Confocal micro‐XRF analysis of light elements with Rh X‐ray tube and its application for painted steel sheet
A confocal micro‐X‐ray fluorescence (XRF) instrument with a vacuum chamber was applied for analysis of light elements for painted steel sheet. Because this instrument is equipped with a Rh‐anode X‐ray tube, light elements are excited more effectively by the Rh‐L lines. However, it was difficult to a...
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| Autor*in: |
Yagi, Ryota [verfasserIn] |
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| Format: |
Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2015 |
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| Rechteinformationen: |
Nutzungsrecht: Copyright © 2015 John Wiley & Sons, Ltd. |
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| Schlagwörter: |
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| Übergeordnetes Werk: |
Enthalten in: X-ray spectrometry - Chichester, [u.a.] : Wiley, 1972, 44(2015), 3, Seite 186-189 |
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| Übergeordnetes Werk: |
volume:44 ; year:2015 ; number:3 ; pages:186-189 |
| Links: |
|---|
| DOI / URN: |
10.1002/xrs.2599 |
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OLC1963849280 |
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| 520 | |a A confocal micro‐X‐ray fluorescence (XRF) instrument with a vacuum chamber was applied for analysis of light elements for painted steel sheet. Because this instrument is equipped with a Rh‐anode X‐ray tube, light elements are excited more effectively by the Rh‐L lines. However, it was difficult to analyze Cl, because the energies of the Cl‐K lines are close to those of the Rh‐L lines. Thus, we applied an Al thin film as a primary X‐ray filter to eliminate the Rh‐L lines and confirmed the feasibility of Cl analysis using a Rh X‐ray tube. Rh‐L scattered X‐rays were observed by using an acrylic plate as a sample. The Rh‐L scattered X‐rays were completely absorbed by a 24 µm thick Al filter. A calibration curve of Cl was prepared by using certified reference materials with different Cl concentrations. The limit of detection for Cl was 11.9 ppm as estimated from the calibration curve. Confocal micro‐XRF with a Rh X‐ray tube enables the analysis of low Z elements including Cl by applying an Al filter. This technique was applied for a practical painted steel sheet sample. The elemental image of Cl was successfully observed after corrosion in NaCl solution as well as other light elemental maps. Copyright © 2015 John Wiley & Sons, Ltd. | ||
| 540 | |a Nutzungsrecht: Copyright © 2015 John Wiley & Sons, Ltd. | ||
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| 650 | 4 | |a confocal micro‐XRF | |
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10.1002/xrs.2599 doi PQ20160617 (DE-627)OLC1963849280 (DE-599)GBVOLC1963849280 (PRQ)p1864-a8ae9e92c5ff10d1eaa8d45ba84dca34b944bbb0fc9e2f95cf62cd53cc6b7e4a3 (KEY)0022066320150000044000300186confocalmicroxrfanalysisoflightelementswithrhxrayt DE-627 ger DE-627 rakwb eng 530 DNB 35.25 bkl 33.07 bkl Yagi, Ryota verfasserin aut Confocal micro‐XRF analysis of light elements with Rh X‐ray tube and its application for painted steel sheet 2015 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier A confocal micro‐X‐ray fluorescence (XRF) instrument with a vacuum chamber was applied for analysis of light elements for painted steel sheet. Because this instrument is equipped with a Rh‐anode X‐ray tube, light elements are excited more effectively by the Rh‐L lines. However, it was difficult to analyze Cl, because the energies of the Cl‐K lines are close to those of the Rh‐L lines. Thus, we applied an Al thin film as a primary X‐ray filter to eliminate the Rh‐L lines and confirmed the feasibility of Cl analysis using a Rh X‐ray tube. Rh‐L scattered X‐rays were observed by using an acrylic plate as a sample. The Rh‐L scattered X‐rays were completely absorbed by a 24 µm thick Al filter. A calibration curve of Cl was prepared by using certified reference materials with different Cl concentrations. The limit of detection