Syntheses, Crystal Structure and Properties of Two 1-D Coordination Polymers Bridged by Dicyanamides
Abstract Two new 1-D coordination polymers [MII (3-Bzpy)2(N(CN)2)2] (M = Cd (1), Cu (2), 3-Bzpy = 3-benzoylpyridine) have been synthesized and structurally characterized by single-crystal X-ray diffraction and IR. Single-crystal X-ray diffraction reveals that the complexes 1 and 2 are isostructural...
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| Autor*in: |
Luo, Yang-Hui [verfasserIn] |
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| Format: |
Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2012 |
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| Schlagwörter: |
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| Anmerkung: |
© Springer Science+Business Media, LLC 2012 |
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| Übergeordnetes Werk: |
Enthalten in: Journal of chemical crystallography - Springer US, 1994, 42(2012), 6 vom: 02. März, Seite 628-632 |
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| Übergeordnetes Werk: |
volume:42 ; year:2012 ; number:6 ; day:02 ; month:03 ; pages:628-632 |
| Links: |
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| DOI / URN: |
10.1007/s10870-012-0293-x |
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OLC2036724000 |
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| 520 | |a Abstract Two new 1-D coordination polymers [MII (3-Bzpy)2(N(CN)2)2] (M = Cd (1), Cu (2), 3-Bzpy = 3-benzoylpyridine) have been synthesized and structurally characterized by single-crystal X-ray diffraction and IR. Single-crystal X-ray diffraction reveals that the complexes 1 and 2 are isostructural and all crystallize in monoclinic P$ 2_{1} $/c space group with cell dimensions: a = 6.3889(16) Å, b = 7.6496(12) Å, c = 26.767(6) Å, β = 99.131(19)°, V = 1291.6(5) $ Å^{3} $, Z = 2 for 1 and a = 6.4483(9) Å, b = 7.5449(10) Å, c = 25.965(4) Å, β = 98.559(10)°, V = 1249.2(3) $ Å^{3} $, Z = 2 for 2. Structure analysis manifest that 1 and 2 are all 1-D chains structures which parallel to the crystallographic b axis through end-to-end coordination by bidentate bridging dicyanamide ligands. Magnetic property of complex 2 was further investigated. Graphical Abstract The paper is about synthesis, crystal structure and magnetic property of two new 1-D coordination polymers. Perspective view down the a-axis of complex 1 with thermal ellipsoids drawn at the 50% probability level . | ||
| 650 | 4 | |a Dicyanamide | |
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| 700 | 1 | |a Sun, Bai-Wang |4 aut | |
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10.1007/s10870-012-0293-x doi (DE-627)OLC2036724000 (DE-He213)s10870-012-0293-x-p DE-627 ger DE-627 rakwb eng 540 VZ 13 ssgn Luo, Yang-Hui verfasserin aut Syntheses, Crystal Structure and Properties of Two 1-D Coordination Polymers Bridged by Dicyanamides 2012 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Springer Science+Business Media, LLC 2012 Abstract Two new 1-D coordination polymers [MII (3-Bzpy)2(N(CN)2)2] (M = Cd (1), Cu (2), 3-Bzpy = 3-benzoylpyridine) have been synthesized and structurally characterized by single-crystal X-ray diffraction and IR. Single-crystal X-ray diffraction reveals that the complexes 1 and 2 are isostructural and all crystallize in monoclinic P$ 2_{1} $/c space group with cell dimensions: a = 6.3889(16) Å, b = 7.6496(12) Å, c = 26.767(6) Å, β = 99.131(19)°, V = 1291.6(5) $ Å^{3} $, Z = 2 for 1 and a = 6.4483(9) Å, b = 7.5449(10) Å, c = 25.965(4) Å, β = 