Formation of Spherical Agglomerates in Cooling Crystallization of Hexahydro‐1,3,5‐trinitro‐1,3,5‐triazine

The production of spherical agglomerates of hexahydro‐1,3,5‐trinitro‐1,3,5‐triazine (RDX) from acetone by cooling crystallization with poly(vinylpyrrolidone) (PVP) is described. It was found that PVP suppresses the nucleation of RDX at the initial stage, but tremendous nucleation of RDX occurred abr...
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Autor*in:	Lee, Jae-Eun [verfasserIn] Kim, Jae-Kyeong Kim, Hyoun-Soo Koo, Kee-Kahb

Format:	Artikel
Sprache:	Englisch

Erschienen:	2017

Rechteinformationen:	Nutzungsrecht: © 2017 WILEY‐VCH Verlag GmbH & Co. KGaA, Weinheim

Schlagwörter:	Nucleation Hexahydro‐1,3,5‐trinitro‐1,3,5‐triazine Poly(vinylpyrrolidone) Cooling crystallization Agglomeration

Übergeordnetes Werk:	Enthalten in: Chemical engineering & technology - Weinheim : Wiley-VCH, 1987, 40(2017), 12, Seite 2197-2203
Übergeordnetes Werk:	volume:40 ; year:2017 ; number:12 ; pages:2197-2203

