Template synthesis and water vapor adsorption by micro- and mesoporous silica gels with high specific surface area
Abstract Micro- and mesoporous silica gels have been synthesized in the basic medium using a mixture of distilled primary alkylamines as a structure-forming agent. The silica gels’ porosity characteristics have been investigated by the method of nitrogen low-temperature adsorption. The specific surf...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Puzyrev, I. S. [verfasserIn] |
|---|
| Format: |
Artikel |
|---|---|
| Sprache: |
Englisch |
| Erschienen: |
2015 |
|---|
| Schlagwörter: |
|---|
| Anmerkung: |
© Pleiades Publishing, Ltd. 2015 |
|---|
| Übergeordnetes Werk: |
Enthalten in: Glass physics and chemistry - Pleiades Publishing, 1993, 41(2015), 2 vom: März, Seite 187-193 |
|---|---|
| Übergeordnetes Werk: |
volume:41 ; year:2015 ; number:2 ; month:03 ; pages:187-193 |
| Links: |
|---|
| DOI / URN: |
10.1134/S1087659615020108 |
|---|
| Katalog-ID: |
OLC2039276823 |
|---|
| LEADER | 01000caa a22002652 4500 | ||
|---|---|---|---|
| 001 | OLC2039276823 | ||
| 003 | DE-627 | ||
| 005 | 20230516072705.0 | ||
| 007 | tu | ||
| 008 | 200819s2015 xx ||||| 00| ||eng c | ||
| 024 | 7 | |a 10.1134/S1087659615020108 |2 doi | |
| 035 | |a (DE-627)OLC2039276823 | ||
| 035 | |a (DE-He213)S1087659615020108-p | ||
| 040 | |a DE-627 |b ger |c DE-627 |e rakwb | ||
| 041 | |a eng | ||
| 082 | 0 | 4 | |a 330 |q VZ |
| 100 | 1 | |a Puzyrev, I. S. |e verfasserin |4 aut | |
| 245 | 1 | 0 | |a Template synthesis and water vapor adsorption by micro- and mesoporous silica gels with high specific surface area |
| 264 | 1 | |c 2015 | |
| 336 | |a Text |b txt |2 rdacontent | ||
| 337 | |a ohne Hilfsmittel zu benutzen |b n |2 rdamedia | ||
| 338 | |a Band |b nc |2 rdacarrier | ||
| 500 | |a © Pleiades Publishing, Ltd. 2015 | ||
| 520 | |a Abstract Micro- and mesoporous silica gels have been synthesized in the basic medium using a mixture of distilled primary alkylamines as a structure-forming agent. The silica gels’ porosity characteristics have been investigated by the method of nitrogen low-temperature adsorption. The specific surface area of mesoporous silica gels is in the range 1392–1568 $ m^{2} $/g, whereas for silica gels containing micropores (aside from mesopores) this value ranges from 887 to 1259 $ m^{2} $/g; the pore volumes are 0.68–0.79 $ cm^{3} $/g and 0.81–0.97 $ cm^{3} $/g, respectively. The 29Si NMR spectroscopy data demonstrate high degree of cohesiveness of the mesoporous silica gel and the predominant cohesiveness type (Q4), while the type Q3 characterizes samples containing both pore types. Adsorption of water vapor on the latter ones starts at lower relative vapor pressure in comparison with mesoporous samples. | ||
| 650 | 4 | |a mesoporous silica gels | |
| 650 | 4 | |a template synthesis | |
| 650 | 4 | |a water vapor adsorption | |
| 700 | 1 | |a Sobina, E. P. |4 aut | |
| 700 | 1 | |a Adamova, L. V. |4 aut | |
| 700 | 1 | |a Kodess, M. I. |4 aut | |
| 700 | 1 | |a Medvedevskikh, S. V. |4 aut | |
| 773 | 0 | 8 | |i Enthalten in |t Glass physics and chemistry |d Pleiades Publishing, 1993 |g 41(2015), 2 vom: März, Seite 187-193 |w (DE-627)182171957 |w (DE-600)1182895-X |w (DE-576)9182171955 |x 1087-6596 |7 nnns |
| 773 | 1 | 8 | |g volume:41 |g year:2015 |g number:2 |g month:03 |g pages:187-193 |
| 856 | 4 | 1 | |u https://doi.org/10.1134/S1087659615020108 |z lizenzpflichtig |3 Volltext |
| 912 | |a GBV_USEFLAG_A | ||
| 912 | |a SYSFLAG_A | ||
| 912 | |a GBV_OLC | ||
| 912 | |a SSG-OLC-TEC | ||
| 912 | |a SSG-OLC-CHE | ||
| 912 | |a SSG-OLC-PHA | ||
| 912 | |a SSG-OLC-DE-84 | ||
| 912 | |a GBV_ILN_70 | ||
| 951 | |a AR | ||
| 952 | |d 41 |j 2015 |e 2 |c 03 |h 187-193 | ||
| author_variant |
i s p is isp e p s ep eps l v a lv lva m i k mi mik s v m sv svm |
|---|---|
| matchkey_str |
article:10876596:2015----::epaeyteiadaevprdopinyiradeooosiiaesi |
