Preparation and characterization of nanosized bismuth doped tin dioxide powders with a novel post treatment process
Abstract Bismuth-doped tin dioxide (BTO) nanopowders were prepared by wet chemical co-precipitation method using tin tetrachloride ($ SnCl_{4} $) and bismuth nitrate (Bi($ NO_{3} $)3) as raw materials. Effects of calcination temperature and post treatment methods on particle size and crystalline pha...
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Gespeichert in:
| Autor*in: |
He, Qiuxing [verfasserIn] |
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| Format: |
Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2007 |
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| Schlagwörter: |
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| Anmerkung: |
© Springer Science+Business Media, LLC 2007 |
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| Übergeordnetes Werk: |
Enthalten in: Journal of materials science - Kluwer Academic Publishers-Plenum Publishers, 1966, 42(2007), 19 vom: 01. Okt., Seite 8292-8297 |
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| Übergeordnetes Werk: |
volume:42 ; year:2007 ; number:19 ; day:01 ; month:10 ; pages:8292-8297 |
| Links: |
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| DOI / URN: |
10.1007/s10853-007-1509-x |
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| Katalog-ID: |
OLC2046331613 |
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| 245 | 1 | 0 | |a Preparation and characterization of nanosized bismuth doped tin dioxide powders with a novel post treatment process |
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| 520 | |a Abstract Bismuth-doped tin dioxide (BTO) nanopowders were prepared by wet chemical co-precipitation method using tin tetrachloride ($ SnCl_{4} $) and bismuth nitrate (Bi($ NO_{3} $)3) as raw materials. Effects of calcination temperature and post treatment methods on particle size and crystalline phase transition of bismuth tin precursor (BTP) were studied by X-ray diffraction (XRD), transmission electron microscopy (TEM), thermogravimetric-differential scanning calorimetric instrument (TG-DSC) and X-ray photoelectron spectroscopy (XPS). The optimal calcination temperature of BTP was found to be about 873 K. A novel post treatment process with polyacrylamide (PAM) in the preparation of nanometerials was presented for the first time. Experimental results showed that nonionic PAM is a highly effective additive, which not only speeds up the filtration of precursor, but also effectively reduces the formation of hard agglomerates. The average size of BTO nanopowders prepared using nonionic PAM as a filtration aid and disperser is smaller than 10 nm. We believe this post treatment method will come into wide use for preparation of many nanosized materials. | ||
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10.1007/s10853-007-1509-x doi (DE-627)OLC2046331613 (DE-He213)s10853-007-1509-x-p DE-627 ger DE-627 rakwb eng 670 VZ He, Qiuxing verfasserin aut Preparation and characterization of nanosized bismuth doped tin dioxide powders with a novel post treatment process 2007 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Springer Science+Business Media, LLC 2007 Abstract Bismuth-doped tin dioxide (BTO) nanopowders were prepared by wet chemical co-precipitation method using tin tetrachloride ($ SnCl_{4} $) and bismuth nitrate (Bi($ NO_{3} $)3) as raw materials. Effects of calcination temperature and post treatment methods on particle size and crystalline phase transition of bismuth tin precursor (BTP) were studied by X-ray diffraction (XRD), transmission electron microscopy (TEM), thermogravimetric-differential scanning calorimetric instrument (TG-DSC) and X-ray photoelectron spectroscopy (XPS). The optimal calcination temperature of BTP was found to be about 873 K. A novel post treatment process with polyacrylamide (PAM) in the preparation of nanometerials was presented for the first time. Experimental results showed that nonionic PAM is a highly effective additive, which not only speeds up the filtration of precursor, but also effectively reduces the formation of hard agglomerates. The average size of BTO nanopowders prepared using nonionic PAM as a filtration aid and disperser is smaller than 10 nm. We believe this post treatment method will come into wide use for preparation of many nanosized materials. SnO2 Calcination Temperature Bi2O3 Post Treatment Process Optimal Calcination Temperature Tu, Weiping aut Hu, Jianqing aut Enthalten in Journal of materials science Kluwer Academic Publishers-Plenum Publishers, 1966 42(2007), 19 vom: 01. Okt., Seite 8292-8297 (DE-627)129546372 (DE-600)218324-9 (DE-576)014996774 0022-2461 nnns volume:42 year:2007 number:19 day:01 month:10 pages:8292-8297 https://doi.org/10.1007/s10853-007-1509-x lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC GBV_ILN_20 GBV_ILN_21 GBV_ILN_23 GBV_ILN_30 GBV_ILN_32 GBV_ILN_40 GBV_ILN_62 GBV_ILN_65 GBV_ILN_70 GBV_ILN_100 GBV_ILN_602 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_4046 GBV_ILN_4305 GBV_ILN_4323 AR 42 2007 19 01 10 8292-8297 |