Links:	Volltext Link aufrufen

DOI / URN:	10.1002/ceat.201700144

Katalog-ID:	OLC1998778479

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520			\|a The production of spherical agglomerates of hexahydro‐1,3,5‐trinitro‐1,3,5‐triazine (RDX) from acetone by cooling crystallization with poly(vinylpyrrolidone) (PVP) is described. It was found that PVP suppresses the nucleation of RDX at the initial stage, but tremendous nucleation of RDX occurred abruptly after the induction period. The rapid nucleation may be associated with the primary nucleation due to the presence of PVP. It can be concluded that the addition of PVP results in the formation of RDX particles with sufficient number density for spherical agglomeration. It was found that such spherical agglomeration propagates very rapidly after nucleation within one minute and the size of spherical agglomerates is affected by the cooling rate. RDX by cooling crystallization from acetone was demonstrated. A proposed mechanism for this process is an extremely rapid nucleation induced due to primary nucleation by a polymeric additive. This rapid nucleation provides a high enough number density of particles for the formation of spherical agglomerates.
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650		4	\|a Nucleation
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650		4	\|a Poly(vinylpyrrolidone)
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650		4	\|a Agglomeration
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allfields	10.1002/ceat.201700144 doi PQ20171228 (DE-627)OLC1998778479 (DE-599)GBVOLC1998778479 (PRQ)wiley_primary_10_1002_ceat_201700144_CEAT2017001443 (KEY)0021869320170000040001202197formationofsphericalagglomeratesincoolingcrystalli DE-627 ger DE-627 rakwb eng 660 DE-101 58.16 bkl 58.17 bkl 58.30 bkl Lee, Jae-Eun verfasserin aut Formation of Spherical Agglomerates in Cooling Crystallization of Hexahydro‐1,3,5‐trinitro‐1,3,5‐triazine 2017 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier The production of spherical agglomerates of hexahydro‐1,3,5‐trinitro‐1,3,5‐triazine (RDX) from acetone by cooling crystallization with poly(vinylpyrrolidone) (PVP) is described. It was found that PVP suppresses the nucleation of RDX at the initial stage, but tremendous nucleation of RDX occurred abruptly after the induction period. The rapid nucleation may be associated with the primary nucleation due to the presence of PVP. It can be concluded that the addition of PVP results in the formation of RDX particles with sufficient number density for spherical agglomeration. It was found that such spherical agglomeration propagates very rapidly after nucleation within one minute and the size of spherical agglomerates is affected by the cooling rate. RDX by cooling crystallization from acetone was demonstrated. A proposed mechanism for this process is an extremely rapid nucleation induced due to primary nucleation by a polymeric additive. This rapid nucleation provides a high enough number density of particles for the formation of spherical agglomerates. Nutzungsrecht: © 2017 WILEY‐VCH Verlag GmbH & Co. KGaA, Weinheim Nucleation Hexahydro‐1,3,5‐trinitro‐1,3,5‐triazine Poly(vinylpyrrolidone) Cooling crystallization Agglomeration Kim, Jae-Kyeong oth Kim, Hyoun-Soo oth Koo, Kee-Kahb oth Enthalten in Chemical engineering & technology Weinheim : Wiley-VCH, 1987 40(2017), 12, Seite 2197-2203 (DE-627)129221465 (DE-600)56471-0 (DE-576)014458179 0930-7516 nnns volume:40 year:2017 number:12 pages:2197-2203 http://dx.doi.org/10.1002/ceat.201700144 Volltext http://onlinelibrary.wiley.com/doi/10.1002/ceat.201700144/abstract GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE SSG-OLC-PHA SSG-OLC-DE-84 58.16 AVZ 58.17 AVZ 58.30 AVZ AR 40 2017 12 2197-2203
spelling	10.1002/ceat.201700144 doi PQ20171228 (DE-627)OLC1998778479 (DE-599)GBVOLC1998778479 (PRQ)wiley_primary_10_1002_ceat_201700144_CEAT2017001443 (KEY)0021869320170000040001202197formationofsphericalagglomeratesincoolingcrystalli DE-627 ger DE-627 rakwb eng 660 DE-101 58.16 bkl 58.17 bkl 58.30 bkl Lee, Jae-Eun verfasserin aut Formation of Spherical Agglomerates in Cooling Crystallization of Hexahydro‐1,3,5‐trinitro‐1,3,5‐triazine 2017 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier The production of spherical agglomerates of hexahydro‐1,3,5‐trinitro‐1,3,5‐triazine (RDX) from acetone by cooling crystallization with poly(vinylpyrrolidone) (PVP) is described. It was found that PVP suppresses the nucleation of RDX at the initial stage, but tremendous nucleation of RDX occurred abruptly after the induction period. The rapid nucleation may be associated with the primary nucleation due to the presence of PVP. It can be concluded that the addition of PVP