Enhancement of photocatalytic activity of $ ZrO_{2} $ nanoparticles by doping with Mg for UV light photocatalytic degradation of methyl violet and methyl blue dyes
Abstract In this study, pristine $ ZrO_{2} $ (600 °C) and Mg (0.02, 0.04, 0.06, 0.08 M)-doped $ ZrO_{2} $ nanoparticles were effectively synthesized at about 10 nm size and achieved complete degradation of methyl violet and methyl blue dyes under UV irradiation. The calcined products were analyzed b...
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| Autor*in: |
Rajesh, G. [verfasserIn] |
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| Format: |
Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2020 |
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| Anmerkung: |
© Springer Science+Business Media, LLC, part of Springer Nature 2020 |
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| Übergeordnetes Werk: |
Enthalten in: Journal of materials science / Materials in electronics - Springer US, 1990, 31(2020), 5 vom: 03. Feb., Seite 4058-4072 |
|---|---|
| Übergeordnetes Werk: |
volume:31 ; year:2020 ; number:5 ; day:03 ; month:02 ; pages:4058-4072 |
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10.1007/s10854-020-02953-3 |
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| 520 | |a Abstract In this study, pristine $ ZrO_{2} $ (600 °C) and Mg (0.02, 0.04, 0.06, 0.08 M)-doped $ ZrO_{2} $ nanoparticles were effectively synthesized at about 10 nm size and achieved complete degradation of methyl violet and methyl blue dyes under UV irradiation. The calcined products were analyzed by XRD, FTIR, UV-DRS, PL, FESEM-EDX, TEM-SAED pattern and XPS techniques. The tetragonal crystal structure of the pristine $ ZrO_{2} $ and Mg (0.02–0.08 M)-doped $ ZrO_{2} $ nanoparticles were affirmed by XRD analysis. The Mg (0.08 M)-doped $ ZrO_{2} $ nanoparticles were approximately in quasi-spherical morphology and high agglomeration was confirmed by FESEM and TEM results. The surface defects and oxygen vacancies were analyzed by PL spectroscopy. The Mg (0.08 M)-doped $ ZrO_{2} $ nanoparticles exhibited enlarged photocatalytic activity with 94% and 90% degradation of methyl violet and methyl blue dyes under UV irradiation. | ||
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10.1007/s10854-020-02953-3 doi (DE-627)OLC2026386811 (DE-He213)s10854-020-02953-3-p DE-627 ger DE-627 rakwb eng 600 670 620 VZ Rajesh, G. verfasserin aut Enhancement of photocatalytic activity of $ ZrO_{2} $ nanoparticles by doping with Mg for UV light photocatalytic degradation of methyl violet and methyl blue dyes 2020 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Springer Science+Business Media, LLC, part of Springer Nature 2020 Abstract In this study, pristine $ ZrO_{2} $ (600 °C) and Mg (0.02, 0.04, 0.06, 0.08 M)-doped $ ZrO_{2} $ nanoparticles were effectively synthesized at about 10 nm size and achieved complete degradation of methyl violet and methyl blue dyes under UV irradiation. The calcined products were analyzed by XRD, FTIR, UV-DRS, PL, FESEM-EDX, TEM-SAED pattern and XPS techniques. The tetragonal crystal structure of the pristine $ ZrO_{2} $ and Mg (0.02–0.08 M)-doped $ ZrO_{2} $ nanoparticles were affirmed by XRD analysis. The Mg (0.08 M)-doped $ ZrO_{2} $ nanoparticles were approximately in quasi-spherical morphology and high agglomeration was confirmed by FESEM and TEM results. The surface defects and oxygen vacancies were analyzed by PL spectroscopy. The Mg (0.08 M)-doped $ ZrO_{2} $ nanoparticles exhibited enlarged photocatalytic activity with 94% and 90% degradation of methyl violet and methyl blue dyes under UV irradiation. Akilandeswari, S. (orcid)0000-0003-3706-2048 aut Govindarajan, D. aut Thirumalai, K. aut Enthalten in Journal of materials science / Materials in electronics Springer US, 1990 31(2020), 5 vom: 03. Feb., Seite 4058-4072 (DE-627)130863289 (DE-600)1030929-9 (DE-576)023106719 0957-4522 nnns volume:31 year:2020 number:5 day:03 month:02 pages:4058-4072 https://doi.org/10.1007/s10854-020-02953-3 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-PHY GBV_ILN_2004 GBV_ILN_2015 AR 31 2020 5 03 02 4058-4072 |
