Determination of acrylamide in Sudanese food by high performance liquid chromatography coupled with LTQ Orbitrap mass spectrometry
A sample preparation method based on modified Quick, Easy, Cheap Effective, Rugged and Safe (QuEChERS) with aluminum oxide (Al2O3) as dispersive solid phase extraction (dSPE) material and high performance liquid chromatography-linear trap quadruple-Orbitrap-mass spectrometry (HPLC LTQ-Orbitrap MS) w...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Elbashir, Abdalla Ahmed [verfasserIn] |
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| Format: |
Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2015 |
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| Rechteinformationen: |
Nutzungsrecht: Copyright © 2014 Elsevier Ltd. All rights reserved. |
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| Schlagwörter: |
Chromatography, High Pressure Liquid - methods |
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| Übergeordnetes Werk: |
Enthalten in: Food chemistry - Amsterdam [u.a.] : Elsevier, 1976, 176(2015), Seite 342-349 |
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| Übergeordnetes Werk: |
volume:176 ; year:2015 ; pages:342-349 |
| Links: |
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| DOI / URN: |
10.1016/j.foodchem.2014.12.091 |
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| 520 | |a A sample preparation method based on modified Quick, Easy, Cheap Effective, Rugged and Safe (QuEChERS) with aluminum oxide (Al2O3) as dispersive solid phase extraction (dSPE) material and high performance liquid chromatography-linear trap quadruple-Orbitrap-mass spectrometry (HPLC LTQ-Orbitrap MS) was established. The performance of two analytical columns namely Kinetex C18 and Rezex ROA-organic acid was compared for acrylamide separation. The method was validated in term of matrix effect, linear range (standard addition method), limit of detection (LOD), limit of quantification (LOQ), precision (RSD%) and recovery. Good linearity (r(2)>0.9979) was achieved using standard addition method in the concentration range 0-200μgkg(-1). The LOD is in the range from 2.91 to 4.04μgkg(-1) and 1.50 to 3.94μgkg(-1) for C18 and ROA columns, respectively. The precision of the method was ⩽7.3% and 5.6% for C18 and ROA columns, respectively. Recoveries of acrylamide ranging from 90% to 97%, (n=3) were obtained. The proposed Al2O3 dSPE method was successfully applied to the analysis of acrylamide in real food samples. | ||
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10.1016/j.foodchem.2014.12.091 doi PQ20160211 (DE-627)OLC1969365803 (DE-599)GBVOLC1969365803 (PRQ)c1305-b3ccc1852991c1e5c2e7da08fcfca78a1adbf181c044f77ca2b3d4d424f32f940 (KEY)0039580320150000176000000342determinationofacrylamideinsudanesefoodbyhighperfo DE-627 ger DE-627 rakwb eng 540 660 DNB 58.34 bkl 58.00 bkl Elbashir, Abdalla Ahmed verfasserin aut Determination of acrylamide in Sudanese food by high performance liquid chromatography coupled with LTQ Orbitrap mass spectrometry 2015 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier A sample preparation method based on modified Quick, Easy, Cheap Effective, Rugged and Safe (QuEChERS) with aluminum oxide (Al2O3) as dispersive solid phase extraction (dSPE) material and high performance liquid chromatography-linear trap quadruple-Orbitrap-mass spectrometry (HPLC LTQ-Orbitrap MS) was established. The performance of two analytical columns namely Kinetex C18 and Rezex ROA-organic acid was compared for acrylamide separation. The method was validated in term of matrix effect, linear range (standard addition method), limit of detection (LOD), limit of quantification (LOQ), precision (RSD%) and recovery. Good linearity (r(2)>0.9979) was achieved using standard addition method in the concentration range 0-200μgkg(-1). The LOD is