Hydrogen-Bonding Interactions in the Crystal Structure of Bis(N-propyl-N-(2-hydroxyethyl)dithiocarbamato-S,S′)nickel(II): Ni[$ S_{2} $CN(nPr)($ CH_{2} $$ CH_{2} $OH)]2
Abstract Two independent molecules of Ni($ S_{2} $CN(Pr)$ CH_{2} $$ CH_{2} $OH)2, each located about a center of inversion, comprise the asymmetric unit. The molecules differ from each other in terms of the relative orientation of the terminal hydroxyl groups. A square planar geometry is found for e...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Tiekink, Edward R. T. [verfasserIn] |
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| Format: |
Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2007 |
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| Schlagwörter: |
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| Anmerkung: |
© Springer Science+Business Media, LLC 2007 |
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| Übergeordnetes Werk: |
Enthalten in: Journal of chemical crystallography - Kluwer Academic Publishers-Plenum Publishers, 1994, 37(2007), 7 vom: 04. Apr., Seite 439-443 |
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| Übergeordnetes Werk: |
volume:37 ; year:2007 ; number:7 ; day:04 ; month:04 ; pages:439-443 |
| Links: |
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| DOI / URN: |
10.1007/s10870-007-9189-6 |
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OLC2036714382 |
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| 520 | |a Abstract Two independent molecules of Ni($ S_{2} $CN(Pr)$ CH_{2} $$ CH_{2} $OH)2, each located about a center of inversion, comprise the asymmetric unit. The molecules differ from each other in terms of the relative orientation of the terminal hydroxyl groups. A square planar geometry is found for each nickel atom defined by four sulfur atoms derived from two symmetrically chelating dithiocarbamate ligands. The crystal packing is dominated by O–H···O interactions that lead to extensive cross linking in all directions. The compound crystallizes in the triclinic space group P-1 with a = 6.4008(11) Å, b = 11.480(2) Å, c = 12.517(2) Å, α = 88.021(2)°, β = 82.491(2)°, γ = 89.986(2)°, and Z = 2. | ||
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| 700 | 1 | |a Wardell, Solange M. S. V. |4 aut | |
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10.1007/s10870-007-9189-6 doi (DE-627)OLC2036714382 (DE-He213)s10870-007-9189-6-p DE-627 ger DE-627 rakwb eng 540 VZ 13 ssgn Tiekink, Edward R. T. verfasserin aut Hydrogen-Bonding Interactions in the Crystal Structure of Bis(N-propyl-N-(2-hydroxyethyl)dithiocarbamato-S,S′)nickel(II): Ni[$ S_{2} $CN(nPr)($ CH_{2} $$ CH_{2} $OH)]2 2007 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Springer Science+Business Media, LLC 2007 Abstract Two independent molecules of Ni($ S_{2} $CN(Pr)$ CH_{2} $$ CH_{2} $OH)2, each located about a center of inversion, comprise the asymmetric unit. The molecules differ from each other in terms of the relative orientation of the terminal hydroxyl groups. A square planar geometry is found for each nickel atom defined by four sulfur atoms derived from two symmetrically chelating dithiocarbamate ligands. The crystal packing is dominated by O–H···O interactions that lead to extensive cross linking in all directions. The compound crystallizes in the triclinic space group P-1 with a = 6.4008(11) Å, b = 11.480(2) Å, c = 12.517(2) Å, α = 88.021(2)°, β = 82.491(2)°, γ = 89.986(2)°, and Z = 2. Nickel Dithiocarbamate Metal complex Hydrogen-bonding Wardell, James L. aut Wardell, Solange M. S. V. aut Enthalten in Journal of chemical crystallography Kluwer Academic Publishers-Plenum Publishers, 1994 37(2007), 7 vom: 04. Apr., Seite 439-443 (DE-627)182237877 (DE-600)1189288-2 (DE-576)039053679 1074-1542 nnns volume:37 year:2007 number:7 day:04 month:04 pages:439-443 https://doi.org/10.1007/s10870-007-9189-6 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-CHE SSG-OLC-GEO SSG-OLC-PHA SSG-OLC-DE-84 SSG-OPC-GGO GBV_ILN_70 GBV_ILN_2027 GBV_ILN_4012 AR 37 2007 7 04 04 439-443 |
