Nano-sulfated zirconia catalyzed biodiesel production from tannery waste sheep fat
Abstract This study makes use of tannery waste to produce biodiesel using a nano-sulfated zirconia catalyst (ferric-manganese-doped sulfated zirconia). It was through a modified wetness impregnation method that the catalyst was prepared which was then characterized by scanning electron microscopy (S...
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Gespeichert in:
| Autor*in: |
Booramurthy, Vijaya Kumar [verfasserIn] |
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| Format: |
Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2020 |
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| Schlagwörter: |
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| Anmerkung: |
© Springer-Verlag GmbH Germany, part of Springer Nature 2020 |
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| Übergeordnetes Werk: |
Enthalten in: Environmental science and pollution research - Springer Berlin Heidelberg, 1994, 27(2020), 17 vom: 09. Feb., Seite 20598-20605 |
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| Übergeordnetes Werk: |
volume:27 ; year:2020 ; number:17 ; day:09 ; month:02 ; pages:20598-20605 |
| Links: |
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| DOI / URN: |
10.1007/s11356-020-07984-1 |
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| Katalog-ID: |
OLC2040585796 |
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| 520 | |a Abstract This study makes use of tannery waste to produce biodiesel using a nano-sulfated zirconia catalyst (ferric-manganese-doped sulfated zirconia). It was through a modified wetness impregnation method that the catalyst was prepared which was then characterized by scanning electron microscopy (SEM), X-ray diffraction (XRD), and Fourier transform infrared spectroscopy (FTIR). The catalytic property of the synthesized catalyst was determined by using it to produce biodiesel from tannery waste sheep fat. A study was carried out to find the effect of the different parameters affecting the process. Optimized conditions of 15:1 methanol to fat molar ratio and catalytic loading of 8 wt% at 65 °C with a stirring rate of 400 rpm for a reaction duration of 300 min gave a maximum yield of 98.7 wt%. The performance of the catalyst during recycling was analyzed by conducting reusability study. The reused catalyst gives a maximum yield above 90 wt% up to five cycles with a catalyst recovery of 88 wt%. ASTM D6751 standard was used to compare the analyzed fuel properties of the biodiesel. | ||
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10.1007/s11356-020-07984-1 doi (DE-627)OLC2040585796 (DE-He213)s11356-020-07984-1-p DE-627 ger DE-627 rakwb eng 570 360 333.7 VZ 690 333.7 540 VZ BIODIV DE-30 fid Booramurthy, Vijaya Kumar verfasserin aut Nano-sulfated zirconia catalyzed biodiesel production from tannery waste sheep fat 2020 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Springer-Verlag GmbH Germany, part of Springer Nature 2020 Abstract This study makes use of tannery waste to produce biodiesel using a nano-sulfated zirconia catalyst (ferric-manganese-doped sulfated zirconia). It was through a modified wetness impregnation method that the catalyst was prepared which was then characterized by scanning electron microscopy (SEM), X-ray diffraction (XRD), and Fourier transform infrared spectroscopy (FTIR). The catalytic property of the synthesized catalyst was determined by using it to produce biodiesel from tannery waste sheep fat. A study was carried out to find the effect of the different parameters affecting the process. Optimized conditions of 15:1 methanol to fat molar ratio and catalytic loading of 8 wt% at 65 °C with a stirring rate of 400 rpm for a reaction duration of 300 min gave a maximum yield of 98.7 wt%. The performance of the catalyst during recycling was analyzed by conducting reusability study. The reused catalyst gives a maximum yield above 90 wt% up to five cycles with a catalyst recovery of 88 wt%. ASTM D6751 standard was used to compare the analyzed fuel