Preparation and characterization of polymer/inorganic nanoparticle composites through electron irradiation
Abstract In this paper, we report a new method to prepare the polymer/inorganic nanoparticle composites using electron irradiation-induced polymerization. The mixture of nanoparticles and MMA solution were co-irradiated by 1.6 MeV electron beam to a dose of 10, 20 and 30 kGy at a dose-rate of 60 kGy...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Wang, Z. G. [verfasserIn] |
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| Format: |
Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2006 |
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| Schlagwörter: |
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| Anmerkung: |
© Springer Science + Business Media, Inc. 2006 |
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| Übergeordnetes Werk: |
Enthalten in: Journal of materials science - Kluwer Academic Publishers, 1966, 41(2006), 7 vom: Apr., Seite 1973-1978 |
|---|---|
| Übergeordnetes Werk: |
volume:41 ; year:2006 ; number:7 ; month:04 ; pages:1973-1978 |
| Links: |
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| DOI / URN: |
10.1007/s10853-006-1120-6 |
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| Katalog-ID: |
OLC2046311604 |
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| 520 | |a Abstract In this paper, we report a new method to prepare the polymer/inorganic nanoparticle composites using electron irradiation-induced polymerization. The mixture of nanoparticles and MMA solution were co-irradiated by 1.6 MeV electron beam to a dose of 10, 20 and 30 kGy at a dose-rate of 60 kGy/h in air at room temperature. The products after irradiation were extracted using a soxhlet extractor with boiling xylene and investigated by X-ray diffraction (XRD), Fourier transmission infrared (FTIR), X-ray photoelectron spectroscopy (XPS), optical absorption spectra (OAP) and photoluminescence (PL). The FTIR and XPS results show that there exist some unextractable PMMA in the nanocomposites after extraction, indicating a strong interaction between the PMMA and nanoparticles. PL results show that new luminescence peaks appear at 415 and 420 nm for the nanocomposites of anatase and γ-$ Al_{2} $$ O_{3} $. | ||
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10.1007/s10853-006-1120-6 doi (DE-627)OLC2046311604 (DE-He213)s10853-006-1120-6-p DE-627 ger DE-627 rakwb eng 670 VZ Wang, Z. G. verfasserin aut Preparation and characterization of polymer/inorganic nanoparticle composites through electron irradiation 2006 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Springer Science + Business Media, Inc. 2006 Abstract In this paper, we report a new method to prepare the polymer/inorganic nanoparticle composites using electron irradiation-induced polymerization. The mixture of nanoparticles and MMA solution were co-irradiated by 1.6 MeV electron beam to a dose of 10, 20 and 30 kGy at a dose-rate of 60 kGy/h in air at room temperature. The products after irradiation were extracted using a soxhlet extractor with boiling xylene and investigated by X-ray diffraction (XRD), Fourier transmission infrared (FTIR), X-ray photoelectron spectroscopy (XPS), optical absorption spectra (OAP) and photoluminescence (PL). The FTIR and XPS results show that there exist some unextractable PMMA in the nanocomposites after extraction, indicating a strong interaction between the PMMA and nanoparticles. PL results show that new luminescence peaks appear at 415 and 420 nm for the nanocomposites of anatase and γ-$ Al_{2} $$ O_{3} $. PMMA Xylene Extractor Soxhlet Extractor Optical Absorption Spectrum Zu, X. T. aut Xiang, X. aut Lian, J. aut Wang, L. M. aut Enthalten in Journal of materials science Kluwer Academic Publishers, 1966 41(2006), 7 vom: Apr., Seite 1973-1978 (DE-627)129546372 (DE-600)218324-9 (DE-576)014996774 0022-2461 nnns volume:41 year:2006 number:7 month:04 pages:1973-1978 https://doi.org/10.1007/s10853-006-1120-6 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC GBV_ILN_20 GBV_ILN_21 GBV_ILN_23 GBV_ILN_30 GBV_ILN_32 GBV_ILN_40 GBV_ILN_62 GBV_ILN_65 GBV_ILN_70 GBV_ILN_100 GBV_ILN_602 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_4046 GBV_ILN_4305 GBV_ILN_4323 AR 41 2006 7 04 1973-1978 |