| hierarchy_sort_str |
2015 |
| publishDate |
2015 |
| allfields |
10.1134/S1087659615020108 doi (DE-627)OLC2039276823 (DE-He213)S1087659615020108-p DE-627 ger DE-627 rakwb eng 330 VZ Puzyrev, I. S. verfasserin aut Template synthesis and water vapor adsorption by micro- and mesoporous silica gels with high specific surface area 2015 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Pleiades Publishing, Ltd. 2015 Abstract Micro- and mesoporous silica gels have been synthesized in the basic medium using a mixture of distilled primary alkylamines as a structure-forming agent. The silica gels’ porosity characteristics have been investigated by the method of nitrogen low-temperature adsorption. The specific surface area of mesoporous silica gels is in the range 1392–1568 $ m^{2} $/g, whereas for silica gels containing micropores (aside from mesopores) this value ranges from 887 to 1259 $ m^{2} $/g; the pore volumes are 0.68–0.79 $ cm^{3} $/g and 0.81–0.97 $ cm^{3} $/g, respectively. The 29Si NMR spectroscopy data demonstrate high degree of cohesiveness of the mesoporous silica gel and the predominant cohesiveness type (Q4), while the type Q3 characterizes samples containing both pore types. Adsorption of water vapor on the latter ones starts at lower relative vapor pressure in comparison with mesoporous samples. mesoporous silica gels template synthesis water vapor adsorption Sobina, E. P. aut Adamova, L. V. aut Kodess, M. I. aut Medvedevskikh, S. V. aut Enthalten in Glass physics and chemistry Pleiades Publishing, 1993 41(2015), 2 vom: März, Seite 187-193 (DE-627)182171957 (DE-600)1182895-X (DE-576)9182171955 1087-6596 nnns volume:41 year:2015 number:2 month:03 pages:187-193 https://doi.org/10.1134/S1087659615020108 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE SSG-OLC-PHA SSG-OLC-DE-84 GBV_ILN_70 AR 41 2015 2 03 187-193 |
| spelling |
10.1134/S1087659615020108 doi (DE-627)OLC2039276823 (DE-He213)S1087659615020108-p DE-627 ger DE-627 rakwb eng 330 VZ Puzyrev, I. S. verfasserin aut Template synthesis and water vapor adsorption by micro- and mesoporous silica gels with high specific surface area 2015 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Pleiades Publishing, Ltd. 2015 Abstract Micro- and mesoporous silica gels have been synthesized in the basic medium using a mixture of distilled primary alkylamines as a structure-forming agent. The silica gels’ porosity characteristics have been investigated by the method of nitrogen low-temperature adsorption. The specific surface area of mesoporous silica gels is in the range 1392–1568 $ m^{2} $/g, whereas for silica gels containing micropores (aside from mesopores) this value ranges from 887 to 1259 $ m^{2} $/g; the pore volumes are 0.68–0.79 $ cm^{3} $/g and 0.81–0.97 $ cm^{3} $/g, respectively. The 29Si NMR spectroscopy data demonstrate high degree of cohesiveness of the mesoporous silica gel and the predominant cohesiveness type (Q4), while the type Q3 characterizes samples containing both pore types. Adsorption of water vapor on the latter ones starts at lower relative vapor pressure in comparison with mesoporous samples. mesoporous silica gels template synthesis water vapor adsorption Sobina, E. P. aut Adamova, L. V. aut Kodess, M. I. aut Medvedevskikh, S. V. aut Enthalten in Glass physics and chemistry Pleiades Publishing, 1993 41(2015), 2 vom: März, Seite 187-193 (DE-627)182171957 (DE-600)1182895-X (DE-576)9182171955 1087-6596 nnns volume:41 year:2015 number:2 month:03 pages:187-193 https://doi.org/10.1134/S1087659615020108 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE SSG-OLC-PHA SSG-OLC-DE-84 GBV_ILN_70 AR 41 2015 2 03 187-193 |
| allfields_unstemmed |
