Synthesis and characterization of novel polyurethanes containing tricyanocyclopropane ring for piezoelectric applications
Summary 1-(2',2',3'-Tricyano-3'-carbomethoxycyclopropyl)-3,4-di-2'-hydroxyethoxybenzene (4) was prepared by the reaction of bromomalononitrile with methyl 3,4-di-(2'-hydroxyethoxy)benzylidenecyanoacetate (3). Diol 4 was condensed with 3,4-toluenediisocyanate and 3,3...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Lee, Ju-Yeon [verfasserIn] |
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| Format: |
Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2001 |
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| Schlagwörter: |
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| Anmerkung: |
© Springer-Verlag Berlin Heidelberg 2001 |
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| Übergeordnetes Werk: |
Enthalten in: Polymer bulletin - Springer-Verlag, 1978, 46(2001), 2-3 vom: Apr., Seite 159-164 |
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| Übergeordnetes Werk: |
volume:46 ; year:2001 ; number:2-3 ; month:04 ; pages:159-164 |
| Links: |
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| DOI / URN: |
10.1007/s002890170070 |
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| Katalog-ID: |
OLC2042622230 |
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| 245 | 1 | 0 | |a Synthesis and characterization of novel polyurethanes containing tricyanocyclopropane ring for piezoelectric applications |
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| 520 | |a Summary 1-(2',2',3'-Tricyano-3'-carbomethoxycyclopropyl)-3,4-di-2'-hydroxyethoxybenzene (4) was prepared by the reaction of bromomalononitrile with methyl 3,4-di-(2'-hydroxyethoxy)benzylidenecyanoacetate (3). Diol 4 was condensed with 3,4-toluenediisocyanate and 3,3'-dimethoxy-4,4'-biphenylenediisocynate to yield polyurethanes 5 and 6 containing multicyanocyclopropane functionalities in the pendant group. The resulting polymers 5 and 6 were soluble in common organic solvents and the inherent viscosities were in the range of 0.25–0.30 dL/g. Polyurethanes 5 and 6 showed a thermal stability up to 300°C in TGA thermograms. Solution-cast films showed Tg values in the range of 100–130°C and piezoelectric coeffcients ($ d_{31} $) of the poled polymer films were 1.8–2.0 pC/N, which are acceptable for piezoelectric device applications. | ||
| 650 | 4 | |a Polymer | |
| 650 | 4 | |a Viscosity | |
| 650 | 4 | |a Thermal Stability | |
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| 650 | 4 | |a Polyurethane | |
| 700 | 1 | |a Park, Eun-Ju |4 aut | |
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10.1007/s002890170070 doi (DE-627)OLC2042622230 (DE-He213)s002890170070-p DE-627 ger DE-627 rakwb eng 540 530 660 VZ BIODIV DE-30 fid Lee, Ju-Yeon verfasserin aut Synthesis and characterization of novel polyurethanes containing tricyanocyclopropane ring for piezoelectric applications 2001 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Springer-Verlag Berlin Heidelberg 2001 Summary 1-(2',2',3'-Tricyano-3'-carbomethoxycyclopropyl)-3,4-di-2'-hydroxyethoxybenzene (4) was prepared by the reaction of bromomalononitrile with methyl 3,4-di-(2'-hydroxyethoxy)benzylidenecyanoacetate (3). Diol 4 was condensed with 3,4-toluenediisocyanate and 3,3'-dimethoxy-4,4'-biphenylenediisocynate to yield polyurethanes 5 and 6 containing multicyanocyclopropane functionalities in the pendant group. The resulting polymers 5 and 6 were soluble in common organic solvents and the inherent viscosities were in the range of 0.25–0.30 dL/g. Polyurethanes 5 and 6 showed a thermal stability up to 300°C in TGA thermograms. Solution-cast films showed Tg values in the range of 100–130°C and piezoelectric coeffcients ($ d_{31} $) of the poled polymer films were 1.8–2.0 pC/N, which are acceptable for piezoelectric device applications. Polymer Viscosity Thermal Stability Organic Solvent Polyurethane Park, Eun-Ju aut Enthalten in Polymer bulletin Springer-Verlag, 1978 46(2001), 2-3 vom: Apr., Seite 159-164 (DE-627)129092916 (DE-600)6871-8 (DE-576)01442861X 0170-0839 nnns volume:46 year:2001 number:2-3 month:04 pages:159-164 https://doi.org/10.1007/s002890170070 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC FID-BIODIV SSG-OLC-TEC SSG-OLC-PHY SSG-OLC-CHE GBV_ILN_21 GBV_ILN_40 GBV_ILN_70 GBV_ILN_95 GBV_ILN_130 GBV_ILN_285 GBV_ILN_2006 GBV_ILN_2018 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2411 GBV_ILN_4012 GBV_ILN_4046 GBV_ILN_4277 GBV_ILN_4323 AR 46 2001 2-3 04 159-164 |