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10.1007/s10853-007-1509-x doi (DE-627)OLC2046331613 (DE-He213)s10853-007-1509-x-p DE-627 ger DE-627 rakwb eng 670 VZ He, Qiuxing verfasserin aut Preparation and characterization of nanosized bismuth doped tin dioxide powders with a novel post treatment process 2007 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Springer Science+Business Media, LLC 2007 Abstract Bismuth-doped tin dioxide (BTO) nanopowders were prepared by wet chemical co-precipitation method using tin tetrachloride ($ SnCl_{4} $) and bismuth nitrate (Bi($ NO_{3} $)3) as raw materials. Effects of calcination temperature and post treatment methods on particle size and crystalline phase transition of bismuth tin precursor (BTP) were studied by X-ray diffraction (XRD), transmission electron microscopy (TEM), thermogravimetric-differential scanning calorimetric instrument (TG-DSC) and X-ray photoelectron spectroscopy (XPS). The optimal calcination temperature of BTP was found to be about 873 K. A novel post treatment process with polyacrylamide (PAM) in the preparation of nanometerials was presented for the first time. Experimental results showed that nonionic PAM is a highly effective additive, which not only speeds up the filtration of precursor, but also effectively reduces the formation of hard agglomerates. The average size of BTO nanopowders prepared using nonionic PAM as a filtration aid and disperser is smaller than 10 nm. We believe this post treatment method will come into wide use for preparation of many nanosized materials. SnO2 Calcination Temperature Bi2O3 Post Treatment Process Optimal Calcination Temperature Tu, Weiping aut Hu, Jianqing aut Enthalten in Journal of materials science Kluwer Academic Publishers-Plenum Publishers, 1966 42(2007), 19 vom: 01. Okt., Seite 8292-8297 (DE-627)129546372 (DE-600)218324-9 (DE-576)014996774 0022-2461 nnns volume:42 year:2007 number:19 day:01 month:10 pages:8292-8297 https://doi.org/10.1007/s10853-007-1509-x lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC GBV_ILN_20 GBV_ILN_21 GBV_ILN_23 GBV_ILN_30 GBV_ILN_32 GBV_ILN_40 GBV_ILN_62 GBV_ILN_65 GBV_ILN_70 GBV_ILN_100 GBV_ILN_602 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_4046 GBV_ILN_4305 GBV_ILN_4323 AR 42 2007 19 01 10 8292-8297 |
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10.1007/s10853-007-1509-x doi (DE-627)OLC2046331613 (DE-He213)s10853-007-1509-x-p DE-627 ger DE-627 rakwb eng 670 VZ He, Qiuxing verfasserin aut Preparation and characterization of nanosized bismuth doped tin dioxide powders with a novel post treatment process 2007 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Springer Science+Business Media, LLC 2007 Abstract Bismuth-doped tin dioxide (BTO) nanopowders were prepared by wet chemical co-precipitation method using tin tetrachloride ($ SnCl_{4} $) and bismuth nitrate (Bi($ NO_{3} $)3) as raw materials. Effects of calcination temperature and post treatment methods on particle size and crystalline phase transition of bismuth tin precursor (BTP) were studied by X-ray diffraction (XRD), transmission electron microscopy (TEM), thermogravimetric-differential scanning calorimetric instrument (TG-DSC) and X-ray photoelectron spectroscopy (XPS). The optimal calcination temperature of BTP was found to be about 873 K. A novel post treatment process with polyacrylamide (PAM) in the preparation of nanometerials was presented for the first time. Experimental results showed that nonionic PAM is a highly effective additive, which not only speeds up the filtration of precursor, but also effectively reduces the formation of hard agglomerates. The average size of BTO nanopowders prepared using nonionic PAM as a filtration aid and disperser is smaller than 10 nm. We believe this post treatment method will come into wide use for preparation of many nanosized materials. SnO2 Calcination Temperature Bi2O3 Post Treatment Process Optimal Calcination Temperature Tu, Weiping aut Hu, Jianqing aut Enthalten in Journal of materials science Kluwer Academic Publishers-Plenum Publishers, 1966 42(2007), 19 vom: 01. Okt., Seite 8292-8297 (DE-627)129546372 (DE-600)218324-9 (DE-576)014996774 0022-2461 nnns volume:42 year:2007 number:19 day:01 month:10 pages:8292-8297 https://doi.org/10.1007/s10853-007-1509-x lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC GBV_ILN_20 GBV_ILN_21 GBV_ILN_23 GBV_ILN_30 GBV_ILN_32 GBV_ILN_40 GBV_ILN_62 GBV_ILN_65 GBV_ILN_70 GBV_ILN_100 GBV_ILN_602 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_4046 GBV_ILN_4305 GBV_ILN_4323 AR 42 2007 19 01 10 8292-8297 |
