Synthesis and characterization of mesoporous zeolite Beta templated by a novel organosiloxane
Abstract In this paper, a novel organosiloxane was prepared and employed as mesoporogen to synthesis mesoporous zeolite Beta successfully. With the increase of organosiloxane to synthesis mixture, the total BET (Brunauer–Emmett–Teller) surface areas of the as-obtained samples increased initially and...
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| Autor*in: |
Li, Bowen [verfasserIn] |
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| Format: |
Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2017 |
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| Schlagwörter: |
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| Anmerkung: |
© Springer Science+Business Media New York 2017 |
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| Übergeordnetes Werk: |
Enthalten in: Journal of porous materials - Springer US, 1995, 24(2017), 6 vom: 22. März, Seite 1673-1678 |
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| Übergeordnetes Werk: |
volume:24 ; year:2017 ; number:6 ; day:22 ; month:03 ; pages:1673-1678 |
| Links: |
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| DOI / URN: |
10.1007/s10934-017-0409-y |
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OLC2043014137 |
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| 520 | |a Abstract In this paper, a novel organosiloxane was prepared and employed as mesoporogen to synthesis mesoporous zeolite Beta successfully. With the increase of organosiloxane to synthesis mixture, the total BET (Brunauer–Emmett–Teller) surface areas of the as-obtained samples increased initially and then decreased. When the mesoporogen/$ SiO_{2} $ ratio was 0.0142, the prepared zeolite sample had the largest BET surface area up to 810 $ m^{2} $/g. The DFT pore size distribution shows that the resulting mesoporous zeolite Beta samples have mesopore size distributions of approximately 2–6 nm. SEM images exhibit the morphology of the samples comprised ellipsoidal particles of 400–500 nm, and its surface is similar to a cracked cauliflower. From the TEM images, large numbers of worm-like mesopores and the basic crystal structure of the mesoporous zeolite Beta are clearly presented. | ||
| 650 | 4 | |a Mesoporous | |
| 650 | 4 | |a Zeolite Beta | |
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| 700 | 1 | |a Song, Guoqiang |4 aut | |
| 700 | 1 | |a Wu, Yibo |4 aut | |
| 700 | 1 | |a Li, Fuxiang |4 aut | |
| 700 | 1 | |a Xue, Jianwei |4 aut | |
| 700 | 1 | |a Lv, Zhiping |4 aut | |
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10.1007/s10934-017-0409-y doi (DE-627)OLC2043014137 (DE-He213)s10934-017-0409-y-p DE-627 ger DE-627 rakwb eng 530 VZ Li, Bowen verfasserin aut Synthesis and characterization of mesoporous zeolite Beta templated by a novel organosiloxane 2017 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Springer Science+Business Media New York 2017 Abstract In this paper, a novel organosiloxane was prepared and employed as mesoporogen to synthesis mesoporous zeolite Beta successfully. With the increase of organosiloxane to synthesis mixture, the total BET (Brunauer–Emmett–Teller) surface areas of the as-obtained samples increased initially and then decreased. When the mesoporogen/$ SiO_{2} $ ratio was 0.0142, the prepared zeolite sample had the largest BET surface area up to 810 $ m^{2} $/g. The DFT pore size distribution shows that the resulting mesoporous zeolite Beta samples have mesopore size distributions of approximately 2–6 nm. SEM images exhibit the morphology of the samples comprised ellipsoidal particles of 400–500 nm, and its surface is similar to a cracked cauliflower. From the TEM images, large numbers of worm-like mesopores and the basic crystal structure of the mesoporous zeolite Beta are clearly presented. Mesoporous Zeolite Beta Synthesis Organosiloxane Song, Guoqiang aut Wu, Yibo aut Li, Fuxiang aut Xue, Jianwei aut Lv, Zhiping aut Enthalten in Journal of porous materials Springer US, 1995 24(2017), 6 vom: 22. März, Seite 1673-1678 (DE-627)211471933 (DE-600)1322952-7 (DE-576)121196038 1380-2224 nnns volume:24 year:2017 number:6 day:22 month:03 pages:1673-1678 https://doi.org/10.1007/s10934-017-0409-y lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-GEO GBV_ILN_70 AR 24 2017 6 22 03 1673-1678 |
