Microgravimetric Apparatus for Sulfidation in Pure Sulfur Vapour at High Temperatures
Abstract A thermobalance for studies of the high-temperature sulfidation of metals and alloys is described. This apparatus permits the determination of mass changes in a sulfidized sample as a function of temperature and sulfur vapour pressure. The main parts of this apparatus are the container with...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Grzesik, Z. [verfasserIn] |
|---|
| Format: |
Artikel |
|---|---|
| Sprache: |
Englisch |
| Erschienen: |
1999 |
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| Anmerkung: |
© Kluwer Academic Publishers 1999 |
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| Übergeordnetes Werk: |
Enthalten in: Journal of thermal analysis and calorimetry - Kluwer Academic Publishers, 1998, 55(1999), 2 vom: März, Seite 551-558 |
|---|---|
| Übergeordnetes Werk: |
volume:55 ; year:1999 ; number:2 ; month:03 ; pages:551-558 |
| Links: |
|---|
| DOI / URN: |
10.1023/A:1010154121328 |
|---|
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OLC2049747446 |
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| 520 | |a Abstract A thermobalance for studies of the high-temperature sulfidation of metals and alloys is described. This apparatus permits the determination of mass changes in a sulfidized sample as a function of temperature and sulfur vapour pressure. The main parts of this apparatus are the container with liquid sulfur and the reaction chamber with the quartz space and quartz spiral. All parts of the apparatus are equipped with thermostating furnaces. The temperature within the apparatus is controlled with an accuracy of 0.5 K. The quartz spiral (diameter 0.2 mm), consisting of 50 coils (diameter 30 mm), permits the recording of mass changes in the sample (about 200 mg) with an accuracy of $ 10^{-5} $ g. Besides heterogeneous kinetics measurements, it has been shown that the self- and chemical diffusion coefficients or the deviation from stoichiometry of the metal sulfides can also be studied as functions of temperature and sulfur pressure by means of equilibration measurements. | ||
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10.1023/A:1010154121328 doi (DE-627)OLC2049747446 (DE-He213)A:1010154121328-p DE-627 ger DE-627 rakwb eng 660 VZ Grzesik, Z. verfasserin aut Microgravimetric Apparatus for Sulfidation in Pure Sulfur Vapour at High Temperatures 1999 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Kluwer Academic Publishers 1999 Abstract A thermobalance for studies of the high-temperature sulfidation of metals and alloys is described. This apparatus permits the determination of mass changes in a sulfidized sample as a function of temperature and sulfur vapour pressure. The main parts of this apparatus are the container with liquid sulfur and the reaction chamber with the quartz space and quartz spiral. All parts of the apparatus are equipped with thermostating furnaces. The temperature within the apparatus is controlled with an accuracy of 0.5 K. The quartz spiral (diameter 0.2 mm), consisting of 50 coils (diameter 30 mm), permits the recording of mass changes in the sample (about 200 mg) with an accuracy of $ 10^{-5} $ g. Besides heterogeneous kinetics measurements, it has been shown that the self- and chemical diffusion coefficients or the deviation from stoichiometry of the metal sulfides can also be studied as functions of temperature and sulfur pressure by means of equilibration measurements. Danielewski, M. aut Mrowec, S. aut Enthalten in Journal of thermal analysis and calorimetry Kluwer Academic Publishers, 1998 55(1999), 2 vom: März, Seite 551-558 (DE-627)244148767 (DE-600)1429493-X (DE-576)066397693 1388-6150 nnns volume:55 year:1999 number:2 month:03 pages:551-558 https://doi.org/10.1023/A:1010154121328 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE GBV_ILN_70 GBV_ILN_2006 AR 55 1999 2 03 551-558 |
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10.1023/A:1010154121328 doi (DE-627)OLC2049747446 (DE-He213)A:1010154121328-p DE-627 ger DE-627 rakwb eng 660 VZ Grzesik, Z. verfasserin aut Microgravimetric Apparatus for Sulfidation in Pure Sulfur Vapour at High Temperatures 1999 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Kluwer Academic Publishers 1999 Abstract A thermobalance for studies of the high-temperature sulfidation of metals and alloys is described. This apparatus permits the determination of mass changes in a sulfidized sample as a function of temperature and sulfur vapour pressure. The main parts of this apparatus are the container with liquid sulfur and the reaction chamber with the quartz space and quartz spiral. All parts of the apparatus are equipped with thermostating furnaces. The temperature within the apparatus is controlled with an accuracy of 0.5 K. The quartz spiral (diameter 0.2 mm), consisting of 