10.1134/S1087659615020108 doi (DE-627)OLC2039276823 (DE-He213)S1087659615020108-p DE-627 ger DE-627 rakwb eng 330 VZ Puzyrev, I. S. verfasserin aut Template synthesis and water vapor adsorption by micro- and mesoporous silica gels with high specific surface area 2015 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Pleiades Publishing, Ltd. 2015 Abstract Micro- and mesoporous silica gels have been synthesized in the basic medium using a mixture of distilled primary alkylamines as a structure-forming agent. The silica gels’ porosity characteristics have been investigated by the method of nitrogen low-temperature adsorption. The specific surface area of mesoporous silica gels is in the range 1392–1568 $ m^{2} $/g, whereas for silica gels containing micropores (aside from mesopores) this value ranges from 887 to 1259 $ m^{2} $/g; the pore volumes are 0.68–0.79 $ cm^{3} $/g and 0.81–0.97 $ cm^{3} $/g, respectively. The 29Si NMR spectroscopy data demonstrate high degree of cohesiveness of the mesoporous silica gel and the predominant cohesiveness type (Q4), while the type Q3 characterizes samples containing both pore types. Adsorption of water vapor on the latter ones starts at lower relative vapor pressure in comparison with mesoporous samples. mesoporous silica gels template synthesis water vapor adsorption Sobina, E. P. aut Adamova, L. V. aut Kodess, M. I. aut Medvedevskikh, S. V. aut Enthalten in Glass physics and chemistry Pleiades Publishing, 1993 41(2015), 2 vom: März, Seite 187-193 (DE-627)182171957 (DE-600)1182895-X (DE-576)9182171955 1087-6596 nnns volume:41 year:2015 number:2 month:03 pages:187-193 https://doi.org/10.1134/S1087659615020108 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE SSG-OLC-PHA SSG-OLC-DE-84 GBV_ILN_70 AR 41 2015 2 03 187-193 |
| allfieldsGer |
10.1134/S1087659615020108 doi (DE-627)OLC2039276823 (DE-He213)S1087659615020108-p DE-627 ger DE-627 rakwb eng 330 VZ Puzyrev, I. S. verfasserin aut Template synthesis and water vapor adsorption by micro- and mesoporous silica gels with high specific surface area 2015 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Pleiades Publishing, Ltd. 2015 Abstract Micro- and mesoporous silica gels have been synthesized in the basic medium using a mixture of distilled primary alkylamines as a structure-forming agent. The silica gels’ porosity characteristics have been investigated by the method of nitrogen low-temperature adsorption. The specific surface area of mesoporous silica gels is in the range 1392–1568 $ m^{2} $/g, whereas for silica gels containing micropores (aside from mesopores) this value ranges from 887 to 1259 $ m^{2} $/g; the pore volumes are 0.68–0.79 $ cm^{3} $/g and 0.81–0.97 $ cm^{3} $/g, respectively. The 29Si NMR spectroscopy data demonstrate high degree of cohesiveness of the mesoporous silica gel and the predominant cohesiveness type (Q4), while the type Q3 characterizes samples containing both pore types. Adsorption of water vapor on the latter ones starts at lower relative vapor pressure in comparison with mesoporous samples. mesoporous silica gels template synthesis water vapor adsorption Sobina, E. P. aut Adamova, L. V. aut Kodess, M. I. aut Medvedevskikh, S. V. aut Enthalten in Glass physics and chemistry Pleiades Publishing, 1993 41(2015), 2 vom: März, Seite 187-193 (DE-627)182171957 (DE-600)1182895-X (DE-576)9182171955 1087-6596 nnns volume:41 year:2015 number:2 month:03 pages:187-193 https://doi.org/10.1134/S1087659615020108 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE SSG-OLC-PHA SSG-OLC-DE-84 GBV_ILN_70 AR 41 2015 2 03 187-193 |
| allfieldsSound |