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10.1007/s10934-017-0409-y doi (DE-627)OLC2043014137 (DE-He213)s10934-017-0409-y-p DE-627 ger DE-627 rakwb eng 530 VZ Li, Bowen verfasserin aut Synthesis and characterization of mesoporous zeolite Beta templated by a novel organosiloxane 2017 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Springer Science+Business Media New York 2017 Abstract In this paper, a novel organosiloxane was prepared and employed as mesoporogen to synthesis mesoporous zeolite Beta successfully. With the increase of organosiloxane to synthesis mixture, the total BET (Brunauer–Emmett–Teller) surface areas of the as-obtained samples increased initially and then decreased. When the mesoporogen/$ SiO_{2} $ ratio was 0.0142, the prepared zeolite sample had the largest BET surface area up to 810 $ m^{2} $/g. The DFT pore size distribution shows that the resulting mesoporous zeolite Beta samples have mesopore size distributions of approximately 2–6 nm. SEM images exhibit the morphology of the samples comprised ellipsoidal particles of 400–500 nm, and its surface is similar to a cracked cauliflower. From the TEM images, large numbers of worm-like mesopores and the basic crystal structure of the mesoporous zeolite Beta are clearly presented. Mesoporous Zeolite Beta Synthesis Organosiloxane Song, Guoqiang aut Wu, Yibo aut Li, Fuxiang aut Xue, Jianwei aut Lv, Zhiping aut Enthalten in Journal of porous materials Springer US, 1995 24(2017), 6 vom: 22. März, Seite 1673-1678 (DE-627)211471933 (DE-600)1322952-7 (DE-576)121196038 1380-2224 nnns volume:24 year:2017 number:6 day:22 month:03 pages:1673-1678 https://doi.org/10.1007/s10934-017-0409-y lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-GEO GBV_ILN_70 AR 24 2017 6 22 03 1673-1678 |
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10.1007/s10934-017-0409-y doi (DE-627)OLC2043014137 (DE-He213)s10934-017-0409-y-p DE-627 ger DE-627 rakwb eng 530 VZ Li, Bowen verfasserin aut Synthesis and characterization of mesoporous zeolite Beta templated by a novel organosiloxane 2017 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Springer Science+Business Media New York 2017 Abstract In this paper, a novel organosiloxane was prepared and employed as mesoporogen to synthesis mesoporous zeolite Beta successfully. With the increase of organosiloxane to synthesis mixture, the total BET (Brunauer–Emmett–Teller) surface areas of the as-obtained samples increased initially and then decreased. When the mesoporogen/$ SiO_{2} $ ratio was 0.0142, the prepared zeolite sample had the largest BET surface area up to 810 $ m^{2} $/g. The DFT pore size distribution shows that the resulting mesoporous zeolite Beta samples have mesopore size distributions of approximately 2–6 nm. SEM images exhibit the morphology of the samples comprised ellipsoidal particles of 400–500 nm, and its surface is similar to a cracked cauliflower. From the TEM images, large numbers of worm-like mesopores and the basic crystal structure of the mesoporous zeolite Beta are clearly presented. Mesoporous Zeolite Beta Synthesis Organosiloxane Song, Guoqiang aut Wu, Yibo aut Li, Fuxiang aut Xue, Jianwei aut Lv, Zhiping aut Enthalten in Journal of porous materials Springer US, 1995 24(2017), 6 vom: 22. März, Seite 1673-1678 (DE-627)211471933 (DE-600)1322952-7 (DE-576)121196038 1380-2224 nnns volume:24 year:2017 number:6 day:22 month:03 pages:1673-1678 https://doi.org/10.1007/s10934-017-0409-y lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-GEO GBV_ILN_70 AR 24 2017 6 22 03 1673-1678 |
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10.1007/s10934-017-0409-y doi (DE-627)OLC2043014137 (DE-He213)s10934-017-0409-y-p DE-627 ger DE-627 rakwb eng 530 VZ Li, Bowen verfasserin aut Synthesis and characterization of mesoporous zeolite Beta templated by a novel organosiloxane 2017 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Springer Science+Business Media New York 2017 Abstract In this paper, a novel organosiloxane was prepared and employed as mesoporogen to synthesis mesoporous zeolite Beta successfully. With the increase of organosiloxane to synthesis mixture, the total BET (Brunauer–Emmett–Teller) surface areas of the as-obtained samples increased initially and then decreased. When the mesoporogen/$ SiO_{2} $ ratio was 0.0142, the prepared zeolite sample had the largest BET surface area up to 810 $ m^{2} $/g. The DFT pore size distribution shows that the resulting mesoporous zeolite Beta samples have mesopore size distributions of approximately 2–6 nm. SEM images exhibit the morphology of the samples comprised ellipsoidal particles of 400–500 nm, and its surface is similar to a cracked cauliflower. From the TEM images, large numbers of worm-like mesopores and the basic crystal structure of the mesoporous zeolite Beta are clearly presented. Mesoporous Zeolite Beta Synthesis Organosiloxane Song, Guoqiang aut Wu, Yibo aut Li, Fuxiang aut Xue, Jianwei aut Lv, Zhiping aut Enthalten in Journal of porous materials Springer US, 1995 24(2017), 6 vom: 22. März, Seite 1673-1678 (DE-627)211471933 (DE-600)1322952-7 (DE-576)121196038 1380-2224 nnns volume:24 year:2017 number:6 day:22 month:03 pages:1673-1678 https://doi.org/10.1007/s10934-017-0409-y lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-GEO GBV_ILN_70 AR 24 2017 6 22 03 1673-1678 |