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10.1007/s002890170070 doi (DE-627)OLC2042622230 (DE-He213)s002890170070-p DE-627 ger DE-627 rakwb eng 540 530 660 VZ BIODIV DE-30 fid Lee, Ju-Yeon verfasserin aut Synthesis and characterization of novel polyurethanes containing tricyanocyclopropane ring for piezoelectric applications 2001 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Springer-Verlag Berlin Heidelberg 2001 Summary 1-(2',2',3'-Tricyano-3'-carbomethoxycyclopropyl)-3,4-di-2'-hydroxyethoxybenzene (4) was prepared by the reaction of bromomalononitrile with methyl 3,4-di-(2'-hydroxyethoxy)benzylidenecyanoacetate (3). Diol 4 was condensed with 3,4-toluenediisocyanate and 3,3'-dimethoxy-4,4'-biphenylenediisocynate to yield polyurethanes 5 and 6 containing multicyanocyclopropane functionalities in the pendant group. The resulting polymers 5 and 6 were soluble in common organic solvents and the inherent viscosities were in the range of 0.25–0.30 dL/g. Polyurethanes 5 and 6 showed a thermal stability up to 300°C in TGA thermograms. Solution-cast films showed Tg values in the range of 100–130°C and piezoelectric coeffcients ($ d_{31} $) of the poled polymer films were 1.8–2.0 pC/N, which are acceptable for piezoelectric device applications. Polymer Viscosity Thermal Stability Organic Solvent Polyurethane Park, Eun-Ju aut Enthalten in Polymer bulletin Springer-Verlag, 1978 46(2001), 2-3 vom: Apr., Seite 159-164 (DE-627)129092916 (DE-600)6871-8 (DE-576)01442861X 0170-0839 nnns volume:46 year:2001 number:2-3 month:04 pages:159-164 https://doi.org/10.1007/s002890170070 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC FID-BIODIV SSG-OLC-TEC SSG-OLC-PHY SSG-OLC-CHE GBV_ILN_21 GBV_ILN_40 GBV_ILN_70 GBV_ILN_95 GBV_ILN_130 GBV_ILN_285 GBV_ILN_2006 GBV_ILN_2018 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2411 GBV_ILN_4012 GBV_ILN_4046 GBV_ILN_4277 GBV_ILN_4323 AR 46 2001 2-3 04 159-164 |
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10.1007/s002890170070 doi (DE-627)OLC2042622230 (DE-He213)s002890170070-p DE-627 ger DE-627 rakwb eng 540 530 660 VZ BIODIV DE-30 fid Lee, Ju-Yeon verfasserin aut Synthesis and characterization of novel polyurethanes containing tricyanocyclopropane ring for piezoelectric applications 2001 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Springer-Verlag Berlin Heidelberg 2001 Summary 1-(2',2',3'-Tricyano-3'-carbomethoxycyclopropyl)-3,4-di-2'-hydroxyethoxybenzene (4) was prepared by the reaction of bromomalononitrile with methyl 3,4-di-(2'-hydroxyethoxy)benzylidenecyanoacetate (3). Diol 4 was condensed with 3,4-toluenediisocyanate and 3,3'-dimethoxy-4,4'-biphenylenediisocynate to yield polyurethanes 5 and 6 containing multicyanocyclopropane functionalities in the pendant group. The resulting polymers 5 and 6 were soluble in common organic solvents and the inherent viscosities were in the range of 0.25–0.30 dL/g. Polyurethanes 5 and 6 showed a thermal stability up to 300°C in TGA thermograms. Solution-cast films showed Tg values in the range of 100–130°C and piezoelectric coeffcients ($ d_{31} $) of the poled polymer films were 1.8–2.0 pC/N, which are acceptable for piezoelectric device applications. Polymer Viscosity Thermal Stability Organic Solvent Polyurethane Park, Eun-Ju aut Enthalten in Polymer bulletin Springer-Verlag, 1978 46(2001), 2-3 vom: Apr., Seite 159-164 (DE-627)129092916 (DE-600)6871-8 (DE-576)01442861X 0170-0839 nnns volume:46 year:2001 number:2-3 month:04 pages:159-164 https://doi.org/10.1007/s002890170070 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC FID-BIODIV SSG-OLC-TEC SSG-OLC-PHY SSG-OLC-CHE GBV_ILN_21 GBV_ILN_40 GBV_ILN_70 GBV_ILN_95 GBV_ILN_130 GBV_ILN_285 GBV_ILN_2006 GBV_ILN_2018 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2411 GBV_ILN_4012 GBV_ILN_4046 GBV_ILN_4277 GBV_ILN_4323 AR 46 2001 2-3 04 159-164 |
