Determination of avermectins: a QuEChERS approach to the analysis of food samples
We present a simple method for extracting avermectines from meat, based on a QuEChERS approach followed by liquid chromatography (LC) coupled to triple quadrupole (QqQ) tandem mass spectrometry (MS/MS). The compounds considered are ivermectin, abamectin, emamectin, eprinomectin, doramectin and moxid...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Antkowiak, S [verfasserIn] |
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| Format: |
Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2015 |
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| Rechteinformationen: |
Nutzungsrecht: Copyright © 2015 Elsevier Ltd. All rights reserved. |
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| Schlagwörter: |
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| Übergeordnetes Werk: |
Enthalten in: Food chemistry - Amsterdam [u.a.] : Elsevier, 1976, 181(2015), Seite 57-63 |
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| Übergeordnetes Werk: |
volume:181 ; year:2015 ; pages:57-63 |
| Links: |
|---|
| DOI / URN: |
10.1016/j.foodchem.2015.02.067 |
|---|
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OLC1969367377 |
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| 520 | |a We present a simple method for extracting avermectines from meat, based on a QuEChERS approach followed by liquid chromatography (LC) coupled to triple quadrupole (QqQ) tandem mass spectrometry (MS/MS). The compounds considered are ivermectin, abamectin, emamectin, eprinomectin, doramectin and moxidectin. The new method has been fully validated according to the requirements of European Decision 657/2002/CE (EU, 2002). The method is suitable for the analysis of avermectins at concentration as low as 2.5 μg kg(-1), and allows high sample throughput. In addition, the detection of avermectins by high resolution mass spectrometry using a quadrupole-Orbritrap (Q-Orbitrap) hybrid instrument has been explored, and the target Selected Ion Monitoring data dependent MS/MS (t-SIM-dd MS/MS) mode has been found to provide excellent performance for residue determination of target analytes. | ||
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10.1016/j.foodchem.2015.02.067 doi PQ20160211 (DE-627)OLC1969367377 (DE-599)GBVOLC1969367377 (PRQ)c1300-b1a0a6c615a925517cdee4d2b9a689f1f240b9f5855fa82c6d7cf2ab8f9c3e1c0 (KEY)0039580320150000181000000057determinationofavermectinsaquechersapproachtothean DE-627 ger DE-627 rakwb eng 540 660 DNB 58.34 bkl 58.00 bkl Antkowiak, S verfasserin aut Determination of avermectins: a QuEChERS approach to the analysis of food samples 2015 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier We present a simple method for extracting avermectines from meat, based on a QuEChERS approach followed by liquid chromatography (LC) coupled to triple quadrupole (QqQ) tandem mass spectrometry (MS/MS). The compounds considered are ivermectin, abamectin, emamectin, eprinomectin, doramectin and moxidectin. The new method has been fully validated according to the requirements of European Decision 657/2002/CE (EU, 2002). The method is suitable for the analysis of avermectins at concentration as low as 2.5 μg kg(-1), and allows high sample throughput. In addition, the detection of avermectins by high resolution mass spectrometry using a quadrupole-Orbritrap (Q-Orbitrap) hybrid instrument has been explored, and the target Selected Ion Monitoring data dependent MS/MS (t-SIM-dd MS/MS) mode has been found to provide excellent performance for residue determination of target analytes. Nutzungsrecht: Copyright © 2015 Elsevier Ltd. All rights reserved. Ivermectin - chemistry Tandem Mass Spectrometry - methods Ivermectin - analogs & derivatives Granados, M oth Centrich, F oth Rúbies, A oth Companyó, R oth Enthalten in Food chemistry Amsterdam [u.a.] : Elsevier, 1976 181(2015), Seite 57-63 (DE-627)129611751 (DE-600)243123-3 (DE-576)015107418 0308-8146 nnns volume:181 year:2015 pages:57-63 http://dx.doi.org/10.1016/j.foodchem.2015.02.067 Volltext http://www.ncbi.nlm.nih.gov/pubmed/25794721 GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE GBV_ILN_70 GBV_ILN_4012 GBV_ILN_4219 58.34 AVZ 58.00 AVZ AR 181 2015 57-63 |
