Synthesis and characterization of dense ultra-high temperature thermal protection materials produced by field activation through spark plasma sintering (SPS): I. Hafnium Diboride

Abstract The consolidation of $ HfB_{2} $ by sintering and reactive sintering using the field-activated process of the spark plasma sintering (SPS) method was investigated. Sintering of the diboride at 1900°C under a pressure of 95 MPa did not result in dense materials. In contrast, reactive sinteri...
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Autor*in:	Anselmi-Tamburini, U. [verfasserIn] Kodera, Y. Gasch, M. Unuvar, C. Munir, Z. A. Ohyanagi, M. Johnson, S. M.

Format:	Artikel
Sprache:	Englisch

Erschienen:	2006

Schlagwörter:	Polymer Significant Role Reaction Mechanism Hafnium Spark Plasma Sinter

Anmerkung:	© Springer Science + Business Media, Inc. 2006

Übergeordnetes Werk:	Enthalten in: Journal of materials science - Kluwer Academic Publishers, 1966, 41(2006), 10 vom: 17. Jan., Seite 3097-3104
Übergeordnetes Werk:	volume:41 ; year:2006 ; number:10 ; day:17 ; month:01 ; pages:3097-3104

Links:	Volltext

DOI / URN:	10.1007/s10853-005-2457-y

Katalog-ID:	OLC2046313372

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520			\|a Abstract The consolidation of $ HfB_{2} $ by sintering and reactive sintering using the field-activated process of the spark plasma sintering (SPS) method was investigated. Sintering of the diboride at 1900°C under a pressure of 95 MPa did not result in dense materials. In contrast, reactive sintering at 1700°C produced about 98% dense $ HfB_{2} $ with a 10 min hold at temperature. In contrast to previous observations, the reaction between the elements and the consolidation of the resulting diboride did not coincide, the latter occurring at a much higher temperature. The reaction mechanism between B and Hf during reactive sintering was investigated. Measured rates of growth of the $ HfB_{2} $ were found to be in agreement with calculated values from diffusion couple experiments, suggesting that the current did not play a significant role in the reactivity.
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allfields	10.1007/s10853-005-2457-y doi (DE-627)OLC2046313372 (DE-He213)s10853-005-2457-y-p DE-627 ger DE-627 rakwb eng 670 VZ Anselmi-Tamburini, U. verfasserin aut Synthesis and characterization of dense ultra-high temperature thermal protection materials produced by field activation through spark plasma sintering (SPS): I. Hafnium Diboride 2006 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Springer Science + Business Media, Inc. 2006 Abstract The consolidation of $ HfB_{2} $ by sintering and reactive sintering using the field-activated process of the spark plasma sintering (SPS) method was investigated. Sintering of the diboride at 1900°C under a pressure of 95 MPa did not result in dense materials. In contrast, reactive sintering at 1700°C produced about 98% dense $ HfB_{2} $ with a 10 min hold at temperature. In contrast to previous observations, the reaction between the elements and the consolidation of the resulting diboride did not coincide, the latter occurring at a much higher temperature. The reaction mechanism between B and Hf during reactive sintering was investigated. Measured rates of growth of the $ HfB_{2} $ were found to be in agreement with calculated values from diffusion couple experiments, suggesting that the current did not play a significant role in the reactivity. Polymer Significant Role Reaction Mechanism Hafnium Spark Plasma Sinter Kodera, Y. aut Gasch, M. aut Unuvar, C. aut Munir, Z. A. aut Ohyanagi, M. aut Johnson, S. M. aut Enthalten in Journal of materials science Kluwer Academic Publishers, 1966 41(2006), 10 vom: 17. Jan., Seite 3097-3104 (DE-627)129546372 (DE-600)218324-9 (DE-576)014996774 0022-2461 nnns volume:41 year:2006 number:10 day:17 month:01 pages:3097-3104 https://doi.org/10.1007/s10853-005-2457-y lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC GBV_ILN_20 GBV_ILN_21 GBV_ILN_23 GBV_ILN_30 GBV_ILN_32 GBV_ILN_40 GBV_ILN_62 GBV_ILN_65 GBV_ILN_70 GBV_ILN_100 GBV_ILN_602 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_4046 GBV_ILN_4305 GBV_ILN_4323 AR 41 2006 10 17 01 3097-3104
