Determination of avermectins: a QuEChERS approach to the analysis of food samples
We present a simple method for extracting avermectines from meat, based on a QuEChERS approach followed by liquid chromatography (LC) coupled to triple quadrupole (QqQ) tandem mass spectrometry (MS/MS). The compounds considered are ivermectin, abamectin, emamectin, eprinomectin, doramectin and moxid...
Ausführliche Beschreibung
Autor*in: |
Antkowiak, S [verfasserIn] |
---|
Format: |
Artikel |
---|---|
Sprache: |
Englisch |
Erschienen: |
2015 |
---|
Rechteinformationen: |
Nutzungsrecht: Copyright © 2015 Elsevier Ltd. All rights reserved. |
---|
Schlagwörter: |
---|
Übergeordnetes Werk: |
Enthalten in: Food chemistry - Amsterdam [u.a.] : Elsevier, 1976, 181(2015), Seite 57-63 |
---|---|
Übergeordnetes Werk: |
volume:181 ; year:2015 ; pages:57-63 |
Links: |
---|
DOI / URN: |
10.1016/j.foodchem.2015.02.067 |
---|
Katalog-ID: |
OLC1969367377 |
---|
LEADER | 01000caa a2200265 4500 | ||
---|---|---|---|
001 | OLC1969367377 | ||
003 | DE-627 | ||
005 | 20220223002843.0 | ||
007 | tu | ||
008 | 160211s2015 xx ||||| 00| ||eng c | ||
024 | 7 | |a 10.1016/j.foodchem.2015.02.067 |2 doi | |
028 | 5 | 2 | |a PQ20160211 |
035 | |a (DE-627)OLC1969367377 | ||
035 | |a (DE-599)GBVOLC1969367377 | ||
035 | |a (PRQ)c1300-b1a0a6c615a925517cdee4d2b9a689f1f240b9f5855fa82c6d7cf2ab8f9c3e1c0 | ||
035 | |a (KEY)0039580320150000181000000057determinationofavermectinsaquechersapproachtothean | ||
040 | |a DE-627 |b ger |c DE-627 |e rakwb | ||
041 | |a eng | ||
082 | 0 | 4 | |a 540 |a 660 |q DNB |
084 | |a 58.34 |2 bkl | ||
084 | |a 58.00 |2 bkl | ||
100 | 1 | |a Antkowiak, S |e verfasserin |4 aut | |
245 | 1 | 0 | |a Determination of avermectins: a QuEChERS approach to the analysis of food samples |
264 | 1 | |c 2015 | |
336 | |a Text |b txt |2 rdacontent | ||
337 | |a ohne Hilfsmittel zu benutzen |b n |2 rdamedia | ||
338 | |a Band |b nc |2 rdacarrier | ||
520 | |a We present a simple method for extracting avermectines from meat, based on a QuEChERS approach followed by liquid chromatography (LC) coupled to triple quadrupole (QqQ) tandem mass spectrometry (MS/MS). The compounds considered are ivermectin, abamectin, emamectin, eprinomectin, doramectin and moxidectin. The new method has been fully validated according to the requirements of European Decision 657/2002/CE (EU, 2002). The method is suitable for the analysis of avermectins at concentration as low as 2.5 μg kg(-1), and allows high sample throughput. In addition, the detection of avermectins by high resolution mass spectrometry using a quadrupole-Orbritrap (Q-Orbitrap) hybrid instrument has been explored, and the target Selected Ion Monitoring data dependent MS/MS (t-SIM-dd MS/MS) mode has been found to provide excellent performance for residue determination of target analytes. | ||
540 | |a Nutzungsrecht: Copyright © 2015 Elsevier Ltd. All rights reserved. | ||
650 | 4 | |a Ivermectin - chemistry | |
650 | 4 | |a Tandem Mass Spectrometry - methods | |
650 | 4 | |a Ivermectin - analogs & derivatives | |
700 | 1 | |a Granados, M |4 oth | |
700 | 1 | |a Centrich, F |4 oth | |
700 | 1 | |a Rúbies, A |4 oth | |
700 | 1 | |a Companyó, R |4 oth | |
773 | 0 | 8 | |i Enthalten in |t Food chemistry |d Amsterdam [u.a.] : Elsevier, 1976 |g 181(2015), Seite 57-63 |w (DE-627)129611751 |w (DE-600)243123-3 |w (DE-576)015107418 |x 0308-8146 |7 nnns |
773 | 1 | 8 | |g volume:181 |g year:2015 |g pages:57-63 |
856 | 4 | 1 | |u http://dx.doi.org/10.1016/j.foodchem.2015.02.067 |3 Volltext |
856 | 4 | 2 | |u http://www.ncbi.nlm.nih.gov/pubmed/25794721 |
912 | |a GBV_USEFLAG_A | ||
912 | |a SYSFLAG_A | ||
912 | |a GBV_OLC | ||
912 | |a SSG-OLC-TEC | ||
912 | |a SSG-OLC-CHE | ||
912 | |a GBV_ILN_70 | ||
912 | |a GBV_ILN_4012 | ||
912 | |a GBV_ILN_4219 | ||
936 | b | k | |a 58.34 |q AVZ |
936 | b | k | |a 58.00 |q AVZ |
951 | |a AR | ||
952 | |d 181 |j 2015 |h 57-63 |
author_variant |
s a sa |
---|---|
matchkey_str |
article:03088146:2015----::eemntooaemcisqehrapoctten |
hierarchy_sort_str |
2015 |
bklnumber |
58.34 58.00 |
publishDate |
2015 |
allfields |
