Determination and dissipation of fipronil and its metabolites in peanut and soil
In this study, a modified quick, easy, cheap, effective, rugged, and safe (QuEChERS) method was established for the extraction and cleanup of fipronil and its three metabolites (fipronil solfone, sulfide, and desulfinyl) in peanut kernel, shell, straw, seedling, and soil samples, and liquid chromato...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Li, Minghui [verfasserIn] |
|---|
| Format: |
Artikel |
|---|---|
| Sprache: |
Englisch |
| Erschienen: |
2015 |
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| Übergeordnetes Werk: |
Enthalten in: Journal of agricultural and food chemistry - Columbus, Ohio : American Chemical Soc., 1953, 63(2015), 18, Seite 4435 |
|---|---|
| Übergeordnetes Werk: |
volume:63 ; year:2015 ; number:18 ; pages:4435 |
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| 520 | |a In this study, a modified quick, easy, cheap, effective, rugged, and safe (QuEChERS) method was established for the extraction and cleanup of fipronil and its three metabolites (fipronil solfone, sulfide, and desulfinyl) in peanut kernel, shell, straw, seedling, and soil samples, and liquid chromatography-tandem mass spectrometry (LC-MS/MS) was used for analysis. The average recoveries were 66-116% at the level of 0.001-0.1 mg/kg with the RSD <19%, and the limit of detection was 0.3 ng/g for all matrices. The dissipation experiment results demonstrated that fipronil dissipated more rapidly in peanut seedling than in soil, with half-lives of <1 day in peanut seedling and 32-57 days in soil depending on the soil pH. The final residues at harvest of peanut kernels were all below 0.02 mg/kg, whereas in peanut shell and straw, the total highest residues were 0.99 and 0.30 mg/kg, respectively. Fipronil-desulfinyl and fipronil-sulfone were the highest residue metabolites in peanut plant (seedling and straw) and soil samples, respectively. | ||
| 650 | 4 | |a Pyrazoles - metabolism | |
| 650 | 4 | |a Arachis hypogaea - chemistry | |
| 650 | 4 | |a Pyrazoles - chemistry | |
| 650 | 4 | |a Insecticides - isolation & purification | |
| 650 | 4 | |a Pyrazoles - isolation & purification | |
| 650 | 4 | |a Soil Pollutants - chemistry | |
| 650 | 4 | |a Soil Pollutants - metabolism | |
| 650 | 4 | |a Tandem Mass Spectrometry - methods | |
| 650 | 4 | |a Pesticide Residues - metabolism | |
| 650 | 4 | |a Insecticides - metabolism | |
| 650 | 4 | |a Pesticide Residues - chemistry | |
| 650 | 4 | |a Pesticide Residues - isolation & purification | |
| 650 | 4 | |a Insecticides - chemistry | |
| 650 | 4 | |a Chromatography, High Pressure Liquid - methods | |
| 650 | 4 | |a Arachis hypogaea - metabolism | |
| 700 | 1 | |a Li, Puyu |4 oth | |
| 700 | 1 | |a Wang, Lin |4 oth | |
| 700 | 1 | |a Feng, Mengyuan |4 oth | |
| 700 | 1 | |a Han, Lijun |4 oth | |
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PQ20160617 (DE-627)OLC1963011902 (DE-599)GBVOLC1963011902 (PRQ)p837-282f8ade13c3b9aaa01e8c6fdc9dd5b0056547bdb2759b891a982c707505914b0 (KEY)0011841920150000063001804435determinationanddissipationoffipronilanditsmetabol DE-627 ger DE-627 rakwb eng 630 640 540 DNB 58.27 bkl 58.34 bkl 42.63 bkl Li, Minghui verfasserin aut Determination and dissipation of fipronil and its metabolites in peanut and soil 2015 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier In this study, a modified quick, easy, cheap, effective, rugged, and safe (QuEChERS) method was established for the extraction and cleanup of fipronil and its three metabolites (fipronil solfone, sulfide, and desulfinyl) in peanut kernel, shell, straw, seedling, and soil samples, and liquid chromatography-tandem mass spectrometry (LC-MS/MS) was used for analysis. The average recoveries were 66-116% at the level of 0.001-0.1 mg/kg with the RSD <19%, and the limit of detection was 0.3 ng/g for all matrices. The dissipation experiment results demonstrated that fipronil dissipated more rapidly in peanut seedling than in soil, with half-lives of <1 day in peanut seedling and 32-57 days in soil depending on the soil pH. The final residues at harvest of peanut kernels were all below 0.02 mg/kg, whereas in peanut shell and straw, the total highest residues were 0.99 and 0.30 mg/kg, respectively. Fipronil-desulfinyl and fipronil-sulfone were the highest residue metabolites in peanut plant (seedling and straw) and soil samples, respectively. Pyrazoles - metabolism Arachis hypogaea - chemistry