for Cl was 11.9 ppm as estimated from the calibration curve. Confocal micro‐XRF with a Rh X‐ray tube enables the analysis of low Z elements including Cl by applying an Al filter. This technique was applied for a practical painted steel sheet sample. The elemental image of Cl was successfully observed after corrosion in NaCl solution as well as other light elemental maps. Copyright © 2015 John Wiley & Sons, Ltd. Nutzungsrecht: Copyright © 2015 John Wiley & Sons, Ltd. polycapillary optics confocal micro‐XRF detection of Cl X‐ray filter Tsuji, Kouichi oth Enthalten in X-ray spectrometry Chichester, [u.a.] : Wiley, 1972 44(2015), 3, Seite 186-189 (DE-627)129290041 (DE-600)120288-1 (DE-576)014471418 0049-8246 nnns volume:44 year:2015 number:3 pages:186-189 http://dx.doi.org/10.1002/xrs.2599 Volltext http://onlinelibrary.wiley.com/doi/10.1002/xrs.2599/abstract http://search.proquest.com/docview/1672997886 GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-PHY SSG-OLC-CHE SSG-OLC-PHA SSG-OLC-DE-84 GBV_ILN_70 GBV_ILN_2279 35.25 AVZ 33.07 AVZ AR 44 2015 3 186-189 |
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10.1002/xrs.2599 doi PQ20160617 (DE-627)OLC1963849280 (DE-599)GBVOLC1963849280 (PRQ)p1864-a8ae9e92c5ff10d1eaa8d45ba84dca34b944bbb0fc9e2f95cf62cd53cc6b7e4a3 (KEY)0022066320150000044000300186confocalmicroxrfanalysisoflightelementswithrhxrayt DE-627 ger DE-627 rakwb eng 530 DNB 35.25 bkl 33.07 bkl Yagi, Ryota verfasserin aut Confocal micro‐XRF analysis of light elements with Rh X‐ray tube and its application for painted steel sheet 2015 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier A confocal micro‐X‐ray fluorescence (XRF) instrument with a vacuum chamber was applied for analysis of light elements for painted steel sheet. Because this instrument is equipped with a Rh‐anode X‐ray tube, light elements are excited more effectively by the Rh‐L lines. However, it was difficult to analyze Cl, because the energies of the Cl‐K lines are close to those of the Rh‐L lines. Thus, we applied an Al thin film as a primary X‐ray filter to eliminate the Rh‐L lines and confirmed the feasibility of Cl analysis using a Rh X‐ray tube. Rh‐L scattered X‐rays were observed by using an acrylic plate as a sample. The Rh‐L scattered X‐rays were completely absorbed by a 24 µm thick Al filter. A calibration curve of Cl was prepared by using certified reference materials with different Cl concentrations. The limit of detection for Cl was 11.9 ppm as estimated from the calibration curve. Confocal micro‐XRF with a Rh X‐ray tube enables the analysis of low Z elements including Cl by applying an Al filter. This technique was applied for a practical painted steel sheet sample. The elemental image of Cl was successfully observed after corrosion in NaCl solution as well as other light elemental maps. Copyright © 2015 John Wiley & Sons, Ltd. Nutzungsrecht: Copyright © 2015 John Wiley & Sons, Ltd. polycapillary optics confocal micro‐XRF detection of Cl X‐ray filter Tsuji, Kouichi oth Enthalten in X-ray spectrometry Chichester, [u.a.] : Wiley, 1972 44(2015), 3, Seite 186-189 (DE-627)129290041 (DE-600)120288-1 (DE-576)014471418 0049-8246 nnns volume:44 year:2015 number:3 pages:186-189 http://dx.doi.org/10.1002/xrs.2599 Volltext http://onlinelibrary.wiley.com/doi/10.1002/xrs.2599/abstract http://search.proquest.com/docview/1672997886 GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-PHY SSG-OLC-CHE SSG-OLC-PHA SSG-OLC-DE-84 GBV_ILN_70 GBV_ILN_2279 35.25 AVZ 33.07 AVZ AR 44 2015 3 186-189 |