98.559(10)°, V = 1249.2(3) $ Å^{3} $, Z = 2 for 2. Structure analysis manifest that 1 and 2 are all 1-D chains structures which parallel to the crystallographic b axis through end-to-end coordination by bidentate bridging dicyanamide ligands. Magnetic property of complex 2 was further investigated. Graphical Abstract The paper is about synthesis, crystal structure and magnetic property of two new 1-D coordination polymers. Perspective view down the a-axis of complex 1 with thermal ellipsoids drawn at the 50% probability level . Dicyanamide 1-D chain Crystal structure Magnetic property Ma, Yu-Tao aut Bao, Qian-Qian aut Sun, Bai-Wang aut Enthalten in Journal of chemical crystallography Springer US, 1994 42(2012), 6 vom: 02. März, Seite 628-632 (DE-627)182237877 (DE-600)1189288-2 (DE-576)039053679 1074-1542 nnns volume:42 year:2012 number:6 day:02 month:03 pages:628-632 https://doi.org/10.1007/s10870-012-0293-x lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-CHE SSG-OLC-GEO SSG-OLC-PHA SSG-OLC-DE-84 SSG-OPC-GGO GBV_ILN_70 GBV_ILN_2027 GBV_ILN_4012 AR 42 2012 6 02 03 628-632 |
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10.1007/s10870-012-0293-x doi (DE-627)OLC2036724000 (DE-He213)s10870-012-0293-x-p DE-627 ger DE-627 rakwb eng 540 VZ 13 ssgn Luo, Yang-Hui verfasserin aut Syntheses, Crystal Structure and Properties of Two 1-D Coordination Polymers Bridged by Dicyanamides 2012 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Springer Science+Business Media, LLC 2012 Abstract Two new 1-D coordination polymers [MII (3-Bzpy)2(N(CN)2)2] (M = Cd (1), Cu (2), 3-Bzpy = 3-benzoylpyridine) have been synthesized and structurally characterized by single-crystal X-ray diffraction and IR. Single-crystal X-ray diffraction reveals that the complexes 1 and 2 are isostructural and all crystallize in monoclinic P$ 2_{1} $/c space group with cell dimensions: a = 6.3889(16) Å, b = 7.6496(12) Å, c = 26.767(6) Å, β = 99.131(19)°, V = 1291.6(5) $ Å^{3} $, Z = 2 for 1 and a = 6.4483(9) Å, b = 7.5449(10) Å, c = 25.965(4) Å, β = 98.559(10)°, V = 1249.2(3) $ Å^{3} $, Z = 2 for 2. Structure analysis manifest that 1 and 2 are all 1-D chains structures which parallel to the crystallographic b axis through end-to-end coordination by bidentate bridging dicyanamide ligands. Magnetic property of complex 2 was further investigated. Graphical Abstract The paper is about synthesis, crystal structure and magnetic property of two new 1-D coordination polymers. Perspective view down the a-axis of complex 1 with thermal ellipsoids drawn at the 50% probability level . Dicyanamide 1-D chain Crystal structure Magnetic property Ma, Yu-Tao aut Bao, Qian-Qian aut Sun, Bai-Wang aut Enthalten in Journal of chemical crystallography Springer US, 1994 42(2012), 6 vom: 02. März, Seite 628-632 (DE-627)182237877 (DE-600)1189288-2 (DE-576)039053679 1074-1542 nnns volume:42 year:2012 number:6 day:02 month:03 pages:628-632 https://doi.org/10.1007/s10870-012-0293-x lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-CHE SSG-OLC-GEO SSG-OLC-PHA SSG-OLC-DE-84 SSG-OPC-GGO GBV_ILN_70 GBV_ILN_2027 GBV_ILN_4012 AR 42 2012 6 02 03 628-632 |
