Crystallisation of M-SiAlON glasses to $ I_{w} $-phase glass-ceramics: preparation and characterisation
Abstract The crystallisation of M-SiAlON glasses (M = Y, Ln) is particularly sensitive to small variations in composition and heat treatment temperature. The formation of $ I_{w} $-phase in the YSiAlON system has been studied but little information concerning its nucleation, thermal stability, mecha...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Diaz, A. [verfasserIn] |
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| Format: |
Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2002 |
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| Schlagwörter: |
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| Anmerkung: |
© Kluwer Academic Publishers 2002 |
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| Übergeordnetes Werk: |
Enthalten in: Journal of materials science - Kluwer Academic Publishers, 1966, 37(2002), 4 vom: Feb., Seite 723-730 |
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| Übergeordnetes Werk: |
volume:37 ; year:2002 ; number:4 ; month:02 ; pages:723-730 |
| Links: |
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| DOI / URN: |
10.1023/A:1013831612767 |
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| Katalog-ID: |
OLC2046272684 |
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| 245 | 1 | 0 | |a Crystallisation of M-SiAlON glasses to $ I_{w} $-phase glass-ceramics: preparation and characterisation |
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| 520 | |a Abstract The crystallisation of M-SiAlON glasses (M = Y, Ln) is particularly sensitive to small variations in composition and heat treatment temperature. The formation of $ I_{w} $-phase in the YSiAlON system has been studied but little information concerning its nucleation, thermal stability, mechanical properties and extension into the lanthanide sialon series is available. In order to better understand the synthesis and to characterise more fully the $ I_{w} $-glass-ceramic materials, a series of glass compositions have been prepared and characterised. These include $ M_{3} $$ Si_{3} $$ Al_{2} $$ O_{12.15} $$ N_{0.90} $ (M = Y, Er, Ce, Yb); $ M_{3.45} $$ Si_{3} $$ Al_{2} $$ O_{12.76} $$ N_{0.95} $ (M = Y, Er); $ Y_{4} $$ Si_{3} $$ Al_{2} $$ O_{13.50} $N and $ Y_{4} $$ Si_{3.37} $$ Al_{1.50} $$ O_{13.50} $N. Heat treatments were performed on these glasses and the resulting crystalline products have been studied by X-ray diffraction (XRD). Differential Thermal Analysis (DTA) in combination with XRD analysis of $ Y_{3.45} $$ Si_{3} $$ Al_{2} $$ O_{12.76} $$ N_{0.95} $ and $ Ce_{3} $$ Si_{2} $$ Al_{2} $$ O_{12.15} $$ N_{0.90} $ parent glass-compositions was used to investigate crystal phase formation. Young's modulus (E), hardness (Hv and fracture toughness (KIC) of the glass-ceramics were measured. Glass-ceramics containing $ I_{w} $-phase as the only detectable crystalline phase have been produced from $ M_{3} $$ Si_{3} $$ Al_{2} $$ O_{12.15} $$ N_{0.90} $ and $ M_{3.45} $$ Si_{3} $$ Al_{2} $$ O_{12.76} $$ N_{0.95} $ (M = Y and Er) compositions. No equivalent phase was found in the Ce- and Yb-sialon compositions. | ||
| 650 | 4 | |a Polymer | |
| 650 | 4 | |a Heat Treatment | |
| 650 | 4 | |a Thermal Stability | |
| 650 | 4 | |a Thermal Analysis | |
