Identification of Failure Mechanism Consistency for NBR Accelerated Test
A consistent failure mechanism is a precondition for accelerated tests, and the accurate identification of the catastrophe point at which the failure mechanism transforms remains a longstanding challenge in accelerated tests. In this study, an independently designed test apparatus was adopted to mon...
Ausführliche Beschreibung
Autor*in: |
He, Jingjing [verfasserIn] |
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Format: |
Artikel |
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Sprache: |
Englisch |
Erschienen: |
2016 |
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Rechteinformationen: |
Nutzungsrecht: © 2014 ASTM International All rights reserved. This material may not be reproduced or copied, in whole or in part, in any printed, mechanical, electronic, film, or other distribution and storage media, without the written consent of the publisher. |
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Übergeordnetes Werk: |
Enthalten in: Journal of testing and evaluation - West Conshohocken, Pa. [u.a.] : Soc., 1973, 44(2016), 1 |
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Übergeordnetes Werk: |
volume:44 ; year:2016 ; number:1 |
Links: |
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DOI / URN: |
10.1520/JTE20130252 |
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Katalog-ID: |
OLC1970432470 |
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520 | |a A consistent failure mechanism is a precondition for accelerated tests, and the accurate identification of the catastrophe point at which the failure mechanism transforms remains a longstanding challenge in accelerated tests. In this study, an independently designed test apparatus was adopted to monitor the variation in the compressive stress of nitrile butadiene rubber (NBR) samples at different temperatures. The deformation of the samples was controlled as a constant so the variation of the stress could be correlated with the mechanical properties of the NBR. In addition, thermal analysis and infrared spectroscopic analysis were conducted for NBR samples without applying external stresses (e.g., free state) at various elevated temperatures. Samples stored at room temperature for two years were also tested and analyzed to provide a baseline. The results indicate that the stress relaxation mechanism for NBR aged at 80°C differs from that for samples aged at 90°C. The dominating aging mechanism for NBR samples stored at room temperature and accelerated at 80°C is free radical oxidation. The main mechanism under 90°C was found to be chain scission. After combining the changes in macroperformance and microstructure, we concluded that the change in aging mechanism occurred between 80°C and 90°C. | ||
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10.1520/JTE20130252 doi PQ20160212 (DE-627)OLC1970432470 (DE-599)GBVOLC1970432470 (PRQ)a612-d6e10b6a8c70633420b1d9b05bcea4cb29521a6c62bf82d72ade8ab68d853fc50 (KEY)0007222220160000044000100000identificationoffailuremechanismconsistencyfornbra DE-627 ger DE-627 rakwb eng 600 DNB 51.30 bkl He, Jingjing verfasserin aut Identification of Failure Mechanism Consistency for NBR Accelerated Test 2016 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier A consistent failure mechanism is a precondition for accelerated tests, and the accurate identification of the catastrophe point at which the failure mechanism transforms remains a longstanding challenge in accelerated tests. In this study, an independently designed test apparatus was adopted to monitor the variation in the compressive stress of nitrile butadiene rubber (NBR) samples at different temperatures. The deformation of the samples was controlled as a constant so the variation of the stress could be correlated with the mechanical properties of the NBR. In addition, thermal analysis and infrared spectroscopic analysis were conducted for NBR samples without applying external stresses (e.g., free state) at various elevated temperatures. Samples stored at room temperature for two years were also tested and analyzed to provide a baseline. The results indicate that the stress relaxation mechanism for NBR aged at 80°C differs from that for samples aged at 90°C. The dominating aging mechanism for NBR samples stored at room temperature and accelerated at 80°C is free radical oxidation. The main mechanism under 90°C was found to be chain scission. After combining