10.1016/j.foodchem.2015.02.067 doi PQ20160211 (DE-627)OLC1969367377 (DE-599)GBVOLC1969367377 (PRQ)c1300-b1a0a6c615a925517cdee4d2b9a689f1f240b9f5855fa82c6d7cf2ab8f9c3e1c0 (KEY)0039580320150000181000000057determinationofavermectinsaquechersapproachtothean DE-627 ger DE-627 rakwb eng 540 660 DNB 58.34 bkl 58.00 bkl Antkowiak, S verfasserin aut Determination of avermectins: a QuEChERS approach to the analysis of food samples 2015 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier We present a simple method for extracting avermectines from meat, based on a QuEChERS approach followed by liquid chromatography (LC) coupled to triple quadrupole (QqQ) tandem mass spectrometry (MS/MS). The compounds considered are ivermectin, abamectin, emamectin, eprinomectin, doramectin and moxidectin. The new method has been fully validated according to the requirements of European Decision 657/2002/CE (EU, 2002). The method is suitable for the analysis of avermectins at concentration as low as 2.5 μg kg(-1), and allows high sample throughput. In addition, the detection of avermectins by high resolution mass spectrometry using a quadrupole-Orbritrap (Q-Orbitrap) hybrid instrument has been explored, and the target Selected Ion Monitoring data dependent MS/MS (t-SIM-dd MS/MS) mode has been found to provide excellent performance for residue determination of target analytes. Nutzungsrecht: Copyright © 2015 Elsevier Ltd. All rights reserved. Ivermectin - chemistry Tandem Mass Spectrometry - methods Ivermectin - analogs & derivatives Granados, M oth Centrich, F oth Rúbies, A oth Companyó, R oth Enthalten in Food chemistry Amsterdam [u.a.] : Elsevier, 1976 181(2015), Seite 57-63 (DE-627)129611751 (DE-600)243123-3 (DE-576)015107418 0308-8146 nnns volume:181 year:2015 pages:57-63 http://dx.doi.org/10.1016/j.foodchem.2015.02.067 Volltext http://www.ncbi.nlm.nih.gov/pubmed/25794721 GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE GBV_ILN_70 GBV_ILN_4012 GBV_ILN_4219 58.34 AVZ 58.00 AVZ AR 181 2015 57-63 |
spelling |
10.1016/j.foodchem.2015.02.067 doi PQ20160211 (DE-627)OLC1969367377 (DE-599)GBVOLC1969367377 (PRQ)c1300-b1a0a6c615a925517cdee4d2b9a689f1f240b9f5855fa82c6d7cf2ab8f9c3e1c0 (KEY)0039580320150000181000000057determinationofavermectinsaquechersapproachtothean DE-627 ger DE-627 rakwb eng 540 660 DNB 58.34 bkl 58.00 bkl Antkowiak, S verfasserin aut Determination of avermectins: a QuEChERS approach to the analysis of food samples 2015 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier We present a simple method for extracting avermectines from meat, based on a QuEChERS approach followed by liquid chromatography (LC) coupled to triple quadrupole (QqQ) tandem mass spectrometry (MS/MS). The compounds considered are ivermectin, abamectin, emamectin, eprinomectin, doramectin and moxidectin. The new method has been fully validated according to the requirements of European Decision 657/2002/CE (EU, 2002). The method is suitable for the analysis of avermectins at concentration as low as 2.5 μg kg(-1), and allows high sample throughput. In addition, the detection of avermectins by high resolution mass spectrometry using a quadrupole-Orbritrap (Q-Orbitrap) hybrid instrument has been explored, and the target Selected Ion Monitoring data dependent MS/MS (t-SIM-dd MS/MS) mode has been found to provide excellent performance for residue determination of target analytes. Nutzungsrecht: Copyright © 2015 Elsevier Ltd. All rights reserved. Ivermectin - chemistry Tandem Mass Spectrometry - methods Ivermectin - analogs & derivatives Granados, M oth Centrich, F oth Rúbies, A oth Companyó, R oth Enthalten in Food chemistry Amsterdam [u.a.] : Elsevier, 1976 181(2015), Seite 57-63 (DE-627)129611751 (DE-600)243123-3 (DE-576)015107418 0308-8146 nnns volume:181 year:2015 pages:57-63 http://dx.doi.org/10.1016/j.foodchem.2015.02.067 Volltext http://www.ncbi.nlm.nih.gov/pubmed/25794721 GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE GBV_ILN_70 GBV_ILN_4012 GBV_ILN_4219 58.34 AVZ 58.00 AVZ AR 181 2015 57-63 |
allfields_unstemmed |