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10.1007/s10870-012-0293-x doi (DE-627)OLC2036724000 (DE-He213)s10870-012-0293-x-p DE-627 ger DE-627 rakwb eng 540 VZ 13 ssgn Luo, Yang-Hui verfasserin aut Syntheses, Crystal Structure and Properties of Two 1-D Coordination Polymers Bridged by Dicyanamides 2012 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Springer Science+Business Media, LLC 2012 Abstract Two new 1-D coordination polymers [MII (3-Bzpy)2(N(CN)2)2] (M = Cd (1), Cu (2), 3-Bzpy = 3-benzoylpyridine) have been synthesized and structurally characterized by single-crystal X-ray diffraction and IR. Single-crystal X-ray diffraction reveals that the complexes 1 and 2 are isostructural and all crystallize in monoclinic P$ 2_{1} $/c space group with cell dimensions: a = 6.3889(16) Å, b = 7.6496(12) Å, c = 26.767(6) Å, β = 99.131(19)°, V = 1291.6(5) $ Å^{3} $, Z = 2 for 1 and a = 6.4483(9) Å, b = 7.5449(10) Å, c = 25.965(4) Å, β = 98.559(10)°, V = 1249.2(3) $ Å^{3} $, Z = 2 for 2. Structure analysis manifest that 1 and 2 are all 1-D chains structures which parallel to the crystallographic b axis through end-to-end coordination by bidentate bridging dicyanamide ligands. Magnetic property of complex 2 was further investigated. Graphical Abstract The paper is about synthesis, crystal structure and magnetic property of two new 1-D coordination polymers. Perspective view down the a-axis of complex 1 with thermal ellipsoids drawn at the 50% probability level . Dicyanamide 1-D chain Crystal structure Magnetic property Ma, Yu-Tao aut Bao, Qian-Qian aut Sun, Bai-Wang aut Enthalten in Journal of chemical crystallography Springer US, 1994 42(2012), 6 vom: 02. März, Seite 628-632 (DE-627)182237877 (DE-600)1189288-2 (DE-576)039053679 1074-1542 nnns volume:42 year:2012 number:6 day:02 month:03 pages:628-632 https://doi.org/10.1007/s10870-012-0293-x lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-CHE SSG-OLC-GEO SSG-OLC-PHA SSG-OLC-DE-84 SSG-OPC-GGO GBV_ILN_70 GBV_ILN_2027 GBV_ILN_4012 AR 42 2012 6 02 03 628-632 |
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10.1007/s10870-012-0293-x doi (DE-627)OLC2036724000 (DE-He213)s10870-012-0293-x-p DE-627 ger DE-627 rakwb eng 540 VZ 13 ssgn Luo, Yang-Hui verfasserin aut Syntheses, Crystal Structure and Properties of Two 1-D Coordination Polymers Bridged by Dicyanamides 2012 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Springer Science+Business Media, LLC 2012 Abstract Two new 1-D coordination polymers [MII (3-Bzpy)2(N(CN)2)2] (M = Cd (1), Cu (2), 3-Bzpy = 3-benzoylpyridine) have been synthesized and structurally characterized by single-crystal X-ray diffraction and IR. Single-crystal X-ray diffraction reveals that the complexes 1 and 2 are isostructural and all crystallize in monoclinic P$ 2_{1} $/c space group with cell dimensions: a = 6.3889(16) Å, b = 7.6496(12) Å, c = 26.767(6) Å, β = 99.131(19)°, V = 1291.6(5) $ Å^{3} $, Z = 2 for 1 and a = 6.4483(9) Å, b = 7.5449(10) Å, c = 25.965(4) Å, β = 98.559(10)°, V = 1249.2(3) $ Å^{3} $, Z = 2 for 2. Structure analysis manifest that 1 and 2 are all 1-D chains structures which parallel to the crystallographic b axis through end-to-end coordination by bidentate bridging dicyanamide ligands. Magnetic property of complex 2 was further investigated. Graphical Abstract The paper is about synthesis, crystal structure and magnetic property of two new 1-D coordination polymers. Perspective view down the a-axis of complex 1 with thermal ellipsoids drawn at the 50% probability level . Dicyanamide 1-D chain Crystal structure Magnetic property Ma, Yu-Tao aut Bao, Qian-Qian aut Sun, Bai-Wang aut Enthalten in Journal of chemical crystallography Springer US, 1994 42(2012), 6 vom: 02. März, Seite 628-632 (DE-627)182237877 (DE-600)1189288-2 (DE-576)039053679 1074-1542 nnns volume:42 year:2012 number:6 day:02 month:03 pages:628-632 https://doi.org/10.1007/s10870-012-0293-x lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-CHE SSG-OLC-GEO SSG-OLC-PHA SSG-OLC-DE-84 SSG-OPC-GGO GBV_ILN_70 GBV_ILN_2027 GBV_ILN_4012 AR 42 2012 6 02 03 628-632 |
