One-step strategy for synthesis of yolk–shell silica spheres using trisiloxane-tailed ionic liquids as a template
Abstract Yolk–shell silica spheres consisting of a core and an outer shell were prepared by a one-step method using a new class of eco-friendly templates, trisiloxane-tailed surface active ionic liquids. The effects of pH, calcination, and template concentration were investigated in detail. Our resu...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Du, Zhiping [verfasserIn] |
|---|
| Format: |
Artikel |
|---|---|
| Sprache: |
Englisch |
| Erschienen: |
2014 |
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| Schlagwörter: |
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| Anmerkung: |
© Springer Science+Business Media New York 2014 |
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| Übergeordnetes Werk: |
Enthalten in: Journal of materials science - Springer US, 1966, 49(2014), 14 vom: 02. Apr., Seite 4919-4926 |
|---|---|
| Übergeordnetes Werk: |
volume:49 ; year:2014 ; number:14 ; day:02 ; month:04 ; pages:4919-4926 |
| Links: |
|---|
| DOI / URN: |
10.1007/s10853-014-8193-4 |
|---|
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OLC2046395875 |
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| 520 | |a Abstract Yolk–shell silica spheres consisting of a core and an outer shell were prepared by a one-step method using a new class of eco-friendly templates, trisiloxane-tailed surface active ionic liquids. The effects of pH, calcination, and template concentration were investigated in detail. Our results showed that yolk–shell silica spheres could be obtained only in alkaline conditions when using trisiloxane-tailed ionic liquids as templates. The particle diameter, core diameter, dimension of void space, and shell thickness, which we measured by transmission electron microscopy and nitrogen adsorption–desorption techniques, could be tuned by precisely varying the template concentration. The organosilicon component of the ionic liquid template contributes to the reaction during the formation of yolk–shell nanostructures, which leads to a firm silica sphere skeleton resulting in essentially identical morphology and void structure before and after calcination. This investigation provides a convenient approach to fabricate yolk–shell silica spheres, which may expand the application of organosilicon ionic liquids in the field of nanomaterials and could be expected to generate tailor-made yolk–shell silica with functionality in both the core and shell. | ||
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10.1007/s10853-014-8193-4 doi (DE-627)OLC2046395875 (DE-He213)s10853-014-8193-4-p DE-627 ger DE-627 rakwb eng 670 VZ Du, Zhiping verfasserin aut One-step strategy for synthesis of yolk–shell silica spheres using trisiloxane-tailed ionic liquids as a template 2014 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Springer Science+Business Media New York 2014 Abstract Yolk–shell silica spheres consisting of a core and an outer shell were prepared by a one-step method using a new class of eco-friendly templates, trisiloxane-tailed surface active ionic liquids. The effects of pH, calcination, and template concentration were investigated in detail. Our results showed that yolk–shell silica spheres could be obtained only in alkaline conditions when using trisiloxane-tailed ionic liquids as templates. The particle diameter, core diameter, dimension of void space, and shell thickness, which we measured by transmission electron microscopy and nitrogen adsorption–desorption techniques, could be tuned by precisely varying the template concentration. The organosilicon component of the ionic liquid template contributes to the reaction during the formation of yolk–shell nanostructures, which leads to a firm silica sphere skeleton resulting in essentially identical morphology and void structure before and after calcination. This investigation provides a convenient approach to fabricate yolk–shell silica spheres, which may expand the application of organosilicon ionic liquids in the field of nanomaterials and could be expected to generate tailor-made yolk–shell silica with functionality in both the core and shell. Calcination Ionic Liquid Shell Thickness Silica Sphere Template Concentration Li, Enze aut Li, Guojin aut Cheng, Fangqin aut Wang, Guoyong aut Enthalten in Journal of materials science Springer US, 1966 49(2014), 14 vom: 02. Apr., Seite 4919-4926 (DE-627)129546372 (DE-600)218324-9 (DE-576)014996774 0022-2461 nnns volume:49 year:2014 number:14 day:02 month:04 pages:4919-4926 https://doi.org/10.1007/s10853-014-8193-4 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC GBV_ILN_20 GBV_ILN_30 GBV_ILN_32 GBV_ILN_70 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_4046 GBV_ILN_4305 GBV_ILN_4323 AR 49 2014 14 02 04 4919-4926 |
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10.1007/s10853-014-8193-4 doi (DE-627)OLC2046395875 (DE-He213)s10853-014-8193-4-p DE-627 ger DE-627 rakwb eng 670 VZ Du, Zhiping verfasserin aut One-step strategy for synthesis of yolk–shell silica spheres using trisiloxane-tailed ionic liquids as a template 2014 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Springer Science+Business Media New York 2014 Abstract Yolk–shell silica spheres consisting of a core and an outer shell were prepared by a one-step method using a new class of eco-friendly templates, trisiloxane-tailed surface active ionic liquids. The effects of pH, calcination, and template concentration were investigated in detail. Our results showed that yolk–shell silica spheres could be obtained only in alkaline conditions when using trisiloxane-tailed ionic liquids as templates. The particle diameter, core diameter, dimension of void space, and shell thickness, which we measured by transmission electron microscopy and nitrogen