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10.1007/s10854-020-02953-3 doi (DE-627)OLC2026386811 (DE-He213)s10854-020-02953-3-p DE-627 ger DE-627 rakwb eng 600 670 620 VZ Rajesh, G. verfasserin aut Enhancement of photocatalytic activity of $ ZrO_{2} $ nanoparticles by doping with Mg for UV light photocatalytic degradation of methyl violet and methyl blue dyes 2020 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Springer Science+Business Media, LLC, part of Springer Nature 2020 Abstract In this study, pristine $ ZrO_{2} $ (600 °C) and Mg (0.02, 0.04, 0.06, 0.08 M)-doped $ ZrO_{2} $ nanoparticles were effectively synthesized at about 10 nm size and achieved complete degradation of methyl violet and methyl blue dyes under UV irradiation. The calcined products were analyzed by XRD, FTIR, UV-DRS, PL, FESEM-EDX, TEM-SAED pattern and XPS techniques. The tetragonal crystal structure of the pristine $ ZrO_{2} $ and Mg (0.02–0.08 M)-doped $ ZrO_{2} $ nanoparticles were affirmed by XRD analysis. The Mg (0.08 M)-doped $ ZrO_{2} $ nanoparticles were approximately in quasi-spherical morphology and high agglomeration was confirmed by FESEM and TEM results. The surface defects and oxygen vacancies were analyzed by PL spectroscopy. The Mg (0.08 M)-doped $ ZrO_{2} $ nanoparticles exhibited enlarged photocatalytic activity with 94% and 90% degradation of methyl violet and methyl blue dyes under UV irradiation. Akilandeswari, S. (orcid)0000-0003-3706-2048 aut Govindarajan, D. aut Thirumalai, K. aut Enthalten in Journal of materials science / Materials in electronics Springer US, 1990 31(2020), 5 vom: 03. Feb., Seite 4058-4072 (DE-627)130863289 (DE-600)1030929-9 (DE-576)023106719 0957-4522 nnns volume:31 year:2020 number:5 day:03 month:02 pages:4058-4072 https://doi.org/10.1007/s10854-020-02953-3 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-PHY GBV_ILN_2004 GBV_ILN_2015 AR 31 2020 5 03 02 4058-4072 |
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10.1007/s10854-020-02953-3 doi (DE-627)OLC2026386811 (DE-He213)s10854-020-02953-3-p DE-627 ger DE-627 rakwb eng 600 670 620 VZ Rajesh, G. verfasserin aut Enhancement of photocatalytic activity of $ ZrO_{2} $ nanoparticles by doping with Mg for UV light photocatalytic degradation of methyl violet and methyl blue dyes 2020 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Springer Science+Business Media, LLC, part of Springer Nature 2020 Abstract In this study, pristine $ ZrO_{2} $ (600 °C) and Mg (0.02, 0.04, 0.06, 0.08 M)-doped $ ZrO_{2} $ nanoparticles were effectively synthesized at about 10 nm size and achieved complete degradation of methyl violet and methyl blue dyes under UV irradiation. The calcined products were analyzed by XRD, FTIR, UV-DRS, PL, FESEM-EDX, TEM-SAED pattern and XPS techniques. The tetragonal crystal structure of the pristine $ ZrO_{2} $ and Mg (0.02–0.08 M)-doped $ ZrO_{2} $ nanoparticles were affirmed by XRD analysis. The Mg (0.08 M)-doped $ ZrO_{2} $ nanoparticles were approximately in quasi-spherical morphology and high agglomeration was confirmed by FESEM and TEM results. The surface defects and oxygen vacancies were analyzed by PL spectroscopy. The Mg (0.08 M)-doped $ ZrO_{2} $ nanoparticles exhibited enlarged photocatalytic activity with 94% and 90% degradation of methyl violet and methyl blue dyes under UV irradiation. Akilandeswari, S. (orcid)0000-0003-3706-2048 aut Govindarajan, D. aut Thirumalai, K. aut Enthalten in Journal of materials science / Materials in electronics Springer US, 1990 31(2020), 5 vom: 03. Feb., Seite 4058-4072 (DE-627)130863289 (DE-600)1030929-9 (DE-576)023106719 0957-4522 nnns volume:31 year:2020 number:5 day:03 month:02 pages:4058-4072 https://doi.org/10.1007/s10854-020-02953-3 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-PHY GBV_ILN_2004 GBV_ILN_2015 AR 31 2020 5 03 02 4058-4072 |
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10.1007/s10854-020-02953-3 doi (DE-627)OLC2026386811 (DE-He213)s10854-020-02953-3-p DE-627 ger DE-627 rakwb eng 600 670 620 VZ Rajesh, G. verfasserin aut Enhancement of photocatalytic activity of $ ZrO_{2} $ nanoparticles by doping with Mg for UV light photocatalytic degradation of methyl violet and methyl blue dyes 2020 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Springer Science+Business Media, LLC, part of Springer Nature 2020 Abstract In this study, pristine $ ZrO_{2} $ (600 °C) and Mg (0.02, 0.04, 0.06, 0.08 M)-doped $ ZrO_{2} $ nanoparticles were effectively synthesized at about 10 nm size and achieved complete degradation of methyl violet and methyl blue dyes under UV irradiation. The calcined products were analyzed by XRD, FTIR, UV-DRS, PL, FESEM-EDX, TEM-SAED pattern and XPS techniques. The tetragonal crystal structure of the pristine $ ZrO_{2} $ and Mg (0.02–0.08 M)-doped $ ZrO_{2} $ nanoparticles were affirmed by XRD analysis. The Mg (0.08 M)-doped $ ZrO_{2} $ nanoparticles were approximately in quasi-spherical morphology and high agglomeration was confirmed by FESEM and TEM results. The