10.1134/S1087659615020108 doi (DE-627)OLC2039276823 (DE-He213)S1087659615020108-p DE-627 ger DE-627 rakwb eng 330 VZ Puzyrev, I. S. verfasserin aut Template synthesis and water vapor adsorption by micro- and mesoporous silica gels with high specific surface area 2015 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Pleiades Publishing, Ltd. 2015 Abstract Micro- and mesoporous silica gels have been synthesized in the basic medium using a mixture of distilled primary alkylamines as a structure-forming agent. The silica gels’ porosity characteristics have been investigated by the method of nitrogen low-temperature adsorption. The specific surface area of mesoporous silica gels is in the range 1392–1568 $ m^{2} $/g, whereas for silica gels containing micropores (aside from mesopores) this value ranges from 887 to 1259 $ m^{2} $/g; the pore volumes are 0.68–0.79 $ cm^{3} $/g and 0.81–0.97 $ cm^{3} $/g, respectively. The 29Si NMR spectroscopy data demonstrate high degree of cohesiveness of the mesoporous silica gel and the predominant cohesiveness type (Q4), while the type Q3 characterizes samples containing both pore types. Adsorption of water vapor on the latter ones starts at lower relative vapor pressure in comparison with mesoporous samples. mesoporous silica gels template synthesis water vapor adsorption Sobina, E. P. aut Adamova, L. V. aut Kodess, M. I. aut Medvedevskikh, S. V. aut Enthalten in Glass physics and chemistry Pleiades Publishing, 1993 41(2015), 2 vom: März, Seite 187-193 (DE-627)182171957 (DE-600)1182895-X (DE-576)9182171955 1087-6596 nnns volume:41 year:2015 number:2 month:03 pages:187-193 https://doi.org/10.1134/S1087659615020108 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE SSG-OLC-PHA SSG-OLC-DE-84 GBV_ILN_70 AR 41 2015 2 03 187-193 |
| language |
English |
| source |
Enthalten in Glass physics and chemistry 41(2015), 2 vom: März, Seite 187-193 volume:41 year:2015 number:2 month:03 pages:187-193 |
| sourceStr |
Enthalten in Glass physics and chemistry 41(2015), 2 vom: März, Seite 187-193 volume:41 year:2015 number:2 month:03 pages:187-193 |
| format_phy_str_mv |
Article |
| institution |
findex.gbv.de |
| topic_facet |
mesoporous silica gels template synthesis water vapor adsorption |
| dewey-raw |
330 |
| isfreeaccess_bool |
false |
| container_title |
Glass physics and chemistry |
| authorswithroles_txt_mv |
Puzyrev, I. S. @@aut@@ Sobina, E. P. @@aut@@ Adamova, L. V. @@aut@@ Kodess, M. I. @@aut@@ Medvedevskikh, S. V. @@aut@@ |
| publishDateDaySort_date |
2015-03-01T00:00:00Z |
| hierarchy_top_id |
182171957 |
| dewey-sort |
3330 |
| id |
OLC2039276823 |
| language_de |
englisch |
| fullrecord |
<?xml version="1.0" encoding="UTF-8"?><collection xmlns="http://www.loc.gov/MARC21/slim"><record><leader>01000caa a22002652 4500</leader><controlfield tag="001">OLC2039276823</controlfield><controlfield tag="003">DE-627</controlfield><controlfield tag="005">20230516072705.0</controlfield><controlfield tag="007">tu</controlfield><controlfield tag="008">200819s2015 xx ||||| 00| ||eng c</controlfield><datafield tag="024" ind1="7" ind2=" "><subfield code="a">10.1134/S1087659615020108</subfield><subfield code="2">doi</subfield></datafield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(DE-627)OLC2039276823</subfield></datafield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(DE-He213)S1087659615020108-p</subfield></datafield><datafield tag="040" ind1=" " ind2=" "><subfield code="a">DE-627</subfield><subfield code="b">ger</subfield><subfield code="c">DE-627</subfield><subfield code="e">rakwb</subfield></datafield><datafield tag="041" ind1=" " ind2=" "><subfield code="a">eng</subfield></datafield><datafield tag="082" ind1="0" ind2="4"><subfield code="a">330</subfield><subfield code="q">VZ</subfield></datafield><datafield tag="100" ind1="1" ind2=" "><subfield code="a">Puzyrev, I. S.</subfield><subfield code="e">verfasserin</subfield><subfield code="4">aut</subfield></datafield><datafield tag="245" ind1="1" ind2="0"><subfield code="a">Template synthesis and water vapor adsorption by micro- and mesoporous silica gels with high specific surface area</subfield></datafield><datafield tag="264" ind1=" " ind2="1"><subfield code="c">2015</subfield></datafield><datafield tag="336" ind1=" " ind2=" "><subfield code="a">Text</subfield><subfield code="b">txt</subfield><subfield code="2">rdacontent</subfield></datafield><datafield tag="337" ind1=" " ind2=" "><subfield code="a">ohne Hilfsmittel zu