Synthesis of silane oligomers containing vinyl and epoxy group for improving the adhesion of addition-cure silicone encapsulant

Two types of silane oligomers containing vinyl and epoxy group (PTGM and PTGE) as adhesion promoters were synthesized by the reaction of trimethylolpropane monoallyl ether with 3-glycidoxypropylmethyldimethoxysilane and 3-glycidoxypropylmethyldiethoxysilane, respectively. Fourier transform infrared...
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Autor*in:	Lai, Xuejun [verfasserIn] Li, Hongqiang Zeng, Xingrong Pan, Kexue

Format:	Artikel
Sprache:	Englisch

Erschienen:	2016

Rechteinformationen:	Nutzungsrecht: © 2016 Taylor & Francis 2016

Schlagwörter:	Silane oligomers containing vinyl and epoxy group addition-cure adhesion promoter silicone encapsulant

Übergeordnetes Werk:	Enthalten in: Journal of adhesion science and technology - Utrecht : VNU Science Press, 1987, 30(2016), 10, Seite 1131
Übergeordnetes Werk:	volume:30 ; year:2016 ; number:10 ; pages:1131

Links:	Volltext Link aufrufen Link aufrufen

DOI / URN:	10.1080/01694243.2016.1142806

Katalog-ID:	OLC197205256X

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520			\|a Two types of silane oligomers containing vinyl and epoxy group (PTGM and PTGE) as adhesion promoters were synthesized by the reaction of trimethylolpropane monoallyl ether with 3-glycidoxypropylmethyldimethoxysilane and 3-glycidoxypropylmethyldiethoxysilane, respectively. Fourier transform infrared spectroscopy, 1 H nuclear magnetic resonance spectroscopy, and gel permeation chromatography were used to characterize their chemical structures. The effect of adhesion promoters on properties of addition-cure silicone encapsulant (ASE) with lots of alumina (Al 2 O 3 ) particles as thermally conductive fillers was investigated. The results showed that PTGM and PTGE could significantly improve both the adhesive strength and mechanical properties of ASE. The viscosity of ASE with no more than 3.0 phr PTGM and PTGE was below 5000 mPa s so that they were suitable for encapsulating process. Observation using scanning electron microscopy revealed that PTGM and PTGE could improve the dispersion of Al 2 O 3 particles in silicone rubber matrix and enhance the bond between the particles and the matrix.
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allfields	10.1080/01694243.2016.1142806 doi PQ20160307 (DE-627)OLC197205256X (DE-599)GBVOLC197205256X (PRQ)i1088-fa432daf28f869056fd3e16594b63270c23df48d10d14dc1da7aa72fe4040f300 (KEY)0153492020160000030001001131synthesisofsilaneoligomerscontainingvinylandepoxyg DE-627 ger DE-627 rakwb eng 530 DNB 33.68 bkl 52.82 bkl 51.20 bkl 58.29 bkl Lai, Xuejun verfasserin aut Synthesis of silane oligomers containing vinyl and epoxy group for improving the adhesion of addition-cure silicone encapsulant 2016 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier Two types of silane oligomers containing vinyl and epoxy group (PTGM and PTGE) as adhesion promoters were synthesized by the reaction of trimethylolpropane monoallyl ether with 3-glycidoxypropylmethyldimethoxysilane and 3-glycidoxypropylmethyldiethoxysilane, respectively. Fourier transform infrared spectroscopy, 1 H nuclear magnetic resonance spectroscopy, and gel permeation chromatography were used to characterize their chemical structures. The effect of adhesion promoters on properties of addition-cure silicone encapsulant (ASE) with lots of alumina (Al 2 O 3 ) particles as thermally conductive fillers was investigated. The results showed that PTGM and PTGE could significantly improve both the adhesive strength and mechanical properties of ASE. The viscosity of ASE with no more than 3.0 phr PTGM and PTGE was below 5000 mPa s so that they were suitable for encapsulating process. Observation using scanning electron microscopy revealed that PTGM and PTGE could improve the dispersion of Al 2 O 3 particles in silicone rubber matrix and enhance the bond between the particles and the matrix. Nutzungsrecht: © 2016 Taylor & Francis 2016 Silane oligomers containing vinyl and epoxy group addition-cure adhesion promoter silicone encapsulant Li, Hongqiang oth Zeng, Xingrong oth Pan, Kexue oth Enthalten in Journal of adhesion science and technology Utrecht : VNU Science Press, 1987 30(2016), 10, Seite 1131 (DE-627)129232998 (DE-600)57687-6 (DE-576)028404866 0169-4243 nnns volume:30 year:2016 number:10 pages:1131 http://dx.doi.org/10.1080/01694243.2016.1142806 Volltext http://www.tandfonline.com/doi/abs/10.1080/01694243.2016.1142806 http://search.proquest.com/docview/1765606194 GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-PHY SSG-OLC-CHE SSG-OLC-PHA SSG-OLC-DE-84 GBV_ILN_70 33.68 AVZ 52.82 AVZ 51.20 AVZ 58.29 AVZ AR 30 2016 10 1131
