Copper and iron based thin film nanocomposites prepared by radio-frequency sputtering. Part II: elaboration and characterization of oxide/oxide thin film nanocomposites using controlled ex-situ oxidation process
Abstract CuO/$ CuFe_{2} $$ O_{4} $ thin films were obtained on glass substrate by ex situ oxidation in air at 450 °C for 12 h from various starting metal/oxide nanocomposites by radio-frequency sputtering technique. The structure and microstructure of the films were examined using grazing incidence...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Chapelle, A. [verfasserIn] |
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| Format: |
Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2013 |
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| Schlagwörter: |
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| Anmerkung: |
© Springer Science+Business Media New York 2013 |
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| Übergeordnetes Werk: |
Enthalten in: Journal of materials science - Springer US, 1966, 48(2013), 8 vom: 08. Jan., Seite 3304-3314 |
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| Übergeordnetes Werk: |
volume:48 ; year:2013 ; number:8 ; day:08 ; month:01 ; pages:3304-3314 |
| Links: |
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| DOI / URN: |
10.1007/s10853-012-7116-5 |
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OLC2046384830 |
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| 245 | 1 | 0 | |a Copper and iron based thin film nanocomposites prepared by radio-frequency sputtering. Part II: elaboration and characterization of oxide/oxide thin film nanocomposites using controlled ex-situ oxidation process |
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| 520 | |a Abstract CuO/$ CuFe_{2} $$ O_{4} $ thin films were obtained on glass substrate by ex situ oxidation in air at 450 °C for 12 h from various starting metal/oxide nanocomposites by radio-frequency sputtering technique. The structure and microstructure of the films were examined using grazing incidence X-ray diffraction, Raman spectroscopy, scanning and transmission electron microscopies, X-ray photoelectron spectroscopy, and electron probe microanalysis. These studies reveal that a self-organized bi-layered microstructure with CuO (surface layer) and $ CuFe_{2} $$ O_{4} $ (heart layer) was systematically obtained. Due to the porosity of the upper layer formed during annealing, an increase in total thickness of the film was observed and is directly correlated to the oxidation of the metallic copper content initially present in the as-deposited sample. A self-organization in two stacked layers CuO/$ CuFe_{2} $$ O_{4} $ with various void fractions ranging from 0 to 41 % can be obtained by controlling the as-deposited elaboration step described in the part I of this paper. The highest porosities were observed for films deposited at low argon pressure and low target-to-substrate distance. Due to their specific self-organization in p- and n-type layers associated with their high porosity, such structured films exhibited the best electrical sensitivity to $ CO_{2} $ gas sensing. The obtained results demonstrated the importance of microstructure control to improve the response of sensing layers. | ||
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| 700 | 1 | |a Presmanes, L. |4 aut | |
| 700 | 1 | |a Tailhades, P. |4 aut | |
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10.1007/s10853-012-7116-5 doi (DE-627)OLC2046384830 (DE-He213)s10853-012-7116-5-p DE-627 ger DE-627 rakwb eng 670 VZ Chapelle, A. verfasserin aut Copper and iron based thin film nanocomposites prepared by radio-frequency sputtering. Part II: elaboration and characterization of oxide/oxide thin film nanocomposites using controlled ex-situ oxidation process 2013 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Springer Science+Business Media New York 2013 Abstract CuO/$ CuFe_{2} $$ O_{4} $ thin films were obtained on glass substrate by ex situ oxidation in air at 450 °C for 12 h from various starting metal/oxide nanocomposites by radio-frequency sputtering technique. The structure and microstructure of the films were examined using grazing incidence X-ray diffraction, Raman spectroscopy, scanning and transmission electron microscopies, X-ray photoelectron spectroscopy, and electron probe microanalysis. These studies reveal that a self-organized bi-layered microstructure with CuO (surface layer) and $ CuFe_{2} $$ O_{4} $ (heart layer) was systematically obtained. Due to the porosity of the upper layer formed during annealing, an increase in total