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10.1016/j.foodchem.2015.02.067 doi PQ20160211 (DE-627)OLC1969367377 (DE-599)GBVOLC1969367377 (PRQ)c1300-b1a0a6c615a925517cdee4d2b9a689f1f240b9f5855fa82c6d7cf2ab8f9c3e1c0 (KEY)0039580320150000181000000057determinationofavermectinsaquechersapproachtothean DE-627 ger DE-627 rakwb eng 540 660 DNB 58.34 bkl 58.00 bkl Antkowiak, S verfasserin aut Determination of avermectins: a QuEChERS approach to the analysis of food samples 2015 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier We present a simple method for extracting avermectines from meat, based on a QuEChERS approach followed by liquid chromatography (LC) coupled to triple quadrupole (QqQ) tandem mass spectrometry (MS/MS). The compounds considered are ivermectin, abamectin, emamectin, eprinomectin, doramectin and moxidectin. The new method has been fully validated according to the requirements of European Decision 657/2002/CE (EU, 2002). The method is suitable for the analysis of avermectins at concentration as low as 2.5 μg kg(-1), and allows high sample throughput. In addition, the detection of avermectins by high resolution mass spectrometry using a quadrupole-Orbritrap (Q-Orbitrap) hybrid instrument has been explored, and the target Selected Ion Monitoring data dependent MS/MS (t-SIM-dd MS/MS) mode has been found to provide excellent performance for residue determination of target analytes. Nutzungsrecht: Copyright © 2015 Elsevier Ltd. All rights reserved. Ivermectin - chemistry Tandem Mass Spectrometry - methods Ivermectin - analogs & derivatives Granados, M oth Centrich, F oth Rúbies, A oth Companyó, R oth Enthalten in Food chemistry Amsterdam [u.a.] : Elsevier, 1976 181(2015), Seite 57-63 (DE-627)129611751 (DE-600)243123-3 (DE-576)015107418 0308-8146 nnns volume:181 year:2015 pages:57-63 http://dx.doi.org/10.1016/j.foodchem.2015.02.067 Volltext http://www.ncbi.nlm.nih.gov/pubmed/25794721 GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE GBV_ILN_70 GBV_ILN_4012 GBV_ILN_4219 58.34 AVZ 58.00 AVZ AR 181 2015 57-63 |
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10.1016/j.foodchem.2015.02.067 doi PQ20160211 (DE-627)OLC1969367377 (DE-599)GBVOLC1969367377 (PRQ)c1300-b1a0a6c615a925517cdee4d2b9a689f1f240b9f5855fa82c6d7cf2ab8f9c3e1c0 (KEY)0039580320150000181000000057determinationofavermectinsaquechersapproachtothean DE-627 ger DE-627 rakwb eng 540 660 DNB 58.34 bkl 58.00 bkl Antkowiak, S verfasserin aut Determination of avermectins: a QuEChERS approach to the analysis of food samples 2015 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier We present a simple method for extracting avermectines from meat, based on a QuEChERS approach followed by liquid chromatography (LC) coupled to triple quadrupole (QqQ) tandem mass spectrometry (MS/MS). The compounds considered are ivermectin, abamectin, emamectin, eprinomectin, doramectin and moxidectin. The new method has been fully validated according to the requirements of European Decision 657/2002/CE (EU, 2002). The method is suitable for the analysis of avermectins at concentration as low as 2.5 μg kg(-1), and allows high sample throughput. In addition, the detection of avermectins by high resolution mass spectrometry using a quadrupole-Orbritrap (Q-Orbitrap) hybrid instrument has been explored, and the target Selected Ion Monitoring data dependent MS/MS (t-SIM-dd MS/MS) mode has been found to provide excellent performance for residue determination of target analytes. Nutzungsrecht: Copyright © 2015 Elsevier Ltd. All rights reserved. Ivermectin - chemistry Tandem Mass Spectrometry - methods Ivermectin - analogs & derivatives Granados, M oth Centrich, F oth Rúbies, A oth Companyó, R oth Enthalten in Food chemistry Amsterdam [u.a.] : Elsevier, 1976 181(2015), Seite 57-63 (DE-627)129611751 (DE-600)243123-3 (DE-576)015107418 0308-8146 nnns volume:181 year:2015 pages:57-63 http://dx.doi.org/10.1016/j.foodchem.2015.02.067 Volltext http://www.ncbi.nlm.nih.gov/pubmed/25794721 GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE GBV_ILN_70 GBV_ILN_4012 GBV_ILN_4219 58.34 AVZ 58.00 AVZ AR 181 2015 57-63 |