the changes in macroperformance and microstructure, we concluded that the change in aging mechanism occurred between 80°C and 90°C. Nutzungsrecht: © 2014 ASTM International All rights reserved. This material may not be reproduced or copied, in whole or in part, in any printed, mechanical, electronic, film, or other distribution and storage media, without the written consent of the publisher. Zhang, Weifang oth Fang, Xiaotong oth Tang, Qingyun oth Enthalten in Journal of testing and evaluation West Conshohocken, Pa. [u.a.] : Soc., 1973 44(2016), 1 (DE-627)129391816 (DE-600)184915-3 (DE-576)014776952 0090-3973 nnns volume:44 year:2016 number:1 http://dx.doi.org/10.1520/JTE20130252 Volltext http://www.astm.org/DIGITAL_LIBRARY/JOURNALS/TESTEVAL/PAGES/JTE20130252.htm GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC GBV_ILN_60 GBV_ILN_70 GBV_ILN_4323 51.30 AVZ AR 44 2016 1 |
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10.1520/JTE20130252 doi PQ20160212 (DE-627)OLC1970432470 (DE-599)GBVOLC1970432470 (PRQ)a612-d6e10b6a8c70633420b1d9b05bcea4cb29521a6c62bf82d72ade8ab68d853fc50 (KEY)0007222220160000044000100000identificationoffailuremechanismconsistencyfornbra DE-627 ger DE-627 rakwb eng 600 DNB 51.30 bkl He, Jingjing verfasserin aut Identification of Failure Mechanism Consistency for NBR Accelerated Test 2016 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier A consistent failure mechanism is a precondition for accelerated tests, and the accurate identification of the catastrophe point at which the failure mechanism transforms remains a longstanding challenge in accelerated tests. In this study, an independently designed test apparatus was adopted to monitor the variation in the compressive stress of nitrile butadiene rubber (NBR) samples at different temperatures. The deformation of the samples was controlled as a constant so the variation of the stress could be correlated with the mechanical properties of the NBR. In addition, thermal analysis and infrared spectroscopic analysis were conducted for NBR samples without applying external stresses (e.g., free state) at various elevated temperatures. Samples stored at room temperature for two years were also tested and analyzed to provide a baseline. The results indicate that the stress relaxation mechanism for NBR aged at 80°C differs from that for samples aged at 90°C. The dominating aging mechanism for NBR samples stored at room temperature and accelerated at 80°C is free radical oxidation. The main mechanism under 90°C was found to be chain scission. After combining the changes in macroperformance and microstructure, we concluded that the change in aging mechanism occurred between 80°C and 90°C. Nutzungsrecht: © 2014 ASTM International All rights reserved. This material may not be reproduced or copied, in whole or in part, in any printed, mechanical, electronic, film, or other distribution and storage media, without the written consent of the publisher. Zhang, Weifang oth Fang, Xiaotong oth Tang, Qingyun oth Enthalten in Journal of testing and evaluation West Conshohocken, Pa. [u.a.] : Soc., 1973 44(2016), 1 (DE-627)129391816 (DE-600)184915-3 (DE-576)014776952 0090-3973 nnns volume:44 year:2016 number:1 http://dx.doi.org/10.1520/JTE20130252 Volltext http://www.astm.org/DIGITAL_LIBRARY/JOURNALS/TESTEVAL/PAGES/JTE20130252.htm GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC GBV_ILN_60 GBV_ILN_70 GBV_ILN_4323 51.30 AVZ AR 44 2016 1 |
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10.1520/JTE20130252 doi PQ20160212 (DE-627)OLC1970432470 (DE-599)GBVOLC1970432470 (PRQ)a612-d6e10b6a8c70633420b1d9b05bcea4cb29521a6c62bf82d72ade8ab68d853fc50 (KEY)0007222220160000044000100000identificationoffailuremechanismconsistencyfornbra DE-627 ger DE-627 rakwb eng 600 DNB 51.30 bkl He, Jingjing verfasserin aut Identification of Failure Mechanism Consistency for NBR Accelerated Test 2016 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier A consistent failure mechanism is a precondition for accelerated tests, and the accurate identification of the catastrophe point at which the failure mechanism transforms remains a longstanding challenge in accelerated tests. In this study, an independently designed test apparatus was adopted to monitor the variation in the compressive stress of nitrile butadiene rubber (NBR) samples at different temperatures. The deformation of the samples was controlled as a constant so the variation of the stress could be correlated