spelling	10.1007/s10853-005-2457-y doi (DE-627)OLC2046313372 (DE-He213)s10853-005-2457-y-p DE-627 ger DE-627 rakwb eng 670 VZ Anselmi-Tamburini, U. verfasserin aut Synthesis and characterization of dense ultra-high temperature thermal protection materials produced by field activation through spark plasma sintering (SPS): I. Hafnium Diboride 2006 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Springer Science + Business Media, Inc. 2006 Abstract The consolidation of $ HfB_{2} $ by sintering and reactive sintering using the field-activated process of the spark plasma sintering (SPS) method was investigated. Sintering of the diboride at 1900°C under a pressure of 95 MPa did not result in dense materials. In contrast, reactive sintering at 1700°C produced about 98% dense $ HfB_{2} $ with a 10 min hold at temperature. In contrast to previous observations, the reaction between the elements and the consolidation of the resulting diboride did not coincide, the latter occurring at a much higher temperature. The reaction mechanism between B and Hf during reactive sintering was investigated. Measured rates of growth of the $ HfB_{2} $ were found to be in agreement with calculated values from diffusion couple experiments, suggesting that the current did not play a significant role in the reactivity. Polymer Significant Role Reaction Mechanism Hafnium Spark Plasma Sinter Kodera, Y. aut Gasch, M. aut Unuvar, C. aut Munir, Z. A. aut Ohyanagi, M. aut Johnson, S. M. aut Enthalten in Journal of materials science Kluwer Academic Publishers, 1966 41(2006), 10 vom: 17. Jan., Seite 3097-3104 (DE-627)129546372 (DE-600)218324-9 (DE-576)014996774 0022-2461 nnns volume:41 year:2006 number:10 day:17 month:01 pages:3097-3104 https://doi.org/10.1007/s10853-005-2457-y lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC GBV_ILN_20 GBV_ILN_21 GBV_ILN_23 GBV_ILN_30 GBV_ILN_32 GBV_ILN_40 GBV_ILN_62 GBV_ILN_65 GBV_ILN_70 GBV_ILN_100 GBV_ILN_602 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_4046 GBV_ILN_4305 GBV_ILN_4323 AR 41 2006 10 17 01 3097-3104
allfields_unstemmed	10.1007/s10853-005-2457-y doi (DE-627)OLC2046313372 (DE-He213)s10853-005-2457-y-p DE-627 ger DE-627 rakwb eng 670 VZ Anselmi-Tamburini, U. verfasserin aut Synthesis and characterization of dense ultra-high temperature thermal protection materials produced by field activation through spark plasma sintering (SPS): I. Hafnium Diboride 2006 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Springer Science + Business Media, Inc. 2006 Abstract The consolidation of $ HfB_{2} $ by sintering and reactive sintering using the field-activated process of the spark plasma sintering (SPS) method was investigated. Sintering of the diboride at 1900°C under a pressure of 95 MPa did not result in dense materials. In contrast, reactive sintering at 1700°C produced about 98% dense $ HfB_{2} $ with a 10 min hold at temperature. In contrast to previous observations, the reaction between the elements and the consolidation of the resulting diboride did not coincide, the latter occurring at a much higher temperature. The reaction mechanism between B and Hf during reactive sintering was investigated. Measured rates of growth of the $ HfB_{2} $ were found to be in agreement with calculated values from diffusion couple experiments, suggesting that the current did not play a significant role in the reactivity. Polymer Significant Role Reaction Mechanism Hafnium Spark Plasma Sinter Kodera, Y. aut Gasch, M. aut Unuvar, C. aut Munir, Z. A. aut Ohyanagi, M. aut Johnson, S. M. aut Enthalten in Journal of materials science Kluwer Academic Publishers, 1966 41(2006), 10 vom: 17. Jan., Seite 3097-3104 (DE-627)129546372 (DE-600)218324-9 (DE-576)014996774 0022-2461 nnns volume:41 year:2006 number:10 day:17 month:01 pages:3097-3104 https://doi.org/10.1007/s10853-005-2457-y lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC GBV_ILN_20 GBV_ILN_21 GBV_ILN_23 GBV_ILN_30 GBV_ILN_32 GBV_ILN_40 GBV_ILN_62 GBV_ILN_65 GBV_ILN_70 GBV_ILN_100 GBV_ILN_602 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_4046 GBV_ILN_4305 GBV_ILN_4323 AR 41 2006 10 17 01 3097-3104