thickness of the film was observed and is directly correlated to the oxidation of the metallic copper content initially present in the as-deposited sample. A self-organization in two stacked layers CuO/$ CuFe_{2} $$ O_{4} $ with various void fractions ranging from 0 to 41 % can be obtained by controlling the as-deposited elaboration step described in the part I of this paper. The highest porosities were observed for films deposited at low argon pressure and low target-to-substrate distance. Due to their specific self-organization in p- and n-type layers associated with their high porosity, such structured films exhibited the best electrical sensitivity to $ CO_{2} $ gas sensing. The obtained results demonstrated the importance of microstructure control to improve the response of sensing layers. Copper oxide Spinel ferrite Gas sensor Barnabé, A. aut Presmanes, L. aut Tailhades, P. aut Enthalten in Journal of materials science Springer US, 1966 48(2013), 8 vom: 08. Jan., Seite 3304-3314 (DE-627)129546372 (DE-600)218324-9 (DE-576)014996774 0022-2461 nnns volume:48 year:2013 number:8 day:08 month:01 pages:3304-3314 https://doi.org/10.1007/s10853-012-7116-5 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC GBV_ILN_20 GBV_ILN_30 GBV_ILN_32 GBV_ILN_70 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_4046 GBV_ILN_4305 GBV_ILN_4323 AR 48 2013 8 08 01 3304-3314 |
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10.1007/s10853-012-7116-5 doi (DE-627)OLC2046384830 (DE-He213)s10853-012-7116-5-p DE-627 ger DE-627 rakwb eng 670 VZ Chapelle, A. verfasserin aut Copper and iron based thin film nanocomposites prepared by radio-frequency sputtering. Part II: elaboration and characterization of oxide/oxide thin film nanocomposites using controlled ex-situ oxidation process 2013 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Springer Science+Business Media New York 2013 Abstract CuO/$ CuFe_{2} $$ O_{4} $ thin films were obtained on glass substrate by ex situ oxidation in air at 450 °C for 12 h from various starting metal/oxide nanocomposites by radio-frequency sputtering technique. The structure and microstructure of the films were examined using grazing incidence X-ray diffraction, Raman spectroscopy, scanning and transmission electron microscopies, X-ray photoelectron spectroscopy, and electron probe microanalysis. These studies reveal that a self-organized bi-layered microstructure with CuO (surface layer) and $ CuFe_{2} $$ O_{4} $ (heart layer) was systematically obtained. Due to the porosity of the upper layer formed during annealing, an increase in total thickness of the film was observed and is directly correlated to the oxidation of the metallic copper content initially present in the as-deposited sample. A self-organization in two stacked layers CuO/$ CuFe_{2} $$ O_{4} $ with various void fractions ranging from 0 to 41 % can be obtained by controlling the as-deposited elaboration step described in the part I of this paper. The highest porosities were observed for films deposited at low argon pressure and low target-to-substrate distance. Due to their specific self-organization in p- and n-type layers associated with their high porosity, such structured films exhibited the best electrical sensitivity to $ CO_{2} $ gas sensing. The obtained results demonstrated the importance of microstructure control to improve the response of sensing layers. Copper oxide Spinel ferrite Gas sensor Barnabé, A. aut Presmanes, L. aut Tailhades, P. aut Enthalten in Journal of materials science Springer US, 1966 48(2013), 8 vom: 08. Jan., Seite 3304-3314 (DE-627)129546372 (DE-600)218324-9 (DE-576)014996774 0022-2461 nnns volume:48 year:2013 number:8 day:08 month:01 pages:3304-3314 https://doi.org/10.1007/s10853-012-7116-5 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC GBV_ILN_20 GBV_ILN_30 GBV_ILN_32 GBV_ILN_70 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_4046 GBV_ILN_4305 GBV_ILN_4323 AR 48 2013 8 08 01 3304-3314 |