10.1016/j.foodchem.2015.02.067 doi PQ20160211 (DE-627)OLC1969367377 (DE-599)GBVOLC1969367377 (PRQ)c1300-b1a0a6c615a925517cdee4d2b9a689f1f240b9f5855fa82c6d7cf2ab8f9c3e1c0 (KEY)0039580320150000181000000057determinationofavermectinsaquechersapproachtothean DE-627 ger DE-627 rakwb eng 540 660 DNB 58.34 bkl 58.00 bkl Antkowiak, S verfasserin aut Determination of avermectins: a QuEChERS approach to the analysis of food samples 2015 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier We present a simple method for extracting avermectines from meat, based on a QuEChERS approach followed by liquid chromatography (LC) coupled to triple quadrupole (QqQ) tandem mass spectrometry (MS/MS). The compounds considered are ivermectin, abamectin, emamectin, eprinomectin, doramectin and moxidectin. The new method has been fully validated according to the requirements of European Decision 657/2002/CE (EU, 2002). The method is suitable for the analysis of avermectins at concentration as low as 2.5 μg kg(-1), and allows high sample throughput. In addition, the detection of avermectins by high resolution mass spectrometry using a quadrupole-Orbritrap (Q-Orbitrap) hybrid instrument has been explored, and the target Selected Ion Monitoring data dependent MS/MS (t-SIM-dd MS/MS) mode has been found to provide excellent performance for residue determination of target analytes. Nutzungsrecht: Copyright © 2015 Elsevier Ltd. All rights reserved. Ivermectin - chemistry Tandem Mass Spectrometry - methods Ivermectin - analogs & derivatives Granados, M oth Centrich, F oth Rúbies, A oth Companyó, R oth Enthalten in Food chemistry Amsterdam [u.a.] : Elsevier, 1976 181(2015), Seite 57-63 (DE-627)129611751 (DE-600)243123-3 (DE-576)015107418 0308-8146 nnns volume:181 year:2015 pages:57-63 http://dx.doi.org/10.1016/j.foodchem.2015.02.067 Volltext http://www.ncbi.nlm.nih.gov/pubmed/25794721 GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE GBV_ILN_70 GBV_ILN_4012 GBV_ILN_4219 58.34 AVZ 58.00 AVZ AR 181 2015 57-63 |
allfieldsGer |
10.1016/j.foodchem.2015.02.067 doi PQ20160211 (DE-627)OLC1969367377 (DE-599)GBVOLC1969367377 (PRQ)c1300-b1a0a6c615a925517cdee4d2b9a689f1f240b9f5855fa82c6d7cf2ab8f9c3e1c0 (KEY)0039580320150000181000000057determinationofavermectinsaquechersapproachtothean DE-627 ger DE-627 rakwb eng 540 660 DNB 58.34 bkl 58.00 bkl Antkowiak, S verfasserin aut Determination of avermectins: a QuEChERS approach to the analysis of food samples 2015 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier We present a simple method for extracting avermectines from meat, based on a QuEChERS approach followed by liquid chromatography (LC) coupled to triple quadrupole (QqQ) tandem mass spectrometry (MS/MS). The compounds considered are ivermectin, abamectin, emamectin, eprinomectin, doramectin and moxidectin. The new method has been fully validated according to the requirements of European Decision 657/2002/CE (EU, 2002). The method is suitable for the analysis of avermectins at concentration as low as 2.5 μg kg(-1), and allows high sample throughput. In addition, the detection of avermectins by high resolution mass spectrometry using a quadrupole-Orbritrap (Q-Orbitrap) hybrid instrument has been explored, and the target Selected Ion Monitoring data dependent MS/MS (t-SIM-dd MS/MS) mode has been found to provide excellent performance for residue determination of target analytes. Nutzungsrecht: Copyright © 2015 Elsevier Ltd. All rights reserved. Ivermectin - chemistry Tandem Mass Spectrometry - methods Ivermectin - analogs & derivatives Granados, M oth Centrich, F oth Rúbies, A oth Companyó, R oth Enthalten in Food chemistry Amsterdam [u.a.] : Elsevier, 1976 181(2015), Seite 57-63 (DE-627)129611751 (DE-600)243123-3 (DE-576)015107418 0308-8146 nnns volume:181 year:2015 pages:57-63 http://dx.doi.org/10.1016/j.foodchem.2015.02.067 Volltext http://www.ncbi.nlm.nih.gov/pubmed/25794721 GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE GBV_ILN_70 GBV_ILN_4012 GBV_ILN_4219 58.34 AVZ 58.00 AVZ AR 181 2015 57-63 |
allfieldsSound |
