DSC and high resolution X-ray diffraction coupling
Abstract Coupling of time-resolved synchrotron X-ray diffraction at both small and wide angles with differential scanning calorimetry is a new technique that allows simultaneous characterization of thermal and structural properties of a sample. The apparatus, called Microcalix, works between –30 and...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Ollivon, M. [verfasserIn] |
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| Format: |
Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2006 |
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| Schlagwörter: |
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| Anmerkung: |
© Springer-Verlag 2006 |
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| Übergeordnetes Werk: |
Enthalten in: Journal of thermal analysis and calorimetry - Kluwer Academic Publishers, 1998, 85(2006), 1 vom: Juli, Seite 219-224 |
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| Übergeordnetes Werk: |
volume:85 ; year:2006 ; number:1 ; month:07 ; pages:219-224 |
| Links: |
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| DOI / URN: |
10.1007/s10973-005-7351-y |
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OLC2049779763 |
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| 520 | |a Abstract Coupling of time-resolved synchrotron X-ray diffraction at both small and wide angles with differential scanning calorimetry is a new technique that allows simultaneous characterization of thermal and structural properties of a sample. The apparatus, called Microcalix, works between –30 and +230°C at scanning rates comprised between 0.01 and 20°C $ min^{–1} $ with a high sensitivity in both measurements using a single sample of small volume (from about 1 to 20 μL). The last version of the instrument is designed for laboratory bench and conventional source but preferably with rotating anode or multilayered mirrors. Measurements under low pressure or under shear as well as recordings of isothermal evolution are also possible. The example of the study of polymorphism of a monounsaturated triglyceride (PPO) will be presented as an application. | ||
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10.1007/s10973-005-7351-y doi (DE-627)OLC2049779763 (DE-He213)s10973-005-7351-y-p DE-627 ger DE-627 rakwb eng 660 VZ Ollivon, M. verfasserin aut DSC and high resolution X-ray diffraction coupling 2006 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Springer-Verlag 2006 Abstract Coupling of time-resolved synchrotron X-ray diffraction at both small and wide angles with differential scanning calorimetry is a new technique that allows simultaneous characterization of thermal and structural properties of a sample. The apparatus, called Microcalix, works between –30 and +230°C at scanning rates comprised between 0.01 and 20°C $ min^{–1} $ with a high sensitivity in both measurements using a single sample of small volume (from about 1 to 20 μL). The last version of the instrument is designed for laboratory bench and conventional source but preferably with rotating anode or multilayered mirrors. Measurements under low pressure or under shear as well as recordings of isothermal evolution are also possible. The example of the study of polymorphism of a monounsaturated triglyceride (PPO) will be presented as an application. lipid structures mesophase and biomaterial studies polymorphism small angle X-ray scattering triacylglycerol Keller, G. aut Bourgaux, C. aut Kalnin, D. aut Villeneuve, P. aut Lesieur, P. aut Enthalten in Journal of thermal analysis and calorimetry Kluwer Academic Publishers, 1998 85(2006), 1 vom: Juli, Seite 219-224 (DE-627)244148767 (DE-600)1429493-X (DE-576)066397693 1388-6150 nnns volume:85 year:2006 number:1 month:07 pages:219-224 https://doi.org/10.1007/s10973-005-7351-y lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE GBV_ILN_70 AR 85 2006 1 07 219-224 |
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Abstract Coupling of time-resolved synchrotron X-ray diffraction at both small and wide angles with differential scanning calorimetry is a new technique that allows simultaneous characterization of thermal and structural properties of a sample. The apparatus, called Microcalix, works between –30 and +230°C at scanning rates comprised between 0.01 and 20°C $ min^{–1} $ with a high sensitivity in both measurements using a single sample of small volume (from about 1 to 20 μL). The last version of the instrument is designed for laboratory bench and conventional source but preferably with rotating anode or multilayered mirrors. Measurements under low pressure or under shear as well as recordings of isothermal evolution are also possible. The example of the study of polymorphism of a monounsaturated triglyceride (PPO) will be presented as an application. © Springer-Verlag 2006 |
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Abstract Coupling of time-resolved synchrotron X-ray diffraction at both small and wide angles with differential scanning calorimetry is a new technique that allows simultaneous characterization of thermal and structural properties of a sample. The apparatus, called Microcalix, works between –30 and +230°C at scanning rates comprised between 0.01 and 20°C $ min^{–1} $ with a high sensitivity in both measurements using a single sample of small volume (from about 1 to 20 μL). The last version of the instrument is designed for laboratory bench and conventional source but preferably with rotating anode or multilayered mirrors. Measurements under low pressure or under shear as well as recordings of isothermal evolution are also possible. The example of the study of polymorphism of a monounsaturated triglyceride (PPO) will be presented as an application. © Springer-Verlag 2006 |