surface defects and oxygen vacancies were analyzed by PL spectroscopy. The Mg (0.08 M)-doped $ ZrO_{2} $ nanoparticles exhibited enlarged photocatalytic activity with 94% and 90% degradation of methyl violet and methyl blue dyes under UV irradiation. Akilandeswari, S. (orcid)0000-0003-3706-2048 aut Govindarajan, D. aut Thirumalai, K. aut Enthalten in Journal of materials science / Materials in electronics Springer US, 1990 31(2020), 5 vom: 03. Feb., Seite 4058-4072 (DE-627)130863289 (DE-600)1030929-9 (DE-576)023106719 0957-4522 nnns volume:31 year:2020 number:5 day:03 month:02 pages:4058-4072 https://doi.org/10.1007/s10854-020-02953-3 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-PHY GBV_ILN_2004 GBV_ILN_2015 AR 31 2020 5 03 02 4058-4072 |
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Enhancement of photocatalytic activity of $ ZrO_{2} $ nanoparticles by doping with Mg for UV light photocatalytic degradation of methyl violet and methyl blue dyes |
| abstract |
Abstract In this study, pristine $ ZrO_{2} $ (600 °C) and Mg (0.02, 0.04, 0.06, 0.08 M)-doped $ ZrO_{2} $ nanoparticles were effectively synthesized at about 10 nm size and achieved complete degradation of methyl violet and methyl blue dyes under UV irradiation. The calcined products were analyzed by XRD, FTIR, UV-DRS, PL, FESEM-EDX, TEM-SAED pattern and XPS techniques. The tetragonal crystal structure of the pristine $ ZrO_{2} $ and Mg (0.02–0.08 M)-doped $ ZrO_{2} $ nanoparticles were affirmed by XRD analysis. The Mg (0.08 M)-doped $ ZrO_{2} $ nanoparticles were approximately in quasi-spherical morphology and high agglomeration was confirmed by FESEM and TEM results. The surface defects and oxygen vacancies were analyzed by PL spectroscopy. The Mg (0.08 M)-doped $ ZrO_{2} $ nanoparticles exhibited enlarged photocatalytic activity with 94% and 90% degradation of methyl violet and methyl blue dyes under UV irradiation. © Springer Science+Business Media, LLC, part of Springer Nature 2020 |
| abstractGer |
Abstract In this study, pristine $ ZrO_{2} $ (600 °C) and Mg (0.02, 0.04, 0.06, 0.08 M)-doped $ ZrO_{2} $ nanoparticles were effectively synthesized at about 10 nm size and achieved complete degradation of methyl violet and methyl blue dyes under UV irradiation. The calcined products were analyzed by XRD, FTIR, UV-DRS, PL, FESEM-EDX, TEM-SAED pattern and XPS techniques. The tetragonal crystal structure of the pristine $ ZrO_{2} $ and Mg (0.02–0.08 M)-doped $ ZrO_{2} $ nanoparticles were affirmed by XRD analysis. The Mg (0.08 M)-doped $ ZrO_{2} $ nanoparticles were approximately in quasi-spherical morphology and high agglomeration was confirmed by FESEM and TEM results. The surface defects and oxygen vacancies were analyzed by PL spectroscopy. The Mg (0.08 M)-doped $ ZrO_{2} $ nanoparticles exhibited enlarged photocatalytic activity with 94% and 90% degradation of methyl violet and methyl blue dyes under UV irradiation. © Springer Science+Business Media, LLC, part of Springer Nature 2020 |
| abstract_unstemmed |
Abstract In this study, pristine $ ZrO_{2} $ (600 °C) and Mg (0.02, 0.04, 0.06, 0.08 M)-doped $ ZrO_{2} $ nanoparticles were effectively synthesized at about 10 nm size and achieved complete degradation of methyl violet and methyl blue dyes under UV irradiation. The calcined products were analyzed by XRD, FTIR, UV-DRS, PL, FESEM-EDX, TEM-SAED pattern and XPS techniques. The tetragonal crystal structure of the pristine $ ZrO_{2} $ and Mg (0.02–0.08 M)-doped $ ZrO_{2} $ nanoparticles were affirmed by XRD analysis. The Mg (0.08 M)-doped $ ZrO_{2} $ nanoparticles were approximately in quasi-spherical morphology and high agglomeration was confirmed by FESEM and TEM results. The surface defects and oxygen vacancies were analyzed by PL spectroscopy. The Mg (0.08 M)-doped $ ZrO_{2} $ nanoparticles exhibited enlarged photocatalytic activity with 94% and 90% degradation of methyl violet and methyl blue dyes under UV irradiation. © Springer Science+Business Media, LLC, part of Springer Nature 2020 |
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| title_short |
Enhancement of photocatalytic activity of $ ZrO_{2} $ nanoparticles by doping with Mg for UV light photocatalytic degradation of methyl violet and methyl blue dyes |
| url |
https://doi.org/10.1007/s10854-020-02953-3 |
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| author2 |
Akilandeswari, S. Govindarajan, D. Thirumalai, K. |
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Akilandeswari, S. Govindarajan, D. Thirumalai, K. |
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