Synthesis of silane oligomers containing vinyl and epoxy group for improving the adhesion of addition-cure silicone encapsulant
Two types of silane oligomers containing vinyl and epoxy group (PTGM and PTGE) as adhesion promoters were synthesized by the reaction of trimethylolpropane monoallyl ether with 3-glycidoxypropylmethyldimethoxysilane and 3-glycidoxypropylmethyldiethoxysilane, respectively. Fourier transform infrared...
Ausführliche Beschreibung
Autor*in: |
Lai, Xuejun [verfasserIn] |
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Format: |
Artikel |
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Sprache: |
Englisch |
Erschienen: |
2016 |
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Rechteinformationen: |
Nutzungsrecht: © 2016 Taylor & Francis 2016 |
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Schlagwörter: |
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Übergeordnetes Werk: |
Enthalten in: Journal of adhesion science and technology - Utrecht : VNU Science Press, 1987, 30(2016), 10, Seite 1131 |
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Übergeordnetes Werk: |
volume:30 ; year:2016 ; number:10 ; pages:1131 |
Links: |
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DOI / URN: |
10.1080/01694243.2016.1142806 |
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spelling |
10.1080/01694243.2016.1142806 doi PQ20160307 (DE-627)OLC197205256X (DE-599)GBVOLC197205256X (PRQ)i1088-fa432daf28f869056fd3e16594b63270c23df48d10d14dc1da7aa72fe4040f300 (KEY)0153492020160000030001001131synthesisofsilaneoligomerscontainingvinylandepoxyg DE-627 ger DE-627 rakwb eng 530 DNB 33.68 bkl 52.82 bkl 51.20 bkl 58.29 bkl Lai, Xuejun verfasserin aut Synthesis of silane oligomers containing vinyl and epoxy group for improving the adhesion of addition-cure silicone encapsulant 2016 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier Two types of silane oligomers containing vinyl and epoxy group (PTGM and PTGE) as adhesion promoters were synthesized by the reaction of trimethylolpropane monoallyl ether with 3-glycidoxypropylmethyldimethoxysilane and 3-glycidoxypropylmethyldiethoxysilane, respectively. Fourier transform infrared spectroscopy, 1 H nuclear magnetic resonance spectroscopy, and gel permeation chromatography were used to characterize their chemical structures. The effect of adhesion promoters on properties of addition-cure silicone encapsulant (ASE) with lots of alumina (Al 2 O 3 ) particles as thermally conductive fillers was investigated. The results showed that PTGM and PTGE could significantly improve both the adhesive strength and mechanical properties of ASE. The viscosity of ASE with no more than 3.0 phr PTGM and PTGE was below 5000 mPa s so that they were suitable for encapsulating process. Observation using scanning electron microscopy revealed that PTGM and PTGE could improve the dispersion of Al 2 O 3 particles in silicone rubber matrix and enhance the bond between the particles and the matrix. Nutzungsrecht: © 2016 Taylor & Francis 2016 Silane oligomers containing vinyl and epoxy group addition-cure adhesion promoter silicone encapsulant Li, Hongqiang oth Zeng, Xingrong oth Pan, Kexue oth Enthalten in Journal of adhesion science and technology Utrecht : VNU Science Press, 1987 30(2016), 10, Seite 1131 (DE-627)129232998 (DE-600)57687-6 (DE-576)028404866 0169-4243 nnns volume:30 year:2016 number:10 pages:1131 http://dx.doi.org/10.1080/01694243.2016.1142806 Volltext http://www.tandfonline.com/doi/abs/10.1080/01694243.2016.1142806 http://search.proquest.com/docview/1765606194 GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-PHY SSG-OLC-CHE SSG-OLC-PHA SSG-OLC-DE-84 GBV_ILN_70 33.68 AVZ 52.82 AVZ 51.20 AVZ 58.29 AVZ AR 30 2016 10 1131 |