benutzen</subfield><subfield code="b">n</subfield><subfield code="2">rdamedia</subfield></datafield><datafield tag="338" ind1=" " ind2=" "><subfield code="a">Band</subfield><subfield code="b">nc</subfield><subfield code="2">rdacarrier</subfield></datafield><datafield tag="500" ind1=" " ind2=" "><subfield code="a">© Pleiades Publishing, Ltd. 2015</subfield></datafield><datafield tag="520" ind1=" " ind2=" "><subfield code="a">Abstract Micro- and mesoporous silica gels have been synthesized in the basic medium using a mixture of distilled primary alkylamines as a structure-forming agent. The silica gels’ porosity characteristics have been investigated by the method of nitrogen low-temperature adsorption. The specific surface area of mesoporous silica gels is in the range 1392–1568 $ m^{2} $/g, whereas for silica gels containing micropores (aside from mesopores) this value ranges from 887 to 1259 $ m^{2} $/g; the pore volumes are 0.68–0.79 $ cm^{3} $/g and 0.81–0.97 $ cm^{3} $/g, respectively. The 29Si NMR spectroscopy data demonstrate high degree of cohesiveness of the mesoporous silica gel and the predominant cohesiveness type (Q4), while the type Q3 characterizes samples containing both pore types. Adsorption of water vapor on the latter ones starts at lower relative vapor pressure in comparison with mesoporous samples.</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">mesoporous silica gels</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">template synthesis</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">water vapor adsorption</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Sobina, E. P.</subfield><subfield code="4">aut</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Adamova, L. V.</subfield><subfield code="4">aut</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Kodess, M. I.</subfield><subfield code="4">aut</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Medvedevskikh, S. V.</subfield><subfield code="4">aut</subfield></datafield><datafield tag="773" ind1="0" ind2="8"><subfield code="i">Enthalten in</subfield><subfield code="t">Glass physics and chemistry</subfield><subfield code="d">Pleiades Publishing, 1993</subfield><subfield code="g">41(2015), 2 vom: März, Seite 187-193</subfield><subfield code="w">(DE-627)182171957</subfield><subfield code="w">(DE-600)1182895-X</subfield><subfield code="w">(DE-576)9182171955</subfield><subfield code="x">1087-6596</subfield><subfield code="7">nnns</subfield></datafield><datafield tag="773" ind1="1" ind2="8"><subfield code="g">volume:41</subfield><subfield code="g">year:2015</subfield><subfield code="g">number:2</subfield><subfield code="g">month:03</subfield><subfield code="g">pages:187-193</subfield></datafield><datafield tag="856" ind1="4" ind2="1"><subfield code="u">https://doi.org/10.1134/S1087659615020108</subfield><subfield code="z">lizenzpflichtig</subfield><subfield code="3">Volltext</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_USEFLAG_A</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">SYSFLAG_A</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_OLC</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">SSG-OLC-TEC</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">SSG-OLC-CHE</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">SSG-OLC-PHA</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">SSG-OLC-DE-84</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_70</subfield></datafield><datafield tag="951" ind1=" " ind2=" "><subfield code="a">AR</subfield></datafield><datafield tag="952" ind1=" " ind2=" "><subfield code="d">41</subfield><subfield code="j">2015</subfield><subfield code="e">2</subfield><subfield code="c">03</subfield><subfield code="h">187-193</subfield></datafield></record></collection>
|
| author |
Puzyrev, I. S. |
| spellingShingle |