properties of the biodiesel. Sulfated zirconia nano-catalyst Wetness impregnation method Transesterification Reusability Biofuel Kasimani, Ramesh aut Pandian, Sivakumar (orcid)0000-0002-4469-4126 aut Ragunathan, Balasubramanian aut Enthalten in Environmental science and pollution research Springer Berlin Heidelberg, 1994 27(2020), 17 vom: 09. Feb., Seite 20598-20605 (DE-627)171335805 (DE-600)1178791-0 (DE-576)038875101 0944-1344 nnns volume:27 year:2020 number:17 day:09 month:02 pages:20598-20605 https://doi.org/10.1007/s11356-020-07984-1 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC FID-BIODIV SSG-OLC-UMW SSG-OLC-ARC SSG-OLC-TEC SSG-OLC-CHE SSG-OLC-FOR SSG-OLC-DE-84 GBV_ILN_252 GBV_ILN_267 GBV_ILN_2018 GBV_ILN_4277 AR 27 2020 17 09 02 20598-20605 |
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10.1007/s11356-020-07984-1 doi (DE-627)OLC2040585796 (DE-He213)s11356-020-07984-1-p DE-627 ger DE-627 rakwb eng 570 360 333.7 VZ 690 333.7 540 VZ BIODIV DE-30 fid Booramurthy, Vijaya Kumar verfasserin aut Nano-sulfated zirconia catalyzed biodiesel production from tannery waste sheep fat 2020 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Springer-Verlag GmbH Germany, part of Springer Nature 2020 Abstract This study makes use of tannery waste to produce biodiesel using a nano-sulfated zirconia catalyst (ferric-manganese-doped sulfated zirconia). It was through a modified wetness impregnation method that the catalyst was prepared which was then characterized by scanning electron microscopy (SEM), X-ray diffraction (XRD), and Fourier transform infrared spectroscopy (FTIR). The catalytic property of the synthesized catalyst was determined by using it to produce biodiesel from tannery waste sheep fat. A study was carried out to find the effect of the different parameters affecting the process. Optimized conditions of 15:1 methanol to fat molar ratio and catalytic loading of 8 wt% at 65 °C with a stirring rate of 400 rpm for a reaction duration of 300 min gave a maximum yield of 98.7 wt%. The performance of the catalyst during recycling was analyzed by conducting reusability study. The reused catalyst gives a maximum yield above 90 wt% up to five cycles with a catalyst recovery of 88 wt%. ASTM D6751 standard was used to compare the analyzed fuel properties of the biodiesel. Sulfated zirconia nano-catalyst Wetness impregnation method Transesterification Reusability Biofuel Kasimani, Ramesh aut Pandian, Sivakumar (orcid)0000-0002-4469-4126 aut Ragunathan, Balasubramanian aut Enthalten in Environmental science and pollution research Springer Berlin Heidelberg, 1994 27(2020), 17 vom: 09. Feb., Seite 20598-20605 (DE-627)171335805 (DE-600)1178791-0 (DE-576)038875101 0944-1344 nnns volume:27 year:2020 number:17 day:09 month:02 pages:20598-20605 https://doi.org/10.1007/s11356-020-07984-1 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC FID-BIODIV SSG-OLC-UMW SSG-OLC-ARC SSG-OLC-TEC SSG-OLC-CHE SSG-OLC-FOR SSG-OLC-DE-84 GBV_ILN_252 GBV_ILN_267 GBV_ILN_2018 GBV_ILN_4277 AR 27 2020 17 09 02 20598-20605 |
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10.1007/s11356-020-07984-1 doi (DE-627)OLC2040585796 (DE-He213)s11356-020-07984-1-p DE-627 ger DE-627 rakwb eng 570 360 333.7 VZ 690 333.7 540 VZ BIODIV DE-30 fid Booramurthy, Vijaya Kumar verfasserin aut Nano-sulfated zirconia catalyzed biodiesel production from tannery waste sheep fat 2020 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Springer-Verlag GmbH Germany, part of Springer Nature 2020 Abstract This study makes use of tannery waste to produce biodiesel using a nano-sulfated zirconia catalyst (ferric-manganese-doped sulfated zirconia). It was through a modified wetness impregnation method that the catalyst was prepared which was then characterized by scanning electron microscopy (SEM), X-ray diffraction (XRD), and Fourier transform infrared spectroscopy (FTIR). The catalytic property of the synthesized catalyst was determined by using it to produce biodiesel from tannery waste sheep fat. A study was carried out to find the effect of the different