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10.1016/j.foodchem.2015.02.067 doi PQ20160211 (DE-627)OLC1969367377 (DE-599)GBVOLC1969367377 (PRQ)c1300-b1a0a6c615a925517cdee4d2b9a689f1f240b9f5855fa82c6d7cf2ab8f9c3e1c0 (KEY)0039580320150000181000000057determinationofavermectinsaquechersapproachtothean DE-627 ger DE-627 rakwb eng 540 660 DNB 58.34 bkl 58.00 bkl Antkowiak, S verfasserin aut Determination of avermectins: a QuEChERS approach to the analysis of food samples 2015 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier We present a simple method for extracting avermectines from meat, based on a QuEChERS approach followed by liquid chromatography (LC) coupled to triple quadrupole (QqQ) tandem mass spectrometry (MS/MS). The compounds considered are ivermectin, abamectin, emamectin, eprinomectin, doramectin and moxidectin. The new method has been fully validated according to the requirements of European Decision 657/2002/CE (EU, 2002). The method is suitable for the analysis of avermectins at concentration as low as 2.5 μg kg(-1), and allows high sample throughput. In addition, the detection of avermectins by high resolution mass spectrometry using a quadrupole-Orbritrap (Q-Orbitrap) hybrid instrument has been explored, and the target Selected Ion Monitoring data dependent MS/MS (t-SIM-dd MS/MS) mode has been found to provide excellent performance for residue determination of target analytes. Nutzungsrecht: Copyright © 2015 Elsevier Ltd. All rights reserved. Ivermectin - chemistry Tandem Mass Spectrometry - methods Ivermectin - analogs & derivatives Granados, M oth Centrich, F oth Rúbies, A oth Companyó, R oth Enthalten in Food chemistry Amsterdam [u.a.] : Elsevier, 1976 181(2015), Seite 57-63 (DE-627)129611751 (DE-600)243123-3 (DE-576)015107418 0308-8146 nnns volume:181 year:2015 pages:57-63 http://dx.doi.org/10.1016/j.foodchem.2015.02.067 Volltext http://www.ncbi.nlm.nih.gov/pubmed/25794721 GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE GBV_ILN_70 GBV_ILN_4012 GBV_ILN_4219 58.34 AVZ 58.00 AVZ AR 181 2015 57-63 |
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10.1016/j.foodchem.2015.02.067 doi PQ20160211 (DE-627)OLC1969367377 (DE-599)GBVOLC1969367377 (PRQ)c1300-b1a0a6c615a925517cdee4d2b9a689f1f240b9f5855fa82c6d7cf2ab8f9c3e1c0 (KEY)0039580320150000181000000057determinationofavermectinsaquechersapproachtothean DE-627 ger DE-627 rakwb eng 540 660 DNB 58.34 bkl 58.00 bkl Antkowiak, S verfasserin aut Determination of avermectins: a QuEChERS approach to the analysis of food samples 2015 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier We present a simple method for extracting avermectines from meat, based on a QuEChERS approach followed by liquid chromatography (LC) coupled to triple quadrupole (QqQ) tandem mass spectrometry (MS/MS). The compounds considered are ivermectin, abamectin, emamectin, eprinomectin, doramectin and moxidectin. The new method has been fully validated according to the requirements of European Decision 657/2002/CE (EU, 2002). The method is suitable for the analysis of avermectins at concentration as low as 2.5 μg kg(-1), and allows high sample throughput. In addition, the detection of avermectins by high resolution mass spectrometry using a quadrupole-Orbritrap (Q-Orbitrap) hybrid instrument has been explored, and the target Selected Ion Monitoring data dependent MS/MS (t-SIM-dd MS/MS) mode has been found to provide excellent performance for residue determination of target analytes. Nutzungsrecht: Copyright © 2015 Elsevier Ltd. All rights reserved. Ivermectin - chemistry Tandem Mass Spectrometry - methods Ivermectin - analogs & derivatives Granados, M oth Centrich, F oth Rúbies, A oth Companyó, R oth Enthalten in Food chemistry Amsterdam [u.a.] : Elsevier, 1976 181(2015), Seite 57-63 (DE-627)129611751 (DE-600)243123-3 (DE-576)015107418 0308-8146 nnns volume:181 year:2015 pages:57-63 http://dx.doi.org/10.1016/j.foodchem.2015.02.067 Volltext http://www.ncbi.nlm.nih.gov/pubmed/25794721 GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE GBV_ILN_70 GBV_ILN_4012 GBV_ILN_4219 58.34 AVZ 58.00 AVZ AR 181 2015 57-63 |