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10.1007/s10853-012-7116-5 doi (DE-627)OLC2046384830 (DE-He213)s10853-012-7116-5-p DE-627 ger DE-627 rakwb eng 670 VZ Chapelle, A. verfasserin aut Copper and iron based thin film nanocomposites prepared by radio-frequency sputtering. Part II: elaboration and characterization of oxide/oxide thin film nanocomposites using controlled ex-situ oxidation process 2013 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Springer Science+Business Media New York 2013 Abstract CuO/$ CuFe_{2} $$ O_{4} $ thin films were obtained on glass substrate by ex situ oxidation in air at 450 °C for 12 h from various starting metal/oxide nanocomposites by radio-frequency sputtering technique. The structure and microstructure of the films were examined using grazing incidence X-ray diffraction, Raman spectroscopy, scanning and transmission electron microscopies, X-ray photoelectron spectroscopy, and electron probe microanalysis. These studies reveal that a self-organized bi-layered microstructure with CuO (surface layer) and $ CuFe_{2} $$ O_{4} $ (heart layer) was systematically obtained. Due to the porosity of the upper layer formed during annealing, an increase in total thickness of the film was observed and is directly correlated to the oxidation of the metallic copper content initially present in the as-deposited sample. A self-organization in two stacked layers CuO/$ CuFe_{2} $$ O_{4} $ with various void fractions ranging from 0 to 41 % can be obtained by controlling the as-deposited elaboration step described in the part I of this paper. The highest porosities were observed for films deposited at low argon pressure and low target-to-substrate distance. Due to their specific self-organization in p- and n-type layers associated with their high porosity, such structured films exhibited the best electrical sensitivity to $ CO_{2} $ gas sensing. The obtained results demonstrated the importance of microstructure control to improve the response of sensing layers. Copper oxide Spinel ferrite Gas sensor Barnabé, A. aut Presmanes, L. aut Tailhades, P. aut Enthalten in Journal of materials science Springer US, 1966 48(2013), 8 vom: 08. Jan., Seite 3304-3314 (DE-627)129546372 (DE-600)218324-9 (DE-576)014996774 0022-2461 nnns volume:48 year:2013 number:8 day:08 month:01 pages:3304-3314 https://doi.org/10.1007/s10853-012-7116-5 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC GBV_ILN_20 GBV_ILN_30 GBV_ILN_32 GBV_ILN_70 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_4046 GBV_ILN_4305 GBV_ILN_4323 AR 48 2013 8 08 01 3304-3314 |
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10.1007/s10853-012-7116-5 doi (DE-627)OLC2046384830 (DE-He213)s10853-012-7116-5-p DE-627 ger DE-627 rakwb eng 670 VZ Chapelle, A. verfasserin aut Copper and iron based thin film nanocomposites prepared by radio-frequency sputtering. Part II: elaboration and characterization of oxide/oxide thin film nanocomposites using controlled ex-situ oxidation process 2013 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Springer Science+Business Media New York 2013 Abstract CuO/$ CuFe_{2} $$ O_{4} $ thin films were obtained on glass substrate by ex situ oxidation in air at 450 °C for 12 h from various starting metal/oxide nanocomposites by radio-frequency sputtering technique. The structure and microstructure of the films were examined using grazing incidence X-ray diffraction, Raman spectroscopy, scanning and transmission electron microscopies, X-ray photoelectron spectroscopy, and electron probe microanalysis. These studies reveal that a self-organized bi-layered microstructure with CuO (surface layer) and $ CuFe_{2} $$ O_{4} $ (heart layer) was systematically obtained. Due to the porosity of the upper layer formed during annealing, an increase in total thickness of the film was observed and is directly correlated to the oxidation of the metallic copper content initially present in the as-deposited sample. A self-organization in two stacked layers CuO/$ CuFe_{2} $$ O_{4} $ with various void fractions ranging from 0 to 41 % can be obtained by controlling the as-deposited elaboration step described in the part I of this paper. The highest porosities were observed for films deposited at low argon pressure and low target-to-substrate distance. Due to their specific self-organization in p- and n-type layers associated with their high porosity, such structured films exhibited the best electrical sensitivity to $ CO_{2} $ gas sensing. The obtained results demonstrated the importance of microstructure control to improve the response of sensing layers. Copper oxide Spinel ferrite Gas sensor Barnabé, A. aut Presmanes, L. aut Tailhades, P. aut Enthalten in Journal of materials science Springer US, 1966 48(2013), 8 vom: 08. Jan., Seite 3304-3314 (DE-627)129546372 (DE-600)218324-9 (DE-576)014996774 0022-2461 nnns volume:48 year:2013 number:8 day:08 month:01 pages:3304-3314 https://doi.org/10.1007/s10853-012-7116-5 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC GBV_ILN_20 GBV_ILN_30 GBV_ILN_32 GBV_ILN_70 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_4046 GBV_ILN_4305 GBV_ILN_4323 AR 48 2013 8 08 01 3304-3314 |