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10.1023/A:1013831612767 doi (DE-627)OLC2046272684 (DE-He213)A:1013831612767-p DE-627 ger DE-627 rakwb eng 670 VZ Diaz, A. verfasserin aut Crystallisation of M-SiAlON glasses to $ I_{w} $-phase glass-ceramics: preparation and characterisation 2002 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Kluwer Academic Publishers 2002 Abstract The crystallisation of M-SiAlON glasses (M = Y, Ln) is particularly sensitive to small variations in composition and heat treatment temperature. The formation of $ I_{w} $-phase in the YSiAlON system has been studied but little information concerning its nucleation, thermal stability, mechanical properties and extension into the lanthanide sialon series is available. In order to better understand the synthesis and to characterise more fully the $ I_{w} $-glass-ceramic materials, a series of glass compositions have been prepared and characterised. These include $ M_{3} $$ Si_{3} $$ Al_{2} $$ O_{12.15} $$ N_{0.90} $ (M = Y, Er, Ce, Yb); $ M_{3.45} $$ Si_{3} $$ Al_{2} $$ O_{12.76} $$ N_{0.95} $ (M = Y, Er); $ Y_{4} $$ Si_{3} $$ Al_{2} $$ O_{13.50} $N and $ Y_{4} $$ Si_{3.37} $$ Al_{1.50} $$ O_{13.50} $N. Heat treatments were performed on these glasses and the resulting crystalline products have been studied by X-ray diffraction (XRD). Differential Thermal Analysis (DTA) in combination with XRD analysis of $ Y_{3.45} $$ Si_{3} $$ Al_{2} $$ O_{12.76} $$ N_{0.95} $ and $ Ce_{3} $$ Si_{2} $$ Al_{2} $$ O_{12.15} $$ N_{0.90} $ parent glass-compositions was used to investigate crystal phase formation. Young's modulus (E), hardness (Hv and fracture toughness (KIC) of the glass-ceramics were measured. Glass-ceramics containing $ I_{w} $-phase as the only detectable crystalline phase have been produced from $ M_{3} $$ Si_{3} $$ Al_{2} $$ O_{12.15} $$ N_{0.90} $ and $ M_{3.45} $$ Si_{3} $$ Al_{2} $$ O_{12.76} $$ N_{0.95} $ (M = Y and Er) compositions. No equivalent phase was found in the Ce- and Yb-sialon compositions. Polymer Heat Treatment Thermal Stability Thermal Analysis Fracture Toughness Hampshire, S. aut Enthalten in Journal of materials science Kluwer Academic Publishers, 1966 37(2002), 4 vom: Feb., Seite 723-730 (DE-627)129546372 (DE-600)218324-9 (DE-576)014996774 0022-2461 nnns volume:37 year:2002 number:4 month:02 pages:723-730 https://doi.org/10.1023/A:1013831612767 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC GBV_ILN_20 GBV_ILN_23 GBV_ILN_30 GBV_ILN_32 GBV_ILN_40 GBV_ILN_62 GBV_ILN_65 GBV_ILN_70 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_4046 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4319 GBV_ILN_4323 AR 37 2002 4 02 723-730 |
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10.1023/A:1013831612767 doi (DE-627)OLC2046272684 (DE-He213)A:1013831612767-p DE-627 ger DE-627 rakwb eng 670 VZ Diaz, A. verfasserin aut Crystallisation of M-SiAlON glasses to $ I_{w} $-phase glass-ceramics: preparation and characterisation 2002 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Kluwer Academic Publishers 2002 Abstract The crystallisation of M-SiAlON glasses (M = Y, Ln) is particularly sensitive to small variations in composition and heat treatment temperature. The formation of $ I_{w} $-phase in the YSiAlON system has been studied but little information concerning its nucleation, thermal stability, mechanical properties and extension into the lanthanide sialon series is available. In order to better understand the synthesis and to characterise more fully the $ I_{w} $-glass-ceramic materials, a series of glass compositions have been prepared and characterised. These include $ M_{3} $$ Si_{3} $$ Al_{2} $$ O_{12.15} $$ N_{0.90} $ (M = Y, Er, Ce, Yb); $ M_{3.45} $$ Si_{3} $$ Al_{2} $$ O_{12.76} $$ N_{0.95} $ (M = Y, Er); $ Y_{4} $$ Si_{3} $$ Al_{2} $$ O_{13.50} $N and $ Y_{4} $$ Si_{3.37} $$ Al_{1.50} $$ O_{13.50} $N. Heat treatments were performed on these glasses and the resulting crystalline products have been studied by X-ray diffraction (XRD). Differential Thermal Analysis (DTA) in combination with XRD analysis of $ Y_{3.45} $$ Si_{3} $$ Al_{2} $$ O_{12.76} $$ N_{0.95} $ and $ Ce_{3} $$ Si_{2} $$ Al_{2} $$ O_{12.15} $$ N_{0.90} $ parent glass-compositions was used to investigate crystal phase formation. Young's modulus (E), hardness (Hv and fracture toughness (KIC) of the glass-ceramics were measured. Glass-ceramics containing $ I_{w} $-phase as the only detectable crystalline phase have been produced from $ M_{3} $$ Si_{3} $$ Al_{2} $$ O_{12.15} $$ N_{0.90} $ and $ M_{3.45} $$ Si_{3} $$ Al_{2} $$ O_{12.76} $$ N_{0.95} $ (M = Y and Er) compositions. No equivalent phase was found in the Ce- and Yb-sialon compositions. Polymer Heat Treatment Thermal Stability Thermal Analysis Fracture Toughness Hampshire, S. aut Enthalten in Journal of materials science Kluwer Academic Publishers, 1966 37(2002), 4 vom: Feb., Seite 723-730 (DE-627)129546372 (DE-600)218324-9 (DE-576)014996774 0022-2461 nnns volume:37 year:2002 number:4 month:02 pages:723-730 https://doi.org/10.1023/A:1013831612767 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC GBV_ILN_20 GBV_ILN_23 GBV_ILN_30 GBV_ILN_32 GBV_ILN_40 GBV_ILN_62 GBV_ILN_65 GBV_ILN_70 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_4046 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4319 GBV_ILN_4323 AR 37 2002 4 02 723-730 |
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10.1023/A:1013831612767 doi (DE-627)OLC2046272684 (DE-He213)A:1013831612767-p DE-627 ger DE-627 rakwb eng 670 VZ Diaz, A. verfasserin aut Crystallisation of M-SiAlON glasses to $ I_{w} $-phase glass-ceramics: preparation and characterisation 2002 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Kluwer Academic Publishers 2002 Abstract The crystallisation of M-SiAlON glasses (M = Y, Ln) is particularly sensitive to small variations in composition and heat treatment temperature. The formation of $ I_{w} $-phase in the YSiAlON system has been studied but little information concerning its nucleation, thermal stability, mechanical properties and extension into the lanthanide sialon series is available. In order to better understand the synthesis and to characterise more fully the $ I_{w} $-glass-ceramic materials, a series of glass compositions have been prepared and characterised. These include $ M_{3} $$ Si_{3} $$ Al_{2} $$ O_{12.15} $$ N_{0.90} $ (M = Y, Er, Ce, Yb); $ M_{3.45} $$ Si_{3} $$ Al_{2} $$ O_{12.76} $$ N_{0.95} $ (M = Y, Er); $ Y_{4} $$ Si_{3} $$ Al_{2} $$ O_{13.50} $N and $ Y_{4} $$ Si_{3.37} $$ Al_{1.50} $$ O_{13.50} $N. Heat treatments were performed on these glasses and the resulting crystalline products have been studied by X-ray diffraction (XRD). Differential Thermal Analysis (DTA) in combination with XRD analysis of $ Y_{3.45} $$ Si_{3} $$ Al_{2} $$ O_{12.76} $$ N_{0.95} $ and $ Ce_{3} $$ Si_{2} $$ Al_{2} $$ O_{12.15} $$ N_{0.90} $ parent glass-compositions was used to investigate crystal phase formation. Young's modulus (E), hardness (Hv and fracture toughness (KIC) of the glass-ceramics were measured. Glass-ceramics containing $ I_{w} $-phase as the only detectable crystalline phase have been produced from $ M_{3} $$ Si_{3} $$ Al_{2} $$ O_{12.15} $$ N_{0.90} $ and $ M_{3.45} $$ Si_{3} $$ Al_{2} $$ O_{12.76} $$ N_{0.95} $ (M = Y and Er) compositions. No equivalent phase was found in the Ce- and Yb-sialon compositions. Polymer Heat Treatment Thermal Stability Thermal Analysis Fracture Toughness Hampshire, S. aut