allfieldsGer	10.1007/s10853-005-2457-y doi (DE-627)OLC2046313372 (DE-He213)s10853-005-2457-y-p DE-627 ger DE-627 rakwb eng 670 VZ Anselmi-Tamburini, U. verfasserin aut Synthesis and characterization of dense ultra-high temperature thermal protection materials produced by field activation through spark plasma sintering (SPS): I. Hafnium Diboride 2006 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Springer Science + Business Media, Inc. 2006 Abstract The consolidation of $ HfB_{2} $ by sintering and reactive sintering using the field-activated process of the spark plasma sintering (SPS) method was investigated. Sintering of the diboride at 1900°C under a pressure of 95 MPa did not result in dense materials. In contrast, reactive sintering at 1700°C produced about 98% dense $ HfB_{2} $ with a 10 min hold at temperature. In contrast to previous observations, the reaction between the elements and the consolidation of the resulting diboride did not coincide, the latter occurring at a much higher temperature. The reaction mechanism between B and Hf during reactive sintering was investigated. Measured rates of growth of the $ HfB_{2} $ were found to be in agreement with calculated values from diffusion couple experiments, suggesting that the current did not play a significant role in the reactivity. Polymer Significant Role Reaction Mechanism Hafnium Spark Plasma Sinter Kodera, Y. aut Gasch, M. aut Unuvar, C. aut Munir, Z. A. aut Ohyanagi, M. aut Johnson, S. M. aut Enthalten in Journal of materials science Kluwer Academic Publishers, 1966 41(2006), 10 vom: 17. Jan., Seite 3097-3104 (DE-627)129546372 (DE-600)218324-9 (DE-576)014996774 0022-2461 nnns volume:41 year:2006 number:10 day:17 month:01 pages:3097-3104 https://doi.org/10.1007/s10853-005-2457-y lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC GBV_ILN_20 GBV_ILN_21 GBV_ILN_23 GBV_ILN_30 GBV_ILN_32 GBV_ILN_40 GBV_ILN_62 GBV_ILN_65 GBV_ILN_70 GBV_ILN_100 GBV_ILN_602 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_4046 GBV_ILN_4305 GBV_ILN_4323 AR 41 2006 10 17 01 3097-3104
allfieldsSound	10.1007/s10853-005-2457-y doi (DE-627)OLC2046313372 (DE-He213)s10853-005-2457-y-p DE-627 ger DE-627 rakwb eng 670 VZ Anselmi-Tamburini, U. verfasserin aut Synthesis and characterization of dense ultra-high temperature thermal protection materials produced by field activation through spark plasma sintering (SPS): I. Hafnium Diboride 2006 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Springer Science + Business Media, Inc. 2006 Abstract The consolidation of $ HfB_{2} $ by sintering and reactive sintering using the field-activated process of the spark plasma sintering (SPS) method was investigated. Sintering of the diboride at 1900°C under a pressure of 95 MPa did not result in dense materials. In contrast, reactive sintering at 1700°C produced about 98% dense $ HfB_{2} $ with a 10 min hold at temperature. In contrast to previous observations, the reaction between the elements and the consolidation of the resulting diboride did not coincide, the latter occurring at a much higher temperature. The reaction mechanism between B and Hf during reactive sintering was investigated. Measured rates of growth of the $ HfB_{2} $ were found to be in agreement with calculated values from diffusion couple experiments, suggesting that the current did not play a significant role in the reactivity. Polymer Significant Role Reaction Mechanism Hafnium Spark Plasma Sinter Kodera, Y. aut Gasch, M. aut Unuvar, C. aut Munir, Z. A. aut Ohyanagi, M. aut Johnson, S. M. aut Enthalten in Journal of materials science Kluwer Academic Publishers, 1966 41(2006), 10 vom: 17. Jan., Seite 3097-3104 (DE-627)129546372 (DE-600)218324-9 (DE-576)014996774 0022-2461 nnns volume:41 year:2006 number:10 day:17 month:01 pages:3097-3104 https://doi.org/10.1007/s10853-005-2457-y lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC GBV_ILN_20 GBV_ILN_21 GBV_ILN_23 GBV_ILN_30 GBV_ILN_32 GBV_ILN_40 GBV_ILN_62 GBV_ILN_65 GBV_ILN_70 GBV_ILN_100 GBV_ILN_602 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_4046 GBV_ILN_4305 GBV_ILN_4323 AR 41 2006 10 17 01 3097-3104
language	English
source	Enthalten in Journal of materials science 41(2006), 10 vom: 17. Jan., Seite 3097-3104 volume:41 year:2006 number:10 day:17 month:01 pages:3097-3104
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author	Anselmi-Tamburini, U.
spellingShingle	Anselmi-Tamburini, U. ddc 670 misc Polymer misc Significant Role misc Reaction Mechanism misc Hafnium misc Spark Plasma Sinter Synthesis and characterization of dense ultra-high temperature thermal protection materials produced by field activation through spark plasma sintering (SPS): I. Hafnium Diboride