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10.1007/s10870-007-9189-6 doi (DE-627)OLC2036714382 (DE-He213)s10870-007-9189-6-p DE-627 ger DE-627 rakwb eng 540 VZ 13 ssgn Tiekink, Edward R. T. verfasserin aut Hydrogen-Bonding Interactions in the Crystal Structure of Bis(N-propyl-N-(2-hydroxyethyl)dithiocarbamato-S,S′)nickel(II): Ni[$ S_{2} $CN(nPr)($ CH_{2} $$ CH_{2} $OH)]2 2007 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Springer Science+Business Media, LLC 2007 Abstract Two independent molecules of Ni($ S_{2} $CN(Pr)$ CH_{2} $$ CH_{2} $OH)2, each located about a center of inversion, comprise the asymmetric unit. The molecules differ from each other in terms of the relative orientation of the terminal hydroxyl groups. A square planar geometry is found for each nickel atom defined by four sulfur atoms derived from two symmetrically chelating dithiocarbamate ligands. The crystal packing is dominated by O–H···O interactions that lead to extensive cross linking in all directions. The compound crystallizes in the triclinic space group P-1 with a = 6.4008(11) Å, b = 11.480(2) Å, c = 12.517(2) Å, α = 88.021(2)°, β = 82.491(2)°, γ = 89.986(2)°, and Z = 2. Nickel Dithiocarbamate Metal complex Hydrogen-bonding Wardell, James L. aut Wardell, Solange M. S. V. aut Enthalten in Journal of chemical crystallography Kluwer Academic Publishers-Plenum Publishers, 1994 37(2007), 7 vom: 04. Apr., Seite 439-443 (DE-627)182237877 (DE-600)1189288-2 (DE-576)039053679 1074-1542 nnns volume:37 year:2007 number:7 day:04 month:04 pages:439-443 https://doi.org/10.1007/s10870-007-9189-6 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-CHE SSG-OLC-GEO SSG-OLC-PHA SSG-OLC-DE-84 SSG-OPC-GGO GBV_ILN_70 GBV_ILN_2027 GBV_ILN_4012 AR 37 2007 7 04 04 439-443 |
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10.1007/s10870-007-9189-6 doi (DE-627)OLC2036714382 (DE-He213)s10870-007-9189-6-p DE-627 ger DE-627 rakwb eng 540 VZ 13 ssgn Tiekink, Edward R. T. verfasserin aut Hydrogen-Bonding Interactions in the Crystal Structure of Bis(N-propyl-N-(2-hydroxyethyl)dithiocarbamato-S,S′)nickel(II): Ni[$ S_{2} $CN(nPr)($ CH_{2} $$ CH_{2} $OH)]2 2007 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Springer Science+Business Media, LLC 2007 Abstract Two independent molecules of Ni($ S_{2} $CN(Pr)$ CH_{2} $$ CH_{2} $OH)2, each located about a center of inversion, comprise the asymmetric unit. The molecules differ from each other in terms of the relative orientation of the terminal hydroxyl groups. A square planar geometry is found for each nickel atom defined by four sulfur atoms derived from two symmetrically chelating dithiocarbamate ligands. The crystal packing is dominated by O–H···O interactions that lead to extensive cross linking in all directions. The compound crystallizes in the triclinic space group P-1 with a = 6.4008(11) Å, b = 11.480(2) Å, c = 12.517(2) Å, α = 88.021(2)°, β = 82.491(2)°, γ = 89.986(2)°, and Z = 2. Nickel Dithiocarbamate Metal complex Hydrogen-bonding Wardell, James L. aut Wardell, Solange M. S. V. aut Enthalten in Journal of chemical crystallography Kluwer Academic Publishers-Plenum Publishers, 1994 37(2007), 7 vom: 04. Apr., Seite 439-443 (DE-627)182237877 (DE-600)1189288-2 (DE-576)039053679 1074-1542 nnns volume:37 year:2007 number:7 day:04 month:04 pages:439-443 https://doi.org/10.1007/s10870-007-9189-6 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-CHE SSG-OLC-GEO SSG-OLC-PHA SSG-OLC-DE-84 SSG-OPC-GGO GBV_ILN_70 GBV_ILN_2027 GBV_ILN_4012 AR 37 2007 7 04 04 439-443 |