in the range from 2.91 to 4.04μgkg(-1) and 1.50 to 3.94μgkg(-1) for C18 and ROA columns, respectively. The precision of the method was ⩽7.3% and 5.6% for C18 and ROA columns, respectively. Recoveries of acrylamide ranging from 90% to 97%, (n=3) were obtained. The proposed Al2O3 dSPE method was successfully applied to the analysis of acrylamide in real food samples. Nutzungsrecht: Copyright © 2014 Elsevier Ltd. All rights reserved. Acrylamide - analysis Chromatography, High Pressure Liquid - methods Acrylamide - chemistry Solid Phase Extraction - methods Mass Spectrometry - methods Omar, Mei Musa Ali oth Schmitz, Oliver J oth Enthalten in Food chemistry Amsterdam [u.a.] : Elsevier, 1976 176(2015), Seite 342-349 (DE-627)129611751 (DE-600)243123-3 (DE-576)015107418 0308-8146 nnns volume:176 year:2015 pages:342-349 http://dx.doi.org/10.1016/j.foodchem.2014.12.091 Volltext http://www.ncbi.nlm.nih.gov/pubmed/25624242 GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE GBV_ILN_70 GBV_ILN_4012 GBV_ILN_4219 58.34 AVZ 58.00 AVZ AR 176 2015 342-349 |
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10.1016/j.foodchem.2014.12.091 doi PQ20160211 (DE-627)OLC1969365803 (DE-599)GBVOLC1969365803 (PRQ)c1305-b3ccc1852991c1e5c2e7da08fcfca78a1adbf181c044f77ca2b3d4d424f32f940 (KEY)0039580320150000176000000342determinationofacrylamideinsudanesefoodbyhighperfo DE-627 ger DE-627 rakwb eng 540 660 DNB 58.34 bkl 58.00 bkl Elbashir, Abdalla Ahmed verfasserin aut Determination of acrylamide in Sudanese food by high performance liquid chromatography coupled with LTQ Orbitrap mass spectrometry 2015 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier A sample preparation method based on modified Quick, Easy, Cheap Effective, Rugged and Safe (QuEChERS) with aluminum oxide (Al2O3) as dispersive solid phase extraction (dSPE) material and high performance liquid chromatography-linear trap quadruple-Orbitrap-mass spectrometry (HPLC LTQ-Orbitrap MS) was established. The performance of two analytical columns namely Kinetex C18 and Rezex ROA-organic acid was compared for acrylamide separation. The method was validated in term of matrix effect, linear range (standard addition method), limit of detection (LOD), limit of quantification (LOQ), precision (RSD%) and recovery. Good linearity (r(2)>0.9979) was achieved using standard addition method in the concentration range 0-200μgkg(-1). The LOD is in the range from 2.91 to 4.04μgkg(-1) and 1.50 to 3.94μgkg(-1) for C18 and ROA columns, respectively. The precision of the method was ⩽7.3% and 5.6% for C18 and ROA columns, respectively. Recoveries of acrylamide ranging from 90% to 97%, (n=3) were obtained. The proposed Al2O3 dSPE method was successfully applied to the analysis of acrylamide in real food samples. Nutzungsrecht: Copyright © 2014 Elsevier Ltd. All rights reserved. Acrylamide - analysis Chromatography, High Pressure Liquid - methods Acrylamide - chemistry Solid Phase Extraction - methods Mass Spectrometry - methods Omar, Mei Musa Ali oth Schmitz, Oliver J oth Enthalten in Food chemistry Amsterdam [u.a.] : Elsevier, 1976 176(2015), Seite 342-349 (DE-627)129611751 (DE-600)243123-3 (DE-576)015107418 0308-8146 nnns volume:176 year:2015 pages:342-349 http://dx.doi.org/10.1016/j.foodchem.2014.12.091 Volltext http://www.ncbi.nlm.nih.gov/pubmed/25624242 GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE GBV_ILN_70 GBV_ILN_4012 GBV_ILN_4219 58.34 AVZ 58.00 AVZ AR 176 2015 342-349 |