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10.1007/s10870-012-0293-x doi (DE-627)OLC2036724000 (DE-He213)s10870-012-0293-x-p DE-627 ger DE-627 rakwb eng 540 VZ 13 ssgn Luo, Yang-Hui verfasserin aut Syntheses, Crystal Structure and Properties of Two 1-D Coordination Polymers Bridged by Dicyanamides 2012 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Springer Science+Business Media, LLC 2012 Abstract Two new 1-D coordination polymers [MII (3-Bzpy)2(N(CN)2)2] (M = Cd (1), Cu (2), 3-Bzpy = 3-benzoylpyridine) have been synthesized and structurally characterized by single-crystal X-ray diffraction and IR. Single-crystal X-ray diffraction reveals that the complexes 1 and 2 are isostructural and all crystallize in monoclinic P$ 2_{1} $/c space group with cell dimensions: a = 6.3889(16) Å, b = 7.6496(12) Å, c = 26.767(6) Å, β = 99.131(19)°, V = 1291.6(5) $ Å^{3} $, Z = 2 for 1 and a = 6.4483(9) Å, b = 7.5449(10) Å, c = 25.965(4) Å, β = 98.559(10)°, V = 1249.2(3) $ Å^{3} $, Z = 2 for 2. Structure analysis manifest that 1 and 2 are all 1-D chains structures which parallel to the crystallographic b axis through end-to-end coordination by bidentate bridging dicyanamide ligands. Magnetic property of complex 2 was further investigated. Graphical Abstract The paper is about synthesis, crystal structure and magnetic property of two new 1-D coordination polymers. Perspective view down the a-axis of complex 1 with thermal ellipsoids drawn at the 50% probability level . Dicyanamide 1-D chain Crystal structure Magnetic property Ma, Yu-Tao aut Bao, Qian-Qian aut Sun, Bai-Wang aut Enthalten in Journal of chemical crystallography Springer US, 1994 42(2012), 6 vom: 02. März, Seite 628-632 (DE-627)182237877 (DE-600)1189288-2 (DE-576)039053679 1074-1542 nnns volume:42 year:2012 number:6 day:02 month:03 pages:628-632 https://doi.org/10.1007/s10870-012-0293-x lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-CHE SSG-OLC-GEO SSG-OLC-PHA SSG-OLC-DE-84 SSG-OPC-GGO GBV_ILN_70 GBV_ILN_2027 GBV_ILN_4012 AR 42 2012 6 02 03 628-632 |
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540 VZ 13 ssgn Syntheses, Crystal Structure and Properties of Two 1-D Coordination Polymers Bridged by Dicyanamides Dicyanamide 1-D chain Crystal structure Magnetic property |
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Syntheses, Crystal Structure and Properties of Two 1-D Coordination Polymers Bridged by Dicyanamides |
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Syntheses, Crystal Structure and Properties of Two 1-D Coordination Polymers Bridged by Dicyanamides |
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Luo, Yang-Hui |
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Journal of chemical crystallography |
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2012 |
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Luo, Yang-Hui Ma, Yu-Tao Bao, Qian-Qian Sun, Bai-Wang |
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syntheses, crystal structure and properties of two 1-d coordination polymers bridged by dicyanamides |
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Syntheses, Crystal Structure and Properties of Two 1-D Coordination Polymers Bridged by Dicyanamides |