10.1016/j.foodchem.2015.02.067 doi PQ20160211 (DE-627)OLC1969367377 (DE-599)GBVOLC1969367377 (PRQ)c1300-b1a0a6c615a925517cdee4d2b9a689f1f240b9f5855fa82c6d7cf2ab8f9c3e1c0 (KEY)0039580320150000181000000057determinationofavermectinsaquechersapproachtothean DE-627 ger DE-627 rakwb eng 540 660 DNB 58.34 bkl 58.00 bkl Antkowiak, S verfasserin aut Determination of avermectins: a QuEChERS approach to the analysis of food samples 2015 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier We present a simple method for extracting avermectines from meat, based on a QuEChERS approach followed by liquid chromatography (LC) coupled to triple quadrupole (QqQ) tandem mass spectrometry (MS/MS). The compounds considered are ivermectin, abamectin, emamectin, eprinomectin, doramectin and moxidectin. The new method has been fully validated according to the requirements of European Decision 657/2002/CE (EU, 2002). The method is suitable for the analysis of avermectins at concentration as low as 2.5 μg kg(-1), and allows high sample throughput. In addition, the detection of avermectins by high resolution mass spectrometry using a quadrupole-Orbritrap (Q-Orbitrap) hybrid instrument has been explored, and the target Selected Ion Monitoring data dependent MS/MS (t-SIM-dd MS/MS) mode has been found to provide excellent performance for residue determination of target analytes. Nutzungsrecht: Copyright © 2015 Elsevier Ltd. All rights reserved. Ivermectin - chemistry Tandem Mass Spectrometry - methods Ivermectin - analogs & derivatives Granados, M oth Centrich, F oth Rúbies, A oth Companyó, R oth Enthalten in Food chemistry Amsterdam [u.a.] : Elsevier, 1976 181(2015), Seite 57-63 (DE-627)129611751 (DE-600)243123-3 (DE-576)015107418 0308-8146 nnns volume:181 year:2015 pages:57-63 http://dx.doi.org/10.1016/j.foodchem.2015.02.067 Volltext http://www.ncbi.nlm.nih.gov/pubmed/25794721 GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE GBV_ILN_70 GBV_ILN_4012 GBV_ILN_4219 58.34 AVZ 58.00 AVZ AR 181 2015 57-63 |
language |
English |
source |
Enthalten in Food chemistry 181(2015), Seite 57-63 volume:181 year:2015 pages:57-63 |
sourceStr |
Enthalten in Food chemistry 181(2015), Seite 57-63 volume:181 year:2015 pages:57-63 |
format_phy_str_mv |
Article |
institution |
findex.gbv.de |
topic_facet |
Ivermectin - chemistry Tandem Mass Spectrometry - methods Ivermectin - analogs & derivatives |
dewey-raw |
540 |
isfreeaccess_bool |
false |
container_title |
Food chemistry |
authorswithroles_txt_mv |
Antkowiak, S @@aut@@ Granados, M @@oth@@ Centrich, F @@oth@@ Rúbies, A @@oth@@ Companyó, R @@oth@@ |
publishDateDaySort_date |
2015-01-01T00:00:00Z |
hierarchy_top_id |
129611751 |
dewey-sort |
3540 |
id |
OLC1969367377 |
language_de |
englisch |
fullrecord |
<?xml version="1.0" encoding="UTF-8"?><collection xmlns="http://www.loc.gov/MARC21/slim"><record><leader>01000caa a2200265 4500</leader><controlfield tag="001">OLC1969367377</controlfield><controlfield tag="003">DE-627</controlfield><controlfield tag="005">20220223002843.0</controlfield><controlfield tag="007">tu</controlfield><controlfield tag="008">160211s2015 xx ||||| 00| ||eng c</controlfield><datafield tag="024" ind1="7" ind2=" "><subfield code="a">10.1016/j.foodchem.2015.02.067</subfield><subfield code="2">doi</subfield></datafield><datafield tag="028" ind1="5" ind2="2"><subfield code="a">PQ20160211</subfield></datafield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(DE-627)OLC1969367377</subfield></datafield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(DE-599)GBVOLC1969367377</subfield></datafield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(PRQ)c1300-b1a0a6c615a925517cdee4d2b9a689f1f240b9f5855fa82c6d7cf2ab8f9c3e1c0</subfield></datafield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(KEY)0039580320150000181000000057determinationofavermectinsaquechersapproachtothean</subfield></datafield><datafield tag="040" ind1=" " ind2=" "><subfield code="a">DE-627</subfield><subfield code="b">ger</subfield><subfield code="c">DE-627</subfield><subfield code="e">rakwb</subfield></datafield><datafield tag="041" ind1=" " ind2=" "><subfield code="a">eng</subfield></datafield><datafield tag="082" ind1="0" ind2="4"><subfield code="a">540</subfield><subfield code="a">660</subfield><subfield code="q">DNB</subfield></datafield><datafield tag="084" ind1=" " ind2=" "><subfield code="a">58.34</subfield><subfield code="2">bkl</subfield></datafield><datafield tag="084" ind1=" " ind2=" "><subfield code="a">58.00</subfield><subfield code="2">bkl</subfield></datafield><datafield tag="100" ind1="1" ind2=" "><subfield code="a">Antkowiak, S</subfield><subfield code="e">verfasserin</subfield><subfield code="4">aut</subfield></datafield><datafield tag="245" ind1="1" ind2="0"><subfield