Preparation of monolithic silica gel and glass by the sol-gel method using N,N-dimethylformamide
Abstract The use of N,N-dimethylformamide (DMF) was found to be effective in the sol-gel synthesis of silica gel and glass monoliths from tetramethoxysi lane (TMOS) by the sol-gel method. Wet gel bodies prepared by gelation of TMOS-DMF-$ CH_{3} $OH-$ H_{2} $O-$ NH_{4} $OH (or $ HNO_{3} $) solutions...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Adachi, Tatsuhiko [verfasserIn] |
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| Format: |
Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
1987 |
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| Schlagwörter: |
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| Anmerkung: |
© Chapman and Hall Ltd. 1987 |
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| Übergeordnetes Werk: |
Enthalten in: Journal of materials science - Kluwer Academic Publishers, 1966, 22(1987), 12 vom: Dez., Seite 4407-4410 |
|---|---|
| Übergeordnetes Werk: |
volume:22 ; year:1987 ; number:12 ; month:12 ; pages:4407-4410 |
| Links: |
|---|
| DOI / URN: |
10.1007/BF01132038 |
|---|
| Katalog-ID: |
OLC2046150872 |
|---|
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| 520 | |a Abstract The use of N,N-dimethylformamide (DMF) was found to be effective in the sol-gel synthesis of silica gel and glass monoliths from tetramethoxysi lane (TMOS) by the sol-gel method. Wet gel bodies prepared by gelation of TMOS-DMF-$ CH_{3} $OH-$ H_{2} $O-$ NH_{4} $OH (or $ HNO_{3} $) solutions could be dried without the occurrence of fracture or cracks when drying conditions were appropriate. Furthermore, the resultant dried gel monoliths could be converted without cracking or bloating to silica glass on heating up to 1050° C and holding there for 2 h, when the composition of the starting solution was appropriate. | ||
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10.1007/BF01132038 doi (DE-627)OLC2046150872 (DE-He213)BF01132038-p DE-627 ger DE-627 rakwb eng 670 VZ Adachi, Tatsuhiko verfasserin aut Preparation of monolithic silica gel and glass by the sol-gel method using N,N-dimethylformamide 1987 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Chapman and Hall Ltd. 1987 Abstract The use of N,N-dimethylformamide (DMF) was found to be effective in the sol-gel synthesis of silica gel and glass monoliths from tetramethoxysi lane (TMOS) by the sol-gel method. Wet gel bodies prepared by gelation of TMOS-DMF-$ CH_{3} $OH-$ H_{2} $O-$ NH_{4} $OH (or $ HNO_{3} $) solutions could be dried without the occurrence of fracture or cracks when drying conditions were appropriate. Furthermore, the resultant dried gel monoliths could be converted without cracking or bloating to silica glass on heating up to 1050° C and holding there for 2 h, when the composition of the starting solution was appropriate. Polymer HNO3 Silica Glass TMOS Tetramethoxysi Lane Sakka, Sumio aut Enthalten in Journal of materials science Kluwer Academic Publishers, 1966 22(1987), 12 vom: Dez., Seite 4407-4410 (DE-627)129546372 (DE-600)218324-9 (DE-576)014996774 0022-2461 nnns volume:22 year:1987 number:12 month:12 pages:4407-4410 https://doi.org/10.1007/BF01132038 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC GBV_ILN_11 GBV_ILN_20 GBV_ILN_23 GBV_ILN_30 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_62 GBV_ILN_65 GBV_ILN_70 GBV_ILN_2004 GBV_ILN_2006 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2057 GBV_ILN_2333 GBV_ILN_4082 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4316 GBV_ILN_4319 GBV_ILN_4323 GBV_ILN_4700 AR 22 1987 12 12 4407-4410 |
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10.1007/BF01132038 doi (DE-627)OLC2046150872 (DE-He213)BF01132038-p DE-627 ger DE-627 rakwb eng 670 VZ Adachi, Tatsuhiko verfasserin aut Preparation of monolithic silica gel and glass by the sol-gel method using N,N-dimethylformamide 1987 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Chapman and Hall Ltd. 1987 Abstract The use of N,N-dimethylformamide (DMF) was found to be effective in the sol-gel synthesis of silica gel and glass monoliths from tetramethoxysi lane (TMOS) by the sol-gel method. Wet gel bodies prepared by gelation of TMOS-DMF-$ CH_{3} $OH-$ H_{2} $O-$ NH_{4} $OH (or $ HNO_{3} $) solutions could be dried without the occurrence of fracture or cracks when drying conditions were appropriate. Furthermore, the resultant dried gel monoliths could be converted without cracking or bloating to silica glass on heating up to 1050° C and holding there for 2 h, when the composition of the starting solution was appropriate. Polymer HNO3 Silica Glass TMOS Tetramethoxysi Lane Sakka, Sumio aut Enthalten in Journal of materials science Kluwer Academic Publishers, 1966 22(1987), 12 vom: Dez., Seite 4407-4410 (DE-627)129546372 (DE-600)218324-9 (DE-576)014996774 0022-2461 nnns volume:22 year:1987 number:12 month:12 pages:4407-4410 https://doi.org/10.1007/BF01132038 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC GBV_ILN_11 GBV_ILN_20 GBV_ILN_23 GBV_ILN_30 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_62 GBV_ILN_65 GBV_ILN_70 GBV_ILN_2004 GBV_ILN_2006 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2057 GBV_ILN_2333 GBV_ILN_4082 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4316 GBV_ILN_4319 GBV_ILN_4323 GBV_ILN_4700 AR 22 1987 12 12 4407-4410 |