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10.1002/xrs.2599 doi PQ20160617 (DE-627)OLC1963849280 (DE-599)GBVOLC1963849280 (PRQ)p1864-a8ae9e92c5ff10d1eaa8d45ba84dca34b944bbb0fc9e2f95cf62cd53cc6b7e4a3 (KEY)0022066320150000044000300186confocalmicroxrfanalysisoflightelementswithrhxrayt DE-627 ger DE-627 rakwb eng 530 DNB 35.25 bkl 33.07 bkl Yagi, Ryota verfasserin aut Confocal micro‐XRF analysis of light elements with Rh X‐ray tube and its application for painted steel sheet 2015 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier A confocal micro‐X‐ray fluorescence (XRF) instrument with a vacuum chamber was applied for analysis of light elements for painted steel sheet. Because this instrument is equipped with a Rh‐anode X‐ray tube, light elements are excited more effectively by the Rh‐L lines. However, it was difficult to analyze Cl, because the energies of the Cl‐K lines are close to those of the Rh‐L lines. Thus, we applied an Al thin film as a primary X‐ray filter to eliminate the Rh‐L lines and confirmed the feasibility of Cl analysis using a Rh X‐ray tube. Rh‐L scattered X‐rays were observed by using an acrylic plate as a sample. The Rh‐L scattered X‐rays were completely absorbed by a 24 µm thick Al filter. A calibration curve of Cl was prepared by using certified reference materials with different Cl concentrations. The limit of detection for Cl was 11.9 ppm as estimated from the calibration curve. Confocal micro‐XRF with a Rh X‐ray tube enables the analysis of low Z elements including Cl by applying an Al filter. This technique was applied for a practical painted steel sheet sample. The elemental image of Cl was successfully observed after corrosion in NaCl solution as well as other light elemental maps. Copyright © 2015 John Wiley & Sons, Ltd. Nutzungsrecht: Copyright © 2015 John Wiley & Sons, Ltd. polycapillary optics confocal micro‐XRF detection of Cl X‐ray filter Tsuji, Kouichi oth Enthalten in X-ray spectrometry Chichester, [u.a.] : Wiley, 1972 44(2015), 3, Seite 186-189 (DE-627)129290041 (DE-600)120288-1 (DE-576)014471418 0049-8246 nnns volume:44 year:2015 number:3 pages:186-189 http://dx.doi.org/10.1002/xrs.2599 Volltext http://onlinelibrary.wiley.com/doi/10.1002/xrs.2599/abstract http://search.proquest.com/docview/1672997886 GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-PHY SSG-OLC-CHE SSG-OLC-PHA SSG-OLC-DE-84 GBV_ILN_70 GBV_ILN_2279 35.25 AVZ 33.07 AVZ AR 44 2015 3 186-189 |
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10.1002/xrs.2599 doi PQ20160617 (DE-627)OLC1963849280 (DE-599)GBVOLC1963849280 (PRQ)p1864-a8ae9e92c5ff10d1eaa8d45ba84dca34b944bbb0fc9e2f95cf62cd53cc6b7e4a3 (KEY)0022066320150000044000300186confocalmicroxrfanalysisoflightelementswithrhxrayt DE-627 ger DE-627 rakwb eng 530 DNB 35.25 bkl 33.07 bkl Yagi, Ryota verfasserin aut Confocal micro‐XRF analysis of light elements with Rh X‐ray tube and its application for painted steel sheet 2015 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier A confocal micro‐X‐ray fluorescence (XRF) instrument with a vacuum chamber was applied for analysis of light elements for painted steel sheet. Because this instrument is equipped with a Rh‐anode X‐ray tube, light elements are excited more effectively by the Rh‐L lines. However, it was difficult to analyze Cl, because the energies of the Cl‐K lines are close to those of the Rh‐L lines. Thus, we applied an Al thin film as a primary X‐ray filter to eliminate the Rh‐L lines and confirmed the feasibility of Cl analysis using a Rh X‐ray tube. Rh‐L scattered X‐rays were observed by using an acrylic plate as a sample. The Rh‐L scattered X‐rays were completely absorbed by a 24 µm thick Al filter. A calibration curve of Cl was prepared by using certified reference materials with different Cl concentrations. The limit of detection for Cl was 11.9 ppm as estimated from the calibration curve. Confocal micro‐XRF with a Rh X‐ray tube enables the analysis of low Z elements including Cl by applying an Al filter. This technique was applied for a practical painted steel sheet sample. The elemental image of Cl was successfully observed after corrosion in NaCl solution as well as other light elemental maps. Copyright © 2015 John Wiley & Sons, Ltd. Nutzungsrecht: Copyright © 2015 John Wiley & Sons, Ltd. polycapillary optics confocal micro‐XRF detection of Cl X‐ray filter Tsuji, Kouichi oth Enthalten in X-ray spectrometry Chichester, [u.a.] : Wiley, 1972 44(2015), 3, Seite 186-189 (DE-627)129290041 (DE-600)120288-1 (DE-576)014471418 0049-8246 nnns volume:44 year:2015 number:3 pages:186-189 http://dx.doi.org/10.1002/xrs.2599 Volltext http://onlinelibrary.wiley.com/doi/10.1002/xrs.2599/abstract http://search.proquest.com/docview/1672997886 GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-PHY SSG-OLC-CHE SSG-OLC-PHA SSG-OLC-DE-84 GBV_ILN_70 GBV_ILN_2279 35.25 AVZ 33.07 AVZ AR 44 2015 3 186-189 |
