Optimization of ethyl ester production assisted by ultrasonic irradiation
This study presents the optimization of the continuous flow potassium hydroxide-catalyzed synthesis of ethyl ester from palm oil with ultrasonic assistance. The process was optimized by application of factorial design and response surface methodology. The independent variables considered were ethano...
Ausführliche Beschreibung
Autor*in: |
Noipin, K [verfasserIn] |
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Sprache: |
Englisch |
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2015 |
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Nutzungsrecht: Copyright © 2014 Elsevier B.V. All rights reserved. © COPYRIGHT 2015 Elsevier B.V. |
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Übergeordnetes Werk: |
Enthalten in: Ultrasonics sonochemistry - Amsterdam [u.a.] : Elsevier, 1994, 22(2015), Seite 548 |
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Übergeordnetes Werk: |
volume:22 ; year:2015 ; pages:548 |
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DOI / URN: |
10.1016/j.ultsonch.2014.07.019 |
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OLC1959813730 |
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520 | |a This study presents the optimization of the continuous flow potassium hydroxide-catalyzed synthesis of ethyl ester from palm oil with ultrasonic assistance. The process was optimized by application of factorial design and response surface methodology. The independent variables considered were ethanol to oil molar ratio, catalyst concentration, reaction temperature and ultrasonic amplitude; and the response was ethyl ester yield. The results show that ethanol to oil molar ratio, catalyst concentration, and ultrasonic amplitude have positive effect on ethyl ester yield, whereas reaction temperature has negative influence on ethyl ester yield. Second-order models were developed to predict the responses analyzed as a function of these three variables, and the developed models predicts the results in the experimental ranges studied adequately. This study shows that ultrasonic irradiation improved the ethyl ester production process to achieve ethyl ester yields above 92%. | ||
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10.1016/j.ultsonch.2014.07.019 doi PQ20160617 (DE-627)OLC1959813730 (DE-599)GBVOLC1959813730 (PRQ)g1052-be20187f1411ab3b985c879249b2d503b2ccd946400c685180f52266fa7bbdb50 (KEY)0238159120150000022000000548optimizationofethylesterproductionassistedbyultras DE-627 ger DE-627 rakwb eng 540 DE-600 Noipin, K verfasserin aut Optimization of ethyl ester production assisted by ultrasonic irradiation 2015 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier This study presents the optimization of the continuous flow potassium hydroxide-catalyzed synthesis of ethyl ester from palm oil with ultrasonic assistance. The process was optimized by application of factorial design and response surface methodology. The independent variables considered were ethanol to oil molar ratio, catalyst concentration, reaction temperature and ultrasonic amplitude; and the response was ethyl ester yield. The results show that ethanol to oil molar ratio, catalyst concentration, and ultrasonic amplitude have positive effect on ethyl ester yield, whereas reaction temperature has negative influence on ethyl ester yield. Second-order models were developed to predict the responses analyzed as a function of these three variables, and the developed models predicts the results in the experimental ranges studied adequately. This study shows that ultrasonic irradiation improved the ethyl ester production process to achieve ethyl ester yields above 92%. Nutzungsrecht: Copyright © 2014 Elsevier B.V. All rights reserved. © COPYRIGHT 2015 Elsevier B.V. Plant Oils - chemistry Potassium Compounds - chemistry Esters - chemical synthesis Hydroxides - chemistry Kumar, S oth Enthalten in Ultrasonics sonochemistry Amsterdam [u.a.] : Elsevier, 1994 22(2015), Seite 548 (DE-627)182456803 (DE-600)1208333-1 (DE-576)043089054 1350-4177 nnns volume:22 year:2015 pages:548 http://dx.doi.org/10.1016/j.ultsonch.2014.07.019 Volltext http://www.ncbi.nlm.nih.gov/pubmed/25116594 GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-PHY SSG-OLC-CHE SSG-OLC-PHA SSG-OLC-DE-84 GBV_ILN_70 GBV_ILN_170 GBV_ILN_2006 GBV_ILN_4012 AR 22 2015 548 |