parameters affecting the process. Optimized conditions of 15:1 methanol to fat molar ratio and catalytic loading of 8 wt% at 65 °C with a stirring rate of 400 rpm for a reaction duration of 300 min gave a maximum yield of 98.7 wt%. The performance of the catalyst during recycling was analyzed by conducting reusability study. The reused catalyst gives a maximum yield above 90 wt% up to five cycles with a catalyst recovery of 88 wt%. ASTM D6751 standard was used to compare the analyzed fuel properties of the biodiesel. Sulfated zirconia nano-catalyst Wetness impregnation method Transesterification Reusability Biofuel Kasimani, Ramesh aut Pandian, Sivakumar (orcid)0000-0002-4469-4126 aut Ragunathan, Balasubramanian aut Enthalten in Environmental science and pollution research Springer Berlin Heidelberg, 1994 27(2020), 17 vom: 09. Feb., Seite 20598-20605 (DE-627)171335805 (DE-600)1178791-0 (DE-576)038875101 0944-1344 nnns volume:27 year:2020 number:17 day:09 month:02 pages:20598-20605 https://doi.org/10.1007/s11356-020-07984-1 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC FID-BIODIV SSG-OLC-UMW SSG-OLC-ARC SSG-OLC-TEC SSG-OLC-CHE SSG-OLC-FOR SSG-OLC-DE-84 GBV_ILN_252 GBV_ILN_267 GBV_ILN_2018 GBV_ILN_4277 AR 27 2020 17 09 02 20598-20605 |
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10.1007/s11356-020-07984-1 doi (DE-627)OLC2040585796 (DE-He213)s11356-020-07984-1-p DE-627 ger DE-627 rakwb eng 570 360 333.7 VZ 690 333.7 540 VZ BIODIV DE-30 fid Booramurthy, Vijaya Kumar verfasserin aut Nano-sulfated zirconia catalyzed biodiesel production from tannery waste sheep fat 2020 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Springer-Verlag GmbH Germany, part of Springer Nature 2020 Abstract This study makes use of tannery waste to produce biodiesel using a nano-sulfated zirconia catalyst (ferric-manganese-doped sulfated zirconia). It was through a modified wetness impregnation method that the catalyst was prepared which was then characterized by scanning electron microscopy (SEM), X-ray diffraction (XRD), and Fourier transform infrared spectroscopy (FTIR). The catalytic property of the synthesized catalyst was determined by using it to produce biodiesel from tannery waste sheep fat. A study was carried out to find the effect of the different parameters affecting the process. Optimized conditions of 15:1 methanol to fat molar ratio and catalytic loading of 8 wt% at 65 °C with a stirring rate of 400 rpm for a reaction duration of 300 min gave a maximum yield of 98.7 wt%. The performance of the catalyst during recycling was analyzed by conducting reusability study. The reused catalyst gives a maximum yield above 90 wt% up to five cycles with a catalyst recovery of 88 wt%. ASTM D6751 standard was used to compare the analyzed fuel properties of the biodiesel. Sulfated zirconia nano-catalyst Wetness impregnation method Transesterification Reusability Biofuel Kasimani, Ramesh aut Pandian, Sivakumar (orcid)0000-0002-4469-4126 aut Ragunathan, Balasubramanian aut Enthalten in Environmental science and pollution research Springer Berlin Heidelberg, 1994 27(2020), 17 vom: 09. Feb., Seite 20598-20605 (DE-627)171335805 (DE-600)1178791-0 (DE-576)038875101 0944-1344 nnns volume:27 year:2020 number:17 day:09 month:02 pages:20598-20605 https://doi.org/10.1007/s11356-020-07984-1 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC FID-BIODIV SSG-OLC-UMW SSG-OLC-ARC SSG-OLC-TEC SSG-OLC-CHE SSG-OLC-FOR SSG-OLC-DE-84 GBV_ILN_252 GBV_ILN_267 GBV_ILN_2018 GBV_ILN_4277 AR 27 2020 17 09 02 20598-20605 |
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Booramurthy, Vijaya Kumar |
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Booramurthy, Vijaya Kumar ddc 570 ddc 690 fid BIODIV misc Sulfated zirconia nano-catalyst misc Wetness impregnation method misc Transesterification misc Reusability misc Biofuel Nano-sulfated zirconia catalyzed biodiesel production from tannery waste sheep fat |
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Nano-sulfated zirconia catalyzed biodiesel production from tannery waste sheep fat |