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10.1007/s10853-012-7116-5 doi (DE-627)OLC2046384830 (DE-He213)s10853-012-7116-5-p DE-627 ger DE-627 rakwb eng 670 VZ Chapelle, A. verfasserin aut Copper and iron based thin film nanocomposites prepared by radio-frequency sputtering. Part II: elaboration and characterization of oxide/oxide thin film nanocomposites using controlled ex-situ oxidation process 2013 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Springer Science+Business Media New York 2013 Abstract CuO/$ CuFe_{2} $$ O_{4} $ thin films were obtained on glass substrate by ex situ oxidation in air at 450 °C for 12 h from various starting metal/oxide nanocomposites by radio-frequency sputtering technique. The structure and microstructure of the films were examined using grazing incidence X-ray diffraction, Raman spectroscopy, scanning and transmission electron microscopies, X-ray photoelectron spectroscopy, and electron probe microanalysis. These studies reveal that a self-organized bi-layered microstructure with CuO (surface layer) and $ CuFe_{2} $$ O_{4} $ (heart layer) was systematically obtained. Due to the porosity of the upper layer formed during annealing, an increase in total thickness of the film was observed and is directly correlated to the oxidation of the metallic copper content initially present in the as-deposited sample. A self-organization in two stacked layers CuO/$ CuFe_{2} $$ O_{4} $ with various void fractions ranging from 0 to 41 % can be obtained by controlling the as-deposited elaboration step described in the part I of this paper. The highest porosities were observed for films deposited at low argon pressure and low target-to-substrate distance. Due to their specific self-organization in p- and n-type layers associated with their high porosity, such structured films exhibited the best electrical sensitivity to $ CO_{2} $ gas sensing. The obtained results demonstrated the importance of microstructure control to improve the response of sensing layers. Copper oxide Spinel ferrite Gas sensor Barnabé, A. aut Presmanes, L. aut Tailhades, P. aut Enthalten in Journal of materials science Springer US, 1966 48(2013), 8 vom: 08. Jan., Seite 3304-3314 (DE-627)129546372 (DE-600)218324-9 (DE-576)014996774 0022-2461 nnns volume:48 year:2013 number:8 day:08 month:01 pages:3304-3314 https://doi.org/10.1007/s10853-012-7116-5 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC GBV_ILN_20 GBV_ILN_30 GBV_ILN_32 GBV_ILN_70 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_4046 GBV_ILN_4305 GBV_ILN_4323 AR 48 2013 8 08 01 3304-3314 |
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Chapelle, A. |
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670 VZ Copper and iron based thin film nanocomposites prepared by radio-frequency sputtering. Part II: elaboration and characterization of oxide/oxide thin film nanocomposites using controlled ex-situ oxidation process Copper oxide Spinel ferrite Gas sensor |
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Copper and iron based thin film nanocomposites prepared by radio-frequency sputtering. Part II: elaboration and characterization of oxide/oxide thin film nanocomposites using controlled ex-situ oxidation process |
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Copper and iron based thin film nanocomposites prepared by radio-frequency sputtering. Part II: elaboration and characterization of oxide/oxide thin film nanocomposites using controlled ex-situ oxidation process |
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Chapelle, A. |
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Chapelle, A. Barnabé, A. Presmanes, L. Tailhades, P. |
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copper and iron based thin film nanocomposites prepared by radio-frequency sputtering. part ii: elaboration and characterization of oxide/oxide thin film nanocomposites using controlled ex-situ oxidation process |
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Copper and iron based thin film nanocomposites prepared by radio-frequency sputtering. Part II: elaboration and characterization of oxide/oxide thin film nanocomposites using controlled ex-situ oxidation process |