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10.1016/j.foodchem.2014.12.091 doi PQ20160211 (DE-627)OLC1969365803 (DE-599)GBVOLC1969365803 (PRQ)c1305-b3ccc1852991c1e5c2e7da08fcfca78a1adbf181c044f77ca2b3d4d424f32f940 (KEY)0039580320150000176000000342determinationofacrylamideinsudanesefoodbyhighperfo DE-627 ger DE-627 rakwb eng 540 660 DNB 58.34 bkl 58.00 bkl Elbashir, Abdalla Ahmed verfasserin aut Determination of acrylamide in Sudanese food by high performance liquid chromatography coupled with LTQ Orbitrap mass spectrometry 2015 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier A sample preparation method based on modified Quick, Easy, Cheap Effective, Rugged and Safe (QuEChERS) with aluminum oxide (Al2O3) as dispersive solid phase extraction (dSPE) material and high performance liquid chromatography-linear trap quadruple-Orbitrap-mass spectrometry (HPLC LTQ-Orbitrap MS) was established. The performance of two analytical columns namely Kinetex C18 and Rezex ROA-organic acid was compared for acrylamide separation. The method was validated in term of matrix effect, linear range (standard addition method), limit of detection (LOD), limit of quantification (LOQ), precision (RSD%) and recovery. Good linearity (r(2)>0.9979) was achieved using standard addition method in the concentration range 0-200μgkg(-1). The LOD is in the range from 2.91 to 4.04μgkg(-1) and 1.50 to 3.94μgkg(-1) for C18 and ROA columns, respectively. The precision of the method was ⩽7.3% and 5.6% for C18 and ROA columns, respectively. Recoveries of acrylamide ranging from 90% to 97%, (n=3) were obtained. The proposed Al2O3 dSPE method was successfully applied to the analysis of acrylamide in real food samples. Nutzungsrecht: Copyright © 2014 Elsevier Ltd. All rights reserved. Acrylamide - analysis Chromatography, High Pressure Liquid - methods Acrylamide - chemistry Solid Phase Extraction - methods Mass Spectrometry - methods Omar, Mei Musa Ali oth Schmitz, Oliver J oth Enthalten in Food chemistry Amsterdam [u.a.] : Elsevier, 1976 176(2015), Seite 342-349 (DE-627)129611751 (DE-600)243123-3 (DE-576)015107418 0308-8146 nnns volume:176 year:2015 pages:342-349 http://dx.doi.org/10.1016/j.foodchem.2014.12.091 Volltext http://www.ncbi.nlm.nih.gov/pubmed/25624242 GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE GBV_ILN_70 GBV_ILN_4012 GBV_ILN_4219 58.34 AVZ 58.00 AVZ AR 176 2015 342-349 |
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10.1016/j.foodchem.2014.12.091 doi PQ20160211 (DE-627)OLC1969365803 (DE-599)GBVOLC1969365803 (PRQ)c1305-b3ccc1852991c1e5c2e7da08fcfca78a1adbf181c044f77ca2b3d4d424f32f940 (KEY)0039580320150000176000000342determinationofacrylamideinsudanesefoodbyhighperfo DE-627 ger DE-627 rakwb eng 540 660 DNB 58.34 bkl 58.00 bkl Elbashir, Abdalla Ahmed verfasserin aut Determination of acrylamide in Sudanese food by high performance liquid chromatography coupled with LTQ Orbitrap mass spectrometry 2015 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier A sample preparation method based on modified Quick, Easy, Cheap Effective, Rugged and Safe (QuEChERS) with aluminum oxide (Al2O3) as dispersive solid phase extraction (dSPE) material and high performance liquid chromatography-linear trap quadruple-Orbitrap-mass spectrometry (HPLC LTQ-Orbitrap MS) was established. The performance of two analytical columns namely Kinetex C18 and Rezex ROA-organic acid was compared for acrylamide separation. The method was validated in term of matrix effect, linear range (standard addition method), limit of detection (LOD), limit of quantification (LOQ), precision (RSD%) and recovery. Good linearity (r(2)>0.9979) was achieved using standard addition method in the concentration range 0-200μgkg(-1). The LOD is in the range from 2.91 to 4.04μgkg(-1) and 1.50 to 3.94μgkg(-1) for C18 and ROA columns, respectively. The precision of the method was ⩽7.3% and 5.6% for C18 and ROA columns, respectively. Recoveries of acrylamide ranging from 90% to 97%, (n=3) were obtained. The proposed Al2O3 dSPE method was successfully applied to the analysis of acrylamide in real food samples. Nutzungsrecht: Copyright © 2014 Elsevier Ltd. All rights reserved. Acrylamide - analysis Chromatography, High Pressure Liquid - methods Acrylamide - chemistry Solid Phase Extraction - methods Mass Spectrometry - methods Omar, Mei Musa Ali oth Schmitz, Oliver J oth Enthalten in Food chemistry Amsterdam [u.a.] : Elsevier, 1976 176(2015), Seite 342-349 (DE-627)129611751 (DE-600)243123-3 (DE-576)015107418 0308-8146 nnns volume:176 year:2015 pages:342-349 http://dx.doi.org/10.1016/j.foodchem.2014.12.091 Volltext http://www.ncbi.nlm.nih.gov/pubmed/25624242 GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE GBV_ILN_70 GBV_ILN_4012 GBV_ILN_4219 58.34 AVZ 58.00 AVZ AR 176 2015 342-349 |