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10.1007/s10853-006-1120-6 doi (DE-627)OLC2046311604 (DE-He213)s10853-006-1120-6-p DE-627 ger DE-627 rakwb eng 670 VZ Wang, Z. G. verfasserin aut Preparation and characterization of polymer/inorganic nanoparticle composites through electron irradiation 2006 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Springer Science + Business Media, Inc. 2006 Abstract In this paper, we report a new method to prepare the polymer/inorganic nanoparticle composites using electron irradiation-induced polymerization. The mixture of nanoparticles and MMA solution were co-irradiated by 1.6 MeV electron beam to a dose of 10, 20 and 30 kGy at a dose-rate of 60 kGy/h in air at room temperature. The products after irradiation were extracted using a soxhlet extractor with boiling xylene and investigated by X-ray diffraction (XRD), Fourier transmission infrared (FTIR), X-ray photoelectron spectroscopy (XPS), optical absorption spectra (OAP) and photoluminescence (PL). The FTIR and XPS results show that there exist some unextractable PMMA in the nanocomposites after extraction, indicating a strong interaction between the PMMA and nanoparticles. PL results show that new luminescence peaks appear at 415 and 420 nm for the nanocomposites of anatase and γ-$ Al_{2} $$ O_{3} $. PMMA Xylene Extractor Soxhlet Extractor Optical Absorption Spectrum Zu, X. T. aut Xiang, X. aut Lian, J. aut Wang, L. M. aut Enthalten in Journal of materials science Kluwer Academic Publishers, 1966 41(2006), 7 vom: Apr., Seite 1973-1978 (DE-627)129546372 (DE-600)218324-9 (DE-576)014996774 0022-2461 nnns volume:41 year:2006 number:7 month:04 pages:1973-1978 https://doi.org/10.1007/s10853-006-1120-6 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC GBV_ILN_20 GBV_ILN_21 GBV_ILN_23 GBV_ILN_30 GBV_ILN_32 GBV_ILN_40 GBV_ILN_62 GBV_ILN_65 GBV_ILN_70 GBV_ILN_100 GBV_ILN_602 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_4046 GBV_ILN_4305 GBV_ILN_4323 AR 41 2006 7 04 1973-1978 |
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10.1007/s10853-006-1120-6 doi (DE-627)OLC2046311604 (DE-He213)s10853-006-1120-6-p DE-627 ger DE-627 rakwb eng 670 VZ Wang, Z. G. verfasserin aut Preparation and characterization of polymer/inorganic nanoparticle composites through electron irradiation 2006 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Springer Science + Business Media, Inc. 2006 Abstract In this paper, we report a new method to prepare the polymer/inorganic nanoparticle composites using electron irradiation-induced polymerization. The mixture of nanoparticles and MMA solution were co-irradiated by 1.6 MeV electron beam to a dose of 10, 20 and 30 kGy at a dose-rate of 60 kGy/h in air at room temperature. The products after irradiation were extracted using a soxhlet extractor with boiling xylene and investigated by X-ray diffraction (XRD), Fourier transmission infrared (FTIR), X-ray photoelectron spectroscopy (XPS), optical absorption spectra (OAP) and photoluminescence (PL). The FTIR and XPS results show that there exist some unextractable PMMA in the nanocomposites after extraction, indicating a strong interaction between the PMMA and nanoparticles. PL results show that new luminescence peaks appear at 415 and 420 nm for the nanocomposites of anatase and γ-$ Al_{2} $$ O_{3} $. PMMA Xylene Extractor Soxhlet Extractor Optical Absorption Spectrum Zu, X. T. aut Xiang, X. aut Lian, J. aut Wang, L. M. aut Enthalten in Journal of materials science Kluwer Academic Publishers, 1966 41(2006), 7 vom: Apr., Seite 1973-1978 (DE-627)129546372 (DE-600)218324-9 (DE-576)014996774 0022-2461 nnns volume:41 year:2006 number:7 month:04 pages:1973-1978 https://doi.org/10.1007/s10853-006-1120-6 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC GBV_ILN_20 GBV_ILN_21 GBV_ILN_23 GBV_ILN_30 GBV_ILN_32 GBV_ILN_40 GBV_ILN_62 GBV_ILN_65 GBV_ILN_70 GBV_ILN_100 GBV_ILN_602 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_4046 GBV_ILN_4305 GBV_ILN_4323 AR 41 2006 7 04 1973-1978 |