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Determination of avermectins: a QuEChERS approach to the analysis of food samples |
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Determination of avermectins: a QuEChERS approach to the analysis of food samples |
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Antkowiak, S |
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determination of avermectins: a quechers approach to the analysis of food samples |
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Determination of avermectins: a QuEChERS approach to the analysis of food samples |
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We present a simple method for extracting avermectines from meat, based on a QuEChERS approach followed by liquid chromatography (LC) coupled to triple quadrupole (QqQ) tandem mass spectrometry (MS/MS). The compounds considered are ivermectin, abamectin, emamectin, eprinomectin, doramectin and moxidectin. The new method has been fully validated according to the requirements of European Decision 657/2002/CE (EU, 2002). The method is suitable for the analysis of avermectins at concentration as low as 2.5 μg kg(-1), and allows high sample throughput. In addition, the detection of avermectins by high resolution mass spectrometry using a quadrupole-Orbritrap (Q-Orbitrap) hybrid instrument has been explored, and the target Selected Ion Monitoring data dependent MS/MS (t-SIM-dd MS/MS) mode has been found to provide excellent performance for residue determination of target analytes. |
| abstractGer |
We present a simple method for extracting avermectines from meat, based on a QuEChERS approach followed by liquid chromatography (LC) coupled to triple quadrupole (QqQ) tandem mass spectrometry (MS/MS). The compounds considered are ivermectin, abamectin, emamectin, eprinomectin, doramectin and moxidectin. The new method has been fully validated according to the requirements of European Decision 657/2002/CE (EU, 2002). The method is suitable for the analysis of avermectins at concentration as low as 2.5 μg kg(-1), and allows high sample throughput. In addition, the detection of avermectins by high resolution mass spectrometry using a quadrupole-Orbritrap (Q-Orbitrap) hybrid instrument has been explored, and the target Selected Ion Monitoring data dependent MS/MS (t-SIM-dd MS/MS) mode has been found to provide excellent performance for residue determination of target analytes. |
| abstract_unstemmed |
We present a simple method for extracting avermectines from meat, based on a QuEChERS approach followed by liquid chromatography (LC) coupled to triple quadrupole (QqQ) tandem mass spectrometry (MS/MS). The compounds considered are ivermectin, abamectin, emamectin, eprinomectin, doramectin and moxidectin. The new method has been fully validated according to the requirements of European Decision 657/2002/CE (EU, 2002). The method is suitable for the analysis of avermectins at concentration as low as 2.5 μg kg(-1), and allows high sample throughput. In addition, the detection of avermectins by high resolution mass spectrometry using a quadrupole-Orbritrap (Q-Orbitrap) hybrid instrument has been explored, and the target Selected Ion Monitoring data dependent MS/MS (t-SIM-dd MS/MS) mode has been found to provide excellent performance for residue determination of target analytes. |
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Determination of avermectins: a QuEChERS approach to the analysis of food samples |
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