results in the formation of RDX particles with sufficient number density for spherical agglomeration. It was found that such spherical agglomeration propagates very rapidly after nucleation within one minute and the size of spherical agglomerates is affected by the cooling rate. RDX by cooling crystallization from acetone was demonstrated. A proposed mechanism for this process is an extremely rapid nucleation induced due to primary nucleation by a polymeric additive. This rapid nucleation provides a high enough number density of particles for the formation of spherical agglomerates. Nutzungsrecht: © 2017 WILEY‐VCH Verlag GmbH & Co. KGaA, Weinheim Nucleation Hexahydro‐1,3,5‐trinitro‐1,3,5‐triazine Poly(vinylpyrrolidone) Cooling crystallization Agglomeration Kim, Jae-Kyeong oth Kim, Hyoun-Soo oth Koo, Kee-Kahb oth Enthalten in Chemical engineering & technology Weinheim : Wiley-VCH, 1987 40(2017), 12, Seite 2197-2203 (DE-627)129221465 (DE-600)56471-0 (DE-576)014458179 0930-7516 nnns volume:40 year:2017 number:12 pages:2197-2203 http://dx.doi.org/10.1002/ceat.201700144 Volltext http://onlinelibrary.wiley.com/doi/10.1002/ceat.201700144/abstract GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE SSG-OLC-PHA SSG-OLC-DE-84 58.16 AVZ 58.17 AVZ 58.30 AVZ AR 40 2017 12 2197-2203
allfields_unstemmed	10.1002/ceat.201700144 doi PQ20171228 (DE-627)OLC1998778479 (DE-599)GBVOLC1998778479 (PRQ)wiley_primary_10_1002_ceat_201700144_CEAT2017001443 (KEY)0021869320170000040001202197formationofsphericalagglomeratesincoolingcrystalli DE-627 ger DE-627 rakwb eng 660 DE-101 58.16 bkl 58.17 bkl 58.30 bkl Lee, Jae-Eun verfasserin aut Formation of Spherical Agglomerates in Cooling Crystallization of Hexahydro‐1,3,5‐trinitro‐1,3,5‐triazine 2017 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier The production of spherical agglomerates of hexahydro‐1,3,5‐trinitro‐1,3,5‐triazine (RDX) from acetone by cooling crystallization with poly(vinylpyrrolidone) (PVP) is described. It was found that PVP suppresses the nucleation of RDX at the initial stage, but tremendous nucleation of RDX occurred abruptly after the induction period. The rapid nucleation may be associated with the primary nucleation due to the presence of PVP. It can be concluded that the addition of PVP results in the formation of RDX particles with sufficient number density for spherical agglomeration. It was found that such spherical agglomeration propagates very rapidly after nucleation within one minute and the size of spherical agglomerates is affected by the cooling rate. RDX by cooling crystallization from acetone was demonstrated. A proposed mechanism for this process is an extremely rapid nucleation induced due to primary nucleation by a polymeric additive. This rapid nucleation provides a high enough number density of particles for the formation of spherical agglomerates. Nutzungsrecht: © 2017 WILEY‐VCH Verlag GmbH & Co. KGaA, Weinheim Nucleation Hexahydro‐1,3,5‐trinitro‐1,3,5‐triazine Poly(vinylpyrrolidone) Cooling crystallization Agglomeration Kim, Jae-Kyeong oth Kim, Hyoun-Soo oth Koo, Kee-Kahb oth Enthalten in Chemical engineering & technology Weinheim : Wiley-VCH, 1987 40(2017), 12, Seite 2197-2203 (DE-627)129221465 (DE-600)56471-0 (DE-576)014458179 0930-7516 nnns volume:40 year:2017 number:12 pages:2197-2203 http://dx.doi.org/10.1002/ceat.201700144 Volltext http://onlinelibrary.wiley.com/doi/10.1002/ceat.201700144/abstract GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE SSG-OLC-PHA SSG-OLC-DE-84 58.16 AVZ 58.17 AVZ 58.30 AVZ AR 40 2017 12 2197-2203
allfieldsGer	10.1002/ceat.201700144 doi PQ20171228 (DE-627)OLC1998778479 (DE-599)GBVOLC1998778479 (PRQ)wiley_primary_10_1002_ceat_201700144_CEAT2017001443 (KEY)0021869320170000040001202197formationofsphericalagglomeratesincoolingcrystalli DE-627 ger DE-627 rakwb eng 660 DE-101 58.16 bkl 58.17 bkl 58.30 bkl Lee, Jae-Eun verfasserin aut Formation of Spherical Agglomerates in Cooling Crystallization of Hexahydro‐1,3,5‐trinitro‐1,3,5‐triazine 2017 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier The production of spherical agglomerates of hexahydro‐1,3,5‐trinitro‐1,3,5‐triazine (RDX) from acetone by cooling crystallization with poly(vinylpyrrolidone) (PVP) is described. It was found that PVP suppresses the nucleation of RDX at the initial stage, but tremendous nucleation of RDX occurred abruptly after the induction period. The rapid nucleation may be associated with the primary nucleation due to the presence of PVP. It can be concluded that the addition of PVP results in the formation of RDX particles with sufficient number density for spherical agglomeration. It was found that such spherical agglomeration propagates very rapidly after nucleation within one minute and