code="a">Determination of avermectins: a QuEChERS approach to the analysis of food samples</subfield></datafield><datafield tag="264" ind1=" " ind2="1"><subfield code="c">2015</subfield></datafield><datafield tag="336" ind1=" " ind2=" "><subfield code="a">Text</subfield><subfield code="b">txt</subfield><subfield code="2">rdacontent</subfield></datafield><datafield tag="337" ind1=" " ind2=" "><subfield code="a">ohne Hilfsmittel zu benutzen</subfield><subfield code="b">n</subfield><subfield code="2">rdamedia</subfield></datafield><datafield tag="338" ind1=" " ind2=" "><subfield code="a">Band</subfield><subfield code="b">nc</subfield><subfield code="2">rdacarrier</subfield></datafield><datafield tag="520" ind1=" " ind2=" "><subfield code="a">We present a simple method for extracting avermectines from meat, based on a QuEChERS approach followed by liquid chromatography (LC) coupled to triple quadrupole (QqQ) tandem mass spectrometry (MS/MS). The compounds considered are ivermectin, abamectin, emamectin, eprinomectin, doramectin and moxidectin. The new method has been fully validated according to the requirements of European Decision 657/2002/CE (EU, 2002). The method is suitable for the analysis of avermectins at concentration as low as 2.5 μg kg(-1), and allows high sample throughput. In addition, the detection of avermectins by high resolution mass spectrometry using a quadrupole-Orbritrap (Q-Orbitrap) hybrid instrument has been explored, and the target Selected Ion Monitoring data dependent MS/MS (t-SIM-dd MS/MS) mode has been found to provide excellent performance for residue determination of target analytes.</subfield></datafield><datafield tag="540" ind1=" " ind2=" "><subfield code="a">Nutzungsrecht: Copyright © 2015 Elsevier Ltd. All rights reserved.</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Ivermectin - chemistry</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Tandem Mass Spectrometry - methods</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Ivermectin - analogs & derivatives</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Granados, M</subfield><subfield code="4">oth</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Centrich, F</subfield><subfield code="4">oth</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Rúbies, A</subfield><subfield code="4">oth</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Companyó, R</subfield><subfield code="4">oth</subfield></datafield><datafield tag="773" ind1="0" ind2="8"><subfield code="i">Enthalten in</subfield><subfield code="t">Food chemistry</subfield><subfield code="d">Amsterdam [u.a.] : Elsevier, 1976</subfield><subfield code="g">181(2015), Seite 57-63</subfield><subfield code="w">(DE-627)129611751</subfield><subfield code="w">(DE-600)243123-3</subfield><subfield code="w">(DE-576)015107418</subfield><subfield code="x">0308-8146</subfield><subfield code="7">nnns</subfield></datafield><datafield tag="773" ind1="1" ind2="8"><subfield code="g">volume:181</subfield><subfield code="g">year:2015</subfield><subfield code="g">pages:57-63</subfield></datafield><datafield tag="856" ind1="4" ind2="1"><subfield code="u">http://dx.doi.org/10.1016/j.foodchem.2015.02.067</subfield><subfield code="3">Volltext</subfield></datafield><datafield tag="856" ind1="4" ind2="2"><subfield code="u">http://www.ncbi.nlm.nih.gov/pubmed/25794721</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_USEFLAG_A</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">SYSFLAG_A</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_OLC</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">SSG-OLC-TEC</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">SSG-OLC-CHE</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_70</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4012</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4219</subfield></datafield><datafield tag="936" ind1="b" ind2="k"><subfield code="a">58.34</subfield><subfield code="q">AVZ</subfield></datafield><datafield tag="936" ind1="b" ind2="k"><subfield code="a">58.00</subfield><subfield code="q">AVZ</subfield></datafield><datafield tag="951" ind1=" " ind2=" "><subfield code="a">AR</subfield></datafield><datafield tag="952" ind1=" " ind2=" "><subfield code="d">181</subfield><subfield code="j">2015</subfield><subfield code="h">57-63</subfield></datafield></record></collection>