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10.1002/xrs.2599 doi PQ20160617 (DE-627)OLC1963849280 (DE-599)GBVOLC1963849280 (PRQ)p1864-a8ae9e92c5ff10d1eaa8d45ba84dca34b944bbb0fc9e2f95cf62cd53cc6b7e4a3 (KEY)0022066320150000044000300186confocalmicroxrfanalysisoflightelementswithrhxrayt DE-627 ger DE-627 rakwb eng 530 DNB 35.25 bkl 33.07 bkl Yagi, Ryota verfasserin aut Confocal micro‐XRF analysis of light elements with Rh X‐ray tube and its application for painted steel sheet 2015 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier A confocal micro‐X‐ray fluorescence (XRF) instrument with a vacuum chamber was applied for analysis of light elements for painted steel sheet. Because this instrument is equipped with a Rh‐anode X‐ray tube, light elements are excited more effectively by the Rh‐L lines. However, it was difficult to analyze Cl, because the energies of the Cl‐K lines are close to those of the Rh‐L lines. Thus, we applied an Al thin film as a primary X‐ray filter to eliminate the Rh‐L lines and confirmed the feasibility of Cl analysis using a Rh X‐ray tube. Rh‐L scattered X‐rays were observed by using an acrylic plate as a sample. The Rh‐L scattered X‐rays were completely absorbed by a 24 µm thick Al filter. A calibration curve of Cl was prepared by using certified reference materials with different Cl concentrations. The limit of detection for Cl was 11.9 ppm as estimated from the calibration curve. Confocal micro‐XRF with a Rh X‐ray tube enables the analysis of low Z elements including Cl by applying an Al filter. This technique was applied for a practical painted steel sheet sample. The elemental image of Cl was successfully observed after corrosion in NaCl solution as well as other light elemental maps. Copyright © 2015 John Wiley & Sons, Ltd. Nutzungsrecht: Copyright © 2015 John Wiley & Sons, Ltd. polycapillary optics confocal micro‐XRF detection of Cl X‐ray filter Tsuji, Kouichi oth Enthalten in X-ray spectrometry Chichester, [u.a.] : Wiley, 1972 44(2015), 3, Seite 186-189 (DE-627)129290041 (DE-600)120288-1 (DE-576)014471418 0049-8246 nnns volume:44 year:2015 number:3 pages:186-189 http://dx.doi.org/10.1002/xrs.2599 Volltext http://onlinelibrary.wiley.com/doi/10.1002/xrs.2599/abstract http://search.proquest.com/docview/1672997886 GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-PHY SSG-OLC-CHE SSG-OLC-PHA SSG-OLC-DE-84 GBV_ILN_70 GBV_ILN_2279 35.25 AVZ 33.07 AVZ AR 44 2015 3 186-189 |
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Because this instrument is equipped with a Rh‐anode X‐ray tube, light elements are excited more effectively by the Rh‐L lines. However, it was difficult to analyze Cl, because the energies of the Cl‐K lines are close to those of the Rh‐L lines. Thus, we applied an Al thin film as a primary X‐ray filter to eliminate the Rh‐L lines and confirmed the feasibility of Cl analysis using a Rh X‐ray tube. Rh‐L scattered X‐rays were observed by using an acrylic plate as a sample. The Rh‐L scattered X‐rays were completely absorbed by a 24 µm thick Al filter. A calibration curve of Cl was prepared by using certified reference materials with different Cl concentrations. The limit of detection for Cl was 11.9 ppm as estimated from the calibration curve. Confocal micro‐XRF with a Rh X‐ray tube enables the analysis of low Z elements including Cl by applying an Al filter. This technique was applied for a practical painted steel sheet sample. The elemental image of Cl was successfully observed after corrosion in NaCl solution as well as other light elemental maps. 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confocal micro‐xrf analysis of light elements with rh x‐ray tube and its application for painted steel sheet |
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Confocal micro‐XRF analysis of light elements with Rh X‐ray tube and its application for painted steel sheet |