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Abstract CuO/$ CuFe_{2} $$ O_{4} $ thin films were obtained on glass substrate by ex situ oxidation in air at 450 °C for 12 h from various starting metal/oxide nanocomposites by radio-frequency sputtering technique. The structure and microstructure of the films were examined using grazing incidence X-ray diffraction, Raman spectroscopy, scanning and transmission electron microscopies, X-ray photoelectron spectroscopy, and electron probe microanalysis. These studies reveal that a self-organized bi-layered microstructure with CuO (surface layer) and $ CuFe_{2} $$ O_{4} $ (heart layer) was systematically obtained. Due to the porosity of the upper layer formed during annealing, an increase in total thickness of the film was observed and is directly correlated to the oxidation of the metallic copper content initially present in the as-deposited sample. A self-organization in two stacked layers CuO/$ CuFe_{2} $$ O_{4} $ with various void fractions ranging from 0 to 41 % can be obtained by controlling the as-deposited elaboration step described in the part I of this paper. The highest porosities were observed for films deposited at low argon pressure and low target-to-substrate distance. Due to their specific self-organization in p- and n-type layers associated with their high porosity, such structured films exhibited the best electrical sensitivity to $ CO_{2} $ gas sensing. The obtained results demonstrated the importance of microstructure control to improve the response of sensing layers. © Springer Science+Business Media New York 2013 |
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Abstract CuO/$ CuFe_{2} $$ O_{4} $ thin films were obtained on glass substrate by ex situ oxidation in air at 450 °C for 12 h from various starting metal/oxide nanocomposites by radio-frequency sputtering technique. The structure and microstructure of the films were examined using grazing incidence X-ray diffraction, Raman spectroscopy, scanning and transmission electron microscopies, X-ray photoelectron spectroscopy, and electron probe microanalysis. These studies reveal that a self-organized bi-layered microstructure with CuO (surface layer) and $ CuFe_{2} $$ O_{4} $ (heart layer) was systematically obtained. Due to the porosity of the upper layer formed during annealing, an increase in total thickness of the film was observed and is directly correlated to the oxidation of the metallic copper content initially present in the as-deposited sample. A self-organization in two stacked layers CuO/$ CuFe_{2} $$ O_{4} $ with various void fractions ranging from 0 to 41 % can be obtained by controlling the as-deposited elaboration step described in the part I of this paper. The highest porosities were observed for films deposited at low argon pressure and low target-to-substrate distance. Due to their specific self-organization in p- and n-type layers associated with their high porosity, such structured films exhibited the best electrical sensitivity to $ CO_{2} $ gas sensing. The obtained results demonstrated the importance of microstructure control to improve the response of sensing layers. © Springer Science+Business Media New York 2013 |
| abstract_unstemmed |
Abstract CuO/$ CuFe_{2} $$ O_{4} $ thin films were obtained on glass substrate by ex situ oxidation in air at 450 °C for 12 h from various starting metal/oxide nanocomposites by radio-frequency sputtering technique. The structure and microstructure of the films were examined using grazing incidence X-ray diffraction, Raman spectroscopy, scanning and transmission electron microscopies, X-ray photoelectron spectroscopy, and electron probe microanalysis. These studies reveal that a self-organized bi-layered microstructure with CuO (surface layer) and $ CuFe_{2} $$ O_{4} $ (heart layer) was systematically obtained. Due to the porosity of the upper layer formed during annealing, an increase in total thickness of the film was observed and is directly correlated to the oxidation of the metallic copper content initially present in the as-deposited sample. A self-organization in two stacked layers CuO/$ CuFe_{2} $$ O_{4} $ with various void fractions ranging from 0 to 41 % can be obtained by controlling the as-deposited elaboration step described in the part I of this paper. The highest porosities were observed for films deposited at low argon pressure and low target-to-substrate distance. Due to their specific self-organization in p- and n-type layers associated with their high porosity, such structured films exhibited the best electrical sensitivity to $ CO_{2} $ gas sensing. The obtained results demonstrated the importance of microstructure control to improve the response of sensing layers. © Springer Science+Business Media New York 2013 |
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Copper and iron based thin film nanocomposites prepared by radio-frequency sputtering. Part II: elaboration and characterization of oxide/oxide thin film nanocomposites using controlled ex-situ oxidation process |
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