spelling	10.1080/01694243.2016.1142806 doi PQ20160307 (DE-627)OLC197205256X (DE-599)GBVOLC197205256X (PRQ)i1088-fa432daf28f869056fd3e16594b63270c23df48d10d14dc1da7aa72fe4040f300 (KEY)0153492020160000030001001131synthesisofsilaneoligomerscontainingvinylandepoxyg DE-627 ger DE-627 rakwb eng 530 DNB 33.68 bkl 52.82 bkl 51.20 bkl 58.29 bkl Lai, Xuejun verfasserin aut Synthesis of silane oligomers containing vinyl and epoxy group for improving the adhesion of addition-cure silicone encapsulant 2016 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier Two types of silane oligomers containing vinyl and epoxy group (PTGM and PTGE) as adhesion promoters were synthesized by the reaction of trimethylolpropane monoallyl ether with 3-glycidoxypropylmethyldimethoxysilane and 3-glycidoxypropylmethyldiethoxysilane, respectively. Fourier transform infrared spectroscopy, 1 H nuclear magnetic resonance spectroscopy, and gel permeation chromatography were used to characterize their chemical structures. The effect of adhesion promoters on properties of addition-cure silicone encapsulant (ASE) with lots of alumina (Al 2 O 3 ) particles as thermally conductive fillers was investigated. The results showed that PTGM and PTGE could significantly improve both the adhesive strength and mechanical properties of ASE. The viscosity of ASE with no more than 3.0 phr PTGM and PTGE was below 5000 mPa s so that they were suitable for encapsulating process. Observation using scanning electron microscopy revealed that PTGM and PTGE could improve the dispersion of Al 2 O 3 particles in silicone rubber matrix and enhance the bond between the particles and the matrix. Nutzungsrecht: © 2016 Taylor & Francis 2016 Silane oligomers containing vinyl and epoxy group addition-cure adhesion promoter silicone encapsulant Li, Hongqiang oth Zeng, Xingrong oth Pan, Kexue oth Enthalten in Journal of adhesion science and technology Utrecht : VNU Science Press, 1987 30(2016), 10, Seite 1131 (DE-627)129232998 (DE-600)57687-6 (DE-576)028404866 0169-4243 nnns volume:30 year:2016 number:10 pages:1131 http://dx.doi.org/10.1080/01694243.2016.1142806 Volltext http://www.tandfonline.com/doi/abs/10.1080/01694243.2016.1142806 http://search.proquest.com/docview/1765606194 GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-PHY SSG-OLC-CHE SSG-OLC-PHA SSG-OLC-DE-84 GBV_ILN_70 33.68 AVZ 52.82 AVZ 51.20 AVZ 58.29 AVZ AR 30 2016 10 1131
allfields_unstemmed	10.1080/01694243.2016.1142806 doi PQ20160307 (DE-627)OLC197205256X (DE-599)GBVOLC197205256X (PRQ)i1088-fa432daf28f869056fd3e16594b63270c23df48d10d14dc1da7aa72fe4040f300 (KEY)0153492020160000030001001131synthesisofsilaneoligomerscontainingvinylandepoxyg DE-627 ger DE-627 rakwb eng 530 DNB 33.68 bkl 52.82 bkl 51.20 bkl 58.29 bkl Lai, Xuejun verfasserin aut Synthesis of silane oligomers containing vinyl and epoxy group for improving the adhesion of addition-cure silicone encapsulant 2016 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier Two types of silane oligomers containing vinyl and epoxy group (PTGM and PTGE) as adhesion promoters were synthesized by the reaction of trimethylolpropane monoallyl ether with 3-glycidoxypropylmethyldimethoxysilane and 3-glycidoxypropylmethyldiethoxysilane, respectively. Fourier transform infrared spectroscopy, 1 H nuclear magnetic resonance spectroscopy, and gel permeation chromatography were used to characterize their chemical structures. The effect of adhesion promoters on properties of addition-cure silicone encapsulant (ASE) with lots of alumina (Al 2 O 3 ) particles as thermally conductive fillers was investigated. The results showed that PTGM and PTGE could significantly improve both the adhesive strength and mechanical properties of ASE. The viscosity of ASE with no more than 3.0 phr PTGM and PTGE was below 5000 mPa s so that they were suitable for encapsulating process. Observation using scanning electron microscopy revealed that PTGM and PTGE could improve the dispersion of Al 2 O 3 particles in silicone rubber matrix and enhance the bond between the particles and the matrix. Nutzungsrecht: © 2016 Taylor & Francis 2016 Silane oligomers containing vinyl and epoxy group addition-cure adhesion promoter silicone encapsulant Li, Hongqiang oth Zeng, Xingrong oth Pan, Kexue oth Enthalten in Journal of adhesion science and technology Utrecht : VNU Science Press, 1987 30(2016), 10, Seite 1131 (DE-627)129232998 (DE-600)57687-6 (DE-576)028404866 0169-4243 nnns volume:30 year:2016 number:10 pages:1131 http://dx.doi.org/10.1080/01694243.2016.1142806 Volltext http://www.tandfonline.com/doi/abs/10.1080/01694243.2016.1142806 http://search.proquest.com/docview/1765606194 GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-PHY SSG-OLC-CHE SSG-OLC-PHA SSG-OLC-DE-84 GBV_ILN_70 33.68 AVZ 52.82 AVZ 51.20 AVZ 58.29 AVZ AR 30 2016 10 1131
allfieldsGer	10.1080/01694243.2016.1142806 doi PQ20160307 (DE-627)OLC197205256X (DE-599)GBVOLC197205256X (PRQ)i1088-fa432daf28f869056fd3e16594b63270c23df48d10d14dc1da7aa72fe4040f300 (KEY)0153492020160000030001001131synthesisofsilaneoligomerscontainingvinylandepoxyg DE-627 ger DE-627 rakwb eng 530 DNB 33.68 bkl 52.82 bkl 51.20 bkl 58.29 bkl Lai, Xuejun verfasserin aut Synthesis of silane oligomers containing vinyl and epoxy group for improving the adhesion of addition-cure silicone encapsulant 2016 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier Two types of silane oligomers containing vinyl and epoxy group (PTGM and PTGE) as adhesion promoters were synthesized by the reaction of trimethylolpropane monoallyl ether with 3-glycidoxypropylmethyldimethoxysilane and 3-glycidoxypropylmethyldiethoxysilane, respectively. Fourier transform infrared spectroscopy, 1 H nuclear magnetic resonance spectroscopy, and gel permeation chromatography were used to characterize their chemical structures. The effect of adhesion promoters on properties of addition-cure silicone encapsulant (ASE) with lots of alumina (Al 2 O 3 ) particles as thermally conductive fillers was investigated. The results showed that PTGM and PTGE could significantly improve both the adhesive strength and mechanical properties of ASE. The viscosity of ASE with no more than 3.0 phr PTGM and PTGE was below 5000 mPa s so that they were suitable for encapsulating process. Observation using scanning electron microscopy revealed that PTGM and PTGE could improve the dispersion of Al 2 O 3 particles in silicone rubber matrix and enhance the bond between the particles and the matrix. Nutzungsrecht: © 2016 Taylor & Francis 2016 Silane oligomers containing vinyl and epoxy group addition-cure adhesion promoter silicone encapsulant Li, Hongqiang oth Zeng, Xingrong oth Pan, Kexue oth Enthalten in Journal of adhesion science and technology Utrecht : VNU Science Press, 1987 30(2016), 10, Seite 1131 (DE-627)129232998 (DE-600)57687-6 (DE-576)028404866 0169-4243 nnns volume:30 year:2016 number:10 pages:1131 http://dx.doi.org/10.1080/01694243.2016.1142806 Volltext http://www.tandfonline.com/doi/abs/10.1080/01694243.2016.1142806 http://search.proquest.com/docview/1765606194 GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-PHY SSG-OLC-CHE SSG-OLC-PHA SSG-OLC-DE-84 GBV_ILN_70 33.68 AVZ 52.82 AVZ 51.20 AVZ 58.29 AVZ AR 30 2016 10 1131
