Synthesis of [alpha]-Nitro Ketoximes from Styrenes and tert-Butyl Nitrite
We have discovered that various α-nitro ketoximes can be synthesized in good yields starting from styrenes and tert-butyl nitrite. The success of the reaction was critically dependent on the use of a mixture solvent of dimethylsulfoxide and water. The reaction can tolerate a wide variety of substitu...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Qi Cao [verfasserIn] |
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| Format: |
Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2015 |
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| Schlagwörter: |
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| Systematik: |
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| Übergeordnetes Werk: |
Enthalten in: Synthetic communications - Philadelphia, Pa. : Taylor & Francis, 1971, 45(2015), 19, Seite 2181 |
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| Übergeordnetes Werk: |
volume:45 ; year:2015 ; number:19 ; pages:2181 |
| Links: |
|---|
| DOI / URN: |
10.1080/00397911.2015.1062988 |
|---|
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OLC1962407551 |
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| 520 | |a We have discovered that various α-nitro ketoximes can be synthesized in good yields starting from styrenes and tert-butyl nitrite. The success of the reaction was critically dependent on the use of a mixture solvent of dimethylsulfoxide and water. The reaction can tolerate a wide variety of substituents including electron-withdrawing and electron-donating groups. | ||
| 650 | 4 | |a Free radical | |
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| 700 | 0 | |a Jidan Liu |4 oth | |
| 700 | 0 | |a Lin Yu |4 oth | |
| 700 | 0 | |a Qingwen Gui |4 oth | |
| 700 | 0 | |a Xiang Chen |4 oth | |
| 700 | 0 | |a Ze Tan |4 oth | |
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10.1080/00397911.2015.1062988 doi PQ20160617 (DE-627)OLC1962407551 (DE-599)GBVOLC1962407551 (PRQ)p872-5322e9ae2a62ddc0b43836d6e32aa47cfa2dcf90fd0e85bbcbb36a73d8747a580 (KEY)0003667620150000045001902181synthesisofalphanitroketoximesfromstyrenesandtertb DE-627 ger DE-627 rakwb eng 670 540 DE-600 VA 7400 AVZ rvk 35.52 bkl Qi Cao verfasserin aut Synthesis of [alpha]-Nitro Ketoximes from Styrenes and tert-Butyl Nitrite 2015 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier We have discovered that various α-nitro ketoximes can be synthesized in good yields starting from styrenes and tert-butyl nitrite. The success of the reaction was critically dependent on the use of a mixture solvent of dimethylsulfoxide and water. The reaction can tolerate a wide variety of substituents including electron-withdrawing and electron-donating groups. Free radical tert-butyl nitrite α-nitro ketoxime Free radicals styrene Jidan Liu oth Lin Yu oth Qingwen Gui oth Xiang Chen oth Ze Tan oth Enthalten in Synthetic communications Philadelphia, Pa. : Taylor & Francis, 1971 45(2015), 19, Seite 2181 (DE-627)129289892 (DE-600)120265-0 (DE-576)014471264 0039-7911 nnns volume:45 year:2015 number:19 pages:2181 http://dx.doi.org/10.1080/00397911.2015.1062988 Volltext http://search.proquest.com/docview/1712315179 GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE SSG-OLC-PHA SSG-OLC-DE-84 GBV_ILN_70 GBV_ILN_120 GBV_ILN_2001 GBV_ILN_2020 VA 7400 35.52 AVZ AR 45 2015 19 2181 |