Puzyrev, I. S. ddc 330 misc mesoporous silica gels misc template synthesis misc water vapor adsorption Template synthesis and water vapor adsorption by micro- and mesoporous silica gels with high specific surface area |
| authorStr |
Puzyrev, I. S. |
| ppnlink_with_tag_str_mv |
@@773@@(DE-627)182171957 |
| format |
Article |
| dewey-ones |
330 - Economics |
| delete_txt_mv |
keep |
| author_role |
aut aut aut aut aut |
| collection |
OLC |
| remote_str |
false |
| illustrated |
Not Illustrated |
| issn |
1087-6596 |
| topic_title |
330 VZ Template synthesis and water vapor adsorption by micro- and mesoporous silica gels with high specific surface area mesoporous silica gels template synthesis water vapor adsorption |
| topic |
ddc 330 misc mesoporous silica gels misc template synthesis misc water vapor adsorption |
| topic_unstemmed |
ddc 330 misc mesoporous silica gels misc template synthesis misc water vapor adsorption |
| topic_browse |
ddc 330 misc mesoporous silica gels misc template synthesis misc water vapor adsorption |
| format_facet |
Aufsätze Gedruckte Aufsätze |
| format_main_str_mv |
Text Zeitschrift/Artikel |
| carriertype_str_mv |
nc |
| hierarchy_parent_title |
Glass physics and chemistry |
| hierarchy_parent_id |
182171957 |
| dewey-tens |
330 - Economics |
| hierarchy_top_title |
Glass physics and chemistry |
| isfreeaccess_txt |
false |
| familylinks_str_mv |
(DE-627)182171957 (DE-600)1182895-X (DE-576)9182171955 |
| title |
Template synthesis and water vapor adsorption by micro- and mesoporous silica gels with high specific surface area |
| ctrlnum |
(DE-627)OLC2039276823 (DE-He213)S1087659615020108-p |
| title_full |
Template synthesis and water vapor adsorption by micro- and mesoporous silica gels with high specific surface area |
| author_sort |
Puzyrev, I. S. |
| journal |
Glass physics and chemistry |
| journalStr |
Glass physics and chemistry |
| lang_code |
eng |
| isOA_bool |
false |
| dewey-hundreds |
300 - Social sciences |
| recordtype |
marc |
| publishDateSort |
2015 |
| contenttype_str_mv |
txt |
| container_start_page |
187 |
| author_browse |
Puzyrev, I. S. Sobina, E. P. Adamova, L. V. Kodess, M. I. Medvedevskikh, S. V. |
| container_volume |
41 |
| class |
330 VZ |
| format_se |
Aufsätze |
| author-letter |
Puzyrev, I. S. |
| doi_str_mv |
10.1134/S1087659615020108 |
| dewey-full |
330 |
| title_sort |
template synthesis and water vapor adsorption by micro- and mesoporous silica gels with high specific surface area |
| title_auth |
Template synthesis and water vapor adsorption by micro- and mesoporous silica gels with high specific surface area |
| abstract |
Abstract Micro- and mesoporous silica gels have been synthesized in the basic medium using a mixture of distilled primary alkylamines as a structure-forming agent. The silica gels’ porosity characteristics have been investigated by the method of nitrogen low-temperature adsorption. The specific surface area of mesoporous silica gels is in the range 1392–1568 $ m^{2} $/g, whereas for silica gels containing micropores (aside from mesopores) this value ranges from 887 to 1259 $ m^{2} $/g; the pore volumes are 0.68–0.79 $ cm^{3} $/g and 0.81–0.97 $ cm^{3} $/g, respectively. The 29Si NMR spectroscopy data demonstrate high degree of cohesiveness of the mesoporous silica gel and the predominant cohesiveness type (Q4), while the type Q3 characterizes samples containing both pore types. Adsorption of water vapor on the latter ones starts at lower relative vapor pressure in comparison with mesoporous samples. © Pleiades Publishing, Ltd. 2015 |
| abstractGer |