|
author |
Antkowiak, S |
spellingShingle |
Antkowiak, S ddc 540 bkl 58.34 bkl 58.00 misc Ivermectin - chemistry misc Tandem Mass Spectrometry - methods misc Ivermectin - analogs & derivatives Determination of avermectins: a QuEChERS approach to the analysis of food samples |
authorStr |
Antkowiak, S |
ppnlink_with_tag_str_mv |
@@773@@(DE-627)129611751 |
format |
Article |
dewey-ones |
540 - Chemistry & allied sciences 660 - Chemical engineering |
delete_txt_mv |
keep |
author_role |
aut |
collection |
OLC |
remote_str |
false |
illustrated |
Not Illustrated |
issn |
0308-8146 |
topic_title |
540 660 DNB 58.34 bkl 58.00 bkl Determination of avermectins: a QuEChERS approach to the analysis of food samples Ivermectin - chemistry Tandem Mass Spectrometry - methods Ivermectin - analogs & derivatives |
topic |
ddc 540 bkl 58.34 bkl 58.00 misc Ivermectin - chemistry misc Tandem Mass Spectrometry - methods misc Ivermectin - analogs & derivatives |
topic_unstemmed |
ddc 540 bkl 58.34 bkl 58.00 misc Ivermectin - chemistry misc Tandem Mass Spectrometry - methods misc Ivermectin - analogs & derivatives |
topic_browse |
ddc 540 bkl 58.34 bkl 58.00 misc Ivermectin - chemistry misc Tandem Mass Spectrometry - methods misc Ivermectin - analogs & derivatives |
format_facet |
Aufsätze Gedruckte Aufsätze |
format_main_str_mv |
Text Zeitschrift/Artikel |
carriertype_str_mv |
nc |
author2_variant |
m g mg f c fc a r ar r c rc |
hierarchy_parent_title |
Food chemistry |
hierarchy_parent_id |
129611751 |
dewey-tens |
540 - Chemistry 660 - Chemical engineering |
hierarchy_top_title |
Food chemistry |
isfreeaccess_txt |
false |
familylinks_str_mv |
(DE-627)129611751 (DE-600)243123-3 (DE-576)015107418 |
title |
Determination of avermectins: a QuEChERS approach to the analysis of food samples |
ctrlnum |
(DE-627)OLC1969367377 (DE-599)GBVOLC1969367377 (PRQ)c1300-b1a0a6c615a925517cdee4d2b9a689f1f240b9f5855fa82c6d7cf2ab8f9c3e1c0 (KEY)0039580320150000181000000057determinationofavermectinsaquechersapproachtothean |
title_full |
Determination of avermectins: a QuEChERS approach to the analysis of food samples |
author_sort |
Antkowiak, S |
journal |
Food chemistry |
journalStr |
Food chemistry |
lang_code |
eng |
isOA_bool |
false |
dewey-hundreds |
500 - Science 600 - Technology |
recordtype |
marc |
publishDateSort |
2015 |
contenttype_str_mv |
txt |
container_start_page |
57 |
author_browse |
Antkowiak, S |
container_volume |
181 |
class |
540 660 DNB 58.34 bkl 58.00 bkl |
format_se |
Aufsätze |
author-letter |
Antkowiak, S |
doi_str_mv |
10.1016/j.foodchem.2015.02.067 |
dewey-full |
540 660 |
title_sort |
determination of avermectins: a quechers approach to the analysis of food samples |
title_auth |
Determination of avermectins: a QuEChERS approach to the analysis of food samples |
abstract |
We present a simple method for extracting avermectines from meat, based on a QuEChERS approach followed by liquid chromatography (LC) coupled to triple quadrupole (QqQ) tandem mass spectrometry (MS/MS). The compounds considered are ivermectin, abamectin, emamectin, eprinomectin, doramectin and moxidectin. The new method has been fully validated according to the requirements of European Decision 657/2002/CE (EU, 2002). The method is suitable for the analysis of avermectins at concentration as low as 2.5 μg kg(-1), and allows high sample throughput. In addition, the detection of avermectins by high resolution mass spectrometry using a quadrupole-Orbritrap (Q-Orbitrap) hybrid instrument has been explored, and the target Selected Ion Monitoring data dependent MS/MS (t-SIM-dd MS/MS) mode has been found to provide excellent performance for residue determination of target analytes. |
abstractGer |