50 coils (diameter 30 mm), permits the recording of mass changes in the sample (about 200 mg) with an accuracy of $ 10^{-5} $ g. Besides heterogeneous kinetics measurements, it has been shown that the self- and chemical diffusion coefficients or the deviation from stoichiometry of the metal sulfides can also be studied as functions of temperature and sulfur pressure by means of equilibration measurements. Danielewski, M. aut Mrowec, S. aut Enthalten in Journal of thermal analysis and calorimetry Kluwer Academic Publishers, 1998 55(1999), 2 vom: März, Seite 551-558 (DE-627)244148767 (DE-600)1429493-X (DE-576)066397693 1388-6150 nnns volume:55 year:1999 number:2 month:03 pages:551-558 https://doi.org/10.1023/A:1010154121328 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE GBV_ILN_70 GBV_ILN_2006 AR 55 1999 2 03 551-558 |
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10.1023/A:1010154121328 doi (DE-627)OLC2049747446 (DE-He213)A:1010154121328-p DE-627 ger DE-627 rakwb eng 660 VZ Grzesik, Z. verfasserin aut Microgravimetric Apparatus for Sulfidation in Pure Sulfur Vapour at High Temperatures 1999 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Kluwer Academic Publishers 1999 Abstract A thermobalance for studies of the high-temperature sulfidation of metals and alloys is described. This apparatus permits the determination of mass changes in a sulfidized sample as a function of temperature and sulfur vapour pressure. The main parts of this apparatus are the container with liquid sulfur and the reaction chamber with the quartz space and quartz spiral. All parts of the apparatus are equipped with thermostating furnaces. The temperature within the apparatus is controlled with an accuracy of 0.5 K. The quartz spiral (diameter 0.2 mm), consisting of 50 coils (diameter 30 mm), permits the recording of mass changes in the sample (about 200 mg) with an accuracy of $ 10^{-5} $ g. Besides heterogeneous kinetics measurements, it has been shown that the self- and chemical diffusion coefficients or the deviation from stoichiometry of the metal sulfides can also be studied as functions of temperature and sulfur pressure by means of equilibration measurements. Danielewski, M. aut Mrowec, S. aut Enthalten in Journal of thermal analysis and calorimetry Kluwer Academic Publishers, 1998 55(1999), 2 vom: März, Seite 551-558 (DE-627)244148767 (DE-600)1429493-X (DE-576)066397693 1388-6150 nnns volume:55 year:1999 number:2 month:03 pages:551-558 https://doi.org/10.1023/A:1010154121328 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE GBV_ILN_70 GBV_ILN_2006 AR 55 1999 2 03 551-558 |
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10.1023/A:1010154121328 doi (DE-627)OLC2049747446 (DE-He213)A:1010154121328-p DE-627 ger DE-627 rakwb eng 660 VZ Grzesik, Z. verfasserin aut Microgravimetric Apparatus for Sulfidation in Pure Sulfur Vapour at High Temperatures 1999 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Kluwer Academic Publishers 1999 Abstract A thermobalance for studies of the high-temperature sulfidation of metals and alloys is described. This apparatus permits the determination of mass changes in a sulfidized sample as a function of temperature and sulfur vapour pressure. The main parts of this apparatus are the container with liquid sulfur and the reaction chamber with the quartz space and quartz spiral. All parts of the apparatus are equipped with thermostating furnaces. The temperature within the apparatus is controlled with an accuracy of 0.5 K. The quartz spiral (diameter 0.2 mm), consisting of 50 coils (diameter 30 mm), permits the recording of mass changes in the sample (about 200 mg) with an accuracy of $ 10^{-5} $ g. Besides heterogeneous kinetics measurements, it has been shown that the self- and chemical diffusion coefficients or the deviation from stoichiometry of the metal sulfides can also be studied as functions of temperature and sulfur pressure by means of equilibration measurements. Danielewski, M. aut Mrowec, S. aut Enthalten in Journal of thermal analysis and calorimetry Kluwer Academic Publishers, 1998 55(1999), 2 vom: März, Seite 551-558 (DE-627)244148767 (DE-600)1429493-X (DE-576)066397693 1388-6150 nnns volume:55 year:1999 number:2 month:03 pages:551-558 https://doi.org/10.1023/A:1010154121328 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE GBV_ILN_70 GBV_ILN_2006 AR 55 1999 2 03 551-558 |