Abstract Micro- and mesoporous silica gels have been synthesized in the basic medium using a mixture of distilled primary alkylamines as a structure-forming agent. The silica gels’ porosity characteristics have been investigated by the method of nitrogen low-temperature adsorption. The specific surface area of mesoporous silica gels is in the range 1392–1568 $ m^{2} $/g, whereas for silica gels containing micropores (aside from mesopores) this value ranges from 887 to 1259 $ m^{2} $/g; the pore volumes are 0.68–0.79 $ cm^{3} $/g and 0.81–0.97 $ cm^{3} $/g, respectively. The 29Si NMR spectroscopy data demonstrate high degree of cohesiveness of the mesoporous silica gel and the predominant cohesiveness type (Q4), while the type Q3 characterizes samples containing both pore types. Adsorption of water vapor on the latter ones starts at lower relative vapor pressure in comparison with mesoporous samples. © Pleiades Publishing, Ltd. 2015 |
| abstract_unstemmed |
Abstract Micro- and mesoporous silica gels have been synthesized in the basic medium using a mixture of distilled primary alkylamines as a structure-forming agent. The silica gels’ porosity characteristics have been investigated by the method of nitrogen low-temperature adsorption. The specific surface area of mesoporous silica gels is in the range 1392–1568 $ m^{2} $/g, whereas for silica gels containing micropores (aside from mesopores) this value ranges from 887 to 1259 $ m^{2} $/g; the pore volumes are 0.68–0.79 $ cm^{3} $/g and 0.81–0.97 $ cm^{3} $/g, respectively. The 29Si NMR spectroscopy data demonstrate high degree of cohesiveness of the mesoporous silica gel and the predominant cohesiveness type (Q4), while the type Q3 characterizes samples containing both pore types. Adsorption of water vapor on the latter ones starts at lower relative vapor pressure in comparison with mesoporous samples. © Pleiades Publishing, Ltd. 2015 |
| collection_details |
GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE SSG-OLC-PHA SSG-OLC-DE-84 GBV_ILN_70 |
| container_issue |
2 |
| title_short |
Template synthesis and water vapor adsorption by micro- and mesoporous silica gels with high specific surface area |
| url |
https://doi.org/10.1134/S1087659615020108 |
| remote_bool |
false |
| author2 |
Sobina, E. P. Adamova, L. V. Kodess, M. I. Medvedevskikh, S. V. |
| author2Str |
Sobina, E. P. Adamova, L. V. Kodess, M. I. Medvedevskikh, S. V. |
| ppnlink |
182171957 |
| mediatype_str_mv |
n |
| isOA_txt |
false |
| hochschulschrift_bool |
false |
| doi_str |
10.1134/S1087659615020108 |
| up_date |
2024-07-03T22:08:43.203Z |
| _version_ |
1803597405964206080 |
| fullrecord_marcxml |
<?xml version="1.0" encoding="UTF-8"?><collection xmlns="http://www.loc.gov/MARC21/slim"><record><leader>01000caa a22002652 4500</leader><controlfield tag="001">OLC2039276823</controlfield><controlfield tag="003">DE-627</controlfield><controlfield tag="005">20230516072705.0</controlfield><controlfield tag="007">tu</controlfield><controlfield tag="008">200819s2015 xx ||||| 00| ||eng c</controlfield><datafield tag="024" ind1="7" ind2=" "><subfield code="a">10.1134/S1087659615020108</subfield><subfield code="2">doi</subfield></datafield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(DE-627)OLC2039276823</subfield></datafield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(DE-He213)S1087659615020108-p</subfield></datafield><datafield tag="040" ind1=" " ind2=" "><subfield code="a">DE-627</subfield><subfield code="b">ger</subfield><subfield code="c">DE-627</subfield><subfield code="e">rakwb</subfield></datafield><datafield tag="041" ind1=" " ind2=" "><subfield code="a">eng</subfield></datafield><datafield tag="082" ind1="0" ind2="4"><subfield code="a">330</subfield><subfield code="q">VZ</subfield></datafield><datafield tag="100" ind1="1" ind2=" "><subfield code="a">Puzyrev, I. S.