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10.1007/s10870-007-9189-6 doi (DE-627)OLC2036714382 (DE-He213)s10870-007-9189-6-p DE-627 ger DE-627 rakwb eng 540 VZ 13 ssgn Tiekink, Edward R. T. verfasserin aut Hydrogen-Bonding Interactions in the Crystal Structure of Bis(N-propyl-N-(2-hydroxyethyl)dithiocarbamato-S,S′)nickel(II): Ni[$ S_{2} $CN(nPr)($ CH_{2} $$ CH_{2} $OH)]2 2007 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Springer Science+Business Media, LLC 2007 Abstract Two independent molecules of Ni($ S_{2} $CN(Pr)$ CH_{2} $$ CH_{2} $OH)2, each located about a center of inversion, comprise the asymmetric unit. The molecules differ from each other in terms of the relative orientation of the terminal hydroxyl groups. A square planar geometry is found for each nickel atom defined by four sulfur atoms derived from two symmetrically chelating dithiocarbamate ligands. The crystal packing is dominated by O–H···O interactions that lead to extensive cross linking in all directions. The compound crystallizes in the triclinic space group P-1 with a = 6.4008(11) Å, b = 11.480(2) Å, c = 12.517(2) Å, α = 88.021(2)°, β = 82.491(2)°, γ = 89.986(2)°, and Z = 2. Nickel Dithiocarbamate Metal complex Hydrogen-bonding Wardell, James L. aut Wardell, Solange M. S. V. aut Enthalten in Journal of chemical crystallography Kluwer Academic Publishers-Plenum Publishers, 1994 37(2007), 7 vom: 04. Apr., Seite 439-443 (DE-627)182237877 (DE-600)1189288-2 (DE-576)039053679 1074-1542 nnns volume:37 year:2007 number:7 day:04 month:04 pages:439-443 https://doi.org/10.1007/s10870-007-9189-6 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-CHE SSG-OLC-GEO SSG-OLC-PHA SSG-OLC-DE-84 SSG-OPC-GGO GBV_ILN_70 GBV_ILN_2027 GBV_ILN_4012 AR 37 2007 7 04 04 439-443 |
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10.1007/s10870-007-9189-6 doi (DE-627)OLC2036714382 (DE-He213)s10870-007-9189-6-p DE-627 ger DE-627 rakwb eng 540 VZ 13 ssgn Tiekink, Edward R. T. verfasserin aut Hydrogen-Bonding Interactions in the Crystal Structure of Bis(N-propyl-N-(2-hydroxyethyl)dithiocarbamato-S,S′)nickel(II): Ni[$ S_{2} $CN(nPr)($ CH_{2} $$ CH_{2} $OH)]2 2007 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Springer Science+Business Media, LLC 2007 Abstract Two independent molecules of Ni($ S_{2} $CN(Pr)$ CH_{2} $$ CH_{2} $OH)2, each located about a center of inversion, comprise the asymmetric unit. The molecules differ from each other in terms of the relative orientation of the terminal hydroxyl groups. A square planar geometry is found for each nickel atom defined by four sulfur atoms derived from two symmetrically chelating dithiocarbamate ligands. The crystal packing is dominated by O–H···O interactions that lead to extensive cross linking in all directions. The compound crystallizes in the triclinic space group P-1 with a = 6.4008(11) Å, b = 11.480(2) Å, c = 12.517(2) Å, α = 88.021(2)°, β = 82.491(2)°, γ = 89.986(2)°, and Z = 2. Nickel Dithiocarbamate Metal complex Hydrogen-bonding Wardell, James L. aut Wardell, Solange M. S. V. aut Enthalten in Journal of chemical crystallography Kluwer Academic Publishers-Plenum Publishers, 1994 37(2007), 7 vom: 04. Apr., Seite 439-443 (DE-627)182237877 (DE-600)1189288-2 (DE-576)039053679 1074-1542 nnns volume:37 year:2007 number:7 day:04 month:04 pages:439-443 https://doi.org/10.1007/s10870-007-9189-6 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-CHE SSG-OLC-GEO SSG-OLC-PHA SSG-OLC-DE-84 SSG-OPC-GGO GBV_ILN_70 GBV_ILN_2027 GBV_ILN_4012 AR 37 2007 7 04 04 439-443 |
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| title_full |
Hydrogen-Bonding Interactions in the Crystal Structure of Bis(N-propyl-N-(2-hydroxyethyl)dithiocarbamato-S,S′)nickel(II): Ni[$ S_{2} $CN(nPr)($ CH_{2} $$ CH_{2} $OH)]2 |
| author_sort |
Tiekink, Edward R. T. |
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Journal of chemical crystallography |
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Journal of chemical crystallography |
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eng |