We present a simple method for extracting avermectines from meat, based on a QuEChERS approach followed by liquid chromatography (LC) coupled to triple quadrupole (QqQ) tandem mass spectrometry (MS/MS). The compounds considered are ivermectin, abamectin, emamectin, eprinomectin, doramectin and moxidectin. The new method has been fully validated according to the requirements of European Decision 657/2002/CE (EU, 2002). The method is suitable for the analysis of avermectins at concentration as low as 2.5 μg kg(-1), and allows high sample throughput. In addition, the detection of avermectins by high resolution mass spectrometry using a quadrupole-Orbritrap (Q-Orbitrap) hybrid instrument has been explored, and the target Selected Ion Monitoring data dependent MS/MS (t-SIM-dd MS/MS) mode has been found to provide excellent performance for residue determination of target analytes. |
abstract_unstemmed |
We present a simple method for extracting avermectines from meat, based on a QuEChERS approach followed by liquid chromatography (LC) coupled to triple quadrupole (QqQ) tandem mass spectrometry (MS/MS). The compounds considered are ivermectin, abamectin, emamectin, eprinomectin, doramectin and moxidectin. The new method has been fully validated according to the requirements of European Decision 657/2002/CE (EU, 2002). The method is suitable for the analysis of avermectins at concentration as low as 2.5 μg kg(-1), and allows high sample throughput. In addition, the detection of avermectins by high resolution mass spectrometry using a quadrupole-Orbritrap (Q-Orbitrap) hybrid instrument has been explored, and the target Selected Ion Monitoring data dependent MS/MS (t-SIM-dd MS/MS) mode has been found to provide excellent performance for residue determination of target analytes. |
collection_details |
GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE GBV_ILN_70 GBV_ILN_4012 GBV_ILN_4219 |
title_short |
Determination of avermectins: a QuEChERS approach to the analysis of food samples |
url |
http://dx.doi.org/10.1016/j.foodchem.2015.02.067 http://www.ncbi.nlm.nih.gov/pubmed/25794721 |
remote_bool |
false |
author2 |
Granados, M Centrich, F Rúbies, A Companyó, R |
author2Str |
Granados, M Centrich, F Rúbies, A Companyó, R |
ppnlink |
129611751 |
mediatype_str_mv |
n |
isOA_txt |
false |
hochschulschrift_bool |
false |
author2_role |
oth oth oth oth |
doi_str |
10.1016/j.foodchem.2015.02.067 |
up_date |
2024-07-04T05:20:18.076Z |
_version_ |
1803624558706556928 |
fullrecord_marcxml |
<?xml version="1.0" encoding="UTF-8"?><collection xmlns="http://www.loc.gov/MARC21/slim"><record><leader>01000caa a2200265 4500</leader><controlfield tag="001">OLC1969367377</controlfield><controlfield tag="003">DE-627</controlfield><controlfield tag="005">20220223002843.0</controlfield><controlfield tag="007">tu</controlfield><controlfield tag="008">160211s2015 xx ||||| 00| ||eng c</controlfield><datafield tag="024" ind1="7" ind2=" "><subfield code="a">10.1016/j.foodchem.2015.02.067</subfield><subfield code="2">doi</subfield></datafield><datafield tag="028" ind1="5" ind2="2"><subfield code="a">PQ20160211</subfield></datafield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(DE-627)OLC1969367377</subfield></datafield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(DE-599)GBVOLC1969367377</subfield></datafield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(PRQ)c1300-b1a0a6c615a925517cdee4d2b9a689f1f240b9f5855fa82c6d7cf2ab8f9c3e1c0</subfield></datafield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(KEY)0039580320150000181000000057determinationofavermectinsaquechersapproachtothean</subfield></datafield><datafield tag="040" ind1=" " ind2=" "><subfield code="a">DE-627</subfield><subfield code="b">ger</subfield><subfield code="c">DE-627</subfield><subfield code="e">rakwb</subfield></datafield><datafield tag="041" ind1=" " ind2=" "><subfield code="a">eng</subfield></datafield><datafield tag="082" ind1="0" ind2="4"><subfield code="a">540</subfield><subfield code="a">660</subfield><subfield code="q">DNB</subfield></datafield><datafield tag="084" ind1=" " ind2=" "><subfield code="a">58.34</subfield><subfield code="2">bkl</subfield></datafield><datafield tag="084" ind1=" " ind2=" "><subfield code="a">58.00</subfield><subfield code="2">bkl</subfield></datafield><datafield tag="100" ind1="1" ind2=" "><subfield code="a">Antkowiak, S</subfield><subfield code="e">verfasserin</subfield><subfield code="4">aut</subfield></datafield><datafield tag="245" ind1="1" ind2="0"><subfield code="a">Determination of avermectins: a QuEChERS approach to the analysis of food samples</subfield></datafield><datafield