Enthalten in Journal of materials science Kluwer Academic Publishers, 1966 37(2002), 4 vom: Feb., Seite 723-730 (DE-627)129546372 (DE-600)218324-9 (DE-576)014996774 0022-2461 nnns volume:37 year:2002 number:4 month:02 pages:723-730 https://doi.org/10.1023/A:1013831612767 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC GBV_ILN_20 GBV_ILN_23 GBV_ILN_30 GBV_ILN_32 GBV_ILN_40 GBV_ILN_62 GBV_ILN_65 GBV_ILN_70 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_4046 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4319 GBV_ILN_4323 AR 37 2002 4 02 723-730 |
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10.1023/A:1013831612767 doi (DE-627)OLC2046272684 (DE-He213)A:1013831612767-p DE-627 ger DE-627 rakwb eng 670 VZ Diaz, A. verfasserin aut Crystallisation of M-SiAlON glasses to $ I_{w} $-phase glass-ceramics: preparation and characterisation 2002 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Kluwer Academic Publishers 2002 Abstract The crystallisation of M-SiAlON glasses (M = Y, Ln) is particularly sensitive to small variations in composition and heat treatment temperature. The formation of $ I_{w} $-phase in the YSiAlON system has been studied but little information concerning its nucleation, thermal stability, mechanical properties and extension into the lanthanide sialon series is available. In order to better understand the synthesis and to characterise more fully the $ I_{w} $-glass-ceramic materials, a series of glass compositions have been prepared and characterised. These include $ M_{3} $$ Si_{3} $$ Al_{2} $$ O_{12.15} $$ N_{0.90} $ (M = Y, Er, Ce, Yb); $ M_{3.45} $$ Si_{3} $$ Al_{2} $$ O_{12.76} $$ N_{0.95} $ (M = Y, Er); $ Y_{4} $$ Si_{3} $$ Al_{2} $$ O_{13.50} $N and $ Y_{4} $$ Si_{3.37} $$ Al_{1.50} $$ O_{13.50} $N. Heat treatments were performed on these glasses and the resulting crystalline products have been studied by X-ray diffraction (XRD). Differential Thermal Analysis (DTA) in combination with XRD analysis of $ Y_{3.45} $$ Si_{3} $$ Al_{2} $$ O_{12.76} $$ N_{0.95} $ and $ Ce_{3} $$ Si_{2} $$ Al_{2} $$ O_{12.15} $$ N_{0.90} $ parent glass-compositions was used to investigate crystal phase formation. Young's modulus (E), hardness (Hv and fracture toughness (KIC) of the glass-ceramics were measured. Glass-ceramics containing $ I_{w} $-phase as the only detectable crystalline phase have been produced from $ M_{3} $$ Si_{3} $$ Al_{2} $$ O_{12.15} $$ N_{0.90} $ and $ M_{3.45} $$ Si_{3} $$ Al_{2} $$ O_{12.76} $$ N_{0.95} $ (M = Y and Er) compositions. No equivalent phase was found in the Ce- and Yb-sialon compositions. Polymer Heat Treatment Thermal Stability Thermal Analysis Fracture Toughness Hampshire, S. aut Enthalten in Journal of materials science Kluwer Academic Publishers, 1966 37(2002), 4 vom: Feb., Seite 723-730 (DE-627)129546372 (DE-600)218324-9 (DE-576)014996774 0022-2461 nnns volume:37 year:2002 number:4 month:02 pages:723-730 https://doi.org/10.1023/A:1013831612767 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC GBV_ILN_20 GBV_ILN_23 GBV_ILN_30 GBV_ILN_32 GBV_ILN_40 GBV_ILN_62 GBV_ILN_65 GBV_ILN_70 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_4046 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4319 GBV_ILN_4323 AR 37 2002 4 02 723-730 |
