Some issues on polymer crystallization kinetics studied by DSC non isothermal tests
Summary In this work constant cooling rate crystallization experiments were carried out by a DSC, working with an iPP and using a very little amount of material, to minimize the heat transfer resistance in the mass of the sample. The resulting data were corrected to take into account also for the ex...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Lamberti, Gaetano [verfasserIn] |
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| Format: |
Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2006 |
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| Schlagwörter: |
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| Anmerkung: |
© Springer-Verlag 2006 |
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| Übergeordnetes Werk: |
Enthalten in: Polymer bulletin - Springer-Verlag, 1978, 56(2006), 6 vom: 02. Feb., Seite 591-598 |
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| Übergeordnetes Werk: |
volume:56 ; year:2006 ; number:6 ; day:02 ; month:02 ; pages:591-598 |
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| DOI / URN: |
10.1007/s00289-006-0518-2 |
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| 520 | |a Summary In this work constant cooling rate crystallization experiments were carried out by a DSC, working with an iPP and using a very little amount of material, to minimize the heat transfer resistance in the mass of the sample. The resulting data were corrected to take into account also for the external heat transfer resistance. The corrected data were compared with data produced in the past, working with larger amounts of the same resin in a less accurate DSC apparatus, confirming that in the field of polymer crystallization kinetics the calorimeter has to be used carefully. The data were also used to check a kinetic model previously tuned under isothermal conditions. Up to 10 °C/min (0.167 K/s) the isothermal model is accurate enough, but faster tests requires an improvement of the model. | ||
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10.1007/s00289-006-0518-2 doi (DE-627)OLC2042628514 (DE-He213)s00289-006-0518-2-p DE-627 ger DE-627 rakwb eng 540 530 660 VZ BIODIV DE-30 fid Lamberti, Gaetano verfasserin aut Some issues on polymer crystallization kinetics studied by DSC non isothermal tests 2006 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Springer-Verlag 2006 Summary In this work constant cooling rate crystallization experiments were carried out by a DSC, working with an iPP and using a very little amount of material, to minimize the heat transfer resistance in the mass of the sample. The resulting data were corrected to take into account also for the external heat transfer resistance. The corrected data were compared with data produced in the past, working with larger amounts of the same resin in a less accurate DSC apparatus, confirming that in the field of polymer crystallization kinetics the calorimeter has to be used carefully. The data were also used to check a kinetic model previously tuned under isothermal conditions. Up to 10 °C/min (0.167 K/s) the isothermal model is accurate enough, but faster tests requires an improvement of the model. Polymer Heat Transfer Crystallization Cool Rate Calorimeter Naddeo, Carlo aut Enthalten in Polymer bulletin Springer-Verlag, 1978 56(2006), 6 vom: 02. Feb., Seite 591-598 (DE-627)129092916 (DE-600)6871-8 (DE-576)01442861X 0170-0839 nnns volume:56 year:2006 number:6 day:02 month:02 pages:591-598 https://doi.org/10.1007/s00289-006-0518-2 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC FID-BIODIV SSG-OLC-TEC SSG-OLC-PHY SSG-OLC-CHE SSG-OLC-PHA SSG-OLC-DE-84 GBV_ILN_40 GBV_ILN_70 GBV_ILN_285 GBV_ILN_2004 GBV_ILN_2006 GBV_ILN_2018 GBV_ILN_2411 GBV_ILN_4012 GBV_ILN_4046 GBV_ILN_4277 AR 56 2006 6 02 02 591-598 |
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10.1007/s00289-006-0518-2 doi (DE-627)OLC2042628514 (DE-He213)s00289-006-0518-2-p DE-627 ger DE-627 rakwb eng 540 530 660 VZ BIODIV DE-30 fid Lamberti, Gaetano verfasserin aut Some issues on polymer crystallization kinetics studied by DSC non isothermal tests 2006 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Springer-Verlag 2006 Summary In this work constant cooling rate crystallization experiments were carried out by a DSC, working with an iPP and using a very little amount of material, to minimize the heat transfer resistance in the mass of the sample. The resulting data were corrected to take into account also for the external heat transfer resistance. The corrected data were compared with data produced in the past, working with larger amounts of the same resin in a less accurate DSC apparatus, confirming that in the field of polymer crystallization