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10.1023/A:1010154121328 doi (DE-627)OLC2049747446 (DE-He213)A:1010154121328-p DE-627 ger DE-627 rakwb eng 660 VZ Grzesik, Z. verfasserin aut Microgravimetric Apparatus for Sulfidation in Pure Sulfur Vapour at High Temperatures 1999 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Kluwer Academic Publishers 1999 Abstract A thermobalance for studies of the high-temperature sulfidation of metals and alloys is described. This apparatus permits the determination of mass changes in a sulfidized sample as a function of temperature and sulfur vapour pressure. The main parts of this apparatus are the container with liquid sulfur and the reaction chamber with the quartz space and quartz spiral. All parts of the apparatus are equipped with thermostating furnaces. The temperature within the apparatus is controlled with an accuracy of 0.5 K. The quartz spiral (diameter 0.2 mm), consisting of 50 coils (diameter 30 mm), permits the recording of mass changes in the sample (about 200 mg) with an accuracy of $ 10^{-5} $ g. Besides heterogeneous kinetics measurements, it has been shown that the self- and chemical diffusion coefficients or the deviation from stoichiometry of the metal sulfides can also be studied as functions of temperature and sulfur pressure by means of equilibration measurements. Danielewski, M. aut Mrowec, S. aut Enthalten in Journal of thermal analysis and calorimetry Kluwer Academic Publishers, 1998 55(1999), 2 vom: März, Seite 551-558 (DE-627)244148767 (DE-600)1429493-X (DE-576)066397693 1388-6150 nnns volume:55 year:1999 number:2 month:03 pages:551-558 https://doi.org/10.1023/A:1010154121328 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE GBV_ILN_70 GBV_ILN_2006 AR 55 1999 2 03 551-558 |
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Abstract A thermobalance for studies of the high-temperature sulfidation of metals and alloys is described. This apparatus permits the determination of mass changes in a sulfidized sample as a function of temperature and sulfur vapour pressure. The main parts of this apparatus are the container with liquid sulfur and the reaction chamber with the quartz space and quartz spiral. All parts of the apparatus are equipped with thermostating furnaces. The temperature within the apparatus is controlled with an accuracy of 0.5 K. The quartz spiral (diameter 0.2 mm), consisting of 50 coils (diameter 30 mm), permits the recording of mass changes in the sample (about 200 mg) with an accuracy of $ 10^{-5} $ g. Besides heterogeneous kinetics measurements, it has been shown that the self- and chemical diffusion coefficients or the deviation from stoichiometry of the metal sulfides can also be studied as functions of temperature and sulfur pressure by means of equilibration measurements. © Kluwer Academic Publishers 1999 |
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Abstract A thermobalance for studies of the high-temperature sulfidation of metals and alloys is described. This apparatus permits the determination of mass changes in a sulfidized sample as a function of temperature and sulfur vapour pressure. The main parts of this apparatus are the container with liquid sulfur and the reaction chamber with the quartz space and quartz spiral. All parts of the apparatus are equipped with thermostating furnaces. The temperature within the apparatus is controlled with an accuracy of 0.5 K. The quartz spiral (diameter 0.2 mm), consisting of 50 coils (diameter 30 mm), permits the recording of mass changes in the sample (about 200 mg) with an accuracy of $ 10^{-5} $ g. Besides heterogeneous kinetics measurements, it has been shown that the self- and chemical diffusion coefficients or the deviation from stoichiometry of the metal sulfides can also be studied as functions of temperature and sulfur pressure by means of equilibration measurements. © Kluwer Academic Publishers 1999 |
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Abstract A thermobalance for studies of the high-temperature sulfidation of metals and alloys is described. This apparatus permits the determination of mass changes in a sulfidized sample as a function of temperature and sulfur vapour pressure. The main parts of this apparatus are the container with liquid sulfur and the reaction chamber with the quartz space and quartz spiral. All parts of the apparatus are equipped with thermostating furnaces. The temperature within the apparatus is controlled with an accuracy of 0.5 K. The quartz spiral (diameter 0.2 mm), consisting of 50 coils (diameter 30 mm), permits the recording of mass changes in the sample (about 200 mg) with an accuracy of $ 10^{-5} $ g. Besides heterogeneous kinetics measurements, it has been shown that the self- and chemical diffusion coefficients or the deviation from stoichiometry of the metal sulfides can also be studied as functions of temperature and sulfur pressure by means of equilibration measurements. © Kluwer Academic Publishers 1999 |