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A confocal micro‐X‐ray fluorescence (XRF) instrument with a vacuum chamber was applied for analysis of light elements for painted steel sheet. Because this instrument is equipped with a Rh‐anode X‐ray tube, light elements are excited more effectively by the Rh‐L lines. However, it was difficult to analyze Cl, because the energies of the Cl‐K lines are close to those of the Rh‐L lines. Thus, we applied an Al thin film as a primary X‐ray filter to eliminate the Rh‐L lines and confirmed the feasibility of Cl analysis using a Rh X‐ray tube. Rh‐L scattered X‐rays were observed by using an acrylic plate as a sample. The Rh‐L scattered X‐rays were completely absorbed by a 24 µm thick Al filter. A calibration curve of Cl was prepared by using certified reference materials with different Cl concentrations. The limit of detection for Cl was 11.9 ppm as estimated from the calibration curve. Confocal micro‐XRF with a Rh X‐ray tube enables the analysis of low Z elements including Cl by applying an Al filter. This technique was applied for a practical painted steel sheet sample. The elemental image of Cl was successfully observed after corrosion in NaCl solution as well as other light elemental maps. Copyright © 2015 John Wiley & Sons, Ltd. |
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A confocal micro‐X‐ray fluorescence (XRF) instrument with a vacuum chamber was applied for analysis of light elements for painted steel sheet. Because this instrument is equipped with a Rh‐anode X‐ray tube, light elements are excited more effectively by the Rh‐L lines. However, it was difficult to analyze Cl, because the energies of the Cl‐K lines are close to those of the Rh‐L lines. Thus, we applied an Al thin film as a primary X‐ray filter to eliminate the Rh‐L lines and confirmed the feasibility of Cl analysis using a Rh X‐ray tube. Rh‐L scattered X‐rays were observed by using an acrylic plate as a sample. The Rh‐L scattered X‐rays were completely absorbed by a 24 µm thick Al filter. A calibration curve of Cl was prepared by using certified reference materials with different Cl concentrations. The limit of detection for Cl was 11.9 ppm as estimated from the calibration curve. Confocal micro‐XRF with a Rh X‐ray tube enables the analysis of low Z elements including Cl by applying an Al filter. This technique was applied for a practical painted steel sheet sample. The elemental image of Cl was successfully observed after corrosion in NaCl solution as well as other light elemental maps. Copyright © 2015 John Wiley & Sons, Ltd. |
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A confocal micro‐X‐ray fluorescence (XRF) instrument with a vacuum chamber was applied for analysis of light elements for painted steel sheet. Because this instrument is equipped with a Rh‐anode X‐ray tube, light elements are excited more effectively by the Rh‐L lines. However, it was difficult to analyze Cl, because the energies of the Cl‐K lines are close to those of the Rh‐L lines. Thus, we applied an Al thin film as a primary X‐ray filter to eliminate the Rh‐L lines and confirmed the feasibility of Cl analysis using a Rh X‐ray tube. Rh‐L scattered X‐rays were observed by using an acrylic plate as a sample. The Rh‐L scattered X‐rays were completely absorbed by a 24 µm thick Al filter. A calibration curve of Cl was prepared by using certified reference materials with different Cl concentrations. The limit of detection for Cl was 11.9 ppm as estimated from the calibration curve. Confocal micro‐XRF with a Rh X‐ray tube enables the analysis of low Z elements including Cl by applying an Al filter. This technique was applied for a practical painted steel sheet sample. The elemental image of Cl was successfully observed after corrosion in NaCl solution as well as other light elemental maps. Copyright © 2015 John Wiley & Sons, Ltd. |
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Confocal micro‐XRF analysis of light elements with Rh X‐ray tube and its application for painted steel sheet |
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