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10.1016/j.foodchem.2014.12.091 doi PQ20160211 (DE-627)OLC1969365803 (DE-599)GBVOLC1969365803 (PRQ)c1305-b3ccc1852991c1e5c2e7da08fcfca78a1adbf181c044f77ca2b3d4d424f32f940 (KEY)0039580320150000176000000342determinationofacrylamideinsudanesefoodbyhighperfo DE-627 ger DE-627 rakwb eng 540 660 DNB 58.34 bkl 58.00 bkl Elbashir, Abdalla Ahmed verfasserin aut Determination of acrylamide in Sudanese food by high performance liquid chromatography coupled with LTQ Orbitrap mass spectrometry 2015 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier A sample preparation method based on modified Quick, Easy, Cheap Effective, Rugged and Safe (QuEChERS) with aluminum oxide (Al2O3) as dispersive solid phase extraction (dSPE) material and high performance liquid chromatography-linear trap quadruple-Orbitrap-mass spectrometry (HPLC LTQ-Orbitrap MS) was established. The performance of two analytical columns namely Kinetex C18 and Rezex ROA-organic acid was compared for acrylamide separation. The method was validated in term of matrix effect, linear range (standard addition method), limit of detection (LOD), limit of quantification (LOQ), precision (RSD%) and recovery. Good linearity (r(2)>0.9979) was achieved using standard addition method in the concentration range 0-200μgkg(-1). The LOD is in the range from 2.91 to 4.04μgkg(-1) and 1.50 to 3.94μgkg(-1) for C18 and ROA columns, respectively. The precision of the method was ⩽7.3% and 5.6% for C18 and ROA columns, respectively. Recoveries of acrylamide ranging from 90% to 97%, (n=3) were obtained. The proposed Al2O3 dSPE method was successfully applied to the analysis of acrylamide in real food samples. Nutzungsrecht: Copyright © 2014 Elsevier Ltd. All rights reserved. Acrylamide - analysis Chromatography, High Pressure Liquid - methods Acrylamide - chemistry Solid Phase Extraction - methods Mass Spectrometry - methods Omar, Mei Musa Ali oth Schmitz, Oliver J oth Enthalten in Food chemistry Amsterdam [u.a.] : Elsevier, 1976 176(2015), Seite 342-349 (DE-627)129611751 (DE-600)243123-3 (DE-576)015107418 0308-8146 nnns volume:176 year:2015 pages:342-349 http://dx.doi.org/10.1016/j.foodchem.2014.12.091 Volltext http://www.ncbi.nlm.nih.gov/pubmed/25624242 GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE GBV_ILN_70 GBV_ILN_4012 GBV_ILN_4219 58.34 AVZ 58.00 AVZ AR 176 2015 342-349 |
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540 660 DNB 58.34 bkl 58.00 bkl Determination of acrylamide in Sudanese food by high performance liquid chromatography coupled with LTQ Orbitrap mass spectrometry Acrylamide - analysis Chromatography, High Pressure Liquid - methods Acrylamide - chemistry Solid Phase Extraction - methods Mass Spectrometry - methods |
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Determination of acrylamide in Sudanese food by high performance liquid chromatography coupled with LTQ Orbitrap mass spectrometry |
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determination of acrylamide in sudanese food by high performance liquid chromatography coupled with ltq orbitrap mass spectrometry |
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Determination of acrylamide in Sudanese food by high performance liquid chromatography coupled with LTQ Orbitrap mass spectrometry |