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<?xml version="1.0" encoding="UTF-8"?><collection xmlns="http://www.loc.gov/MARC21/slim"><record><leader>01000caa a22002652 4500</leader><controlfield tag="001">OLC2049779763</controlfield><controlfield tag="003">DE-627</controlfield><controlfield tag="005">20230503165611.0</controlfield><controlfield tag="007">tu</controlfield><controlfield tag="008">200819s2006 xx ||||| 00| ||eng c</controlfield><datafield tag="024" ind1="7" ind2=" "><subfield code="a">10.1007/s10973-005-7351-y</subfield><subfield code="2">doi</subfield></datafield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(DE-627)OLC2049779763</subfield></datafield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(DE-He213)s10973-005-7351-y-p</subfield></datafield><datafield tag="040" ind1=" " ind2=" "><subfield code="a">DE-627</subfield><subfield code="b">ger</subfield><subfield code="c">DE-627</subfield><subfield code="e">rakwb</subfield></datafield><datafield tag="041" ind1=" " ind2=" "><subfield code="a">eng</subfield></datafield><datafield tag="082" ind1="0" ind2="4"><subfield code="a">660</subfield><subfield code="q">VZ</subfield></datafield><datafield tag="100" ind1="1" ind2=" "><subfield code="a">Ollivon, M.</subfield><subfield code="e">verfasserin</subfield><subfield code="4">aut</subfield></datafield><datafield tag="245" ind1="1" ind2="0"><subfield code="a">DSC and high resolution X-ray diffraction coupling</subfield></datafield><datafield tag="264" ind1=" " ind2="1"><subfield code="c">2006</subfield></datafield><datafield tag="336" ind1=" " ind2=" "><subfield code="a">Text</subfield><subfield code="b">txt</subfield><subfield code="2">rdacontent</subfield></datafield><datafield tag="337" ind1=" " ind2=" "><subfield code="a">ohne Hilfsmittel zu benutzen</subfield><subfield code="b">n</subfield><subfield code="2">rdamedia</subfield></datafield><datafield tag="338" ind1=" " ind2=" "><subfield code="a">Band</subfield><subfield code="b">nc</subfield><subfield code="2">rdacarrier</subfield></datafield><datafield tag="500" ind1=" " ind2=" "><subfield code="a">© Springer-Verlag 2006</subfield></datafield><datafield tag="520" ind1=" " ind2=" "><subfield code="a">Abstract Coupling of time-resolved synchrotron X-ray diffraction at both small and wide angles with differential scanning calorimetry is a new technique that allows simultaneous characterization of thermal and structural properties of a sample. The apparatus, called Microcalix, works between –30 and +230°C at scanning rates comprised between 0.01 and 20°C $ min^{–1} $ with a high sensitivity in both measurements using a single sample of small volume (from about 1 to 20 μL). The last version of the instrument is designed for laboratory bench and conventional source but preferably with rotating anode or multilayered mirrors. Measurements under low pressure or under shear as well as recordings of isothermal evolution are also possible. The example of the study of polymorphism of a monounsaturated triglyceride (PPO) will be presented as an application.</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">lipid structures</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">mesophase and biomaterial studies</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">polymorphism</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">small angle X-ray scattering</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">triacylglycerol</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Keller, G.</subfield><subfield code="4">aut</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Bourgaux, C.</subfield><subfield code="4">aut</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Kalnin, D.</subfield><subfield code="4">aut</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Villeneuve, P.</subfield><subfield code="4">aut</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Lesieur, P.</subfield><subfield code="4">aut</subfield></datafield><datafield tag="773" ind1="0" ind2="8"><subfield code="i">Enthalten in</subfield><subfield code="t">Journal of thermal analysis and calorimetry</subfield><subfield code="d">Kluwer Academic Publishers, 1998</subfield><subfield code="g">85(2006), 1 vom: Juli, Seite 219-224</subfield><subfield code="w">(DE-627)244148767</subfield><subfield code="w">(DE-600)1429493-X</subfield><subfield code="w">(DE-576)066397693</subfield><subfield code="x">1388-6150</subfield><subfield code="7">nnns</subfield></datafield><datafield tag="773" ind1="1" ind2="8"><subfield code="g">volume:85</subfield><subfield code="g">year:2006</subfield><subfield code="g">number:1</subfield><subfield code="g">month:07</subfield><subfield code="g">pages:219-224</subfield></datafield><datafield tag="856" ind1="4" ind2="1"><subfield code="u">https://doi.org/10.1007/s10973-005-7351-y</subfield><subfield code="z">lizenzpflichtig</subfield><subfield code="3">Volltext</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_USEFLAG_A</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">SYSFLAG_A</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_OLC</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">SSG-OLC-TEC</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">SSG-OLC-CHE</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_70</subfield></datafield><datafield tag="951" ind1=" " ind2=" "><subfield code="a">AR</subfield></datafield><datafield tag="952" ind1=" " ind2=" "><subfield code="d">85</subfield><subfield code="j">2006</subfield><subfield code="e">1</subfield><subfield code="c">07</subfield><subfield code="h">219-224</subfield></datafield></record></collection>
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