kinetics the calorimeter has to be used carefully. The data were also used to check a kinetic model previously tuned under isothermal conditions. Up to 10 °C/min (0.167 K/s) the isothermal model is accurate enough, but faster tests requires an improvement of the model. Polymer Heat Transfer Crystallization Cool Rate Calorimeter Naddeo, Carlo aut Enthalten in Polymer bulletin Springer-Verlag, 1978 56(2006), 6 vom: 02. Feb., Seite 591-598 (DE-627)129092916 (DE-600)6871-8 (DE-576)01442861X 0170-0839 nnns volume:56 year:2006 number:6 day:02 month:02 pages:591-598 https://doi.org/10.1007/s00289-006-0518-2 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC FID-BIODIV SSG-OLC-TEC SSG-OLC-PHY SSG-OLC-CHE SSG-OLC-PHA SSG-OLC-DE-84 GBV_ILN_40 GBV_ILN_70 GBV_ILN_285 GBV_ILN_2004 GBV_ILN_2006 GBV_ILN_2018 GBV_ILN_2411 GBV_ILN_4012 GBV_ILN_4046 GBV_ILN_4277 AR 56 2006 6 02 02 591-598 |
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10.1007/s00289-006-0518-2 doi (DE-627)OLC2042628514 (DE-He213)s00289-006-0518-2-p DE-627 ger DE-627 rakwb eng 540 530 660 VZ BIODIV DE-30 fid Lamberti, Gaetano verfasserin aut Some issues on polymer crystallization kinetics studied by DSC non isothermal tests 2006 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Springer-Verlag 2006 Summary In this work constant cooling rate crystallization experiments were carried out by a DSC, working with an iPP and using a very little amount of material, to minimize the heat transfer resistance in the mass of the sample. The resulting data were corrected to take into account also for the external heat transfer resistance. The corrected data were compared with data produced in the past, working with larger amounts of the same resin in a less accurate DSC apparatus, confirming that in the field of polymer crystallization kinetics the calorimeter has to be used carefully. The data were also used to check a kinetic model previously tuned under isothermal conditions. Up to 10 °C/min (0.167 K/s) the isothermal model is accurate enough, but faster tests requires an improvement of the model. Polymer Heat Transfer Crystallization Cool Rate Calorimeter Naddeo, Carlo aut Enthalten in Polymer bulletin Springer-Verlag, 1978 56(2006), 6 vom: 02. Feb., Seite 591-598 (DE-627)129092916 (DE-600)6871-8 (DE-576)01442861X 0170-0839 nnns volume:56 year:2006 number:6 day:02 month:02 pages:591-598 https://doi.org/10.1007/s00289-006-0518-2 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC FID-BIODIV SSG-OLC-TEC SSG-OLC-PHY SSG-OLC-CHE SSG-OLC-PHA SSG-OLC-DE-84 GBV_ILN_40 GBV_ILN_70 GBV_ILN_285 GBV_ILN_2004 GBV_ILN_2006 GBV_ILN_2018 GBV_ILN_2411 GBV_ILN_4012 GBV_ILN_4046 GBV_ILN_4277 AR 56 2006 6 02 02 591-598 |
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10.1007/s00289-006-0518-2 doi (DE-627)OLC2042628514 (DE-He213)s00289-006-0518-2-p DE-627 ger DE-627 rakwb eng 540 530 660 VZ BIODIV DE-30 fid Lamberti, Gaetano verfasserin aut Some issues on polymer crystallization kinetics studied by DSC non isothermal tests 2006 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Springer-Verlag 2006 Summary In this work constant cooling rate crystallization experiments were carried out by a DSC, working with an iPP and using a very little amount of material, to minimize the heat transfer resistance in the mass of the sample. The resulting data were corrected to take into account also for the external heat transfer resistance. The corrected data were compared with data produced in the past, working with larger amounts of the same resin in a less accurate DSC apparatus, confirming that in the field of polymer crystallization kinetics the calorimeter has to be used carefully. The data were also used to check a kinetic model previously tuned under isothermal conditions. Up to 10 °C/min (0.167 K/s) the isothermal model is accurate enough, but faster tests requires an improvement of the model. Polymer Heat Transfer Crystallization Cool Rate Calorimeter Naddeo, Carlo aut Enthalten in Polymer bulletin Springer-Verlag, 1978 56(2006), 6 vom: 02. Feb., Seite 591-598 (DE-627)129092916 (DE-600)6871-8 (DE-576)01442861X 0170-0839 nnns volume:56 year:2006 number:6 day:02 month:02 pages:591-598 https://doi.org/10.1007/s00289-006-0518-2 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC FID-BIODIV SSG-OLC-TEC SSG-OLC-PHY SSG-OLC-CHE SSG-OLC-PHA SSG-OLC-DE-84 GBV_ILN_40 GBV_ILN_70 GBV_ILN_285 GBV_ILN_2004 GBV_ILN_2006 GBV_ILN_2018 GBV_ILN_2411 GBV_ILN_4012 GBV_ILN_4046 GBV_ILN_4277 AR 56 2006 6 02 02 591-598 |