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<?xml version="1.0" encoding="UTF-8"?><collection xmlns="http://www.loc.gov/MARC21/slim"><record><leader>01000caa a22002652 4500</leader><controlfield tag="001">OLC2049747446</controlfield><controlfield tag="003">DE-627</controlfield><controlfield tag="005">20230503165424.0</controlfield><controlfield tag="007">tu</controlfield><controlfield tag="008">200819s1999 xx ||||| 00| ||eng c</controlfield><datafield tag="024" ind1="7" ind2=" "><subfield code="a">10.1023/A:1010154121328</subfield><subfield code="2">doi</subfield></datafield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(DE-627)OLC2049747446</subfield></datafield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(DE-He213)A:1010154121328-p</subfield></datafield><datafield tag="040" ind1=" " ind2=" "><subfield code="a">DE-627</subfield><subfield code="b">ger</subfield><subfield code="c">DE-627</subfield><subfield code="e">rakwb</subfield></datafield><datafield tag="041" ind1=" " ind2=" "><subfield code="a">eng</subfield></datafield><datafield tag="082" ind1="0" ind2="4"><subfield code="a">660</subfield><subfield code="q">VZ</subfield></datafield><datafield tag="100" ind1="1" ind2=" "><subfield code="a">Grzesik, Z.</subfield><subfield code="e">verfasserin</subfield><subfield code="4">aut</subfield></datafield><datafield tag="245" ind1="1" ind2="0"><subfield code="a">Microgravimetric Apparatus for Sulfidation in Pure Sulfur Vapour at High Temperatures</subfield></datafield><datafield tag="264" ind1=" " ind2="1"><subfield code="c">1999</subfield></datafield><datafield tag="336" ind1=" " ind2=" "><subfield code="a">Text</subfield><subfield code="b">txt</subfield><subfield code="2">rdacontent</subfield></datafield><datafield tag="337" ind1=" " ind2=" "><subfield code="a">ohne Hilfsmittel zu benutzen</subfield><subfield code="b">n</subfield><subfield code="2">rdamedia</subfield></datafield><datafield tag="338" ind1=" " ind2=" "><subfield code="a">Band</subfield><subfield code="b">nc</subfield><subfield code="2">rdacarrier</subfield></datafield><datafield tag="500" ind1=" " ind2=" "><subfield code="a">© Kluwer Academic Publishers 1999</subfield></datafield><datafield tag="520" ind1=" " ind2=" "><subfield code="a">Abstract A thermobalance for studies of the high-temperature sulfidation of metals and alloys is described. This apparatus permits the determination of mass changes in a sulfidized sample as a function of temperature and sulfur vapour pressure. The main parts of this apparatus are the container with liquid sulfur and the reaction chamber with the quartz space and quartz spiral. All parts of the apparatus are equipped with thermostating furnaces. The temperature within the apparatus is controlled with an accuracy of 0.5 K. The quartz spiral (diameter 0.2 mm), consisting of 50 coils (diameter 30 mm), permits the recording of mass changes in the sample (about 200 mg) with an accuracy of $ 10^{-5} $ g. Besides heterogeneous kinetics measurements, it has been shown that the self- and chemical diffusion coefficients or the deviation from stoichiometry of the metal sulfides can also be studied as functions of temperature and sulfur pressure by means of equilibration measurements.</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Danielewski, M.</subfield><subfield code="4">aut</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Mrowec, S.</subfield><subfield code="4">aut</subfield></datafield><datafield tag="773" ind1="0" ind2="8"><subfield code="i">Enthalten in</subfield><subfield code="t">Journal of thermal analysis and calorimetry</subfield><subfield code="d">Kluwer Academic Publishers, 1998</subfield><subfield code="g">55(1999), 2 vom: März, Seite 551-558</subfield><subfield code="w">(DE-627)244148767</subfield><subfield code="w">(DE-600)1429493-X</subfield><subfield code="w">(DE-576)066397693</subfield><subfield code="x">1388-6150</subfield><subfield code="7">nnns</subfield></datafield><datafield tag="773" ind1="1" ind2="8"><subfield code="g">volume:55</subfield><subfield code="g">year:1999</subfield><subfield code="g">number:2</subfield><subfield code="g">month:03</subfield><subfield code="g">pages:551-558</subfield></datafield><datafield tag="856" ind1="4" ind2="1"><subfield code="u">https://doi.org/10.1023/A:1010154121328</subfield><subfield code="z">lizenzpflichtig</subfield><subfield code="3">Volltext</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_USEFLAG_A</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">SYSFLAG_A</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_OLC</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">SSG-OLC-TEC</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">SSG-OLC-CHE</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_70</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2006</subfield></datafield><datafield tag="951" ind1=" " ind2=" "><subfield code="a">AR</subfield></datafield><datafield tag="952" ind1=" " ind2=" "><subfield code="d">55</subfield><subfield code="j">1999</subfield><subfield code="e">2</subfield><subfield code="c">03</subfield><subfield code="h">551-558</subfield></datafield></record></collection>
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