Pyrazoles - chemistry Insecticides - isolation & purification Pyrazoles - isolation & purification Soil Pollutants - chemistry Soil Pollutants - metabolism Tandem Mass Spectrometry - methods Pesticide Residues - metabolism Insecticides - metabolism Pesticide Residues - chemistry Pesticide Residues - isolation & purification Insecticides - chemistry Chromatography, High Pressure Liquid - methods Arachis hypogaea - metabolism Li, Puyu oth Wang, Lin oth Feng, Mengyuan oth Han, Lijun oth Enthalten in Journal of agricultural and food chemistry Columbus, Ohio : American Chemical Soc., 1953 63(2015), 18, Seite 4435 (DE-627)129602795 (DE-600)241619-0 (DE-576)015096610 0021-8561 nnns volume:63 year:2015 number:18 pages:4435 http://www.ncbi.nlm.nih.gov/pubmed/25664639 GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE SSG-OLC-PHA SSG-OLC-DE-84 SSG-OPC-FOR GBV_ILN_70 GBV_ILN_2006 GBV_ILN_4219 58.27 AVZ 58.34 AVZ 42.63 AVZ AR 63 2015 18 4435 |
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PQ20160617 (DE-627)OLC1963011902 (DE-599)GBVOLC1963011902 (PRQ)p837-282f8ade13c3b9aaa01e8c6fdc9dd5b0056547bdb2759b891a982c707505914b0 (KEY)0011841920150000063001804435determinationanddissipationoffipronilanditsmetabol DE-627 ger DE-627 rakwb eng 630 640 540 DNB 58.27 bkl 58.34 bkl 42.63 bkl Li, Minghui verfasserin aut Determination and dissipation of fipronil and its metabolites in peanut and soil 2015 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier In this study, a modified quick, easy, cheap, effective, rugged, and safe (QuEChERS) method was established for the extraction and cleanup of fipronil and its three metabolites (fipronil solfone, sulfide, and desulfinyl) in peanut kernel, shell, straw, seedling, and soil samples, and liquid chromatography-tandem mass spectrometry (LC-MS/MS) was used for analysis. The average recoveries were 66-116% at the level of 0.001-0.1 mg/kg with the RSD <19%, and the limit of detection was 0.3 ng/g for all matrices. The dissipation experiment results demonstrated that fipronil dissipated more rapidly in peanut seedling than in soil, with half-lives of <1 day in peanut seedling and 32-57 days in soil depending on the soil pH. The final residues at harvest of peanut kernels were all below 0.02 mg/kg, whereas in peanut shell and straw, the total highest residues were 0.99 and 0.30 mg/kg, respectively. Fipronil-desulfinyl and fipronil-sulfone were the highest residue metabolites in peanut plant (seedling and straw) and soil samples, respectively. Pyrazoles - metabolism Arachis hypogaea - chemistry Pyrazoles - chemistry Insecticides - isolation & purification Pyrazoles - isolation & purification Soil Pollutants - chemistry Soil Pollutants - metabolism Tandem Mass Spectrometry - methods Pesticide Residues - metabolism Insecticides - metabolism Pesticide Residues - chemistry Pesticide Residues - isolation & purification Insecticides - chemistry Chromatography, High Pressure Liquid - methods Arachis hypogaea - metabolism Li, Puyu oth Wang, Lin oth Feng, Mengyuan oth Han, Lijun oth Enthalten in Journal of agricultural and food chemistry Columbus, Ohio : American Chemical Soc., 1953 63(2015), 18, Seite 4435 (DE-627)129602795 (DE-600)241619-0 (DE-576)015096610 0021-8561 nnns volume:63 year:2015 number:18 pages:4435 http://www.ncbi.nlm.nih.gov/pubmed/25664639 GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE SSG-OLC-PHA SSG-OLC-DE-84 SSG-OPC-FOR GBV_ILN_70 GBV_ILN_2006 GBV_ILN_4219 58.27 AVZ 58.34 AVZ 42.63 AVZ AR 63 2015 18 4435 |
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PQ20160617 (DE-627)OLC1963011902 (DE-599)GBVOLC1963011902 (PRQ)p837-282f8ade13c3b9aaa01e8c6fdc9dd5b0056547bdb2759b891a982c707505914b0 (KEY)0011841920150000063001804435determinationanddissipationoffipronilanditsmetabol DE-627 ger DE-627 rakwb eng 630 640 540 DNB 58.27 bkl 58.34 bkl 42.63 bkl Li, Minghui verfasserin aut Determination and dissipation of fipronil and its metabolites in peanut and soil 2015 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier In this study, a modified quick, easy, cheap, effective, rugged, and safe (QuEChERS) method was established for the extraction and cleanup of fipronil and its three metabolites (fipronil solfone, sulfide, and desulfinyl) in peanut kernel, shell, straw, seedling, and soil samples, and liquid chromatography-tandem mass spectrometry (LC-MS/MS) was used for analysis. The average recoveries were 66-116% at the level of 0.001-0.1 mg/kg with the RSD <19%, and