Preparation and characterization of bowl-like porous ZnO film by electrodeposition using two-dimensional photonic crystal template
Abstract A rapid and low-cost method combining electrodeposition with two-dimensional (2D) photonic crystal template technique to prepare large scale bowl-like porous ZnO films is described. The 2D photonic crystal templates were fabricated by self-assembly of monodispersed polystyrene (PS) microsph...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Tan, Zong [verfasserIn] |
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| Format: |
Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2013 |
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| Schlagwörter: |
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| Anmerkung: |
© Springer Science+Business Media New York 2013 |
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| Übergeordnetes Werk: |
Enthalten in: Journal of materials science / Materials in electronics - Springer US, 1990, 24(2013), 7 vom: 28. Feb., Seite 2630-2635 |
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| Übergeordnetes Werk: |
volume:24 ; year:2013 ; number:7 ; day:28 ; month:02 ; pages:2630-2635 |
| Links: |
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| DOI / URN: |
10.1007/s10854-013-1144-z |
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| Katalog-ID: |
OLC2026269246 |
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| 520 | |a Abstract A rapid and low-cost method combining electrodeposition with two-dimensional (2D) photonic crystal template technique to prepare large scale bowl-like porous ZnO films is described. The 2D photonic crystal templates were fabricated by self-assembly of monodispersed polystyrene (PS) microspheres on indium-tin-oxide coated glass substrates using spinning coating method. The interstitial spaces among the spheres of the templates were filled with ZnO via electrodeposition from an aqueous solution containing 0.02 M zinc nitrate as electrolyte under a constant potential of −1.0 V at 65 °C for 10 min. After removal of the PS photonic crystal template, bowl-like porous ZnO film was obtained. The entire process can be accomplished within 30 min. Scanning electron microscopic images showed good homogeneity in morphology, X-ray diffraction spectra demonstrated the wurtzite structure of the obtained ZnO film, and transmission electron microscopy indicated the single-crystallinity of the ZnO. Ultraviolet–visible (UV–vis) spectrophotometer was used to detect the absorption in UV–vis region of the PS template, opal ZnO-PS composite and inverse opal ZnO respectively. Two strong emission bands at 400 and 550 nm were displayed in photoluminescence spectrum. | ||
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10.1007/s10854-013-1144-z doi (DE-627)OLC2026269246 (DE-He213)s10854-013-1144-z-p DE-627 ger DE-627 rakwb eng 600 670 620 VZ Tan, Zong verfasserin aut Preparation and characterization of bowl-like porous ZnO film by electrodeposition using two-dimensional photonic crystal template 2013 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Springer Science+Business Media New York 2013 Abstract A rapid and low-cost method combining electrodeposition with two-dimensional (2D) photonic crystal template technique to prepare large scale bowl-like porous ZnO films is described. The 2D photonic crystal templates were fabricated by self-assembly of monodispersed polystyrene (PS) microspheres on indium-tin-oxide coated glass substrates using spinning coating method. The interstitial spaces among the spheres of the templates were filled with ZnO via electrodeposition from an aqueous solution containing 0.02 M zinc nitrate as electrolyte under a constant potential of −1.0 V at 65 °C for 10 min. After removal of the PS photonic crystal template, bowl-like porous ZnO film was obtained. The entire process can be accomplished within 30 min. Scanning electron microscopic images showed good homogeneity in morphology, X-ray diffraction spectra demonstrated the wurtzite structure of the obtained ZnO film, and transmission electron microscopy indicated the single-crystallinity of the ZnO. Ultraviolet–visible (UV–vis) spectrophotometer was used to detect the absorption in UV–vis region of the PS template, opal ZnO-PS composite and inverse opal ZnO respectively. Two strong emission bands at 400 and 550 nm were displayed in photoluminescence spectrum. Photonic Crystal Surface Free Energy Spin Coating Method Opal Template Inverse Opal Structure Feng, Zhi-Hui aut Yu, Li-Ping aut Enthalten in Journal of materials science / Materials in electronics Springer US, 1990 24(2013), 7 vom: 28. Feb., Seite 2630-2635 (DE-627)130863289 (DE-600)1030929-9 (DE-576)023106719 0957-4522 nnns volume:24 year:2013 number:7 day:28 month:02 pages:2630-2635 https://doi.org/10.1007/s10854-013-1144-z lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-PHY GBV_ILN_20 GBV_ILN_30 GBV_ILN_32 GBV_ILN_70 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2015 GBV_ILN_4046 GBV_ILN_4305 GBV_ILN_4323 AR 24 2013 7 28 02 2630-2635 |