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10.1080/01694243.2016.1142806 doi PQ20160307 (DE-627)OLC197205256X (DE-599)GBVOLC197205256X (PRQ)i1088-fa432daf28f869056fd3e16594b63270c23df48d10d14dc1da7aa72fe4040f300 (KEY)0153492020160000030001001131synthesisofsilaneoligomerscontainingvinylandepoxyg DE-627 ger DE-627 rakwb eng 530 DNB 33.68 bkl 52.82 bkl 51.20 bkl 58.29 bkl Lai, Xuejun verfasserin aut Synthesis of silane oligomers containing vinyl and epoxy group for improving the adhesion of addition-cure silicone encapsulant 2016 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier Two types of silane oligomers containing vinyl and epoxy group (PTGM and PTGE) as adhesion promoters were synthesized by the reaction of trimethylolpropane monoallyl ether with 3-glycidoxypropylmethyldimethoxysilane and 3-glycidoxypropylmethyldiethoxysilane, respectively. Fourier transform infrared spectroscopy, 1 H nuclear magnetic resonance spectroscopy, and gel permeation chromatography were used to characterize their chemical structures. The effect of adhesion promoters on properties of addition-cure silicone encapsulant (ASE) with lots of alumina (Al 2 O 3 ) particles as thermally conductive fillers was investigated. The results showed that PTGM and PTGE could significantly improve both the adhesive strength and mechanical properties of ASE. The viscosity of ASE with no more than 3.0 phr PTGM and PTGE was below 5000 mPa s so that they were suitable for encapsulating process. Observation using scanning electron microscopy revealed that PTGM and PTGE could improve the dispersion of Al 2 O 3 particles in silicone rubber matrix and enhance the bond between the particles and the matrix. Nutzungsrecht: © 2016 Taylor & Francis 2016 Silane oligomers containing vinyl and epoxy group addition-cure adhesion promoter silicone encapsulant Li, Hongqiang oth Zeng, Xingrong oth Pan, Kexue oth Enthalten in Journal of adhesion science and technology Utrecht : VNU Science Press, 1987 30(2016), 10, Seite 1131 (DE-627)129232998 (DE-600)57687-6 (DE-576)028404866 0169-4243 nnns volume:30 year:2016 number:10 pages:1131 http://dx.doi.org/10.1080/01694243.2016.1142806 Volltext http://www.tandfonline.com/doi/abs/10.1080/01694243.2016.1142806 http://search.proquest.com/docview/1765606194 GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-PHY SSG-OLC-CHE SSG-OLC-PHA SSG-OLC-DE-84 GBV_ILN_70 33.68 AVZ 52.82 AVZ 51.20 AVZ 58.29 AVZ AR 30 2016 10 1131 |
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10.1080/01694243.2016.1142806 doi PQ20160307 (DE-627)OLC197205256X (DE-599)GBVOLC197205256X (PRQ)i1088-fa432daf28f869056fd3e16594b63270c23df48d10d14dc1da7aa72fe4040f300 (KEY)0153492020160000030001001131synthesisofsilaneoligomerscontainingvinylandepoxyg DE-627 ger DE-627 rakwb eng 530 DNB 33.68 bkl 52.82 bkl 51.20 bkl 58.29 bkl Lai, Xuejun verfasserin aut Synthesis of silane oligomers containing vinyl and epoxy group for improving the adhesion of addition-cure silicone encapsulant 2016 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier Two types of silane oligomers containing vinyl and epoxy group (PTGM and PTGE) as adhesion promoters were synthesized by the reaction of trimethylolpropane monoallyl ether with 3-glycidoxypropylmethyldimethoxysilane and 3-glycidoxypropylmethyldiethoxysilane, respectively. Fourier transform infrared spectroscopy, 1 H nuclear magnetic resonance spectroscopy, and gel permeation chromatography were used to characterize their chemical structures. The effect of adhesion promoters on properties of addition-cure silicone encapsulant (ASE) with lots of alumina (Al 2 O 3 ) particles as thermally conductive fillers was investigated. The results showed that PTGM and PTGE could significantly improve both the adhesive strength and mechanical properties of ASE. The viscosity of ASE with no more than 3.0 phr PTGM and PTGE was below 5000 mPa s so that they were suitable for encapsulating process. Observation using scanning electron microscopy revealed that PTGM and PTGE could improve the dispersion of Al 2 O 3 particles in silicone rubber matrix and enhance the bond between the particles and the matrix. Nutzungsrecht: © 2016 Taylor & Francis 2016 Silane oligomers containing vinyl