the limit of detection was 0.3 ng/g for all matrices. The dissipation experiment results demonstrated that fipronil dissipated more rapidly in peanut seedling than in soil, with half-lives of <1 day in peanut seedling and 32-57 days in soil depending on the soil pH. The final residues at harvest of peanut kernels were all below 0.02 mg/kg, whereas in peanut shell and straw, the total highest residues were 0.99 and 0.30 mg/kg, respectively. Fipronil-desulfinyl and fipronil-sulfone were the highest residue metabolites in peanut plant (seedling and straw) and soil samples, respectively. Pyrazoles - metabolism Arachis hypogaea - chemistry Pyrazoles - chemistry Insecticides - isolation & purification Pyrazoles - isolation & purification Soil Pollutants - chemistry Soil Pollutants - metabolism Tandem Mass Spectrometry - methods Pesticide Residues - metabolism Insecticides - metabolism Pesticide Residues - chemistry Pesticide Residues - isolation & purification Insecticides - chemistry Chromatography, High Pressure Liquid - methods Arachis hypogaea - metabolism Li, Puyu oth Wang, Lin oth Feng, Mengyuan oth Han, Lijun oth Enthalten in Journal of agricultural and food chemistry Columbus, Ohio : American Chemical Soc., 1953 63(2015), 18, Seite 4435 (DE-627)129602795 (DE-600)241619-0 (DE-576)015096610 0021-8561 nnns volume:63 year:2015 number:18 pages:4435 http://www.ncbi.nlm.nih.gov/pubmed/25664639 GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE SSG-OLC-PHA SSG-OLC-DE-84 SSG-OPC-FOR GBV_ILN_70 GBV_ILN_2006 GBV_ILN_4219 58.27 AVZ 58.34 AVZ 42.63 AVZ AR 63 2015 18 4435 |
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PQ20160617 (DE-627)OLC1963011902 (DE-599)GBVOLC1963011902 (PRQ)p837-282f8ade13c3b9aaa01e8c6fdc9dd5b0056547bdb2759b891a982c707505914b0 (KEY)0011841920150000063001804435determinationanddissipationoffipronilanditsmetabol DE-627 ger DE-627 rakwb eng 630 640 540 DNB 58.27 bkl 58.34 bkl 42.63 bkl Li, Minghui verfasserin aut Determination and dissipation of fipronil and its metabolites in peanut and soil 2015 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier In this study, a modified quick, easy, cheap, effective, rugged, and safe (QuEChERS) method was established for the extraction and cleanup of fipronil and its three metabolites (fipronil solfone, sulfide, and desulfinyl) in peanut kernel, shell, straw, seedling, and soil samples, and liquid chromatography-tandem mass spectrometry (LC-MS/MS) was used for analysis. The average recoveries were 66-116% at the level of 0.001-0.1 mg/kg with the RSD <19%, and the limit of detection was 0.3 ng/g for all matrices. The dissipation experiment results demonstrated that fipronil dissipated more rapidly in peanut seedling than in soil, with half-lives of <1 day in peanut seedling and 32-57 days in soil depending on the soil pH. The final residues at harvest of peanut kernels were all below 0.02 mg/kg, whereas in peanut shell and straw, the total highest residues were 0.99 and 0.30 mg/kg, respectively. Fipronil-desulfinyl and fipronil-sulfone were the highest residue metabolites in peanut plant (seedling and straw) and soil samples, respectively. Pyrazoles - metabolism Arachis hypogaea - chemistry Pyrazoles - chemistry Insecticides - isolation & purification Pyrazoles - isolation & purification Soil Pollutants - chemistry Soil Pollutants - metabolism Tandem Mass Spectrometry - methods Pesticide Residues - metabolism Insecticides - metabolism Pesticide Residues - chemistry Pesticide Residues - isolation & purification Insecticides - chemistry Chromatography, High Pressure Liquid - methods Arachis hypogaea - metabolism Li, Puyu oth Wang, Lin oth Feng, Mengyuan oth Han, Lijun oth Enthalten in Journal of agricultural and food chemistry Columbus, Ohio : American Chemical Soc., 1953 63(2015), 18, Seite 4435 (DE-627)129602795 (DE-600)241619-0 (DE-576)015096610 0021-8561 nnns volume:63 year:2015 number:18 pages:4435 http://www.ncbi.nlm.nih.gov/pubmed/25664639 GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE SSG-OLC-PHA SSG-OLC-DE-84 SSG-OPC-FOR GBV_ILN_70 GBV_ILN_2006 GBV_ILN_4219 58.27 AVZ 58.34 AVZ 42.63 AVZ AR 63 2015 18 4435 |