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10.1023/A:1013831612767 doi (DE-627)OLC2046272684 (DE-He213)A:1013831612767-p DE-627 ger DE-627 rakwb eng 670 VZ Diaz, A. verfasserin aut Crystallisation of M-SiAlON glasses to $ I_{w} $-phase glass-ceramics: preparation and characterisation 2002 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Kluwer Academic Publishers 2002 Abstract The crystallisation of M-SiAlON glasses (M = Y, Ln) is particularly sensitive to small variations in composition and heat treatment temperature. The formation of $ I_{w} $-phase in the YSiAlON system has been studied but little information concerning its nucleation, thermal stability, mechanical properties and extension into the lanthanide sialon series is available. In order to better understand the synthesis and to characterise more fully the $ I_{w} $-glass-ceramic materials, a series of glass compositions have been prepared and characterised. These include $ M_{3} $$ Si_{3} $$ Al_{2} $$ O_{12.15} $$ N_{0.90} $ (M = Y, Er, Ce, Yb); $ M_{3.45} $$ Si_{3} $$ Al_{2} $$ O_{12.76} $$ N_{0.95} $ (M = Y, Er); $ Y_{4} $$ Si_{3} $$ Al_{2} $$ O_{13.50} $N and $ Y_{4} $$ Si_{3.37} $$ Al_{1.50} $$ O_{13.50} $N. Heat treatments were performed on these glasses and the resulting crystalline products have been studied by X-ray diffraction (XRD). Differential Thermal Analysis (DTA) in combination with XRD analysis of $ Y_{3.45} $$ Si_{3} $$ Al_{2} $$ O_{12.76} $$ N_{0.95} $ and $ Ce_{3} $$ Si_{2} $$ Al_{2} $$ O_{12.15} $$ N_{0.90} $ parent glass-compositions was used to investigate crystal phase formation. Young's modulus (E), hardness (Hv and fracture toughness (KIC) of the glass-ceramics were measured. Glass-ceramics containing $ I_{w} $-phase as the only detectable crystalline phase have been produced from $ M_{3} $$ Si_{3} $$ Al_{2} $$ O_{12.15} $$ N_{0.90} $ and $ M_{3.45} $$ Si_{3} $$ Al_{2} $$ O_{12.76} $$ N_{0.95} $ (M = Y and Er) compositions. No equivalent phase was found in the Ce- and Yb-sialon compositions. Polymer Heat Treatment Thermal Stability Thermal Analysis Fracture Toughness Hampshire, S. aut Enthalten in Journal of materials science Kluwer Academic Publishers, 1966 37(2002), 4 vom: Feb., Seite 723-730 (DE-627)129546372 (DE-600)218324-9 (DE-576)014996774 0022-2461 nnns volume:37 year:2002 number:4 month:02 pages:723-730 https://doi.org/10.1023/A:1013831612767 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC GBV_ILN_20 GBV_ILN_23 GBV_ILN_30 GBV_ILN_32 GBV_ILN_40 GBV_ILN_62 GBV_ILN_65 GBV_ILN_70 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_4046 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4319 GBV_ILN_4323 AR 37 2002 4 02 723-730 |
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The formation of $ I_{w} $-phase in the YSiAlON system has been studied but little information concerning its nucleation, thermal stability, mechanical properties and extension into the lanthanide sialon series is available. In order to better understand the synthesis and to characterise more fully the $ I_{w} $-glass-ceramic materials, a series of glass compositions have been prepared and characterised. These include $ M_{3} $$ Si_{3} $$ Al_{2} $$ O_{12.15} $$ N_{0.90} $ (M = Y, Er, Ce, Yb); $ M_{3.45} $$ Si_{3} $$ Al_{2} $$ O_{12.76} $$ N_{0.95} $ (M = Y, Er); $ Y_{4} $$ Si_{3} $$ Al_{2} $$ O_{13.50} $N and $ Y_{4} $$ Si_{3.37} $$ Al_{1.50} $$ O_{13.50} $N. Heat treatments were performed on these glasses and the resulting crystalline products have been studied by X-ray diffraction (XRD). Differential Thermal Analysis (DTA) in combination with XRD analysis of $ Y_{3.45} $$ Si_{3} $$ Al_{2} $$ O_{12.76} $$ N_{0.95} $ and $ Ce_{3} $$ Si_{2} $$ Al_{2} $$ O_{12.15} $$ N_{0.90} $ parent glass-compositions was used to investigate crystal phase formation. Young's modulus (E), hardness (Hv and fracture toughness (KIC) of the glass-ceramics were measured. Glass-ceramics containing $ I_{w} $-phase as the only detectable crystalline phase have been produced from $ M_{3} $$ Si_{3} $$ Al_{2} $$ O_{12.15} $$ N_{0.90} $ and $ M_{3.45} $$ Si_{3} $$ Al_{2} $$ O_{12.76} $$ N_{0.95} $ (M = Y and Er) compositions. 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Diaz, A. |