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10.1007/s10854-013-1144-z doi (DE-627)OLC2026269246 (DE-He213)s10854-013-1144-z-p DE-627 ger DE-627 rakwb eng 600 670 620 VZ Tan, Zong verfasserin aut Preparation and characterization of bowl-like porous ZnO film by electrodeposition using two-dimensional photonic crystal template 2013 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Springer Science+Business Media New York 2013 Abstract A rapid and low-cost method combining electrodeposition with two-dimensional (2D) photonic crystal template technique to prepare large scale bowl-like porous ZnO films is described. The 2D photonic crystal templates were fabricated by self-assembly of monodispersed polystyrene (PS) microspheres on indium-tin-oxide coated glass substrates using spinning coating method. The interstitial spaces among the spheres of the templates were filled with ZnO via electrodeposition from an aqueous solution containing 0.02 M zinc nitrate as electrolyte under a constant potential of −1.0 V at 65 °C for 10 min. After removal of the PS photonic crystal template, bowl-like porous ZnO film was obtained. The entire process can be accomplished within 30 min. Scanning electron microscopic images showed good homogeneity in morphology, X-ray diffraction spectra demonstrated the wurtzite structure of the obtained ZnO film, and transmission electron microscopy indicated the single-crystallinity of the ZnO. Ultraviolet–visible (UV–vis) spectrophotometer was used to detect the absorption in UV–vis region of the PS template, opal ZnO-PS composite and inverse opal ZnO respectively. Two strong emission bands at 400 and 550 nm were displayed in photoluminescence spectrum. Photonic Crystal Surface Free Energy Spin Coating Method Opal Template Inverse Opal Structure Feng, Zhi-Hui aut Yu, Li-Ping aut Enthalten in Journal of materials science / Materials in electronics Springer US, 1990 24(2013), 7 vom: 28. Feb., Seite 2630-2635 (DE-627)130863289 (DE-600)1030929-9 (DE-576)023106719 0957-4522 nnns volume:24 year:2013 number:7 day:28 month:02 pages:2630-2635 https://doi.org/10.1007/s10854-013-1144-z lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-PHY GBV_ILN_20 GBV_ILN_30 GBV_ILN_32 GBV_ILN_70 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2015 GBV_ILN_4046 GBV_ILN_4305 GBV_ILN_4323 AR 24 2013 7 28 02 2630-2635 |
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10.1007/s10854-013-1144-z doi (DE-627)OLC2026269246 (DE-He213)s10854-013-1144-z-p DE-627 ger DE-627 rakwb eng 600 670 620 VZ Tan, Zong verfasserin aut Preparation and characterization of bowl-like porous ZnO film by electrodeposition using two-dimensional photonic crystal template 2013 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Springer Science+Business Media New York 2013 Abstract A rapid and low-cost method combining electrodeposition with two-dimensional (2D) photonic crystal template technique to prepare large scale bowl-like porous ZnO films is described. The 2D photonic crystal templates were fabricated by self-assembly of monodispersed polystyrene (PS) microspheres on indium-tin-oxide coated glass substrates using spinning coating method. The interstitial spaces among the spheres of the templates were filled with ZnO via electrodeposition from an aqueous solution containing 0.02 M zinc nitrate as electrolyte under a constant potential of −1.0 V at 65 °C for 10 min. After removal of the PS photonic crystal template, bowl-like porous ZnO film was obtained. The entire process can be accomplished within 30 min. Scanning electron microscopic images showed good homogeneity in morphology, X-ray diffraction spectra demonstrated the wurtzite structure of the obtained ZnO film, and transmission electron microscopy indicated the single-crystallinity of the ZnO. Ultraviolet–visible (UV–vis) spectrophotometer was used to detect the absorption in UV–vis region of the PS template, opal ZnO-PS composite and inverse opal ZnO respectively. Two strong emission bands at 400 and 550 nm were displayed in photoluminescence spectrum. Photonic Crystal Surface Free Energy Spin Coating Method Opal Template Inverse Opal Structure Feng, Zhi-Hui aut Yu, Li-Ping aut Enthalten in Journal of materials science / Materials in electronics Springer US, 1990 24(2013), 7 vom: 28. Feb., Seite 2630-2635 (DE-627)130863289 (DE-600)1030929-9 (DE-576)023106719 0957-4522 nnns volume:24 year:2013 number:7 day:28 month:02 pages:2630-2635 https://doi.org/10.1007/s10854-013-1144-z lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-PHY GBV_ILN_20 GBV_ILN_30 GBV_ILN_32 GBV_ILN_70 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2015 GBV_ILN_4046 GBV_ILN_4305 GBV_ILN_4323 AR 24 2013 7 28 02 2630-2635 |