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10.1007/s00289-006-0518-2 doi (DE-627)OLC2042628514 (DE-He213)s00289-006-0518-2-p DE-627 ger DE-627 rakwb eng 540 530 660 VZ BIODIV DE-30 fid Lamberti, Gaetano verfasserin aut Some issues on polymer crystallization kinetics studied by DSC non isothermal tests 2006 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Springer-Verlag 2006 Summary In this work constant cooling rate crystallization experiments were carried out by a DSC, working with an iPP and using a very little amount of material, to minimize the heat transfer resistance in the mass of the sample. The resulting data were corrected to take into account also for the external heat transfer resistance. The corrected data were compared with data produced in the past, working with larger amounts of the same resin in a less accurate DSC apparatus, confirming that in the field of polymer crystallization kinetics the calorimeter has to be used carefully. The data were also used to check a kinetic model previously tuned under isothermal conditions. Up to 10 °C/min (0.167 K/s) the isothermal model is accurate enough, but faster tests requires an improvement of the model. Polymer Heat Transfer Crystallization Cool Rate Calorimeter Naddeo, Carlo aut Enthalten in Polymer bulletin Springer-Verlag, 1978 56(2006), 6 vom: 02. Feb., Seite 591-598 (DE-627)129092916 (DE-600)6871-8 (DE-576)01442861X 0170-0839 nnns volume:56 year:2006 number:6 day:02 month:02 pages:591-598 https://doi.org/10.1007/s00289-006-0518-2 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC FID-BIODIV SSG-OLC-TEC SSG-OLC-PHY SSG-OLC-CHE SSG-OLC-PHA SSG-OLC-DE-84 GBV_ILN_40 GBV_ILN_70 GBV_ILN_285 GBV_ILN_2004 GBV_ILN_2006 GBV_ILN_2018 GBV_ILN_2411 GBV_ILN_4012 GBV_ILN_4046 GBV_ILN_4277 AR 56 2006 6 02 02 591-598 |
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Some issues on polymer crystallization kinetics studied by DSC non isothermal tests |
| abstract |
Summary In this work constant cooling rate crystallization experiments were carried out by a DSC, working with an iPP and using a very little amount of material, to minimize the heat transfer resistance in the mass of the sample. The resulting data were corrected to take into account also for the external heat transfer resistance. The corrected data were compared with data produced in the past, working with larger amounts of the same resin in a less accurate DSC apparatus, confirming that in the field of polymer crystallization kinetics the calorimeter has to be used carefully. The data were also used to check a kinetic model previously tuned under isothermal conditions. Up to 10 °C/min (0.167 K/s) the isothermal model is accurate enough, but faster tests requires an improvement of the model. © Springer-Verlag 2006 |
| abstractGer |
Summary In this work constant cooling rate crystallization experiments were carried out by a DSC, working with an iPP and using a very little amount of material, to minimize the heat transfer resistance in the mass of the sample. The resulting data were corrected to take into account also for the external heat transfer resistance. The corrected data were compared with data produced in the past, working with larger amounts of the same resin in a less accurate DSC apparatus, confirming that in the field of polymer crystallization kinetics the calorimeter has to be used carefully. The data were also used to check a kinetic model previously tuned under isothermal conditions. Up to 10 °C/min (0.167 K/s) the isothermal model is accurate enough, but faster tests requires an improvement of the model. © Springer-Verlag 2006 |
| abstract_unstemmed |
Summary In this work constant cooling rate crystallization experiments were carried out by a DSC, working with an iPP and using a very little amount of material, to minimize the heat transfer resistance in the mass of the sample. The resulting data were corrected to take into account also for the external heat transfer resistance. The corrected data were compared with data produced in the past, working with larger amounts of the same resin in a less accurate DSC apparatus, confirming that in the field of polymer crystallization kinetics the calorimeter has to be used carefully. The data were also used to check a kinetic model previously tuned under isothermal conditions. Up to 10 °C/min (0.167 K/s) the isothermal model is accurate enough, but faster tests requires an improvement of the model. © Springer-Verlag 2006 |
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| container_issue |
6 |
| title_short |
Some issues on polymer crystallization kinetics studied by DSC non isothermal tests |
| url |
https://doi.org/10.1007/s00289-006-0518-2 |
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false |
| author2 |
Naddeo, Carlo |
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Naddeo, Carlo |
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| doi_str |
10.1007/s00289-006-0518-2 |
| up_date |
2024-07-03T16:01:42.743Z |
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