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10.1007/BF01132038 doi (DE-627)OLC2046150872 (DE-He213)BF01132038-p DE-627 ger DE-627 rakwb eng 670 VZ Adachi, Tatsuhiko verfasserin aut Preparation of monolithic silica gel and glass by the sol-gel method using N,N-dimethylformamide 1987 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Chapman and Hall Ltd. 1987 Abstract The use of N,N-dimethylformamide (DMF) was found to be effective in the sol-gel synthesis of silica gel and glass monoliths from tetramethoxysi lane (TMOS) by the sol-gel method. Wet gel bodies prepared by gelation of TMOS-DMF-$ CH_{3} $OH-$ H_{2} $O-$ NH_{4} $OH (or $ HNO_{3} $) solutions could be dried without the occurrence of fracture or cracks when drying conditions were appropriate. Furthermore, the resultant dried gel monoliths could be converted without cracking or bloating to silica glass on heating up to 1050° C and holding there for 2 h, when the composition of the starting solution was appropriate. Polymer HNO3 Silica Glass TMOS Tetramethoxysi Lane Sakka, Sumio aut Enthalten in Journal of materials science Kluwer Academic Publishers, 1966 22(1987), 12 vom: Dez., Seite 4407-4410 (DE-627)129546372 (DE-600)218324-9 (DE-576)014996774 0022-2461 nnns volume:22 year:1987 number:12 month:12 pages:4407-4410 https://doi.org/10.1007/BF01132038 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC GBV_ILN_11 GBV_ILN_20 GBV_ILN_23 GBV_ILN_30 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_62 GBV_ILN_65 GBV_ILN_70 GBV_ILN_2004 GBV_ILN_2006 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2057 GBV_ILN_2333 GBV_ILN_4082 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4316 GBV_ILN_4319 GBV_ILN_4323 GBV_ILN_4700 AR 22 1987 12 12 4407-4410 |
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10.1007/BF01132038 doi (DE-627)OLC2046150872 (DE-He213)BF01132038-p DE-627 ger DE-627 rakwb eng 670 VZ Adachi, Tatsuhiko verfasserin aut Preparation of monolithic silica gel and glass by the sol-gel method using N,N-dimethylformamide 1987 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Chapman and Hall Ltd. 1987 Abstract The use of N,N-dimethylformamide (DMF) was found to be effective in the sol-gel synthesis of silica gel and glass monoliths from tetramethoxysi lane (TMOS) by the sol-gel method. Wet gel bodies prepared by gelation of TMOS-DMF-$ CH_{3} $OH-$ H_{2} $O-$ NH_{4} $OH (or $ HNO_{3} $) solutions could be dried without the occurrence of fracture or cracks when drying conditions were appropriate. Furthermore, the resultant dried gel monoliths could be converted without cracking or bloating to silica glass on heating up to 1050° C and holding there for 2 h, when the composition of the starting solution was appropriate. Polymer HNO3 Silica Glass TMOS Tetramethoxysi Lane Sakka, Sumio aut Enthalten in Journal of materials science Kluwer Academic Publishers, 1966 22(1987), 12 vom: Dez., Seite 4407-4410 (DE-627)129546372 (DE-600)218324-9 (DE-576)014996774 0022-2461 nnns volume:22 year:1987 number:12 month:12 pages:4407-4410 https://doi.org/10.1007/BF01132038 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC GBV_ILN_11 GBV_ILN_20 GBV_ILN_23 GBV_ILN_30 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_62 GBV_ILN_65 GBV_ILN_70 GBV_ILN_2004 GBV_ILN_2006 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2057 GBV_ILN_2333 GBV_ILN_4082 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4316 GBV_ILN_4319 GBV_ILN_4323 GBV_ILN_4700 AR 22 1987 12 12 4407-4410 |
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10.1007/BF01132038 doi (DE-627)OLC2046150872 (DE-He213)BF01132038-p DE-627 ger DE-627 rakwb eng 670 VZ Adachi, Tatsuhiko verfasserin aut Preparation of monolithic silica gel and glass by the sol-gel method using N,N-dimethylformamide 1987 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Chapman and Hall Ltd. 1987 Abstract The use of N,N-dimethylformamide (DMF) was found to be effective in the sol-gel synthesis of silica gel and glass monoliths from tetramethoxysi lane (TMOS) by the sol-gel method. Wet gel bodies prepared by gelation of TMOS-DMF-$ CH_{3} $OH-$ H_{2} $O-$ NH_{4} $OH (or $ HNO_{3} $) solutions could be dried without the occurrence of fracture or cracks when drying conditions were appropriate. Furthermore, the resultant dried gel monoliths could be converted without cracking or bloating to silica