allfieldsSound	10.1080/01694243.2016.1142806 doi PQ20160307 (DE-627)OLC197205256X (DE-599)GBVOLC197205256X (PRQ)i1088-fa432daf28f869056fd3e16594b63270c23df48d10d14dc1da7aa72fe4040f300 (KEY)0153492020160000030001001131synthesisofsilaneoligomerscontainingvinylandepoxyg DE-627 ger DE-627 rakwb eng 530 DNB 33.68 bkl 52.82 bkl 51.20 bkl 58.29 bkl Lai, Xuejun verfasserin aut Synthesis of silane oligomers containing vinyl and epoxy group for improving the adhesion of addition-cure silicone encapsulant 2016 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier Two types of silane oligomers containing vinyl and epoxy group (PTGM and PTGE) as adhesion promoters were synthesized by the reaction of trimethylolpropane monoallyl ether with 3-glycidoxypropylmethyldimethoxysilane and 3-glycidoxypropylmethyldiethoxysilane, respectively. Fourier transform infrared spectroscopy, 1 H nuclear magnetic resonance spectroscopy, and gel permeation chromatography were used to characterize their chemical structures. The effect of adhesion promoters on properties of addition-cure silicone encapsulant (ASE) with lots of alumina (Al 2 O 3 ) particles as thermally conductive fillers was investigated. The results showed that PTGM and PTGE could significantly improve both the adhesive strength and mechanical properties of ASE. The viscosity of ASE with no more than 3.0 phr PTGM and PTGE was below 5000 mPa s so that they were suitable for encapsulating process. Observation using scanning electron microscopy revealed that PTGM and PTGE could improve the dispersion of Al 2 O 3 particles in silicone rubber matrix and enhance the bond between the particles and the matrix. Nutzungsrecht: © 2016 Taylor & Francis 2016 Silane oligomers containing vinyl and epoxy group addition-cure adhesion promoter silicone encapsulant Li, Hongqiang oth Zeng, Xingrong oth Pan, Kexue oth Enthalten in Journal of adhesion science and technology Utrecht : VNU Science Press, 1987 30(2016), 10, Seite 1131 (DE-627)129232998 (DE-600)57687-6 (DE-576)028404866 0169-4243 nnns volume:30 year:2016 number:10 pages:1131 http://dx.doi.org/10.1080/01694243.2016.1142806 Volltext http://www.tandfonline.com/doi/abs/10.1080/01694243.2016.1142806 http://search.proquest.com/docview/1765606194 GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-PHY SSG-OLC-CHE SSG-OLC-PHA SSG-OLC-DE-84 GBV_ILN_70 33.68 AVZ 52.82 AVZ 51.20 AVZ 58.29 AVZ AR 30 2016 10 1131
language	English
source	Enthalten in Journal of adhesion science and technology 30(2016), 10, Seite 1131 volume:30 year:2016 number:10 pages:1131
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topic_facet	Silane oligomers containing vinyl and epoxy group addition-cure adhesion promoter silicone encapsulant
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author	Lai, Xuejun
spellingShingle	Lai, Xuejun ddc 530 bkl 33.68 bkl 52.82 bkl 51.20 bkl 58.29 misc Silane oligomers containing vinyl and epoxy group misc addition-cure misc adhesion promoter misc silicone encapsulant Synthesis of silane oligomers containing vinyl and epoxy group for improving the adhesion of addition-cure silicone encapsulant
authorStr	Lai, Xuejun
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topic_title	530 DNB 33.68 bkl 52.82 bkl 51.20 bkl 58.29 bkl Synthesis of silane oligomers containing vinyl and epoxy group for improving the adhesion of addition-cure silicone encapsulant Silane oligomers containing vinyl and epoxy group addition-cure adhesion promoter silicone encapsulant
topic	ddc 530 bkl 33.68 bkl 52.82 bkl 51.20 bkl 58.29 misc Silane oligomers containing vinyl and epoxy group misc addition-cure misc adhesion promoter misc silicone encapsulant
topic_unstemmed	ddc 530 bkl 33.68 bkl 52.82 bkl 51.20 bkl 58.29 misc Silane oligomers containing vinyl and epoxy group misc addition-cure misc adhesion promoter misc silicone encapsulant
topic_browse	ddc 530 bkl 33.68 bkl 52.82 bkl 51.20 bkl 58.29 misc Silane oligomers containing vinyl and epoxy group misc addition-cure misc adhesion promoter misc silicone encapsulant
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title	Synthesis of silane oligomers containing vinyl and epoxy group for improving the adhesion of addition-cure silicone encapsulant
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title_full	Synthesis of silane oligomers containing vinyl and epoxy group for improving the adhesion of addition-cure silicone encapsulant
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title_sort	synthesis of silane oligomers containing vinyl and epoxy group for improving the adhesion of addition-cure silicone encapsulant