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10.1007/s10853-007-1509-x doi (DE-627)OLC2046331613 (DE-He213)s10853-007-1509-x-p DE-627 ger DE-627 rakwb eng 670 VZ He, Qiuxing verfasserin aut Preparation and characterization of nanosized bismuth doped tin dioxide powders with a novel post treatment process 2007 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Springer Science+Business Media, LLC 2007 Abstract Bismuth-doped tin dioxide (BTO) nanopowders were prepared by wet chemical co-precipitation method using tin tetrachloride ($ SnCl_{4} $) and bismuth nitrate (Bi($ NO_{3} $)3) as raw materials. Effects of calcination temperature and post treatment methods on particle size and crystalline phase transition of bismuth tin precursor (BTP) were studied by X-ray diffraction (XRD), transmission electron microscopy (TEM), thermogravimetric-differential scanning calorimetric instrument (TG-DSC) and X-ray photoelectron spectroscopy (XPS). The optimal calcination temperature of BTP was found to be about 873 K. A novel post treatment process with polyacrylamide (PAM) in the preparation of nanometerials was presented for the first time. Experimental results showed that nonionic PAM is a highly effective additive, which not only speeds up the filtration of precursor, but also effectively reduces the formation of hard agglomerates. The average size of BTO nanopowders prepared using nonionic PAM as a filtration aid and disperser is smaller than 10 nm. We believe this post treatment method will come into wide use for preparation of many nanosized materials. SnO2 Calcination Temperature Bi2O3 Post Treatment Process Optimal Calcination Temperature Tu, Weiping aut Hu, Jianqing aut Enthalten in Journal of materials science Kluwer Academic Publishers-Plenum Publishers, 1966 42(2007), 19 vom: 01. Okt., Seite 8292-8297 (DE-627)129546372 (DE-600)218324-9 (DE-576)014996774 0022-2461 nnns volume:42 year:2007 number:19 day:01 month:10 pages:8292-8297 https://doi.org/10.1007/s10853-007-1509-x lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC GBV_ILN_20 GBV_ILN_21 GBV_ILN_23 GBV_ILN_30 GBV_ILN_32 GBV_ILN_40 GBV_ILN_62 GBV_ILN_65 GBV_ILN_70 GBV_ILN_100 GBV_ILN_602 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_4046 GBV_ILN_4305 GBV_ILN_4323 AR 42 2007 19 01 10 8292-8297 |
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10.1007/s10853-007-1509-x doi (DE-627)OLC2046331613 (DE-He213)s10853-007-1509-x-p DE-627 ger DE-627 rakwb eng 670 VZ He, Qiuxing verfasserin aut Preparation and characterization of nanosized bismuth doped tin dioxide powders with a novel post treatment process 2007 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Springer Science+Business Media, LLC 2007 Abstract Bismuth-doped tin dioxide (BTO) nanopowders were prepared by wet chemical co-precipitation method using tin tetrachloride ($ SnCl_{4} $) and bismuth nitrate (Bi($ NO_{3} $)3) as raw materials. Effects of calcination temperature and post treatment methods on particle size and crystalline phase transition of bismuth tin precursor (BTP) were studied by X-ray diffraction (XRD), transmission electron microscopy (TEM), thermogravimetric-differential scanning calorimetric instrument (TG-DSC) and X-ray photoelectron spectroscopy (XPS). The optimal calcination temperature of BTP was found to be about 873 K. A novel post treatment process with polyacrylamide (PAM) in the preparation of nanometerials was presented for the first time. Experimental results showed that nonionic PAM is a highly effective additive, which not only speeds up the filtration of precursor, but also effectively reduces the formation of hard agglomerates. The average size of BTO nanopowders prepared using nonionic PAM as a filtration aid and disperser is smaller than 10 nm. We believe this post treatment method will come into wide use for preparation of many nanosized materials. SnO2 Calcination Temperature Bi2O3 Post Treatment Process Optimal Calcination Temperature Tu, Weiping aut Hu, Jianqing aut Enthalten in Journal of materials science Kluwer Academic Publishers-Plenum Publishers, 1966 42(2007), 19 vom: 01. Okt., Seite 8292-8297 (DE-627)129546372 (DE-600)218324-9 (DE-576)014996774 0022-2461 nnns volume:42 year:2007 number:19 day:01 month:10 pages:8292-8297 https://doi.org/10.1007/s10853-007-1509-x lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC GBV_ILN_20 GBV_ILN_21 GBV_ILN_23 GBV_ILN_30 GBV_ILN_32 GBV_ILN_40 GBV_ILN_62 GBV_ILN_65 GBV_ILN_70 GBV_ILN_100 GBV_ILN_602 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_4046 GBV_ILN_4305 GBV_ILN_4323 AR 42 2007 19 01 10 8292-8297 |