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Abstract Two new 1-D coordination polymers [MII (3-Bzpy)2(N(CN)2)2] (M = Cd (1), Cu (2), 3-Bzpy = 3-benzoylpyridine) have been synthesized and structurally characterized by single-crystal X-ray diffraction and IR. Single-crystal X-ray diffraction reveals that the complexes 1 and 2 are isostructural and all crystallize in monoclinic P$ 2_{1} $/c space group with cell dimensions: a = 6.3889(16) Å, b = 7.6496(12) Å, c = 26.767(6) Å, β = 99.131(19)°, V = 1291.6(5) $ Å^{3} $, Z = 2 for 1 and a = 6.4483(9) Å, b = 7.5449(10) Å, c = 25.965(4) Å, β = 98.559(10)°, V = 1249.2(3) $ Å^{3} $, Z = 2 for 2. Structure analysis manifest that 1 and 2 are all 1-D chains structures which parallel to the crystallographic b axis through end-to-end coordination by bidentate bridging dicyanamide ligands. Magnetic property of complex 2 was further investigated. Graphical Abstract The paper is about synthesis, crystal structure and magnetic property of two new 1-D coordination polymers. Perspective view down the a-axis of complex 1 with thermal ellipsoids drawn at the 50% probability level . © Springer Science+Business Media, LLC 2012 |
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Abstract Two new 1-D coordination polymers [MII (3-Bzpy)2(N(CN)2)2] (M = Cd (1), Cu (2), 3-Bzpy = 3-benzoylpyridine) have been synthesized and structurally characterized by single-crystal X-ray diffraction and IR. Single-crystal X-ray diffraction reveals that the complexes 1 and 2 are isostructural and all crystallize in monoclinic P$ 2_{1} $/c space group with cell dimensions: a = 6.3889(16) Å, b = 7.6496(12) Å, c = 26.767(6) Å, β = 99.131(19)°, V = 1291.6(5) $ Å^{3} $, Z = 2 for 1 and a = 6.4483(9) Å, b = 7.5449(10) Å, c = 25.965(4) Å, β = 98.559(10)°, V = 1249.2(3) $ Å^{3} $, Z = 2 for 2. Structure analysis manifest that 1 and 2 are all 1-D chains structures which parallel to the crystallographic b axis through end-to-end coordination by bidentate bridging dicyanamide ligands. Magnetic property of complex 2 was further investigated. Graphical Abstract The paper is about synthesis, crystal structure and magnetic property of two new 1-D coordination polymers. Perspective view down the a-axis of complex 1 with thermal ellipsoids drawn at the 50% probability level . © Springer Science+Business Media, LLC 2012 |
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Abstract Two new 1-D coordination polymers [MII (3-Bzpy)2(N(CN)2)2] (M = Cd (1), Cu (2), 3-Bzpy = 3-benzoylpyridine) have been synthesized and structurally characterized by single-crystal X-ray diffraction and IR. Single-crystal X-ray diffraction reveals that the complexes 1 and 2 are isostructural and all crystallize in monoclinic P$ 2_{1} $/c space group with cell dimensions: a = 6.3889(16) Å, b = 7.6496(12) Å, c = 26.767(6) Å, β = 99.131(19)°, V = 1291.6(5) $ Å^{3} $, Z = 2 for 1 and a = 6.4483(9) Å, b = 7.5449(10) Å, c = 25.965(4) Å, β = 98.559(10)°, V = 1249.2(3) $ Å^{3} $, Z = 2 for 2. Structure analysis manifest that 1 and 2 are all 1-D chains structures which parallel to the crystallographic b axis through end-to-end coordination by bidentate bridging dicyanamide ligands. Magnetic property of complex 2 was further investigated. Graphical Abstract The paper is about synthesis, crystal structure and magnetic property of two new 1-D coordination polymers. Perspective view down the a-axis of complex 1 with thermal ellipsoids drawn at the 50% probability level . © Springer Science+Business Media, LLC 2012 |
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Syntheses, Crystal Structure and Properties of Two 1-D Coordination Polymers Bridged by Dicyanamides |
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