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10.1016/j.ultsonch.2014.07.019 doi PQ20160617 (DE-627)OLC1959813730 (DE-599)GBVOLC1959813730 (PRQ)g1052-be20187f1411ab3b985c879249b2d503b2ccd946400c685180f52266fa7bbdb50 (KEY)0238159120150000022000000548optimizationofethylesterproductionassistedbyultras DE-627 ger DE-627 rakwb eng 540 DE-600 Noipin, K verfasserin aut Optimization of ethyl ester production assisted by ultrasonic irradiation 2015 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier This study presents the optimization of the continuous flow potassium hydroxide-catalyzed synthesis of ethyl ester from palm oil with ultrasonic assistance. The process was optimized by application of factorial design and response surface methodology. The independent variables considered were ethanol to oil molar ratio, catalyst concentration, reaction temperature and ultrasonic amplitude; and the response was ethyl ester yield. The results show that ethanol to oil molar ratio, catalyst concentration, and ultrasonic amplitude have positive effect on ethyl ester yield, whereas reaction temperature has negative influence on ethyl ester yield. Second-order models were developed to predict the responses analyzed as a function of these three variables, and the developed models predicts the results in the experimental ranges studied adequately. This study shows that ultrasonic irradiation improved the ethyl ester production process to achieve ethyl ester yields above 92%. Nutzungsrecht: Copyright © 2014 Elsevier B.V. All rights reserved. © COPYRIGHT 2015 Elsevier B.V. Plant Oils - chemistry Potassium Compounds - chemistry Esters - chemical synthesis Hydroxides - chemistry Kumar, S oth Enthalten in Ultrasonics sonochemistry Amsterdam [u.a.] : Elsevier, 1994 22(2015), Seite 548 (DE-627)182456803 (DE-600)1208333-1 (DE-576)043089054 1350-4177 nnns volume:22 year:2015 pages:548 http://dx.doi.org/10.1016/j.ultsonch.2014.07.019 Volltext http://www.ncbi.nlm.nih.gov/pubmed/25116594 GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-PHY SSG-OLC-CHE SSG-OLC-PHA SSG-OLC-DE-84 GBV_ILN_70 GBV_ILN_170 GBV_ILN_2006 GBV_ILN_4012 AR 22 2015 548 |
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10.1016/j.ultsonch.2014.07.019 doi PQ20160617 (DE-627)OLC1959813730 (DE-599)GBVOLC1959813730 (PRQ)g1052-be20187f1411ab3b985c879249b2d503b2ccd946400c685180f52266fa7bbdb50 (KEY)0238159120150000022000000548optimizationofethylesterproductionassistedbyultras DE-627 ger DE-627 rakwb eng 540 DE-600 Noipin, K verfasserin aut Optimization of ethyl ester production assisted by ultrasonic irradiation 2015 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier This study presents the optimization of the continuous flow potassium hydroxide-catalyzed synthesis of ethyl ester from palm oil with ultrasonic assistance. The process was optimized by application of factorial design and response surface methodology. The independent variables considered were ethanol to oil molar ratio, catalyst concentration, reaction temperature and ultrasonic amplitude; and the response was ethyl ester yield. The results show that ethanol to oil molar ratio, catalyst concentration, and ultrasonic amplitude have positive effect on ethyl ester yield, whereas reaction temperature has negative influence on ethyl ester yield. Second-order models were developed to predict the responses analyzed as a function of these three variables, and the developed models predicts the results in the experimental ranges studied adequately. This study shows that ultrasonic irradiation improved the ethyl ester production process to achieve ethyl ester yields above 92%. Nutzungsrecht: Copyright © 2014 Elsevier B.V. All rights reserved. © COPYRIGHT 2015 Elsevier B.V. Plant Oils - chemistry Potassium Compounds - chemistry Esters - chemical synthesis Hydroxides - chemistry Kumar, S oth Enthalten in Ultrasonics sonochemistry Amsterdam [u.a.] : Elsevier, 1994 22(2015), Seite 548 (DE-627)182456803 (DE-600)1208333-1 (DE-576)043089054 1350-4177 nnns volume:22 year:2015 pages:548 http://dx.doi.org/10.1016/j.ultsonch.2014.07.019 Volltext http://www.ncbi.nlm.nih.gov/pubmed/25116594 GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-PHY SSG-OLC-CHE SSG-OLC-PHA SSG-OLC-DE-84 GBV_ILN_70 GBV_ILN_170 GBV_ILN_2006 GBV_ILN_4012 AR 22 2015 548 |