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Booramurthy, Vijaya Kumar Kasimani, Ramesh Pandian, Sivakumar Ragunathan, Balasubramanian |
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nano-sulfated zirconia catalyzed biodiesel production from tannery waste sheep fat |
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Nano-sulfated zirconia catalyzed biodiesel production from tannery waste sheep fat |
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Abstract This study makes use of tannery waste to produce biodiesel using a nano-sulfated zirconia catalyst (ferric-manganese-doped sulfated zirconia). It was through a modified wetness impregnation method that the catalyst was prepared which was then characterized by scanning electron microscopy (SEM), X-ray diffraction (XRD), and Fourier transform infrared spectroscopy (FTIR). The catalytic property of the synthesized catalyst was determined by using it to produce biodiesel from tannery waste sheep fat. A study was carried out to find the effect of the different parameters affecting the process. Optimized conditions of 15:1 methanol to fat molar ratio and catalytic loading of 8 wt% at 65 °C with a stirring rate of 400 rpm for a reaction duration of 300 min gave a maximum yield of 98.7 wt%. The performance of the catalyst during recycling was analyzed by conducting reusability study. The reused catalyst gives a maximum yield above 90 wt% up to five cycles with a catalyst recovery of 88 wt%. ASTM D6751 standard was used to compare the analyzed fuel properties of the biodiesel. © Springer-Verlag GmbH Germany, part of Springer Nature 2020 |
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Abstract This study makes use of tannery waste to produce biodiesel using a nano-sulfated zirconia catalyst (ferric-manganese-doped sulfated zirconia). It was through a modified wetness impregnation method that the catalyst was prepared which was then characterized by scanning electron microscopy (SEM), X-ray diffraction (XRD), and Fourier transform infrared spectroscopy (FTIR). The catalytic property of the synthesized catalyst was determined by using it to produce biodiesel from tannery waste sheep fat. A study was carried out to find the effect of the different parameters affecting the process. Optimized conditions of 15:1 methanol to fat molar ratio and catalytic loading of 8 wt% at 65 °C with a stirring rate of 400 rpm for a reaction duration of 300 min gave a maximum yield of 98.7 wt%. The performance of the catalyst during recycling was analyzed by conducting reusability study. The reused catalyst gives a maximum yield above 90 wt% up to five cycles with a catalyst recovery of 88 wt%. ASTM D6751 standard was used to compare the analyzed fuel properties of the biodiesel. © Springer-Verlag GmbH Germany, part of Springer Nature 2020 |
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Abstract This study makes use of tannery waste to produce biodiesel using a nano-sulfated zirconia catalyst (ferric-manganese-doped sulfated zirconia). It was through a modified wetness impregnation method that the catalyst was prepared which was then characterized by scanning electron microscopy (SEM), X-ray diffraction (XRD), and Fourier transform infrared spectroscopy (FTIR). The catalytic property of the synthesized catalyst was determined by using it to produce biodiesel from tannery waste sheep fat. A study was carried out to find the effect of the different parameters affecting the process. Optimized conditions of 15:1 methanol to fat molar ratio and catalytic loading of 8 wt% at 65 °C with a stirring rate of 400 rpm for a reaction duration of 300 min gave a maximum yield of 98.7 wt%. The performance of the catalyst during recycling was analyzed by conducting reusability study. The reused catalyst gives a maximum yield above 90 wt% up to five cycles with a catalyst recovery of 88 wt%. ASTM D6751 standard was used to compare the analyzed fuel properties of the biodiesel. © Springer-Verlag GmbH Germany, part of Springer Nature 2020 |
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