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preparation and characterization of nanosized bismuth doped tin dioxide powders with a novel post treatment process |
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Preparation and characterization of nanosized bismuth doped tin dioxide powders with a novel post treatment process |
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Abstract Bismuth-doped tin dioxide (BTO) nanopowders were prepared by wet chemical co-precipitation method using tin tetrachloride ($ SnCl_{4} $) and bismuth nitrate (Bi($ NO_{3} $)3) as raw materials. Effects of calcination temperature and post treatment methods on particle size and crystalline phase transition of bismuth tin precursor (BTP) were studied by X-ray diffraction (XRD), transmission electron microscopy (TEM), thermogravimetric-differential scanning calorimetric instrument (TG-DSC) and X-ray photoelectron spectroscopy (XPS). The optimal calcination temperature of BTP was found to be about 873 K. A novel post treatment process with polyacrylamide (PAM) in the preparation of nanometerials was presented for the first time. Experimental results showed that nonionic PAM is a highly effective additive, which not only speeds up the filtration of precursor, but also effectively reduces the formation of hard agglomerates. The average size of BTO nanopowders prepared using nonionic PAM as a filtration aid and disperser is smaller than 10 nm. We believe this post treatment method will come into wide use for preparation of many nanosized materials. © Springer Science+Business Media, LLC 2007 |
| abstractGer |
Abstract Bismuth-doped tin dioxide (BTO) nanopowders were prepared by wet chemical co-precipitation method using tin tetrachloride ($ SnCl_{4} $) and bismuth nitrate (Bi($ NO_{3} $)3) as raw materials. Effects of calcination temperature and post treatment methods on particle size and crystalline phase transition of bismuth tin precursor (BTP) were studied by X-ray diffraction (XRD), transmission electron microscopy (TEM), thermogravimetric-differential scanning calorimetric instrument (TG-DSC) and X-ray photoelectron spectroscopy (XPS). The optimal calcination temperature of BTP was found to be about 873 K. A novel post treatment process with polyacrylamide (PAM) in the preparation of nanometerials was presented for the first time. Experimental results showed that nonionic PAM is a highly effective additive, which not only speeds up the filtration of precursor, but also effectively reduces the formation of hard agglomerates. The average size of BTO nanopowders prepared using nonionic PAM as a filtration aid and disperser is smaller than 10 nm. We believe this post treatment method will come into wide use for preparation of many nanosized materials. © Springer Science+Business Media, LLC 2007 |
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Abstract Bismuth-doped tin dioxide (BTO) nanopowders were prepared by wet chemical co-precipitation method using tin tetrachloride ($ SnCl_{4} $) and bismuth nitrate (Bi($ NO_{3} $)3) as raw materials. Effects of calcination temperature and post treatment methods on particle size and crystalline phase transition of bismuth tin precursor (BTP) were studied by X-ray diffraction (XRD), transmission electron microscopy (TEM), thermogravimetric-differential scanning calorimetric instrument (TG-DSC) and X-ray photoelectron spectroscopy (XPS). The optimal calcination temperature of BTP was found to be about 873 K. A novel post treatment process with polyacrylamide (PAM) in the preparation of nanometerials was presented for the first time. Experimental results showed that nonionic PAM is a highly effective additive, which not only speeds up the filtration of precursor, but also effectively reduces the formation of hard agglomerates. The average size of BTO nanopowders prepared using nonionic PAM as a filtration aid and disperser is smaller than 10 nm. We believe this post treatment method will come into wide use for preparation of many nanosized materials. © Springer Science+Business Media, LLC 2007 |
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