with the mechanical properties of the NBR. In addition, thermal analysis and infrared spectroscopic analysis were conducted for NBR samples without applying external stresses (e.g., free state) at various elevated temperatures. Samples stored at room temperature for two years were also tested and analyzed to provide a baseline. The results indicate that the stress relaxation mechanism for NBR aged at 80°C differs from that for samples aged at 90°C. The dominating aging mechanism for NBR samples stored at room temperature and accelerated at 80°C is free radical oxidation. The main mechanism under 90°C was found to be chain scission. After combining the changes in macroperformance and microstructure, we concluded that the change in aging mechanism occurred between 80°C and 90°C. Nutzungsrecht: © 2014 ASTM International All rights reserved. This material may not be reproduced or copied, in whole or in part, in any printed, mechanical, electronic, film, or other distribution and storage media, without the written consent of the publisher. Zhang, Weifang oth Fang, Xiaotong oth Tang, Qingyun oth Enthalten in Journal of testing and evaluation West Conshohocken, Pa. [u.a.] : Soc., 1973 44(2016), 1 (DE-627)129391816 (DE-600)184915-3 (DE-576)014776952 0090-3973 nnns volume:44 year:2016 number:1 http://dx.doi.org/10.1520/JTE20130252 Volltext http://www.astm.org/DIGITAL_LIBRARY/JOURNALS/TESTEVAL/PAGES/JTE20130252.htm GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC GBV_ILN_60 GBV_ILN_70 GBV_ILN_4323 51.30 AVZ AR 44 2016 1 |
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10.1520/JTE20130252 doi PQ20160212 (DE-627)OLC1970432470 (DE-599)GBVOLC1970432470 (PRQ)a612-d6e10b6a8c70633420b1d9b05bcea4cb29521a6c62bf82d72ade8ab68d853fc50 (KEY)0007222220160000044000100000identificationoffailuremechanismconsistencyfornbra DE-627 ger DE-627 rakwb eng 600 DNB 51.30 bkl He, Jingjing verfasserin aut Identification of Failure Mechanism Consistency for NBR Accelerated Test 2016 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier A consistent failure mechanism is a precondition for accelerated tests, and the accurate identification of the catastrophe point at which the failure mechanism transforms remains a longstanding challenge in accelerated tests. In this study, an independently designed test apparatus was adopted to monitor the variation in the compressive stress of nitrile butadiene rubber (NBR) samples at different temperatures. The deformation of the samples was controlled as a constant so the variation of the stress could be correlated with the mechanical properties of the NBR. In addition, thermal analysis and infrared spectroscopic analysis were conducted for NBR samples without applying external stresses (e.g., free state) at various elevated temperatures. Samples stored at room temperature for two years were also tested and analyzed to provide a baseline. The results indicate that the stress relaxation mechanism for NBR aged at 80°C differs from that for samples aged at 90°C. The dominating aging mechanism for NBR samples stored at room temperature and accelerated at 80°C is free radical oxidation. The main mechanism under 90°C was found to be chain scission. After combining the changes in macroperformance and microstructure, we concluded that the change in aging mechanism occurred between 80°C and 90°C. Nutzungsrecht: © 2014 ASTM International All rights reserved. This material may not be reproduced or copied, in whole or in part, in any printed, mechanical, electronic, film, or other distribution and storage media, without the written consent of the publisher. Zhang, Weifang oth Fang, Xiaotong oth Tang, Qingyun oth Enthalten in Journal of testing and evaluation West Conshohocken, Pa. [u.a.] : Soc., 1973 44(2016), 1 (DE-627)129391816 (DE-600)184915-3 (DE-576)014776952 0090-3973 nnns volume:44 year:2016 number:1 http://dx.doi.org/10.1520/JTE20130252 Volltext http://www.astm.org/DIGITAL_LIBRARY/JOURNALS/TESTEVAL/PAGES/JTE20130252.htm GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC GBV_ILN_60 GBV_ILN_70 GBV_ILN_4323 51.30 AVZ AR 44 2016 1 |
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He, Jingjing |
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He, Jingjing |
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identification of failure mechanism consistency for nbr accelerated test |
title_auth |
Identification of Failure Mechanism Consistency for NBR Accelerated Test |
abstract |