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topic_title	670 VZ Synthesis and characterization of dense ultra-high temperature thermal protection materials produced by field activation through spark plasma sintering (SPS): I. Hafnium Diboride Polymer Significant Role Reaction Mechanism Hafnium Spark Plasma Sinter
topic	ddc 670 misc Polymer misc Significant Role misc Reaction Mechanism misc Hafnium misc Spark Plasma Sinter
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title	Synthesis and characterization of dense ultra-high temperature thermal protection materials produced by field activation through spark plasma sintering (SPS): I. Hafnium Diboride
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title_full	Synthesis and characterization of dense ultra-high temperature thermal protection materials produced by field activation through spark plasma sintering (SPS): I. Hafnium Diboride
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title_sort	synthesis and characterization of dense ultra-high temperature thermal protection materials produced by field activation through spark plasma sintering (sps): i. hafnium diboride
title_auth	Synthesis and characterization of dense ultra-high temperature thermal protection materials produced by field activation through spark plasma sintering (SPS): I. Hafnium Diboride
abstract	Abstract The consolidation of $ HfB_{2} $ by sintering and reactive sintering using the field-activated process of the spark plasma sintering (SPS) method was investigated. Sintering of the diboride at 1900°C under a pressure of 95 MPa did not result in dense materials. In contrast, reactive sintering at 1700°C produced about 98% dense $ HfB_{2} $ with a 10 min hold at temperature. In contrast to previous observations, the reaction between the elements and the consolidation of the resulting diboride did not coincide, the latter occurring at a much higher temperature. The reaction mechanism between B and Hf during reactive sintering was investigated. Measured rates of growth of the $ HfB_{2} $ were found to be in agreement with calculated values from diffusion couple experiments, suggesting that the current did not play a significant role in the reactivity. © Springer Science + Business Media, Inc. 2006
abstractGer	Abstract The consolidation of $ HfB_{2} $ by sintering and reactive sintering using the field-activated process of the spark plasma sintering (SPS) method was investigated. Sintering of the diboride at 1900°C under a pressure of 95 MPa did not result in dense materials. In contrast, reactive sintering at 1700°C produced about 98% dense $ HfB_{2} $ with a 10 min hold at temperature. In contrast to previous observations, the reaction between the elements and the consolidation of the resulting diboride did not coincide, the latter occurring at a much higher temperature. The reaction mechanism between B and Hf during reactive sintering was investigated. Measured rates of growth of the $ HfB_{2} $ were found to be in agreement with calculated values from diffusion couple experiments, suggesting that the current did not play a significant role in the reactivity. © Springer Science + Business Media, Inc. 2006
abstract_unstemmed	Abstract The consolidation of $ HfB_{2} $ by sintering and reactive sintering using the field-activated process of the spark plasma sintering (SPS) method was investigated. Sintering of the diboride at 1900°C under a pressure of 95 MPa did not result in dense materials. In contrast, reactive sintering at 1700°C produced about 98% dense $ HfB_{2} $ with a 10 min hold at temperature. In contrast to previous observations, the reaction between the elements and the consolidation of the resulting diboride did not coincide, the latter occurring at a much higher temperature. The reaction mechanism between B and Hf during reactive sintering was investigated. Measured rates of growth of the $ HfB_{2} $ were found to be in agreement with calculated values from diffusion couple experiments, suggesting that the current did not play a significant role in the reactivity. © Springer Science + Business Media, Inc. 2006
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container_issue	10
title_short	Synthesis and characterization of dense ultra-high temperature thermal protection materials produced by field activation through spark plasma sintering (SPS): I. Hafnium Diboride
url	https://doi.org/10.1007/s10853-005-2457-y
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