adsorption–desorption techniques, could be tuned by precisely varying the template concentration. The organosilicon component of the ionic liquid template contributes to the reaction during the formation of yolk–shell nanostructures, which leads to a firm silica sphere skeleton resulting in essentially identical morphology and void structure before and after calcination. This investigation provides a convenient approach to fabricate yolk–shell silica spheres, which may expand the application of organosilicon ionic liquids in the field of nanomaterials and could be expected to generate tailor-made yolk–shell silica with functionality in both the core and shell. Calcination Ionic Liquid Shell Thickness Silica Sphere Template Concentration Li, Enze aut Li, Guojin aut Cheng, Fangqin aut Wang, Guoyong aut Enthalten in Journal of materials science Springer US, 1966 49(2014), 14 vom: 02. Apr., Seite 4919-4926 (DE-627)129546372 (DE-600)218324-9 (DE-576)014996774 0022-2461 nnns volume:49 year:2014 number:14 day:02 month:04 pages:4919-4926 https://doi.org/10.1007/s10853-014-8193-4 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC GBV_ILN_20 GBV_ILN_30 GBV_ILN_32 GBV_ILN_70 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_4046 GBV_ILN_4305 GBV_ILN_4323 AR 49 2014 14 02 04 4919-4926 |
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10.1007/s10853-014-8193-4 doi (DE-627)OLC2046395875 (DE-He213)s10853-014-8193-4-p DE-627 ger DE-627 rakwb eng 670 VZ Du, Zhiping verfasserin aut One-step strategy for synthesis of yolk–shell silica spheres using trisiloxane-tailed ionic liquids as a template 2014 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Springer Science+Business Media New York 2014 Abstract Yolk–shell silica spheres consisting of a core and an outer shell were prepared by a one-step method using a new class of eco-friendly templates, trisiloxane-tailed surface active ionic liquids. The effects of pH, calcination, and template concentration were investigated in detail. Our results showed that yolk–shell silica spheres could be obtained only in alkaline conditions when using trisiloxane-tailed ionic liquids as templates. The particle diameter, core diameter, dimension of void space, and shell thickness, which we measured by transmission electron microscopy and nitrogen adsorption–desorption techniques, could be tuned by precisely varying the template concentration. The organosilicon component of the ionic liquid template contributes to the reaction during the formation of yolk–shell nanostructures, which leads to a firm silica sphere skeleton resulting in essentially identical morphology and void structure before and after calcination. This investigation provides a convenient approach to fabricate yolk–shell silica spheres, which may expand the application of organosilicon ionic liquids in the field of nanomaterials and could be expected to generate tailor-made yolk–shell silica with functionality in both the core and shell. Calcination Ionic Liquid Shell Thickness Silica Sphere Template Concentration Li, Enze aut Li, Guojin aut Cheng, Fangqin aut Wang, Guoyong aut Enthalten in Journal of materials science Springer US, 1966 49(2014), 14 vom: 02. Apr., Seite 4919-4926 (DE-627)129546372 (DE-600)218324-9 (DE-576)014996774 0022-2461 nnns volume:49 year:2014 number:14 day:02 month:04 pages:4919-4926 https://doi.org/10.1007/s10853-014-8193-4 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC GBV_ILN_20 GBV_ILN_30 GBV_ILN_32 GBV_ILN_70 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_4046 GBV_ILN_4305 GBV_ILN_4323 AR 49 2014 14 02 04 4919-4926 |
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10.1007/s10853-014-8193-4 doi (DE-627)OLC2046395875 (DE-He213)s10853-014-8193-4-p DE-627 ger DE-627 rakwb eng 670 VZ Du, Zhiping verfasserin aut One-step strategy for synthesis of yolk–shell silica spheres using trisiloxane-tailed ionic liquids as a template 2014 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Springer Science+Business Media New York 2014 Abstract Yolk–shell silica spheres consisting of a core and an outer shell were prepared by a one-step method using a new class of eco-friendly templates, trisiloxane-tailed surface active ionic liquids. The effects of pH, calcination, and template concentration were investigated in detail. Our results showed that yolk–shell silica spheres could be obtained only in alkaline conditions when using trisiloxane-tailed ionic liquids as templates. The particle diameter, core diameter, dimension of void space, and shell thickness, which we measured by transmission electron microscopy and nitrogen adsorption–desorption techniques, could be tuned by precisely varying the template concentration. The organosilicon component of the ionic liquid template contributes to the reaction during the formation of yolk–shell nanostructures, which leads to a firm silica sphere skeleton resulting in essentially identical morphology and void structure before and after calcination. This investigation provides a convenient approach to fabricate yolk–shell silica spheres, which may expand the application of organosilicon ionic liquids in the field of nanomaterials and could be expected to generate tailor-made yolk–shell silica with functionality in both the core and shell. Calcination Ionic Liquid Shell Thickness Silica Sphere Template Concentration Li, Enze aut Li, Guojin aut Cheng, Fangqin aut Wang, Guoyong aut Enthalten in Journal of materials science Springer US, 1966 49(2014), 14 vom: 02. Apr., Seite 4919-4926 (DE-627)129546372 (DE-600)218324-9 (DE-576)014996774 0022-2461 nnns volume:49 year:2014 number:14 day:02 month:04 pages:4919-4926 https://doi.org/10.1007/s10853-014-8193-4 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC GBV_ILN_20 GBV_ILN_30 GBV_ILN_32 GBV_ILN_70 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_4046 GBV_ILN_4305 GBV_ILN_4323 AR 49 2014 14 02 04 4919-4926 |