the size of spherical agglomerates is affected by the cooling rate. RDX by cooling crystallization from acetone was demonstrated. A proposed mechanism for this process is an extremely rapid nucleation induced due to primary nucleation by a polymeric additive. This rapid nucleation provides a high enough number density of particles for the formation of spherical agglomerates. Nutzungsrecht: © 2017 WILEY‐VCH Verlag GmbH & Co. KGaA, Weinheim Nucleation Hexahydro‐1,3,5‐trinitro‐1,3,5‐triazine Poly(vinylpyrrolidone) Cooling crystallization Agglomeration Kim, Jae-Kyeong oth Kim, Hyoun-Soo oth Koo, Kee-Kahb oth Enthalten in Chemical engineering & technology Weinheim : Wiley-VCH, 1987 40(2017), 12, Seite 2197-2203 (DE-627)129221465 (DE-600)56471-0 (DE-576)014458179 0930-7516 nnns volume:40 year:2017 number:12 pages:2197-2203 http://dx.doi.org/10.1002/ceat.201700144 Volltext http://onlinelibrary.wiley.com/doi/10.1002/ceat.201700144/abstract GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE SSG-OLC-PHA SSG-OLC-DE-84 58.16 AVZ 58.17 AVZ 58.30 AVZ AR 40 2017 12 2197-2203
allfieldsSound	10.1002/ceat.201700144 doi PQ20171228 (DE-627)OLC1998778479 (DE-599)GBVOLC1998778479 (PRQ)wiley_primary_10_1002_ceat_201700144_CEAT2017001443 (KEY)0021869320170000040001202197formationofsphericalagglomeratesincoolingcrystalli DE-627 ger DE-627 rakwb eng 660 DE-101 58.16 bkl 58.17 bkl 58.30 bkl Lee, Jae-Eun verfasserin aut Formation of Spherical Agglomerates in Cooling Crystallization of Hexahydro‐1,3,5‐trinitro‐1,3,5‐triazine 2017 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier The production of spherical agglomerates of hexahydro‐1,3,5‐trinitro‐1,3,5‐triazine (RDX) from acetone by cooling crystallization with poly(vinylpyrrolidone) (PVP) is described. It was found that PVP suppresses the nucleation of RDX at the initial stage, but tremendous nucleation of RDX occurred abruptly after the induction period. The rapid nucleation may be associated with the primary nucleation due to the presence of PVP. It can be concluded that the addition of PVP results in the formation of RDX particles with sufficient number density for spherical agglomeration. It was found that such spherical agglomeration propagates very rapidly after nucleation within one minute and the size of spherical agglomerates is affected by the cooling rate. RDX by cooling crystallization from acetone was demonstrated. A proposed mechanism for this process is an extremely rapid nucleation induced due to primary nucleation by a polymeric additive. This rapid nucleation provides a high enough number density of particles for the formation of spherical agglomerates. Nutzungsrecht: © 2017 WILEY‐VCH Verlag GmbH & Co. KGaA, Weinheim Nucleation Hexahydro‐1,3,5‐trinitro‐1,3,5‐triazine Poly(vinylpyrrolidone) Cooling crystallization Agglomeration Kim, Jae-Kyeong oth Kim, Hyoun-Soo oth Koo, Kee-Kahb oth Enthalten in Chemical engineering & technology Weinheim : Wiley-VCH, 1987 40(2017), 12, Seite 2197-2203 (DE-627)129221465 (DE-600)56471-0 (DE-576)014458179 0930-7516 nnns volume:40 year:2017 number:12 pages:2197-2203 http://dx.doi.org/10.1002/ceat.201700144 Volltext http://onlinelibrary.wiley.com/doi/10.1002/ceat.201700144/abstract GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE SSG-OLC-PHA SSG-OLC-DE-84 58.16 AVZ 58.17 AVZ 58.30 AVZ AR 40 2017 12 2197-2203
language	English
source	Enthalten in Chemical engineering & technology 40(2017), 12, Seite 2197-2203 volume:40 year:2017 number:12 pages:2197-2203
sourceStr	Enthalten in Chemical engineering & technology 40(2017), 12, Seite 2197-2203 volume:40 year:2017 number:12 pages:2197-2203
format_phy_str_mv	Article
institution	findex.gbv.de
topic_facet	Nucleation Hexahydro‐1,3,5‐trinitro‐1,3,5‐triazine Poly(vinylpyrrolidone) Cooling crystallization Agglomeration
dewey-raw	660
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author	Lee, Jae-Eun
spellingShingle	Lee, Jae-Eun ddc 660 bkl 58.16 bkl 58.17 bkl 58.30 misc Nucleation misc Hexahydro‐1,3,5‐trinitro‐1,3,5‐triazine misc Poly(vinylpyrrolidone) misc Cooling crystallization misc Agglomeration Formation of Spherical Agglomerates in Cooling Crystallization of Hexahydro‐1,3,5‐trinitro‐1,3,5‐triazine
authorStr	Lee, Jae-Eun
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topic_title	660 DE-101 58.16 bkl 58.17 bkl 58.30 bkl Formation of Spherical Agglomerates in Cooling Crystallization of Hexahydro‐1,3,5‐trinitro‐1,3,5‐triazine Nucleation Hexahydro‐1,3,5‐trinitro‐1,3,5‐triazine Poly(vinylpyrrolidone) Cooling crystallization Agglomeration
topic	ddc 660 bkl 58.16 bkl 58.17 bkl 58.30 misc Nucleation misc Hexahydro‐1,3,5‐trinitro‐1,3,5‐triazine misc Poly(vinylpyrrolidone) misc Cooling crystallization misc Agglomeration