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10.1007/s10854-013-1144-z doi (DE-627)OLC2026269246 (DE-He213)s10854-013-1144-z-p DE-627 ger DE-627 rakwb eng 600 670 620 VZ Tan, Zong verfasserin aut Preparation and characterization of bowl-like porous ZnO film by electrodeposition using two-dimensional photonic crystal template 2013 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Springer Science+Business Media New York 2013 Abstract A rapid and low-cost method combining electrodeposition with two-dimensional (2D) photonic crystal template technique to prepare large scale bowl-like porous ZnO films is described. The 2D photonic crystal templates were fabricated by self-assembly of monodispersed polystyrene (PS) microspheres on indium-tin-oxide coated glass substrates using spinning coating method. The interstitial spaces among the spheres of the templates were filled with ZnO via electrodeposition from an aqueous solution containing 0.02 M zinc nitrate as electrolyte under a constant potential of −1.0 V at 65 °C for 10 min. After removal of the PS photonic crystal template, bowl-like porous ZnO film was obtained. The entire process can be accomplished within 30 min. Scanning electron microscopic images showed good homogeneity in morphology, X-ray diffraction spectra demonstrated the wurtzite structure of the obtained ZnO film, and transmission electron microscopy indicated the single-crystallinity of the ZnO. Ultraviolet–visible (UV–vis) spectrophotometer was used to detect the absorption in UV–vis region of the PS template, opal ZnO-PS composite and inverse opal ZnO respectively. Two strong emission bands at 400 and 550 nm were displayed in photoluminescence spectrum. Photonic Crystal Surface Free Energy Spin Coating Method Opal Template Inverse Opal Structure Feng, Zhi-Hui aut Yu, Li-Ping aut Enthalten in Journal of materials science / Materials in electronics Springer US, 1990 24(2013), 7 vom: 28. Feb., Seite 2630-2635 (DE-627)130863289 (DE-600)1030929-9 (DE-576)023106719 0957-4522 nnns volume:24 year:2013 number:7 day:28 month:02 pages:2630-2635 https://doi.org/10.1007/s10854-013-1144-z lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-PHY GBV_ILN_20 GBV_ILN_30 GBV_ILN_32 GBV_ILN_70 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2015 GBV_ILN_4046 GBV_ILN_4305 GBV_ILN_4323 AR 24 2013 7 28 02 2630-2635 |
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10.1007/s10854-013-1144-z doi (DE-627)OLC2026269246 (DE-He213)s10854-013-1144-z-p DE-627 ger DE-627 rakwb eng 600 670 620 VZ Tan, Zong verfasserin aut Preparation and characterization of bowl-like porous ZnO film by electrodeposition using two-dimensional photonic crystal template 2013 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Springer Science+Business Media New York 2013 Abstract A rapid and low-cost method combining electrodeposition with two-dimensional (2D) photonic crystal template technique to prepare large scale bowl-like porous ZnO films is described. The 2D photonic crystal templates were fabricated by self-assembly of monodispersed polystyrene (PS) microspheres on indium-tin-oxide coated glass substrates using spinning coating method. The interstitial spaces among the spheres of the templates were filled with ZnO via electrodeposition from an aqueous solution containing 0.02 M zinc nitrate as electrolyte under a constant potential of −1.0 V at 65 °C for 10 min. After removal of the PS photonic crystal template, bowl-like porous ZnO film was obtained. The entire process can be accomplished within 30 min. Scanning electron microscopic images showed good homogeneity in morphology, X-ray diffraction spectra demonstrated the wurtzite structure of the obtained ZnO film, and transmission electron microscopy indicated the single-crystallinity of the ZnO. Ultraviolet–visible (UV–vis) spectrophotometer was used to detect the absorption in UV–vis region of the PS template, opal ZnO-PS composite and inverse opal ZnO respectively. Two strong emission bands at 400 and 550 nm were displayed in photoluminescence spectrum. Photonic Crystal Surface Free Energy Spin Coating Method Opal Template Inverse Opal Structure Feng, Zhi-Hui aut Yu, Li-Ping aut Enthalten in Journal of materials science / Materials in electronics Springer US, 1990 24(2013), 7 vom: 28. Feb., Seite 2630-2635 (DE-627)130863289 (DE-600)1030929-9 (DE-576)023106719 0957-4522 nnns volume:24 year:2013 number:7 day:28 month:02 pages:2630-2635 https://doi.org/10.1007/s10854-013-1144-z lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-PHY GBV_ILN_20 GBV_ILN_30 GBV_ILN_32 GBV_ILN_70 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2015 GBV_ILN_4046 GBV_ILN_4305 GBV_ILN_4323 AR 24 2013 7 28 02 2630-2635 |
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Preparation and characterization of bowl-like porous ZnO film by electrodeposition using two-dimensional photonic crystal template |
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Preparation and characterization of bowl-like porous ZnO film by electrodeposition using two-dimensional photonic crystal template |