| abstract |
A sample preparation method based on modified Quick, Easy, Cheap Effective, Rugged and Safe (QuEChERS) with aluminum oxide (Al2O3) as dispersive solid phase extraction (dSPE) material and high performance liquid chromatography-linear trap quadruple-Orbitrap-mass spectrometry (HPLC LTQ-Orbitrap MS) was established. The performance of two analytical columns namely Kinetex C18 and Rezex ROA-organic acid was compared for acrylamide separation. The method was validated in term of matrix effect, linear range (standard addition method), limit of detection (LOD), limit of quantification (LOQ), precision (RSD%) and recovery. Good linearity (r(2)>0.9979) was achieved using standard addition method in the concentration range 0-200μgkg(-1). The LOD is in the range from 2.91 to 4.04μgkg(-1) and 1.50 to 3.94μgkg(-1) for C18 and ROA columns, respectively. The precision of the method was ⩽7.3% and 5.6% for C18 and ROA columns, respectively. Recoveries of acrylamide ranging from 90% to 97%, (n=3) were obtained. The proposed Al2O3 dSPE method was successfully applied to the analysis of acrylamide in real food samples. |
| abstractGer |
A sample preparation method based on modified Quick, Easy, Cheap Effective, Rugged and Safe (QuEChERS) with aluminum oxide (Al2O3) as dispersive solid phase extraction (dSPE) material and high performance liquid chromatography-linear trap quadruple-Orbitrap-mass spectrometry (HPLC LTQ-Orbitrap MS) was established. The performance of two analytical columns namely Kinetex C18 and Rezex ROA-organic acid was compared for acrylamide separation. The method was validated in term of matrix effect, linear range (standard addition method), limit of detection (LOD), limit of quantification (LOQ), precision (RSD%) and recovery. Good linearity (r(2)>0.9979) was achieved using standard addition method in the concentration range 0-200μgkg(-1). The LOD is in the range from 2.91 to 4.04μgkg(-1) and 1.50 to 3.94μgkg(-1) for C18 and ROA columns, respectively. The precision of the method was ⩽7.3% and 5.6% for C18 and ROA columns, respectively. Recoveries of acrylamide ranging from 90% to 97%, (n=3) were obtained. The proposed Al2O3 dSPE method was successfully applied to the analysis of acrylamide in real food samples. |
| abstract_unstemmed |
A sample preparation method based on modified Quick, Easy, Cheap Effective, Rugged and Safe (QuEChERS) with aluminum oxide (Al2O3) as dispersive solid phase extraction (dSPE) material and high performance liquid chromatography-linear trap quadruple-Orbitrap-mass spectrometry (HPLC LTQ-Orbitrap MS) was established. The performance of two analytical columns namely Kinetex C18 and Rezex ROA-organic acid was compared for acrylamide separation. The method was validated in term of matrix effect, linear range (standard addition method), limit of detection (LOD), limit of quantification (LOQ), precision (RSD%) and recovery. Good linearity (r(2)>0.9979) was achieved using standard addition method in the concentration range 0-200μgkg(-1). The LOD is in the range from 2.91 to 4.04μgkg(-1) and 1.50 to 3.94μgkg(-1) for C18 and ROA columns, respectively. The precision of the method was ⩽7.3% and 5.6% for C18 and ROA columns, respectively. Recoveries of acrylamide ranging from 90% to 97%, (n=3) were obtained. The proposed Al2O3 dSPE method was successfully applied to the analysis of acrylamide in real food samples. |
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Determination of acrylamide in Sudanese food by high performance liquid chromatography coupled with LTQ Orbitrap mass spectrometry |
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http://dx.doi.org/10.1016/j.foodchem.2014.12.091 http://www.ncbi.nlm.nih.gov/pubmed/25624242 |
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