glass on heating up to 1050° C and holding there for 2 h, when the composition of the starting solution was appropriate. Polymer HNO3 Silica Glass TMOS Tetramethoxysi Lane Sakka, Sumio aut Enthalten in Journal of materials science Kluwer Academic Publishers, 1966 22(1987), 12 vom: Dez., Seite 4407-4410 (DE-627)129546372 (DE-600)218324-9 (DE-576)014996774 0022-2461 nnns volume:22 year:1987 number:12 month:12 pages:4407-4410 https://doi.org/10.1007/BF01132038 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC GBV_ILN_11 GBV_ILN_20 GBV_ILN_23 GBV_ILN_30 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_62 GBV_ILN_65 GBV_ILN_70 GBV_ILN_2004 GBV_ILN_2006 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2057 GBV_ILN_2333 GBV_ILN_4082 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4316 GBV_ILN_4319 GBV_ILN_4323 GBV_ILN_4700 AR 22 1987 12 12 4407-4410 |
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Adachi, Tatsuhiko |
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670 VZ Preparation of monolithic silica gel and glass by the sol-gel method using N,N-dimethylformamide Polymer HNO3 Silica Glass TMOS Tetramethoxysi Lane |
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ddc 670 misc Polymer misc HNO3 misc Silica Glass misc TMOS misc Tetramethoxysi Lane |
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ddc 670 misc Polymer misc HNO3 misc Silica Glass misc TMOS misc Tetramethoxysi Lane |
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Preparation of monolithic silica gel and glass by the sol-gel method using N,N-dimethylformamide |
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Preparation of monolithic silica gel and glass by the sol-gel method using N,N-dimethylformamide |
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Adachi, Tatsuhiko |
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Journal of materials science |
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Journal of materials science |
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1987 |
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4407 |
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Adachi, Tatsuhiko Sakka, Sumio |
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670 VZ |
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10.1007/BF01132038 |
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670 |
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preparation of monolithic silica gel and glass by the sol-gel method using n,n-dimethylformamide |
| title_auth |
Preparation of monolithic silica gel and glass by the sol-gel method using N,N-dimethylformamide |
| abstract |
Abstract The use of N,N-dimethylformamide (DMF) was found to be effective in the sol-gel synthesis of silica gel and glass monoliths from tetramethoxysi lane (TMOS) by the sol-gel method. Wet gel bodies prepared by gelation of TMOS-DMF-$ CH_{3} $OH-$ H_{2} $O-$ NH_{4} $OH (or $ HNO_{3} $) solutions could be dried without the occurrence of fracture or cracks when drying conditions were appropriate. Furthermore, the resultant dried gel monoliths could be converted without cracking or bloating to silica glass on heating up to 1050° C and holding there for 2 h, when the composition of the starting solution was appropriate. © Chapman and Hall Ltd. 1987 |
| abstractGer |
Abstract The use of N,N-dimethylformamide (DMF) was found to be effective in the sol-gel synthesis of silica gel and glass monoliths from tetramethoxysi lane (TMOS) by the sol-gel method. Wet gel bodies prepared by gelation of TMOS-DMF-$ CH_{3} $OH-$ H_{2} $O-$ NH_{4} $OH (or $ HNO_{3} $) solutions could be dried without the occurrence of fracture or cracks when drying conditions were appropriate. Furthermore, the resultant dried gel monoliths could be converted without cracking or bloating to silica glass on heating up to 1050° C and holding there for 2 h, when the composition of the starting solution was appropriate. © Chapman and Hall Ltd. 1987 |
| abstract_unstemmed |
Abstract The use of N,N-dimethylformamide (DMF) was found to be effective in the sol-gel synthesis of silica gel and glass monoliths from tetramethoxysi lane (TMOS) by the sol-gel method. Wet gel bodies prepared by gelation of TMOS-DMF-$ CH_{3} $OH-$ H_{2} $O-$ NH_{4} $OH (or $ HNO_{3} $) solutions could be dried without the occurrence of fracture or cracks when drying conditions were appropriate. Furthermore, the resultant dried gel monoliths could be converted without cracking or bloating to silica glass on heating up to 1050° C and holding there for 2 h, when the composition of the starting solution was appropriate. © Chapman and Hall Ltd. 1987 |
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Preparation of monolithic silica gel and glass by the sol-gel method using N,N-dimethylformamide |
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