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Tan, Zong |
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Journal of materials science / Materials in electronics |
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Tan, Zong Feng, Zhi-Hui Yu, Li-Ping |
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600 670 620 |
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preparation and characterization of bowl-like porous zno film by electrodeposition using two-dimensional photonic crystal template |
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Preparation and characterization of bowl-like porous ZnO film by electrodeposition using two-dimensional photonic crystal template |
| abstract |
Abstract A rapid and low-cost method combining electrodeposition with two-dimensional (2D) photonic crystal template technique to prepare large scale bowl-like porous ZnO films is described. The 2D photonic crystal templates were fabricated by self-assembly of monodispersed polystyrene (PS) microspheres on indium-tin-oxide coated glass substrates using spinning coating method. The interstitial spaces among the spheres of the templates were filled with ZnO via electrodeposition from an aqueous solution containing 0.02 M zinc nitrate as electrolyte under a constant potential of −1.0 V at 65 °C for 10 min. After removal of the PS photonic crystal template, bowl-like porous ZnO film was obtained. The entire process can be accomplished within 30 min. Scanning electron microscopic images showed good homogeneity in morphology, X-ray diffraction spectra demonstrated the wurtzite structure of the obtained ZnO film, and transmission electron microscopy indicated the single-crystallinity of the ZnO. Ultraviolet–visible (UV–vis) spectrophotometer was used to detect the absorption in UV–vis region of the PS template, opal ZnO-PS composite and inverse opal ZnO respectively. Two strong emission bands at 400 and 550 nm were displayed in photoluminescence spectrum. © Springer Science+Business Media New York 2013 |
| abstractGer |
Abstract A rapid and low-cost method combining electrodeposition with two-dimensional (2D) photonic crystal template technique to prepare large scale bowl-like porous ZnO films is described. The 2D photonic crystal templates were fabricated by self-assembly of monodispersed polystyrene (PS) microspheres on indium-tin-oxide coated glass substrates using spinning coating method. The interstitial spaces among the spheres of the templates were filled with ZnO via electrodeposition from an aqueous solution containing 0.02 M zinc nitrate as electrolyte under a constant potential of −1.0 V at 65 °C for 10 min. After removal of the PS photonic crystal template, bowl-like porous ZnO film was obtained. The entire process can be accomplished within 30 min. Scanning electron microscopic images showed good homogeneity in morphology, X-ray diffraction spectra demonstrated the wurtzite structure of the obtained ZnO film, and transmission electron microscopy indicated the single-crystallinity of the ZnO. Ultraviolet–visible (UV–vis) spectrophotometer was used to detect the absorption in UV–vis region of the PS template, opal ZnO-PS composite and inverse opal ZnO respectively. Two strong emission bands at 400 and 550 nm were displayed in photoluminescence spectrum. © Springer Science+Business Media New York 2013 |
| abstract_unstemmed |
Abstract A rapid and low-cost method combining electrodeposition with two-dimensional (2D) photonic crystal template technique to prepare large scale bowl-like porous ZnO films is described. The 2D photonic crystal templates were fabricated by self-assembly of monodispersed polystyrene (PS) microspheres on indium-tin-oxide coated glass substrates using spinning coating method. The interstitial spaces among the spheres of the templates were filled with ZnO via electrodeposition from an aqueous solution containing 0.02 M zinc nitrate as electrolyte under a constant potential of −1.0 V at 65 °C for 10 min. After removal of the PS photonic crystal template, bowl-like porous ZnO film was obtained. The entire process can be accomplished within 30 min. Scanning electron microscopic images showed good homogeneity in morphology, X-ray diffraction spectra demonstrated the wurtzite structure of the obtained ZnO film, and transmission electron microscopy indicated the single-crystallinity of the ZnO. Ultraviolet–visible (UV–vis) spectrophotometer was used to detect the absorption in UV–vis region of the PS template, opal ZnO-PS composite and inverse opal ZnO respectively. Two strong emission bands at 400 and 550 nm were displayed in photoluminescence spectrum. © Springer Science+Business Media New York 2013 |
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Preparation and characterization of bowl-like porous ZnO film by electrodeposition using two-dimensional photonic crystal template |
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