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Diaz, A. ddc 670 misc Polymer misc Heat Treatment misc Thermal Stability misc Thermal Analysis misc Fracture Toughness Crystallisation of M-SiAlON glasses to $ I_{w} $-phase glass-ceramics: preparation and characterisation |
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670 VZ Crystallisation of M-SiAlON glasses to $ I_{w} $-phase glass-ceramics: preparation and characterisation Polymer Heat Treatment Thermal Stability Thermal Analysis Fracture Toughness |
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crystallisation of m-sialon glasses to $ i_{w} $-phase glass-ceramics: preparation and characterisation |
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Crystallisation of M-SiAlON glasses to $ I_{w} $-phase glass-ceramics: preparation and characterisation |
| abstract |
Abstract The crystallisation of M-SiAlON glasses (M = Y, Ln) is particularly sensitive to small variations in composition and heat treatment temperature. The formation of $ I_{w} $-phase in the YSiAlON system has been studied but little information concerning its nucleation, thermal stability, mechanical properties and extension into the lanthanide sialon series is available. In order to better understand the synthesis and to characterise more fully the $ I_{w} $-glass-ceramic materials, a series of glass compositions have been prepared and characterised. These include $ M_{3} $$ Si_{3} $$ Al_{2} $$ O_{12.15} $$ N_{0.90} $ (M = Y, Er, Ce, Yb); $ M_{3.45} $$ Si_{3} $$ Al_{2} $$ O_{12.76} $$ N_{0.95} $ (M = Y, Er); $ Y_{4} $$ Si_{3} $$ Al_{2} $$ O_{13.50} $N and $ Y_{4} $$ Si_{3.37} $$ Al_{1.50} $$ O_{13.50} $N. Heat treatments were performed on these glasses and the resulting crystalline products have been studied by X-ray diffraction (XRD). Differential Thermal Analysis (DTA) in combination with XRD analysis of $ Y_{3.45} $$ Si_{3} $$ Al_{2} $$ O_{12.76} $$ N_{0.95} $ and $ Ce_{3} $$ Si_{2} $$ Al_{2} $$ O_{12.15} $$ N_{0.90} $ parent glass-compositions was used to investigate crystal phase formation. Young's modulus (E), hardness (Hv and fracture toughness (KIC) of the glass-ceramics were measured. Glass-ceramics containing $ I_{w} $-phase as the only detectable crystalline phase have been produced from $ M_{3} $$ Si_{3} $$ Al_{2} $$ O_{12.15} $$ N_{0.90} $ and $ M_{3.45} $$ Si_{3} $$ Al_{2} $$ O_{12.76} $$ N_{0.95} $ (M = Y and Er) compositions. No equivalent phase was found in the Ce- and Yb-sialon compositions. © Kluwer Academic Publishers 2002 |
| abstractGer |
Abstract The crystallisation of M-SiAlON glasses (M = Y, Ln) is particularly sensitive to small variations in composition and heat treatment temperature. The formation of $ I_{w} $-phase in the YSiAlON system has been studied but little information concerning its nucleation, thermal stability, mechanical properties and extension into the lanthanide sialon series is available. In order to better understand the synthesis and to characterise more fully the $ I_{w} $-glass-ceramic materials, a series of glass compositions have been prepared and characterised. These include $ M_{3} $$ Si_{3} $$ Al_{2} $$ O_{12.15} $$ N_{0.90} $ (M = Y, Er, Ce, Yb); $ M_{3.45} $$ Si_{3} $$ Al_{2} $$ O_{12.76} $$ N_{0.95} $ (M = Y, Er); $ Y_{4} $$ Si_{3} $$ Al_{2} $$ O_{13.50} $N and $ Y_{4} $$ Si_{3.37} $$ Al_{1.50} $$ O_{13.50} $N. Heat treatments were performed on these glasses and the resulting crystalline products have been studied by X-ray diffraction (XRD). Differential Thermal Analysis (DTA) in combination with XRD analysis of $ Y_{3.45} $$ Si_{3} $$ Al_{2} $$ O_{12.76} $$ N_{0.95} $ and $ Ce_{3} $$ Si_{2} $$ Al_{2} $$ O_{12.15} $$ N_{0.90} $ parent glass-compositions was used to investigate crystal phase formation. Young's modulus (E), hardness (Hv and fracture toughness (KIC) of the glass-ceramics were measured. Glass-ceramics containing $ I_{w} $-phase as the only detectable crystalline phase have been produced from $ M_{3} $$ Si_{3} $$ Al_{2} $$ O_{12.15} $$ N_{0.90} $ and $ M_{3.45} $$ Si_{3} $$ Al_{2} $$ O_{12.76} $$ N_{0.95} $ (M = Y and Er) compositions. No equivalent phase was found in the Ce- and Yb-sialon compositions. © Kluwer Academic Publishers 2002 |
| abstract_unstemmed |
Abstract The crystallisation of M-SiAlON glasses (M = Y, Ln) is particularly sensitive to small variations in composition and heat treatment temperature. The formation of $ I_{w} $-phase in the YSiAlON system has been studied but little information concerning its nucleation, thermal stability, mechanical properties and extension into the lanthanide sialon series is available. In order to better understand the synthesis and to characterise more fully the $ I_{w} $-glass-ceramic materials, a series of glass compositions have been prepared and characterised. These include $ M_{3} $$ Si_{3} $$ Al_{2} $$ O_{12.15} $$ N_{0.90} $ (M = Y, Er, Ce, Yb); $ M_{3.45} $$ Si_{3} $$ Al_{2} $$ O_{12.76} $$ N_{0.95} $ (M = Y, Er); $ Y_{4} $$ Si_{3} $$ Al_{2} $$ O_{13.50} $N and $ Y_{4} $$ Si_{3.37} $$ Al_{1.50} $$ O_{13.50} $N. Heat treatments were performed on these glasses and the resulting crystalline products have been studied by X-ray diffraction (XRD). Differential Thermal Analysis (DTA) in combination with XRD analysis of $ Y_{3.45} $$ Si_{3} $$ Al_{2} $$ O_{12.76} $$ N_{0.95} $ and $ Ce_{3} $$ Si_{2} $$ Al_{2} $$ O_{12.15} $$ N_{0.90} $ parent glass-compositions was used to investigate crystal phase formation. Young's modulus (E), hardness (Hv and fracture toughness (KIC) of the glass-ceramics were measured. Glass-ceramics containing $ I_{w} $-phase as the only detectable crystalline phase have been produced from $ M_{3} $$ Si_{3} $$ Al_{2} $$ O_{12.15} $$ N_{0.90} $ and $ M_{3.45} $$ Si_{3} $$ Al_{2} $$ O_{12.76} $$ N_{0.95} $ (M = Y and Er) compositions. No equivalent phase was found in the Ce- and Yb-sialon compositions. © Kluwer Academic Publishers 2002 |
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The formation of $ I_{w} $-phase in the YSiAlON system has been studied but little information concerning its nucleation, thermal stability, mechanical properties and extension into the lanthanide sialon series is available. In order to better understand the synthesis and to characterise more fully the $ I_{w} $-glass-ceramic materials, a series of glass compositions have been prepared and characterised. These include $ M_{3} $$ Si_{3} $$ Al_{2} $$ O_{12.15} $$ N_{0.90} $ (M = Y, Er, Ce, Yb); $ M_{3.45} $$ Si_{3} $$ Al_{2} $$ O_{12.76} $$ N_{0.95} $ (M = Y, Er); $ Y_{4} $$ Si_{3} $$ Al_{2} $$ O_{13.50} $N and $ Y_{4} $$ Si_{3.37} $$ Al_{1.50} $$ O_{13.50} $N. Heat treatments were performed on these glasses and the resulting crystalline products have been studied by X-ray diffraction (XRD). Differential Thermal Analysis (DTA) in combination with XRD analysis of $ Y_{3.45} $$ Si_{3} $$ Al_{2} $$ O_{12.76} $$ N_{0.95} $ and $ Ce_{3} $$ Si_{2} $$ Al_{2} $$ O_{12.15} $$ N_{0.90} $ parent glass-compositions was used to investigate crystal phase formation. Young's modulus (E), hardness (Hv and fracture toughness (KIC) of the glass-ceramics were measured. Glass-ceramics containing $ I_{w} $-phase as the only detectable crystalline phase have been produced from $ M_{3} $$ Si_{3} $$ Al_{2} $$ O_{12.15} $$ N_{0.90} $ and $ M_{3.45} $$ Si_{3} $$ Al_{2} $$ O_{12.76} $$ N_{0.95} $ (M = Y and Er) compositions. No equivalent phase was found in the Ce- and Yb-sialon compositions.