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10.1016/j.ultsonch.2014.07.019 doi PQ20160617 (DE-627)OLC1959813730 (DE-599)GBVOLC1959813730 (PRQ)g1052-be20187f1411ab3b985c879249b2d503b2ccd946400c685180f52266fa7bbdb50 (KEY)0238159120150000022000000548optimizationofethylesterproductionassistedbyultras DE-627 ger DE-627 rakwb eng 540 DE-600 Noipin, K verfasserin aut Optimization of ethyl ester production assisted by ultrasonic irradiation 2015 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier This study presents the optimization of the continuous flow potassium hydroxide-catalyzed synthesis of ethyl ester from palm oil with ultrasonic assistance. The process was optimized by application of factorial design and response surface methodology. The independent variables considered were ethanol to oil molar ratio, catalyst concentration, reaction temperature and ultrasonic amplitude; and the response was ethyl ester yield. The results show that ethanol to oil molar ratio, catalyst concentration, and ultrasonic amplitude have positive effect on ethyl ester yield, whereas reaction temperature has negative influence on ethyl ester yield. Second-order models were developed to predict the responses analyzed as a function of these three variables, and the developed models predicts the results in the experimental ranges studied adequately. This study shows that ultrasonic irradiation improved the ethyl ester production process to achieve ethyl ester yields above 92%. Nutzungsrecht: Copyright © 2014 Elsevier B.V. All rights reserved. © COPYRIGHT 2015 Elsevier B.V. Plant Oils - chemistry Potassium Compounds - chemistry Esters - chemical synthesis Hydroxides - chemistry Kumar, S oth Enthalten in Ultrasonics sonochemistry Amsterdam [u.a.] : Elsevier, 1994 22(2015), Seite 548 (DE-627)182456803 (DE-600)1208333-1 (DE-576)043089054 1350-4177 nnns volume:22 year:2015 pages:548 http://dx.doi.org/10.1016/j.ultsonch.2014.07.019 Volltext http://www.ncbi.nlm.nih.gov/pubmed/25116594 GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-PHY SSG-OLC-CHE SSG-OLC-PHA SSG-OLC-DE-84 GBV_ILN_70 GBV_ILN_170 GBV_ILN_2006 GBV_ILN_4012 AR 22 2015 548 |
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10.1016/j.ultsonch.2014.07.019 doi PQ20160617 (DE-627)OLC1959813730 (DE-599)GBVOLC1959813730 (PRQ)g1052-be20187f1411ab3b985c879249b2d503b2ccd946400c685180f52266fa7bbdb50 (KEY)0238159120150000022000000548optimizationofethylesterproductionassistedbyultras DE-627 ger DE-627 rakwb eng 540 DE-600 Noipin, K verfasserin aut Optimization of ethyl ester production assisted by ultrasonic irradiation 2015 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier This study presents the optimization of the continuous flow potassium hydroxide-catalyzed synthesis of ethyl ester from palm oil with ultrasonic assistance. The process was optimized by application of factorial design and response surface methodology. The independent variables considered were ethanol to oil molar ratio, catalyst concentration, reaction temperature and ultrasonic amplitude; and the response was ethyl ester yield. The results show that ethanol to oil molar ratio, catalyst concentration, and ultrasonic amplitude have positive effect on ethyl ester yield, whereas reaction temperature has negative influence on ethyl ester yield. Second-order models were developed to predict the responses analyzed as a function of these three variables, and the developed models predicts the results in the experimental ranges studied adequately. This study shows that ultrasonic irradiation improved the ethyl ester production process to achieve ethyl ester yields above 92%. Nutzungsrecht: Copyright © 2014 Elsevier B.V. All rights reserved. © COPYRIGHT 2015 Elsevier B.V. Plant Oils - chemistry Potassium Compounds - chemistry Esters - chemical synthesis Hydroxides - chemistry Kumar, S oth Enthalten in Ultrasonics sonochemistry Amsterdam [u.a.] : Elsevier, 1994 22(2015), Seite 548 (DE-627)182456803 (DE-600)1208333-1 (DE-576)043089054 1350-4177 nnns volume:22 year:2015 pages:548 http://dx.doi.org/10.1016/j.ultsonch.2014.07.019 Volltext http://www.ncbi.nlm.nih.gov/pubmed/25116594 GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-PHY SSG-OLC-CHE SSG-OLC-PHA SSG-OLC-DE-84 GBV_ILN_70 GBV_ILN_170 GBV_ILN_2006 GBV_ILN_4012 AR 22 2015 548 |
