minutes for completion. A number of organic solvents were employed with essentially no change in t the results.3 The intermediate carbonium ion, I, is proposed to account for this reaction. The results of the reaction are shown in Table I. |
| abstract_unstemmed |
We wish to report that the acid catalyzed reaction of trimethylsilyl enol ethers with 2-mercaptoethanol gives hemithio ketals in moderate to good yield (eq 1).1 The reaction is analogous to the recently reported reaction of trimethylsilyl enol ethers with diols.2 The reaction is exothermic and rapid, requiring from 10 to 30 minutes for completion. A number of organic solvents were employed with essentially no change in t the results.3 The intermediate carbonium ion, I, is proposed to account for this reaction. The results of the reaction are shown in Table I. |
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