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10.1007/s10853-006-1120-6 doi (DE-627)OLC2046311604 (DE-He213)s10853-006-1120-6-p DE-627 ger DE-627 rakwb eng 670 VZ Wang, Z. G. verfasserin aut Preparation and characterization of polymer/inorganic nanoparticle composites through electron irradiation 2006 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Springer Science + Business Media, Inc. 2006 Abstract In this paper, we report a new method to prepare the polymer/inorganic nanoparticle composites using electron irradiation-induced polymerization. The mixture of nanoparticles and MMA solution were co-irradiated by 1.6 MeV electron beam to a dose of 10, 20 and 30 kGy at a dose-rate of 60 kGy/h in air at room temperature. The products after irradiation were extracted using a soxhlet extractor with boiling xylene and investigated by X-ray diffraction (XRD), Fourier transmission infrared (FTIR), X-ray photoelectron spectroscopy (XPS), optical absorption spectra (OAP) and photoluminescence (PL). The FTIR and XPS results show that there exist some unextractable PMMA in the nanocomposites after extraction, indicating a strong interaction between the PMMA and nanoparticles. PL results show that new luminescence peaks appear at 415 and 420 nm for the nanocomposites of anatase and γ-$ Al_{2} $$ O_{3} $. PMMA Xylene Extractor Soxhlet Extractor Optical Absorption Spectrum Zu, X. T. aut Xiang, X. aut Lian, J. aut Wang, L. M. aut Enthalten in Journal of materials science Kluwer Academic Publishers, 1966 41(2006), 7 vom: Apr., Seite 1973-1978 (DE-627)129546372 (DE-600)218324-9 (DE-576)014996774 0022-2461 nnns volume:41 year:2006 number:7 month:04 pages:1973-1978 https://doi.org/10.1007/s10853-006-1120-6 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC GBV_ILN_20 GBV_ILN_21 GBV_ILN_23 GBV_ILN_30 GBV_ILN_32 GBV_ILN_40 GBV_ILN_62 GBV_ILN_65 GBV_ILN_70 GBV_ILN_100 GBV_ILN_602 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_4046 GBV_ILN_4305 GBV_ILN_4323 AR 41 2006 7 04 1973-1978 |
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10.1007/s10853-006-1120-6 doi (DE-627)OLC2046311604 (DE-He213)s10853-006-1120-6-p DE-627 ger DE-627 rakwb eng 670 VZ Wang, Z. G. verfasserin aut Preparation and characterization of polymer/inorganic nanoparticle composites through electron irradiation 2006 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Springer Science + Business Media, Inc. 2006 Abstract In this paper, we report a new method to prepare the polymer/inorganic nanoparticle composites using electron irradiation-induced polymerization. The mixture of nanoparticles and MMA solution were co-irradiated by 1.6 MeV electron beam to a dose of 10, 20 and 30 kGy at a dose-rate of 60 kGy/h in air at room temperature. The products after irradiation were extracted using a soxhlet extractor with boiling xylene and investigated by X-ray diffraction (XRD), Fourier transmission infrared (FTIR), X-ray photoelectron spectroscopy (XPS), optical absorption spectra (OAP) and photoluminescence (PL). The FTIR and XPS results show that there exist some unextractable PMMA in the nanocomposites after extraction, indicating a strong interaction between the PMMA and nanoparticles. PL results show that new luminescence peaks appear at 415 and 420 nm for the nanocomposites of anatase and γ-$ Al_{2} $$ O_{3} $. PMMA Xylene Extractor Soxhlet Extractor Optical Absorption Spectrum Zu, X. T. aut Xiang, X. aut Lian, J. aut Wang, L. M. aut Enthalten in Journal of materials science Kluwer Academic Publishers, 1966 41(2006), 7 vom: Apr., Seite 1973-1978 (DE-627)129546372 (DE-600)218324-9 (DE-576)014996774 0022-2461 nnns volume:41 year:2006 number:7 month:04 pages:1973-1978 https://doi.org/10.1007/s10853-006-1120-6 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC GBV_ILN_20 GBV_ILN_21 GBV_ILN_23 GBV_ILN_30 GBV_ILN_32 GBV_ILN_40 GBV_ILN_62 GBV_ILN_65 GBV_ILN_70 GBV_ILN_100 GBV_ILN_602 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_4046 GBV_ILN_4305 GBV_ILN_4323 AR 41 2006 7 04 1973-1978 |