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This study presents the optimization of the continuous flow potassium hydroxide-catalyzed synthesis of ethyl ester from palm oil with ultrasonic assistance. The process was optimized by application of factorial design and response surface methodology. The independent variables considered were ethanol to oil molar ratio, catalyst concentration, reaction temperature and ultrasonic amplitude; and the response was ethyl ester yield. The results show that ethanol to oil molar ratio, catalyst concentration, and ultrasonic amplitude have positive effect on ethyl ester yield, whereas reaction temperature has negative influence on ethyl ester yield. Second-order models were developed to predict the responses analyzed as a function of these three variables, and the developed models predicts the results in the experimental ranges studied adequately. This study shows that ultrasonic irradiation improved the ethyl ester production process to achieve ethyl ester yields above 92%. |
abstractGer |
This study presents the optimization of the continuous flow potassium hydroxide-catalyzed synthesis of ethyl ester from palm oil with ultrasonic assistance. The process was optimized by application of factorial design and response surface methodology. The independent variables considered were ethanol to oil molar ratio, catalyst concentration, reaction temperature and ultrasonic amplitude; and the response was ethyl ester yield. The results show that ethanol to oil molar ratio, catalyst concentration, and ultrasonic amplitude have positive effect on ethyl ester yield, whereas reaction temperature has negative influence on ethyl ester yield. Second-order models were developed to predict the responses analyzed as a function of these three variables, and the developed models predicts the results in the experimental ranges studied adequately. This study shows that ultrasonic irradiation improved the ethyl ester production process to achieve ethyl ester yields above 92%. |
abstract_unstemmed |
This study presents the optimization of the continuous flow potassium hydroxide-catalyzed synthesis of ethyl ester from palm oil with ultrasonic assistance. The process was optimized by application of factorial design and response surface methodology. The independent variables considered were ethanol to oil molar ratio, catalyst concentration, reaction temperature and ultrasonic amplitude; and the response was ethyl ester yield. The results show that ethanol to oil molar ratio, catalyst concentration, and ultrasonic amplitude have positive effect on ethyl ester yield, whereas reaction temperature has negative influence on ethyl ester yield. Second-order models were developed to predict the responses analyzed as a function of these three variables, and the developed models predicts the results in the experimental ranges studied adequately. This study shows that ultrasonic irradiation improved the ethyl ester production process to achieve ethyl ester yields above 92%. |
collection_details |
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title_short |
Optimization of ethyl ester production assisted by ultrasonic irradiation |
url |
http://dx.doi.org/10.1016/j.ultsonch.2014.07.019 http://www.ncbi.nlm.nih.gov/pubmed/25116594 |
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author2 |
Kumar, S |
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doi_str |
10.1016/j.ultsonch.2014.07.019 |
up_date |
2024-07-03T18:53:21.657Z |
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