title_auth	Synthesis of silane oligomers containing vinyl and epoxy group for improving the adhesion of addition-cure silicone encapsulant
abstract	Two types of silane oligomers containing vinyl and epoxy group (PTGM and PTGE) as adhesion promoters were synthesized by the reaction of trimethylolpropane monoallyl ether with 3-glycidoxypropylmethyldimethoxysilane and 3-glycidoxypropylmethyldiethoxysilane, respectively. Fourier transform infrared spectroscopy, 1 H nuclear magnetic resonance spectroscopy, and gel permeation chromatography were used to characterize their chemical structures. The effect of adhesion promoters on properties of addition-cure silicone encapsulant (ASE) with lots of alumina (Al 2 O 3 ) particles as thermally conductive fillers was investigated. The results showed that PTGM and PTGE could significantly improve both the adhesive strength and mechanical properties of ASE. The viscosity of ASE with no more than 3.0 phr PTGM and PTGE was below 5000 mPa s so that they were suitable for encapsulating process. Observation using scanning electron microscopy revealed that PTGM and PTGE could improve the dispersion of Al 2 O 3 particles in silicone rubber matrix and enhance the bond between the particles and the matrix.
abstractGer	Two types of silane oligomers containing vinyl and epoxy group (PTGM and PTGE) as adhesion promoters were synthesized by the reaction of trimethylolpropane monoallyl ether with 3-glycidoxypropylmethyldimethoxysilane and 3-glycidoxypropylmethyldiethoxysilane, respectively. Fourier transform infrared spectroscopy, 1 H nuclear magnetic resonance spectroscopy, and gel permeation chromatography were used to characterize their chemical structures. The effect of adhesion promoters on properties of addition-cure silicone encapsulant (ASE) with lots of alumina (Al 2 O 3 ) particles as thermally conductive fillers was investigated. The results showed that PTGM and PTGE could significantly improve both the adhesive strength and mechanical properties of ASE. The viscosity of ASE with no more than 3.0 phr PTGM and PTGE was below 5000 mPa s so that they were suitable for encapsulating process. Observation using scanning electron microscopy revealed that PTGM and PTGE could improve the dispersion of Al 2 O 3 particles in silicone rubber matrix and enhance the bond between the particles and the matrix.
abstract_unstemmed	Two types of silane oligomers containing vinyl and epoxy group (PTGM and PTGE) as adhesion promoters were synthesized by the reaction of trimethylolpropane monoallyl ether with 3-glycidoxypropylmethyldimethoxysilane and 3-glycidoxypropylmethyldiethoxysilane, respectively. Fourier transform infrared spectroscopy, 1 H nuclear magnetic resonance spectroscopy, and gel permeation chromatography were used to characterize their chemical structures. The effect of adhesion promoters on properties of addition-cure silicone encapsulant (ASE) with lots of alumina (Al 2 O 3 ) particles as thermally conductive fillers was investigated. The results showed that PTGM and PTGE could significantly improve both the adhesive strength and mechanical properties of ASE. The viscosity of ASE with no more than 3.0 phr PTGM and PTGE was below 5000 mPa s so that they were suitable for encapsulating process. Observation using scanning electron microscopy revealed that PTGM and PTGE could improve the dispersion of Al 2 O 3 particles in silicone rubber matrix and enhance the bond between the particles and the matrix.
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container_issue	10
title_short	Synthesis of silane oligomers containing vinyl and epoxy group for improving the adhesion of addition-cure silicone encapsulant
url	http://dx.doi.org/10.1080/01694243.2016.1142806 http://www.tandfonline.com/doi/abs/10.1080/01694243.2016.1142806 http://search.proquest.com/docview/1765606194
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author2	Li, Hongqiang Zeng, Xingrong Pan, Kexue
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up_date	2024-07-03T21:58:58.510Z
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