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Preparation and characterization of polymer/inorganic nanoparticle composites through electron irradiation |
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Preparation and characterization of polymer/inorganic nanoparticle composites through electron irradiation |
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Wang, Z. G. Zu, X. T. Xiang, X. Lian, J. Wang, L. M. |
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preparation and characterization of polymer/inorganic nanoparticle composites through electron irradiation |
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Preparation and characterization of polymer/inorganic nanoparticle composites through electron irradiation |
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Abstract In this paper, we report a new method to prepare the polymer/inorganic nanoparticle composites using electron irradiation-induced polymerization. The mixture of nanoparticles and MMA solution were co-irradiated by 1.6 MeV electron beam to a dose of 10, 20 and 30 kGy at a dose-rate of 60 kGy/h in air at room temperature. The products after irradiation were extracted using a soxhlet extractor with boiling xylene and investigated by X-ray diffraction (XRD), Fourier transmission infrared (FTIR), X-ray photoelectron spectroscopy (XPS), optical absorption spectra (OAP) and photoluminescence (PL). The FTIR and XPS results show that there exist some unextractable PMMA in the nanocomposites after extraction, indicating a strong interaction between the PMMA and nanoparticles. PL results show that new luminescence peaks appear at 415 and 420 nm for the nanocomposites of anatase and γ-$ Al_{2} $$ O_{3} $. © Springer Science + Business Media, Inc. 2006 |
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Abstract In this paper, we report a new method to prepare the polymer/inorganic nanoparticle composites using electron irradiation-induced polymerization. The mixture of nanoparticles and MMA solution were co-irradiated by 1.6 MeV electron beam to a dose of 10, 20 and 30 kGy at a dose-rate of 60 kGy/h in air at room temperature. The products after irradiation were extracted using a soxhlet extractor with boiling xylene and investigated by X-ray diffraction (XRD), Fourier transmission infrared (FTIR), X-ray photoelectron spectroscopy (XPS), optical absorption spectra (OAP) and photoluminescence (PL). The FTIR and XPS results show that there exist some unextractable PMMA in the nanocomposites after extraction, indicating a strong interaction between the PMMA and nanoparticles. PL results show that new luminescence peaks appear at 415 and 420 nm for the nanocomposites of anatase and γ-$ Al_{2} $$ O_{3} $. © Springer Science + Business Media, Inc. 2006 |
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Abstract In this paper, we report a new method to prepare the polymer/inorganic nanoparticle composites using electron irradiation-induced polymerization. The mixture of nanoparticles and MMA solution were co-irradiated by 1.6 MeV electron beam to a dose of 10, 20 and 30 kGy at a dose-rate of 60 kGy/h in air at room temperature. The products after irradiation were extracted using a soxhlet extractor with boiling xylene and investigated by X-ray diffraction (XRD), Fourier transmission infrared (FTIR), X-ray photoelectron spectroscopy (XPS), optical absorption spectra (OAP) and photoluminescence (PL). The FTIR and XPS results show that there exist some unextractable PMMA in the nanocomposites after extraction, indicating a strong interaction between the PMMA and nanoparticles. PL results show that new luminescence peaks appear at 415 and 420 nm for the nanocomposites of anatase and γ-$ Al_{2} $$ O_{3} $. © Springer Science + Business Media, Inc. 2006 |
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Preparation and characterization of polymer/inorganic nanoparticle composites through electron irradiation |
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