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The average recoveries were 66-116% at the level of 0.001-0.1 mg/kg with the RSD <19%, and the limit of detection was 0.3 ng/g for all matrices. The dissipation experiment results demonstrated that fipronil dissipated more rapidly in peanut seedling than in soil, with half-lives of <1 day in peanut seedling and 32-57 days in soil depending on the soil pH. The final residues at harvest of peanut kernels were all below 0.02 mg/kg, whereas in peanut shell and straw, the total highest residues were 0.99 and 0.30 mg/kg, respectively. 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Li, Minghui ddc 630 bkl 58.27 bkl 58.34 bkl 42.63 misc Pyrazoles - metabolism misc Arachis hypogaea - chemistry misc Pyrazoles - chemistry misc Insecticides - isolation & purification misc Pyrazoles - isolation & purification misc Soil Pollutants - chemistry misc Soil Pollutants - metabolism misc Tandem Mass Spectrometry - methods misc Pesticide Residues - metabolism misc Insecticides - metabolism misc Pesticide Residues - chemistry misc Pesticide Residues - isolation & purification misc Insecticides - chemistry misc Chromatography, High Pressure Liquid - methods misc Arachis hypogaea - metabolism Determination and dissipation of fipronil and its metabolites in peanut and soil |
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630 640 540 DNB 58.27 bkl 58.34 bkl 42.63 bkl Determination and dissipation of fipronil and its metabolites in peanut and soil Pyrazoles - metabolism Arachis hypogaea - chemistry Pyrazoles - chemistry Insecticides - isolation & purification Pyrazoles - isolation & purification Soil Pollutants - chemistry Soil Pollutants - metabolism Tandem Mass Spectrometry - methods Pesticide Residues - metabolism Insecticides - metabolism Pesticide Residues - chemistry Pesticide Residues - isolation & purification Insecticides - chemistry Chromatography, High Pressure Liquid - methods Arachis hypogaea - metabolism |
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Determination and dissipation of fipronil and its metabolites in peanut and soil |
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Determination and dissipation of fipronil and its metabolites in peanut and soil |
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determination and dissipation of fipronil and its metabolites in peanut and soil |
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Determination and dissipation of fipronil and its metabolites in peanut and soil |
| abstract |
In this study, a modified quick, easy, cheap, effective, rugged, and safe (QuEChERS) method was established for the extraction and cleanup of fipronil and its three metabolites (fipronil solfone, sulfide, and desulfinyl) in peanut kernel, shell, straw, seedling, and soil samples, and liquid chromatography-tandem mass spectrometry (LC-MS/MS) was used for analysis. The average recoveries were 66-116% at the level of 0.001-0.1 mg/kg with the RSD <19%, and the limit of detection was 0.3 ng/g for all matrices. The dissipation experiment results demonstrated that fipronil dissipated more rapidly in peanut seedling than in soil, with half-lives of <1 day in peanut seedling and 32-57 days in soil depending on the soil pH. The final residues at harvest of peanut kernels were all below 0.02 mg/kg, whereas in peanut shell and straw, the total highest residues were 0.99 and 0.30 mg/kg, respectively. Fipronil-desulfinyl and fipronil-sulfone were the highest residue metabolites in peanut plant (seedling and straw) and soil samples, respectively. |
| abstractGer |
In this study, a modified quick, easy, cheap, effective, rugged, and safe (QuEChERS) method was established for the extraction and cleanup of fipronil and its three metabolites (fipronil solfone, sulfide, and desulfinyl) in peanut kernel, shell, straw, seedling, and soil samples, and liquid chromatography-tandem mass spectrometry (LC-MS/MS) was used for analysis. The average recoveries were 66-116% at the level of 0.001-0.1 mg/kg with the RSD <19%, and the limit of detection was 0.3 ng/g for all matrices. The dissipation experiment results demonstrated that fipronil dissipated more rapidly in peanut seedling than in soil, with half-lives of <1 day in peanut seedling and 32-57 days in soil depending on the soil pH. The final residues at harvest of peanut kernels were all below 0.02 mg/kg, whereas in peanut shell and straw, the total highest residues were 0.99 and 0.30 mg/kg, respectively. Fipronil-desulfinyl and fipronil-sulfone were the highest residue metabolites in peanut plant (seedling and straw) and soil samples, respectively. |
| abstract_unstemmed |