and epoxy group addition-cure adhesion promoter silicone encapsulant Li, Hongqiang oth Zeng, Xingrong oth Pan, Kexue oth Enthalten in Journal of adhesion science and technology Utrecht : VNU Science Press, 1987 30(2016), 10, Seite 1131 (DE-627)129232998 (DE-600)57687-6 (DE-576)028404866 0169-4243 nnns volume:30 year:2016 number:10 pages:1131 http://dx.doi.org/10.1080/01694243.2016.1142806 Volltext http://www.tandfonline.com/doi/abs/10.1080/01694243.2016.1142806 http://search.proquest.com/docview/1765606194 GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-PHY SSG-OLC-CHE SSG-OLC-PHA SSG-OLC-DE-84 GBV_ILN_70 33.68 AVZ 52.82 AVZ 51.20 AVZ 58.29 AVZ AR 30 2016 10 1131 |
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10.1080/01694243.2016.1142806 doi PQ20160307 (DE-627)OLC197205256X (DE-599)GBVOLC197205256X (PRQ)i1088-fa432daf28f869056fd3e16594b63270c23df48d10d14dc1da7aa72fe4040f300 (KEY)0153492020160000030001001131synthesisofsilaneoligomerscontainingvinylandepoxyg DE-627 ger DE-627 rakwb eng 530 DNB 33.68 bkl 52.82 bkl 51.20 bkl 58.29 bkl Lai, Xuejun verfasserin aut Synthesis of silane oligomers containing vinyl and epoxy group for improving the adhesion of addition-cure silicone encapsulant 2016 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier Two types of silane oligomers containing vinyl and epoxy group (PTGM and PTGE) as adhesion promoters were synthesized by the reaction of trimethylolpropane monoallyl ether with 3-glycidoxypropylmethyldimethoxysilane and 3-glycidoxypropylmethyldiethoxysilane, respectively. Fourier transform infrared spectroscopy, 1 H nuclear magnetic resonance spectroscopy, and gel permeation chromatography were used to characterize their chemical structures. The effect of adhesion promoters on properties of addition-cure silicone encapsulant (ASE) with lots of alumina (Al 2 O 3 ) particles as thermally conductive fillers was investigated. The results showed that PTGM and PTGE could significantly improve both the adhesive strength and mechanical properties of ASE. The viscosity of ASE with no more than 3.0 phr PTGM and PTGE was below 5000 mPa s so that they were suitable for encapsulating process. Observation using scanning electron microscopy revealed that PTGM and PTGE could improve the dispersion of Al 2 O 3 particles in silicone rubber matrix and enhance the bond between the particles and the matrix. Nutzungsrecht: © 2016 Taylor & Francis 2016 Silane oligomers containing vinyl and epoxy group addition-cure adhesion promoter silicone encapsulant Li, Hongqiang oth Zeng, Xingrong oth Pan, Kexue oth Enthalten in Journal of adhesion science and technology Utrecht : VNU Science Press, 1987 30(2016), 10, Seite 1131 (DE-627)129232998 (DE-600)57687-6 (DE-576)028404866 0169-4243 nnns volume:30 year:2016 number:10 pages:1131 http://dx.doi.org/10.1080/01694243.2016.1142806 Volltext http://www.tandfonline.com/doi/abs/10.1080/01694243.2016.1142806 http://search.proquest.com/docview/1765606194 GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-PHY SSG-OLC-CHE SSG-OLC-PHA SSG-OLC-DE-84 GBV_ILN_70 33.68 AVZ 52.82 AVZ 51.20 AVZ 58.29 AVZ AR 30 2016 10 1131 |
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Lai, Xuejun ddc 530 bkl 33.68 bkl 52.82 bkl 51.20 bkl 58.29 misc Silane oligomers containing vinyl and epoxy group misc addition-cure misc adhesion promoter misc silicone encapsulant Synthesis of silane oligomers containing vinyl and epoxy group for improving the adhesion of addition-cure silicone encapsulant |
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530 DNB 33.68 bkl 52.82 bkl 51.20 bkl 58.29 bkl Synthesis of silane oligomers containing vinyl and epoxy group for improving the adhesion of addition-cure silicone encapsulant Silane oligomers containing vinyl and epoxy group addition-cure adhesion promoter silicone encapsulant |
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Synthesis of silane oligomers containing vinyl and epoxy group for improving the adhesion of addition-cure silicone encapsulant |