</subfield><subfield code="e">verfasserin</subfield><subfield code="4">aut</subfield></datafield><datafield tag="245" ind1="1" ind2="0"><subfield code="a">Template synthesis and water vapor adsorption by micro- and mesoporous silica gels with high specific surface area</subfield></datafield><datafield tag="264" ind1=" " ind2="1"><subfield code="c">2015</subfield></datafield><datafield tag="336" ind1=" " ind2=" "><subfield code="a">Text</subfield><subfield code="b">txt</subfield><subfield code="2">rdacontent</subfield></datafield><datafield tag="337" ind1=" " ind2=" "><subfield code="a">ohne Hilfsmittel zu benutzen</subfield><subfield code="b">n</subfield><subfield code="2">rdamedia</subfield></datafield><datafield tag="338" ind1=" " ind2=" "><subfield code="a">Band</subfield><subfield code="b">nc</subfield><subfield code="2">rdacarrier</subfield></datafield><datafield tag="500" ind1=" " ind2=" "><subfield code="a">© Pleiades Publishing, Ltd. 2015</subfield></datafield><datafield tag="520" ind1=" " ind2=" "><subfield code="a">Abstract Micro- and mesoporous silica gels have been synthesized in the basic medium using a mixture of distilled primary alkylamines as a structure-forming agent. The silica gels’ porosity characteristics have been investigated by the method of nitrogen low-temperature adsorption. The specific surface area of mesoporous silica gels is in the range 1392–1568 $ m^{2} $/g, whereas for silica gels containing micropores (aside from mesopores) this value ranges from 887 to 1259 $ m^{2} $/g; the pore volumes are 0.68–0.79 $ cm^{3} $/g and 0.81–0.97 $ cm^{3} $/g, respectively. The 29Si NMR spectroscopy data demonstrate high degree of cohesiveness of the mesoporous silica gel and the predominant cohesiveness type (Q4), while the type Q3 characterizes samples containing both pore types. Adsorption of water vapor on the latter ones starts at lower relative vapor pressure in comparison with mesoporous samples.</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">mesoporous silica gels</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">template synthesis</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">water vapor adsorption</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Sobina, E. P.</subfield><subfield code="4">aut</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Adamova, L. V.</subfield><subfield code="4">aut</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Kodess, M. I.</subfield><subfield code="4">aut</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Medvedevskikh, S. V.</subfield><subfield code="4">aut</subfield></datafield><datafield tag="773" ind1="0" ind2="8"><subfield code="i">Enthalten in</subfield><subfield code="t">Glass physics and chemistry</subfield><subfield code="d">Pleiades Publishing, 1993</subfield><subfield code="g">41(2015), 2 vom: März, Seite 187-193</subfield><subfield code="w">(DE-627)182171957</subfield><subfield code="w">(DE-600)1182895-X</subfield><subfield code="w">(DE-576)9182171955</subfield><subfield code="x">1087-6596</subfield><subfield code="7">nnns</subfield></datafield><datafield tag="773" ind1="1" ind2="8"><subfield code="g">volume:41</subfield><subfield code="g">year:2015</subfield><subfield code="g">number:2</subfield><subfield code="g">month:03</subfield><subfield code="g">pages:187-193</subfield></datafield><datafield tag="856" ind1="4" ind2="1"><subfield code="u">https://doi.org/10.1134/S1087659615020108</subfield><subfield code="z">lizenzpflichtig</subfield><subfield code="3">Volltext</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_USEFLAG_A</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">SYSFLAG_A</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_OLC</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">SSG-OLC-TEC</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">SSG-OLC-CHE</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">SSG-OLC-PHA</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">SSG-OLC-DE-84</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_70</subfield></datafield><datafield tag="951" ind1=" " ind2=" "><subfield code="a">AR</subfield></datafield><datafield tag="952" ind1=" " ind2=" "><subfield code="d">41</subfield><subfield code="j">2015</subfield><subfield code="e">2</subfield><subfield code="c">03</subfield><subfield code="h">187-193</subfield></datafield></record></collection>
|
| score |
7.3987913 |