In this study, a modified quick, easy, cheap, effective, rugged, and safe (QuEChERS) method was established for the extraction and cleanup of fipronil and its three metabolites (fipronil solfone, sulfide, and desulfinyl) in peanut kernel, shell, straw, seedling, and soil samples, and liquid chromatography-tandem mass spectrometry (LC-MS/MS) was used for analysis. The average recoveries were 66-116% at the level of 0.001-0.1 mg/kg with the RSD <19%, and the limit of detection was 0.3 ng/g for all matrices. The dissipation experiment results demonstrated that fipronil dissipated more rapidly in peanut seedling than in soil, with half-lives of <1 day in peanut seedling and 32-57 days in soil depending on the soil pH. The final residues at harvest of peanut kernels were all below 0.02 mg/kg, whereas in peanut shell and straw, the total highest residues were 0.99 and 0.30 mg/kg, respectively. Fipronil-desulfinyl and fipronil-sulfone were the highest residue metabolites in peanut plant (seedling and straw) and soil samples, respectively. |
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Determination and dissipation of fipronil and its metabolites in peanut and soil |
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Li, Puyu Wang, Lin Feng, Mengyuan Han, Lijun |
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<?xml version="1.0" encoding="UTF-8"?><collection xmlns="http://www.loc.gov/MARC21/slim"><record><leader>01000caa a2200265 4500</leader><controlfield tag="001">OLC1963011902</controlfield><controlfield tag="003">DE-627</controlfield><controlfield tag="005">20230518194835.0</controlfield><controlfield tag="007">tu</controlfield><controlfield tag="008">160206s2015 xx ||||| 00| ||eng c</controlfield><datafield tag="028" ind1="5" ind2="2"><subfield code="a">PQ20160617</subfield></datafield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(DE-627)OLC1963011902</subfield></datafield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(DE-599)GBVOLC1963011902</subfield></datafield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(PRQ)p837-282f8ade13c3b9aaa01e8c6fdc9dd5b0056547bdb2759b891a982c707505914b0</subfield></datafield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(KEY)0011841920150000063001804435determinationanddissipationoffipronilanditsmetabol</subfield></datafield><datafield tag="040" ind1=" " ind2=" "><subfield code="a">DE-627</subfield><subfield code="b">ger</subfield><subfield code="c">DE-627</subfield><subfield code="e">rakwb</subfield></datafield><datafield tag="041" ind1=" " ind2=" "><subfield code="a">eng</subfield></datafield><datafield tag="082" ind1="0" ind2="4"><subfield code="a">630</subfield><subfield code="a">640</subfield><subfield code="a">540</subfield><subfield code="q">DNB</subfield></datafield><datafield tag="084" ind1=" " ind2=" "><subfield code="a">58.27</subfield><subfield code="2">bkl</subfield></datafield><datafield tag="084" ind1=" " ind2=" "><subfield code="a">58.34</subfield><subfield code="2">bkl</subfield></datafield><datafield tag="084" ind1=" " ind2=" "><subfield code="a">42.63</subfield><subfield code="2">bkl</subfield></datafield><datafield tag="100" ind1="1" ind2=" "><subfield code="a">Li, Minghui</subfield><subfield code="e">verfasserin</subfield><subfield code="4">aut</subfield></datafield><datafield tag="245" ind1="1" ind2="0"><subfield code="a">Determination and dissipation of fipronil and its metabolites in peanut and soil</subfield></datafield><datafield tag="264" ind1=" " ind2="1"><subfield code="c">2015</subfield></datafield><datafield tag="336" ind1=" " ind2=" "><subfield code="a">Text</subfield><subfield code="b">txt</subfield><subfield code="2">rdacontent</subfield></datafield><datafield tag="337" ind1=" " ind2=" "><subfield code="a">ohne Hilfsmittel zu benutzen</subfield><subfield code="b">n</subfield><subfield code="2">rdamedia</subfield></datafield><datafield tag="338" ind1=" " ind2=" "><subfield code="a">Band</subfield><subfield code="b">nc</subfield><subfield code="2">rdacarrier</subfield></datafield><datafield tag="520" ind1=" " ind2=" "><subfield code="a">In this study, a modified quick, easy, cheap, effective, rugged, and safe (QuEChERS) method was established for the extraction and cleanup of fipronil and its three metabolites (fipronil solfone, sulfide, and desulfinyl) in peanut kernel, shell, straw, seedling, and soil samples, and liquid chromatography-tandem mass spectrometry (LC-MS/MS) was used for analysis. The average recoveries were 66-116% at the level of 0.001-0.1 mg/kg with the RSD <19%, and the limit of detection was 0.3 ng/g for all matrices. The dissipation experiment results demonstrated that fipronil dissipated more rapidly in peanut seedling than in soil, with half-lives of <1 day in peanut seedling and 32-57 days in soil depending on the soil pH. The final residues at harvest of peanut kernels were all below 0.02 mg/kg, whereas in peanut shell and straw, the total highest residues were 0.99 and 0.30 mg/kg, respectively. Fipronil-desulfinyl and fipronil-sulfone were the highest residue metabolites in peanut plant (seedling and straw) and soil samples, respectively.