A consistent failure mechanism is a precondition for accelerated tests, and the accurate identification of the catastrophe point at which the failure mechanism transforms remains a longstanding challenge in accelerated tests. In this study, an independently designed test apparatus was adopted to monitor the variation in the compressive stress of nitrile butadiene rubber (NBR) samples at different temperatures. The deformation of the samples was controlled as a constant so the variation of the stress could be correlated with the mechanical properties of the NBR. In addition, thermal analysis and infrared spectroscopic analysis were conducted for NBR samples without applying external stresses (e.g., free state) at various elevated temperatures. Samples stored at room temperature for two years were also tested and analyzed to provide a baseline. The results indicate that the stress relaxation mechanism for NBR aged at 80°C differs from that for samples aged at 90°C. The dominating aging mechanism for NBR samples stored at room temperature and accelerated at 80°C is free radical oxidation. The main mechanism under 90°C was found to be chain scission. After combining the changes in macroperformance and microstructure, we concluded that the change in aging mechanism occurred between 80°C and 90°C. |
abstractGer |
A consistent failure mechanism is a precondition for accelerated tests, and the accurate identification of the catastrophe point at which the failure mechanism transforms remains a longstanding challenge in accelerated tests. In this study, an independently designed test apparatus was adopted to monitor the variation in the compressive stress of nitrile butadiene rubber (NBR) samples at different temperatures. The deformation of the samples was controlled as a constant so the variation of the stress could be correlated with the mechanical properties of the NBR. In addition, thermal analysis and infrared spectroscopic analysis were conducted for NBR samples without applying external stresses (e.g., free state) at various elevated temperatures. Samples stored at room temperature for two years were also tested and analyzed to provide a baseline. The results indicate that the stress relaxation mechanism for NBR aged at 80°C differs from that for samples aged at 90°C. The dominating aging mechanism for NBR samples stored at room temperature and accelerated at 80°C is free radical oxidation. The main mechanism under 90°C was found to be chain scission. After combining the changes in macroperformance and microstructure, we concluded that the change in aging mechanism occurred between 80°C and 90°C. |
abstract_unstemmed |
A consistent failure mechanism is a precondition for accelerated tests, and the accurate identification of the catastrophe point at which the failure mechanism transforms remains a longstanding challenge in accelerated tests. In this study, an independently designed test apparatus was adopted to monitor the variation in the compressive stress of nitrile butadiene rubber (NBR) samples at different temperatures. The deformation of the samples was controlled as a constant so the variation of the stress could be correlated with the mechanical properties of the NBR. In addition, thermal analysis and infrared spectroscopic analysis were conducted for NBR samples without applying external stresses (e.g., free state) at various elevated temperatures. Samples stored at room temperature for two years were also tested and analyzed to provide a baseline. The results indicate that the stress relaxation mechanism for NBR aged at 80°C differs from that for samples aged at 90°C. The dominating aging mechanism for NBR samples stored at room temperature and accelerated at 80°C is free radical oxidation. The main mechanism under 90°C was found to be chain scission. After combining the changes in macroperformance and microstructure, we concluded that the change in aging mechanism occurred between 80°C and 90°C. |
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title_short |
Identification of Failure Mechanism Consistency for NBR Accelerated Test |
url |
http://dx.doi.org/10.1520/JTE20130252 http://www.astm.org/DIGITAL_LIBRARY/JOURNALS/TESTEVAL/PAGES/JTE20130252.htm |
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author2 |
Zhang, Weifang Fang, Xiaotong Tang, Qingyun |
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Zhang, Weifang Fang, Xiaotong Tang, Qingyun |
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