topic_unstemmed	ddc 660 bkl 58.16 bkl 58.17 bkl 58.30 misc Nucleation misc Hexahydro‐1,3,5‐trinitro‐1,3,5‐triazine misc Poly(vinylpyrrolidone) misc Cooling crystallization misc Agglomeration
topic_browse	ddc 660 bkl 58.16 bkl 58.17 bkl 58.30 misc Nucleation misc Hexahydro‐1,3,5‐trinitro‐1,3,5‐triazine misc Poly(vinylpyrrolidone) misc Cooling crystallization misc Agglomeration
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title	Formation of Spherical Agglomerates in Cooling Crystallization of Hexahydro‐1,3,5‐trinitro‐1,3,5‐triazine
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title_full	Formation of Spherical Agglomerates in Cooling Crystallization of Hexahydro‐1,3,5‐trinitro‐1,3,5‐triazine
author_sort	Lee, Jae-Eun
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title_sort	formation of spherical agglomerates in cooling crystallization of hexahydro‐1,3,5‐trinitro‐1,3,5‐triazine
title_auth	Formation of Spherical Agglomerates in Cooling Crystallization of Hexahydro‐1,3,5‐trinitro‐1,3,5‐triazine
abstract	The production of spherical agglomerates of hexahydro‐1,3,5‐trinitro‐1,3,5‐triazine (RDX) from acetone by cooling crystallization with poly(vinylpyrrolidone) (PVP) is described. It was found that PVP suppresses the nucleation of RDX at the initial stage, but tremendous nucleation of RDX occurred abruptly after the induction period. The rapid nucleation may be associated with the primary nucleation due to the presence of PVP. It can be concluded that the addition of PVP results in the formation of RDX particles with sufficient number density for spherical agglomeration. It was found that such spherical agglomeration propagates very rapidly after nucleation within one minute and the size of spherical agglomerates is affected by the cooling rate. RDX by cooling crystallization from acetone was demonstrated. A proposed mechanism for this process is an extremely rapid nucleation induced due to primary nucleation by a polymeric additive. This rapid nucleation provides a high enough number density of particles for the formation of spherical agglomerates.
abstractGer	The production of spherical agglomerates of hexahydro‐1,3,5‐trinitro‐1,3,5‐triazine (RDX) from acetone by cooling crystallization with poly(vinylpyrrolidone) (PVP) is described. It was found that PVP suppresses the nucleation of RDX at the initial stage, but tremendous nucleation of RDX occurred abruptly after the induction period. The rapid nucleation may be associated with the primary nucleation due to the presence of PVP. It can be concluded that the addition of PVP results in the formation of RDX particles with sufficient number density for spherical agglomeration. It was found that such spherical agglomeration propagates very rapidly after nucleation within one minute and the size of spherical agglomerates is affected by the cooling rate. RDX by cooling crystallization from acetone was demonstrated. A proposed mechanism for this process is an extremely rapid nucleation induced due to primary nucleation by a polymeric additive. This rapid nucleation provides a high enough number density of particles for the formation of spherical agglomerates.
abstract_unstemmed	The production of spherical agglomerates of hexahydro‐1,3,5‐trinitro‐1,3,5‐triazine (RDX) from acetone by cooling crystallization with poly(vinylpyrrolidone) (PVP) is described. It was found that PVP suppresses the nucleation of RDX at the initial stage, but tremendous nucleation of RDX occurred abruptly after the induction period. The rapid nucleation may be associated with the primary nucleation due to the presence of PVP. It can be concluded that the addition of PVP results in the formation of RDX particles with sufficient number density for spherical agglomeration. It was found that such spherical agglomeration propagates very rapidly after nucleation within one minute and the size of spherical agglomerates is affected by the cooling rate. RDX by cooling crystallization from acetone was demonstrated. A proposed mechanism for this process is an extremely rapid nucleation induced due to primary nucleation by a polymeric additive. This rapid nucleation provides a high enough number density of particles for the formation of spherical agglomerates.
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title_short	Formation of Spherical Agglomerates in Cooling Crystallization of Hexahydro‐1,3,5‐trinitro‐1,3,5‐triazine
url	http://dx.doi.org/10.1002/ceat.201700144 http://onlinelibrary.wiley.com/doi/10.1002/ceat.201700144/abstract
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author2	Kim, Jae-Kyeong Kim, Hyoun-Soo Koo, Kee-Kahb
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up_date	2024-07-04T05:41:50.383Z
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