</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Polymer</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Heat Treatment</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Thermal Stability</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Thermal Analysis</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Fracture Toughness</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Hampshire, S.</subfield><subfield code="4">aut</subfield></datafield><datafield tag="773" ind1="0" ind2="8"><subfield code="i">Enthalten in</subfield><subfield code="t">Journal of materials science</subfield><subfield code="d">Kluwer Academic Publishers, 1966</subfield><subfield code="g">37(2002), 4 vom: Feb., Seite 723-730</subfield><subfield code="w">(DE-627)129546372</subfield><subfield code="w">(DE-600)218324-9</subfield><subfield code="w">(DE-576)014996774</subfield><subfield code="x">0022-2461</subfield><subfield code="7">nnns</subfield></datafield><datafield tag="773" ind1="1" ind2="8"><subfield code="g">volume:37</subfield><subfield code="g">year:2002</subfield><subfield code="g">number:4</subfield><subfield code="g">month:02</subfield><subfield code="g">pages:723-730</subfield></datafield><datafield tag="856" ind1="4" ind2="1"><subfield code="u">https://doi.org/10.1023/A:1013831612767</subfield><subfield code="z">lizenzpflichtig</subfield><subfield code="3">Volltext</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_USEFLAG_A</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">SYSFLAG_A</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_OLC</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">SSG-OLC-TEC</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_20</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_23</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_30</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_32</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_40</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_62</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_65</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_70</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2004</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2005</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2006</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2015</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2020</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4046</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4305</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4306</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4319</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4323</subfield></datafield><datafield tag="951" ind1=" " ind2=" "><subfield code="a">AR</subfield></datafield><datafield tag="952" ind1=" " ind2=" "><subfield code="d">37</subfield><subfield code="j">2002</subfield><subfield code="e">4</subfield><subfield code="c">02</subfield><subfield code="h">723-730</subfield></datafield></record></collection>
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