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10.1007/s10934-017-0409-y doi (DE-627)OLC2043014137 (DE-He213)s10934-017-0409-y-p DE-627 ger DE-627 rakwb eng 530 VZ Li, Bowen verfasserin aut Synthesis and characterization of mesoporous zeolite Beta templated by a novel organosiloxane 2017 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Springer Science+Business Media New York 2017 Abstract In this paper, a novel organosiloxane was prepared and employed as mesoporogen to synthesis mesoporous zeolite Beta successfully. With the increase of organosiloxane to synthesis mixture, the total BET (Brunauer–Emmett–Teller) surface areas of the as-obtained samples increased initially and then decreased. When the mesoporogen/$ SiO_{2} $ ratio was 0.0142, the prepared zeolite sample had the largest BET surface area up to 810 $ m^{2} $/g. The DFT pore size distribution shows that the resulting mesoporous zeolite Beta samples have mesopore size distributions of approximately 2–6 nm. SEM images exhibit the morphology of the samples comprised ellipsoidal particles of 400–500 nm, and its surface is similar to a cracked cauliflower. From the TEM images, large numbers of worm-like mesopores and the basic crystal structure of the mesoporous zeolite Beta are clearly presented. Mesoporous Zeolite Beta Synthesis Organosiloxane Song, Guoqiang aut Wu, Yibo aut Li, Fuxiang aut Xue, Jianwei aut Lv, Zhiping aut Enthalten in Journal of porous materials Springer US, 1995 24(2017), 6 vom: 22. März, Seite 1673-1678 (DE-627)211471933 (DE-600)1322952-7 (DE-576)121196038 1380-2224 nnns volume:24 year:2017 number:6 day:22 month:03 pages:1673-1678 https://doi.org/10.1007/s10934-017-0409-y lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-GEO GBV_ILN_70 AR 24 2017 6 22 03 1673-1678 |
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Synthesis and characterization of mesoporous zeolite Beta templated by a novel organosiloxane |
| abstract |
Abstract In this paper, a novel organosiloxane was prepared and employed as mesoporogen to synthesis mesoporous zeolite Beta successfully. With the increase of organosiloxane to synthesis mixture, the total BET (Brunauer–Emmett–Teller) surface areas of the as-obtained samples increased initially and then decreased. When the mesoporogen/$ SiO_{2} $ ratio was 0.0142, the prepared zeolite sample had the largest BET surface area up to 810 $ m^{2} $/g. The DFT pore size distribution shows that the resulting mesoporous zeolite Beta samples have mesopore size distributions of approximately 2–6 nm. SEM images exhibit the morphology of the samples comprised ellipsoidal particles of 400–500 nm, and its surface is similar to a cracked cauliflower. From the TEM images, large numbers of worm-like mesopores and the basic crystal structure of the mesoporous zeolite Beta are clearly presented. © Springer Science+Business Media New York 2017 |
| abstractGer |
Abstract In this paper, a novel organosiloxane was prepared and employed as mesoporogen to synthesis mesoporous zeolite Beta successfully. With the increase of organosiloxane to synthesis mixture, the total BET (Brunauer–Emmett–Teller) surface areas of the as-obtained samples increased initially and then decreased. When the mesoporogen/$ SiO_{2} $ ratio was 0.0142, the prepared zeolite sample had the largest BET surface area up to 810 $ m^{2} $/g. The DFT pore size distribution shows that the resulting mesoporous zeolite Beta samples have mesopore size distributions of approximately 2–6 nm. SEM images exhibit the morphology of the samples comprised ellipsoidal particles of 400–500 nm, and its surface is similar to a cracked cauliflower. From the TEM images, large numbers of worm-like mesopores and the basic crystal structure of the mesoporous zeolite Beta are clearly presented. © Springer Science+Business Media New York 2017 |
| abstract_unstemmed |
Abstract In this paper, a novel organosiloxane was prepared and employed as mesoporogen to synthesis mesoporous zeolite Beta successfully. With the increase of organosiloxane to synthesis mixture, the total BET (Brunauer–Emmett–Teller) surface areas of the as-obtained samples increased initially and then decreased. When the mesoporogen/$ SiO_{2} $ ratio was 0.0142, the prepared zeolite sample had the largest BET surface area up to 810 $ m^{2} $/g. The DFT pore size distribution shows that the resulting mesoporous zeolite Beta samples have mesopore size distributions of approximately 2–6 nm. SEM images exhibit the morphology of the samples comprised ellipsoidal particles of 400–500 nm, and its surface is similar to a cracked cauliflower. From the TEM images, large numbers of worm-like mesopores and the basic crystal structure of the mesoporous zeolite Beta are clearly presented. © Springer Science+Business Media New York 2017 |
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Synthesis and characterization of mesoporous zeolite Beta templated by a novel organosiloxane |
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Song, Guoqiang Wu, Yibo Li, Fuxiang Xue, Jianwei Lv, Zhiping |
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