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One-step strategy for synthesis of yolk–shell silica spheres using trisiloxane-tailed ionic liquids as a template |
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One-step strategy for synthesis of yolk–shell silica spheres using trisiloxane-tailed ionic liquids as a template |
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Du, Zhiping |
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Journal of materials science |
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Journal of materials science |
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2014 |
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Du, Zhiping Li, Enze Li, Guojin Cheng, Fangqin Wang, Guoyong |
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670 VZ |
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Du, Zhiping |
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10.1007/s10853-014-8193-4 |
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670 |
| title_sort |
one-step strategy for synthesis of yolk–shell silica spheres using trisiloxane-tailed ionic liquids as a template |
| title_auth |
One-step strategy for synthesis of yolk–shell silica spheres using trisiloxane-tailed ionic liquids as a template |
| abstract |
Abstract Yolk–shell silica spheres consisting of a core and an outer shell were prepared by a one-step method using a new class of eco-friendly templates, trisiloxane-tailed surface active ionic liquids. The effects of pH, calcination, and template concentration were investigated in detail. Our results showed that yolk–shell silica spheres could be obtained only in alkaline conditions when using trisiloxane-tailed ionic liquids as templates. The particle diameter, core diameter, dimension of void space, and shell thickness, which we measured by transmission electron microscopy and nitrogen adsorption–desorption techniques, could be tuned by precisely varying the template concentration. The organosilicon component of the ionic liquid template contributes to the reaction during the formation of yolk–shell nanostructures, which leads to a firm silica sphere skeleton resulting in essentially identical morphology and void structure before and after calcination. This investigation provides a convenient approach to fabricate yolk–shell silica spheres, which may expand the application of organosilicon ionic liquids in the field of nanomaterials and could be expected to generate tailor-made yolk–shell silica with functionality in both the core and shell. © Springer Science+Business Media New York 2014 |
| abstractGer |
Abstract Yolk–shell silica spheres consisting of a core and an outer shell were prepared by a one-step method using a new class of eco-friendly templates, trisiloxane-tailed surface active ionic liquids. The effects of pH, calcination, and template concentration were investigated in detail. Our results showed that yolk–shell silica spheres could be obtained only in alkaline conditions when using trisiloxane-tailed ionic liquids as templates. The particle diameter, core diameter, dimension of void space, and shell thickness, which we measured by transmission electron microscopy and nitrogen adsorption–desorption techniques, could be tuned by precisely varying the template concentration. The organosilicon component of the ionic liquid template contributes to the reaction during the formation of yolk–shell nanostructures, which leads to a firm silica sphere skeleton resulting in essentially identical morphology and void structure before and after calcination. This investigation provides a convenient approach to fabricate yolk–shell silica spheres, which may expand the application of organosilicon ionic liquids in the field of nanomaterials and could be expected to generate tailor-made yolk–shell silica with functionality in both the core and shell. © Springer Science+Business Media New York 2014 |
| abstract_unstemmed |
Abstract Yolk–shell silica spheres consisting of a core and an outer shell were prepared by a one-step method using a new class of eco-friendly templates, trisiloxane-tailed surface active ionic liquids. The effects of pH, calcination, and template concentration were investigated in detail. Our results showed that yolk–shell silica spheres could be obtained only in alkaline conditions when using trisiloxane-tailed ionic liquids as templates. The particle diameter, core diameter, dimension of void space, and shell thickness, which we measured by transmission electron microscopy and nitrogen adsorption–desorption techniques, could be tuned by precisely varying the template concentration. The organosilicon component of the ionic liquid template contributes to the reaction during the formation of yolk–shell nanostructures, which leads to a firm silica sphere skeleton resulting in essentially identical morphology and void structure before and after calcination. This investigation provides a convenient approach to fabricate yolk–shell silica spheres, which may expand the application of organosilicon ionic liquids in the field of nanomaterials and could be expected to generate tailor-made yolk–shell silica with functionality in both the core and shell. © Springer Science+Business Media New York 2014 |
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14 |
| title_short |
One-step strategy for synthesis of yolk–shell silica spheres using trisiloxane-tailed ionic liquids as a template |
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https://doi.org/10.1007/s10853-014-8193-4 |
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Li, Enze Li, Guojin Cheng, Fangqin Wang, Guoyong |
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2024-07-04T04:59:01.140Z |
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