tag="264" ind1=" " ind2="1"><subfield code="c">2015</subfield></datafield><datafield tag="336" ind1=" " ind2=" "><subfield code="a">Text</subfield><subfield code="b">txt</subfield><subfield code="2">rdacontent</subfield></datafield><datafield tag="337" ind1=" " ind2=" "><subfield code="a">ohne Hilfsmittel zu benutzen</subfield><subfield code="b">n</subfield><subfield code="2">rdamedia</subfield></datafield><datafield tag="338" ind1=" " ind2=" "><subfield code="a">Band</subfield><subfield code="b">nc</subfield><subfield code="2">rdacarrier</subfield></datafield><datafield tag="520" ind1=" " ind2=" "><subfield code="a">We present a simple method for extracting avermectines from meat, based on a QuEChERS approach followed by liquid chromatography (LC) coupled to triple quadrupole (QqQ) tandem mass spectrometry (MS/MS). The compounds considered are ivermectin, abamectin, emamectin, eprinomectin, doramectin and moxidectin. The new method has been fully validated according to the requirements of European Decision 657/2002/CE (EU, 2002). The method is suitable for the analysis of avermectins at concentration as low as 2.5 μg kg(-1), and allows high sample throughput. In addition, the detection of avermectins by high resolution mass spectrometry using a quadrupole-Orbritrap (Q-Orbitrap) hybrid instrument has been explored, and the target Selected Ion Monitoring data dependent MS/MS (t-SIM-dd MS/MS) mode has been found to provide excellent performance for residue determination of target analytes.</subfield></datafield><datafield tag="540" ind1=" " ind2=" "><subfield code="a">Nutzungsrecht: Copyright © 2015 Elsevier Ltd. All rights reserved.</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Ivermectin - chemistry</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Tandem Mass Spectrometry - methods</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Ivermectin - analogs & derivatives</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Granados, M</subfield><subfield code="4">oth</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Centrich, F</subfield><subfield code="4">oth</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Rúbies, A</subfield><subfield code="4">oth</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Companyó, R</subfield><subfield code="4">oth</subfield></datafield><datafield tag="773" ind1="0" ind2="8"><subfield code="i">Enthalten in</subfield><subfield code="t">Food chemistry</subfield><subfield code="d">Amsterdam [u.a.] : Elsevier, 1976</subfield><subfield code="g">181(2015), Seite 57-63</subfield><subfield code="w">(DE-627)129611751</subfield><subfield code="w">(DE-600)243123-3</subfield><subfield code="w">(DE-576)015107418</subfield><subfield code="x">0308-8146</subfield><subfield code="7">nnns</subfield></datafield><datafield tag="773" ind1="1" ind2="8"><subfield code="g">volume:181</subfield><subfield code="g">year:2015</subfield><subfield code="g">pages:57-63</subfield></datafield><datafield tag="856" ind1="4" ind2="1"><subfield code="u">http://dx.doi.org/10.1016/j.foodchem.2015.02.067</subfield><subfield code="3">Volltext</subfield></datafield><datafield tag="856" ind1="4" ind2="2"><subfield code="u">http://www.ncbi.nlm.nih.gov/pubmed/25794721</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_USEFLAG_A</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">SYSFLAG_A</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_OLC</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">SSG-OLC-TEC</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">SSG-OLC-CHE</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_70</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4012</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4219</subfield></datafield><datafield tag="936" ind1="b" ind2="k"><subfield code="a">58.34</subfield><subfield code="q">AVZ</subfield></datafield><datafield tag="936" ind1="b" ind2="k"><subfield code="a">58.00</subfield><subfield code="q">AVZ</subfield></datafield><datafield tag="951" ind1=" " ind2=" "><subfield code="a">AR</subfield></datafield><datafield tag="952" ind1=" " ind2=" "><subfield code="d">181</subfield><subfield code="j">2015</subfield><subfield code="h">57-63</subfield></datafield></record></collection>
|
score |
7.401454 |