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10.1080/00397911.2015.1062988 doi PQ20160617 (DE-627)OLC1962407551 (DE-599)GBVOLC1962407551 (PRQ)p872-5322e9ae2a62ddc0b43836d6e32aa47cfa2dcf90fd0e85bbcbb36a73d8747a580 (KEY)0003667620150000045001902181synthesisofalphanitroketoximesfromstyrenesandtertb DE-627 ger DE-627 rakwb eng 670 540 DE-600 VA 7400 AVZ rvk 35.52 bkl Qi Cao verfasserin aut Synthesis of [alpha]-Nitro Ketoximes from Styrenes and tert-Butyl Nitrite 2015 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier We have discovered that various α-nitro ketoximes can be synthesized in good yields starting from styrenes and tert-butyl nitrite. The success of the reaction was critically dependent on the use of a mixture solvent of dimethylsulfoxide and water. The reaction can tolerate a wide variety of substituents including electron-withdrawing and electron-donating groups. Free radical tert-butyl nitrite α-nitro ketoxime Free radicals styrene Jidan Liu oth Lin Yu oth Qingwen Gui oth Xiang Chen oth Ze Tan oth Enthalten in Synthetic communications Philadelphia, Pa. : Taylor & Francis, 1971 45(2015), 19, Seite 2181 (DE-627)129289892 (DE-600)120265-0 (DE-576)014471264 0039-7911 nnns volume:45 year:2015 number:19 pages:2181 http://dx.doi.org/10.1080/00397911.2015.1062988 Volltext http://search.proquest.com/docview/1712315179 GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE SSG-OLC-PHA SSG-OLC-DE-84 GBV_ILN_70 GBV_ILN_120 GBV_ILN_2001 GBV_ILN_2020 VA 7400 35.52 AVZ AR 45 2015 19 2181 |
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10.1080/00397911.2015.1062988 doi PQ20160617 (DE-627)OLC1962407551 (DE-599)GBVOLC1962407551 (PRQ)p872-5322e9ae2a62ddc0b43836d6e32aa47cfa2dcf90fd0e85bbcbb36a73d8747a580 (KEY)0003667620150000045001902181synthesisofalphanitroketoximesfromstyrenesandtertb DE-627 ger DE-627 rakwb eng 670 540 DE-600 VA 7400 AVZ rvk 35.52 bkl Qi Cao verfasserin aut Synthesis of [alpha]-Nitro Ketoximes from Styrenes and tert-Butyl Nitrite 2015 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier We have discovered that various α-nitro ketoximes can be synthesized in good yields starting from styrenes and tert-butyl nitrite. The success of the reaction was critically dependent on the use of a mixture solvent of dimethylsulfoxide and water. The reaction can tolerate a wide variety of substituents including electron-withdrawing and electron-donating groups. Free radical tert-butyl nitrite α-nitro ketoxime Free radicals styrene Jidan Liu oth Lin Yu oth Qingwen Gui oth Xiang Chen oth Ze Tan oth Enthalten in Synthetic communications Philadelphia, Pa. : Taylor & Francis, 1971 45(2015), 19, Seite 2181 (DE-627)129289892 (DE-600)120265-0 (DE-576)014471264 0039-7911 nnns volume:45 year:2015 number:19 pages:2181 http://dx.doi.org/10.1080/00397911.2015.1062988 Volltext http://search.proquest.com/docview/1712315179 GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE SSG-OLC-PHA SSG-OLC-DE-84 GBV_ILN_70 GBV_ILN_120 GBV_ILN_2001 GBV_ILN_2020 VA 7400 35.52 AVZ AR 45 2015 19 2181 |
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10.1080/00397911.2015.1062988 doi PQ20160617 (DE-627)OLC1962407551 (DE-599)GBVOLC1962407551 (PRQ)p872-5322e9ae2a62ddc0b43836d6e32aa47cfa2dcf90fd0e85bbcbb36a73d8747a580 (KEY)0003667620150000045001902181synthesisofalphanitroketoximesfromstyrenesandtertb DE-627 ger DE-627 rakwb eng 670 540 DE-600 VA 7400 AVZ rvk 35.52 bkl Qi Cao verfasserin aut Synthesis of [alpha]-Nitro Ketoximes from Styrenes and tert-Butyl Nitrite 2015 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier We have discovered that various α-nitro ketoximes can be synthesized in good yields starting from styrenes and tert-butyl nitrite. The success of the reaction was critically dependent on the use of a mixture solvent of dimethylsulfoxide and water. The reaction can tolerate a wide variety of substituents including electron-withdrawing and electron-donating groups. Free radical tert-butyl nitrite α-nitro ketoxime Free radicals styrene Jidan Liu oth Lin Yu oth Qingwen Gui oth Xiang Chen oth Ze Tan oth Enthalten in Synthetic communications Philadelphia, Pa. : Taylor & Francis, 1971 45(2015), 19, Seite 2181 (DE-627)129289892 (DE-600)120265-0 (DE-576)014471264 0039-7911 nnns volume:45 year:2015 number:19 pages:2181 http://dx.doi.org/10.1080/00397911.2015.1062988 Volltext http://search.proquest.com/docview/1712315179 GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE SSG-OLC-PHA SSG-OLC-DE-84 GBV_ILN_70 GBV_ILN_120 GBV_ILN_2001 GBV_ILN_2020 VA 7400 35.52 AVZ AR 45 2015 19 2181 |