</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Pyrazoles - metabolism</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Arachis hypogaea - chemistry</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Pyrazoles - chemistry</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Insecticides - isolation & purification</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Pyrazoles - isolation & purification</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Soil Pollutants - chemistry</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Soil Pollutants - metabolism</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Tandem Mass Spectrometry - methods</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Pesticide Residues - metabolism</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Insecticides - metabolism</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Pesticide Residues - chemistry</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Pesticide Residues - isolation & purification</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Insecticides - chemistry</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Chromatography, High Pressure Liquid - methods</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Arachis hypogaea - metabolism</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Li, Puyu</subfield><subfield code="4">oth</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Wang, Lin</subfield><subfield code="4">oth</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Feng, Mengyuan</subfield><subfield code="4">oth</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Han, Lijun</subfield><subfield code="4">oth</subfield></datafield><datafield tag="773" ind1="0" ind2="8"><subfield code="i">Enthalten in</subfield><subfield code="t">Journal of agricultural and food chemistry</subfield><subfield code="d">Columbus, Ohio : American Chemical Soc., 1953</subfield><subfield code="g">63(2015), 18, Seite 4435</subfield><subfield code="w">(DE-627)129602795</subfield><subfield code="w">(DE-600)241619-0</subfield><subfield code="w">(DE-576)015096610</subfield><subfield code="x">0021-8561</subfield><subfield code="7">nnns</subfield></datafield><datafield tag="773" ind1="1" ind2="8"><subfield code="g">volume:63</subfield><subfield code="g">year:2015</subfield><subfield code="g">number:18</subfield><subfield code="g">pages:4435</subfield></datafield><datafield tag="856" ind1="4" ind2="2"><subfield code="u">http://www.ncbi.nlm.nih.gov/pubmed/25664639</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_USEFLAG_A</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">SYSFLAG_A</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_OLC</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">SSG-OLC-TEC</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">SSG-OLC-CHE</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">SSG-OLC-PHA</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">SSG-OLC-DE-84</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">SSG-OPC-FOR</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_70</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2006</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4219</subfield></datafield><datafield tag="936" ind1="b" ind2="k"><subfield code="a">58.27</subfield><subfield code="q">AVZ</subfield></datafield><datafield tag="936" ind1="b" ind2="k"><subfield code="a">58.34</subfield><subfield code="q">AVZ</subfield></datafield><datafield tag="936" ind1="b" ind2="k"><subfield code="a">42.63</subfield><subfield code="q">AVZ</subfield></datafield><datafield tag="951" ind1=" " ind2=" "><subfield code="a">AR</subfield></datafield><datafield tag="952" ind1=" " ind2=" "><subfield code="d">63</subfield><subfield code="j">2015</subfield><subfield code="e">18</subfield><subfield code="h">4435</subfield></datafield></record></collection>
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