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10.1007/s002890170070 doi (DE-627)OLC2042622230 (DE-He213)s002890170070-p DE-627 ger DE-627 rakwb eng 540 530 660 VZ BIODIV DE-30 fid Lee, Ju-Yeon verfasserin aut Synthesis and characterization of novel polyurethanes containing tricyanocyclopropane ring for piezoelectric applications 2001 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Springer-Verlag Berlin Heidelberg 2001 Summary 1-(2',2',3'-Tricyano-3'-carbomethoxycyclopropyl)-3,4-di-2'-hydroxyethoxybenzene (4) was prepared by the reaction of bromomalononitrile with methyl 3,4-di-(2'-hydroxyethoxy)benzylidenecyanoacetate (3). Diol 4 was condensed with 3,4-toluenediisocyanate and 3,3'-dimethoxy-4,4'-biphenylenediisocynate to yield polyurethanes 5 and 6 containing multicyanocyclopropane functionalities in the pendant group. The resulting polymers 5 and 6 were soluble in common organic solvents and the inherent viscosities were in the range of 0.25–0.30 dL/g. Polyurethanes 5 and 6 showed a thermal stability up to 300°C in TGA thermograms. Solution-cast films showed Tg values in the range of 100–130°C and piezoelectric coeffcients ($ d_{31} $) of the poled polymer films were 1.8–2.0 pC/N, which are acceptable for piezoelectric device applications. Polymer Viscosity Thermal Stability Organic Solvent Polyurethane Park, Eun-Ju aut Enthalten in Polymer bulletin Springer-Verlag, 1978 46(2001), 2-3 vom: Apr., Seite 159-164 (DE-627)129092916 (DE-600)6871-8 (DE-576)01442861X 0170-0839 nnns volume:46 year:2001 number:2-3 month:04 pages:159-164 https://doi.org/10.1007/s002890170070 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC FID-BIODIV SSG-OLC-TEC SSG-OLC-PHY SSG-OLC-CHE GBV_ILN_21 GBV_ILN_40 GBV_ILN_70 GBV_ILN_95 GBV_ILN_130 GBV_ILN_285 GBV_ILN_2006 GBV_ILN_2018 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2411 GBV_ILN_4012 GBV_ILN_4046 GBV_ILN_4277 GBV_ILN_4323 AR 46 2001 2-3 04 159-164 |
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10.1007/s002890170070 doi (DE-627)OLC2042622230 (DE-He213)s002890170070-p DE-627 ger DE-627 rakwb eng 540 530 660 VZ BIODIV DE-30 fid Lee, Ju-Yeon verfasserin aut Synthesis and characterization of novel polyurethanes containing tricyanocyclopropane ring for piezoelectric applications 2001 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Springer-Verlag Berlin Heidelberg 2001 Summary 1-(2',2',3'-Tricyano-3'-carbomethoxycyclopropyl)-3,4-di-2'-hydroxyethoxybenzene (4) was prepared by the reaction of bromomalononitrile with methyl 3,4-di-(2'-hydroxyethoxy)benzylidenecyanoacetate (3). Diol 4 was condensed with 3,4-toluenediisocyanate and 3,3'-dimethoxy-4,4'-biphenylenediisocynate to yield polyurethanes 5 and 6 containing multicyanocyclopropane functionalities in the pendant group. The resulting polymers 5 and 6 were soluble in common organic solvents and the inherent viscosities were in the range of 0.25–0.30 dL/g. Polyurethanes 5 and 6 showed a thermal stability up to 300°C in TGA thermograms. Solution-cast films showed Tg values in the range of 100–130°C and piezoelectric coeffcients ($ d_{31} $) of the poled polymer films were 1.8–2.0 pC/N, which are acceptable for piezoelectric device applications. Polymer Viscosity Thermal Stability Organic Solvent Polyurethane Park, Eun-Ju aut Enthalten in Polymer bulletin Springer-Verlag, 1978 46(2001), 2-3 vom: Apr., Seite 159-164 (DE-627)129092916 (DE-600)6871-8 (DE-576)01442861X 0170-0839 nnns volume:46 year:2001 number:2-3 month:04 pages:159-164 https://doi.org/10.1007/s002890170070 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC FID-BIODIV SSG-OLC-TEC SSG-OLC-PHY SSG-OLC-CHE GBV_ILN_21 GBV_ILN_40 GBV_ILN_70 GBV_ILN_95 GBV_ILN_130 GBV_ILN_285 GBV_ILN_2006 GBV_ILN_2018 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2411 GBV_ILN_4012 GBV_ILN_4046 GBV_ILN_4277 GBV_ILN_4323 AR 46 2001 2-3 04 159-164 |