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10.1080/00397911.2015.1062988 doi PQ20160617 (DE-627)OLC1962407551 (DE-599)GBVOLC1962407551 (PRQ)p872-5322e9ae2a62ddc0b43836d6e32aa47cfa2dcf90fd0e85bbcbb36a73d8747a580 (KEY)0003667620150000045001902181synthesisofalphanitroketoximesfromstyrenesandtertb DE-627 ger DE-627 rakwb eng 670 540 DE-600 VA 7400 AVZ rvk 35.52 bkl Qi Cao verfasserin aut Synthesis of [alpha]-Nitro Ketoximes from Styrenes and tert-Butyl Nitrite 2015 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier We have discovered that various α-nitro ketoximes can be synthesized in good yields starting from styrenes and tert-butyl nitrite. The success of the reaction was critically dependent on the use of a mixture solvent of dimethylsulfoxide and water. The reaction can tolerate a wide variety of substituents including electron-withdrawing and electron-donating groups. Free radical tert-butyl nitrite α-nitro ketoxime Free radicals styrene Jidan Liu oth Lin Yu oth Qingwen Gui oth Xiang Chen oth Ze Tan oth Enthalten in Synthetic communications Philadelphia, Pa. : Taylor & Francis, 1971 45(2015), 19, Seite 2181 (DE-627)129289892 (DE-600)120265-0 (DE-576)014471264 0039-7911 nnns volume:45 year:2015 number:19 pages:2181 http://dx.doi.org/10.1080/00397911.2015.1062988 Volltext http://search.proquest.com/docview/1712315179 GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE SSG-OLC-PHA SSG-OLC-DE-84 GBV_ILN_70 GBV_ILN_120 GBV_ILN_2001 GBV_ILN_2020 VA 7400 35.52 AVZ AR 45 2015 19 2181 |
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Synthesis of [alpha]-Nitro Ketoximes from Styrenes and tert-Butyl Nitrite |
| abstract |
We have discovered that various α-nitro ketoximes can be synthesized in good yields starting from styrenes and tert-butyl nitrite. The success of the reaction was critically dependent on the use of a mixture solvent of dimethylsulfoxide and water. The reaction can tolerate a wide variety of substituents including electron-withdrawing and electron-donating groups. |
| abstractGer |
We have discovered that various α-nitro ketoximes can be synthesized in good yields starting from styrenes and tert-butyl nitrite. The success of the reaction was critically dependent on the use of a mixture solvent of dimethylsulfoxide and water. The reaction can tolerate a wide variety of substituents including electron-withdrawing and electron-donating groups. |
| abstract_unstemmed |
We have discovered that various α-nitro ketoximes can be synthesized in good yields starting from styrenes and tert-butyl nitrite. The success of the reaction was critically dependent on the use of a mixture solvent of dimethylsulfoxide and water. The reaction can tolerate a wide variety of substituents including electron-withdrawing and electron-donating groups. |
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| container_issue |
19 |
| title_short |
Synthesis of [alpha]-Nitro Ketoximes from Styrenes and tert-Butyl Nitrite |
| url |
http://dx.doi.org/10.1080/00397911.2015.1062988 http://search.proquest.com/docview/1712315179 |
| remote_bool |
false |
| author2 |
Jidan Liu Lin Yu Qingwen Gui Xiang Chen Ze Tan |
| author2Str |
Jidan Liu Lin Yu Qingwen Gui Xiang Chen Ze Tan |
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| doi_str |
10.1080/00397911.2015.1062988 |
| up_date |
2024-07-04T03:30:07.578Z |
| _version_ |
1803617627111686144 |
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