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synthesis of silane oligomers containing vinyl and epoxy group for improving the adhesion of addition-cure silicone encapsulant |
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Synthesis of silane oligomers containing vinyl and epoxy group for improving the adhesion of addition-cure silicone encapsulant |
abstract |
Two types of silane oligomers containing vinyl and epoxy group (PTGM and PTGE) as adhesion promoters were synthesized by the reaction of trimethylolpropane monoallyl ether with 3-glycidoxypropylmethyldimethoxysilane and 3-glycidoxypropylmethyldiethoxysilane, respectively. Fourier transform infrared spectroscopy, 1 H nuclear magnetic resonance spectroscopy, and gel permeation chromatography were used to characterize their chemical structures. The effect of adhesion promoters on properties of addition-cure silicone encapsulant (ASE) with lots of alumina (Al 2 O 3 ) particles as thermally conductive fillers was investigated. The results showed that PTGM and PTGE could significantly improve both the adhesive strength and mechanical properties of ASE. The viscosity of ASE with no more than 3.0 phr PTGM and PTGE was below 5000 mPa s so that they were suitable for encapsulating process. Observation using scanning electron microscopy revealed that PTGM and PTGE could improve the dispersion of Al 2 O 3 particles in silicone rubber matrix and enhance the bond between the particles and the matrix. |
abstractGer |
Two types of silane oligomers containing vinyl and epoxy group (PTGM and PTGE) as adhesion promoters were synthesized by the reaction of trimethylolpropane monoallyl ether with 3-glycidoxypropylmethyldimethoxysilane and 3-glycidoxypropylmethyldiethoxysilane, respectively. Fourier transform infrared spectroscopy, 1 H nuclear magnetic resonance spectroscopy, and gel permeation chromatography were used to characterize their chemical structures. The effect of adhesion promoters on properties of addition-cure silicone encapsulant (ASE) with lots of alumina (Al 2 O 3 ) particles as thermally conductive fillers was investigated. The results showed that PTGM and PTGE could significantly improve both the adhesive strength and mechanical properties of ASE. The viscosity of ASE with no more than 3.0 phr PTGM and PTGE was below 5000 mPa s so that they were suitable for encapsulating process. Observation using scanning electron microscopy revealed that PTGM and PTGE could improve the dispersion of Al 2 O 3 particles in silicone rubber matrix and enhance the bond between the particles and the matrix. |
abstract_unstemmed |
Two types of silane oligomers containing vinyl and epoxy group (PTGM and PTGE) as adhesion promoters were synthesized by the reaction of trimethylolpropane monoallyl ether with 3-glycidoxypropylmethyldimethoxysilane and 3-glycidoxypropylmethyldiethoxysilane, respectively. Fourier transform infrared spectroscopy, 1 H nuclear magnetic resonance spectroscopy, and gel permeation chromatography were used to characterize their chemical structures. The effect of adhesion promoters on properties of addition-cure silicone encapsulant (ASE) with lots of alumina (Al 2 O 3 ) particles as thermally conductive fillers was investigated. The results showed that PTGM and PTGE could significantly improve both the adhesive strength and mechanical properties of ASE. The viscosity of ASE with no more than 3.0 phr PTGM and PTGE was below 5000 mPa s so that they were suitable for encapsulating process. Observation using scanning electron microscopy revealed that PTGM and PTGE could improve the dispersion of Al 2 O 3 particles in silicone rubber matrix and enhance the bond between the particles and the matrix. |
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title_short |
Synthesis of silane oligomers containing vinyl and epoxy group for improving the adhesion of addition-cure silicone encapsulant |
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