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540 530 660 VZ BIODIV DE-30 fid Synthesis and characterization of novel polyurethanes containing tricyanocyclopropane ring for piezoelectric applications Polymer Viscosity Thermal Stability Organic Solvent Polyurethane |
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Synthesis and characterization of novel polyurethanes containing tricyanocyclopropane ring for piezoelectric applications |
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Synthesis and characterization of novel polyurethanes containing tricyanocyclopropane ring for piezoelectric applications |
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Lee, Ju-Yeon |
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synthesis and characterization of novel polyurethanes containing tricyanocyclopropane ring for piezoelectric applications |
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Synthesis and characterization of novel polyurethanes containing tricyanocyclopropane ring for piezoelectric applications |
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Summary 1-(2',2',3'-Tricyano-3'-carbomethoxycyclopropyl)-3,4-di-2'-hydroxyethoxybenzene (4) was prepared by the reaction of bromomalononitrile with methyl 3,4-di-(2'-hydroxyethoxy)benzylidenecyanoacetate (3). Diol 4 was condensed with 3,4-toluenediisocyanate and 3,3'-dimethoxy-4,4'-biphenylenediisocynate to yield polyurethanes 5 and 6 containing multicyanocyclopropane functionalities in the pendant group. The resulting polymers 5 and 6 were soluble in common organic solvents and the inherent viscosities were in the range of 0.25–0.30 dL/g. Polyurethanes 5 and 6 showed a thermal stability up to 300°C in TGA thermograms. Solution-cast films showed Tg values in the range of 100–130°C and piezoelectric coeffcients ($ d_{31} $) of the poled polymer films were 1.8–2.0 pC/N, which are acceptable for piezoelectric device applications. © Springer-Verlag Berlin Heidelberg 2001 |
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Summary 1-(2',2',3'-Tricyano-3'-carbomethoxycyclopropyl)-3,4-di-2'-hydroxyethoxybenzene (4) was prepared by the reaction of bromomalononitrile with methyl 3,4-di-(2'-hydroxyethoxy)benzylidenecyanoacetate (3). Diol 4 was condensed with 3,4-toluenediisocyanate and 3,3'-dimethoxy-4,4'-biphenylenediisocynate to yield polyurethanes 5 and 6 containing multicyanocyclopropane functionalities in the pendant group. The resulting polymers 5 and 6 were soluble in common organic solvents and the inherent viscosities were in the range of 0.25–0.30 dL/g. Polyurethanes 5 and 6 showed a thermal stability up to 300°C in TGA thermograms. Solution-cast films showed Tg values in the range of 100–130°C and piezoelectric coeffcients ($ d_{31} $) of the poled polymer films were 1.8–2.0 pC/N, which are acceptable for piezoelectric device applications. © Springer-Verlag Berlin Heidelberg 2001 |
| abstract_unstemmed |
Summary 1-(2',2',3'-Tricyano-3'-carbomethoxycyclopropyl)-3,4-di-2'-hydroxyethoxybenzene (4) was prepared by the reaction of bromomalononitrile with methyl 3,4-di-(2'-hydroxyethoxy)benzylidenecyanoacetate (3). Diol 4 was condensed with 3,4-toluenediisocyanate and 3,3'-dimethoxy-4,4'-biphenylenediisocynate to yield polyurethanes 5 and 6 containing multicyanocyclopropane functionalities in the pendant group. The resulting polymers 5 and 6 were soluble in common organic solvents and the inherent viscosities were in the range of 0.25–0.30 dL/g. Polyurethanes 5 and 6 showed a thermal stability up to 300°C in TGA thermograms. Solution-cast films showed Tg values in the range of 100–130°C and piezoelectric coeffcients ($ d_{31} $) of the poled polymer films were 1.8–2.0 pC/N, which are acceptable for piezoelectric device applications. © Springer-Verlag Berlin Heidelberg 2001 |
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Synthesis and characterization of novel polyurethanes containing tricyanocyclopropane ring for piezoelectric applications |
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