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500 - Science |
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2007 |
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439 |
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Tiekink, Edward R. T. Wardell, James L. Wardell, Solange M. S. V. |
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37 |
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540 VZ 13 ssgn |
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Aufsätze |
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Tiekink, Edward R. T. |
| doi_str_mv |
10.1007/s10870-007-9189-6 |
| dewey-full |
540 |
| title_sort |
hydrogen-bonding interactions in the crystal structure of bis(n-propyl-n-(2-hydroxyethyl)dithiocarbamato-s,s′)nickel(ii): ni[$ s_{2} $cn(npr)($ ch_{2} $$ ch_{2} $oh)]2 |
| title_auth |
Hydrogen-Bonding Interactions in the Crystal Structure of Bis(N-propyl-N-(2-hydroxyethyl)dithiocarbamato-S,S′)nickel(II): Ni[$ S_{2} $CN(nPr)($ CH_{2} $$ CH_{2} $OH)]2 |
| abstract |
Abstract Two independent molecules of Ni($ S_{2} $CN(Pr)$ CH_{2} $$ CH_{2} $OH)2, each located about a center of inversion, comprise the asymmetric unit. The molecules differ from each other in terms of the relative orientation of the terminal hydroxyl groups. A square planar geometry is found for each nickel atom defined by four sulfur atoms derived from two symmetrically chelating dithiocarbamate ligands. The crystal packing is dominated by O–H···O interactions that lead to extensive cross linking in all directions. The compound crystallizes in the triclinic space group P-1 with a = 6.4008(11) Å, b = 11.480(2) Å, c = 12.517(2) Å, α = 88.021(2)°, β = 82.491(2)°, γ = 89.986(2)°, and Z = 2. © Springer Science+Business Media, LLC 2007 |
| abstractGer |
Abstract Two independent molecules of Ni($ S_{2} $CN(Pr)$ CH_{2} $$ CH_{2} $OH)2, each located about a center of inversion, comprise the asymmetric unit. The molecules differ from each other in terms of the relative orientation of the terminal hydroxyl groups. A square planar geometry is found for each nickel atom defined by four sulfur atoms derived from two symmetrically chelating dithiocarbamate ligands. The crystal packing is dominated by O–H···O interactions that lead to extensive cross linking in all directions. The compound crystallizes in the triclinic space group P-1 with a = 6.4008(11) Å, b = 11.480(2) Å, c = 12.517(2) Å, α = 88.021(2)°, β = 82.491(2)°, γ = 89.986(2)°, and Z = 2. © Springer Science+Business Media, LLC 2007 |
| abstract_unstemmed |
Abstract Two independent molecules of Ni($ S_{2} $CN(Pr)$ CH_{2} $$ CH_{2} $OH)2, each located about a center of inversion, comprise the asymmetric unit. The molecules differ from each other in terms of the relative orientation of the terminal hydroxyl groups. A square planar geometry is found for each nickel atom defined by four sulfur atoms derived from two symmetrically chelating dithiocarbamate ligands. The crystal packing is dominated by O–H···O interactions that lead to extensive cross linking in all directions. The compound crystallizes in the triclinic space group P-1 with a = 6.4008(11) Å, b = 11.480(2) Å, c = 12.517(2) Å, α = 88.021(2)°, β = 82.491(2)°, γ = 89.986(2)°, and Z = 2. © Springer Science+Business Media, LLC 2007 |
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7 |
| title_short |
Hydrogen-Bonding Interactions in the Crystal Structure of Bis(N-propyl-N-(2-hydroxyethyl)dithiocarbamato-S,S′)nickel(II): Ni[$ S_{2} $CN(nPr)($ CH_{2} $$ CH_{2} $OH)]2 |
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https://doi.org/10.1007/s10870-007-9189-6 |
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Wardell, James L. Wardell, Solange M. S. V. |
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2024-07-04T04:01:14.151Z |
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