Thermogravimetry study of ion exchange and hydration in layered oxide materials
Abstract The behavior in aqueous solutions of the two types of layered perovskite-like structures, $ NaLnTiO_{4} $ titanates (Ln = Nd, La) belonging to the family of Ruddlesden–Popper phases and $ ANdTa_{2} $$ O_{7} $ tantalates (A = Na, Cs, H) belonging to the family of Dion–Jacobson phases, has be...
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| Autor*in: |
Silyukov, Oleg [verfasserIn] |
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| Format: |
Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2012 |
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| Schlagwörter: |
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| Anmerkung: |
© Akadémiai Kiadó, Budapest, Hungary 2012 |
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| Übergeordnetes Werk: |
Enthalten in: Journal of thermal analysis and calorimetry - Springer Netherlands, 1998, 110(2012), 1 vom: 08. Feb., Seite 187-192 |
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| Übergeordnetes Werk: |
volume:110 ; year:2012 ; number:1 ; day:08 ; month:02 ; pages:187-192 |
| Links: |
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| DOI / URN: |
10.1007/s10973-012-2198-5 |
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| Katalog-ID: |
OLC2049814895 |
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| 520 | |a Abstract The behavior in aqueous solutions of the two types of layered perovskite-like structures, $ NaLnTiO_{4} $ titanates (Ln = Nd, La) belonging to the family of Ruddlesden–Popper phases and $ ANdTa_{2} $$ O_{7} $ tantalates (A = Na, Cs, H) belonging to the family of Dion–Jacobson phases, has been studied by means of thermogravimetric analysis and powder X-ray diffraction. In the case of $ NaLnTiO_{4} $ compounds, the substitution of protons for sodium cations and the water intercalation into the interlayer space of the crystal structure were observed and proton-containing layered oxides with general formula $ H_{x} $$ Na_{1−x} $$ LnTiO_{4} $·y$ H_{2} $O (0.63 < x < 1, 0 < y < 0.74) have been obtained. Investigation on the hydration in layered tantalates $ ANdTa_{2} $$ O_{7} $ (A = H, Na, Cs) showed that $ NaNdTa_{2} $$ O_{7} $ and $ HNdTa_{2} $$ O_{7} $ form compounds intercalated by water molecules. Two steps of water intercalation were observed for $ NaNdTa_{2} $$ O_{7} $ and $ HNdTa_{2} $$ O_{7} $. Stable hydrated compounds $ HNdTa_{2} $$ O_{7} $·0.$ 84H_{2} $O, $ NaNdTa_{2} $$ O_{7} $·0.$ 60H_{2} $O, and $ NaNdTa_{2} $$ O_{7} $·1.$ 35H_{2} $O were synthesized. | ||
| 650 | 4 | |a Thermogravimetry | |
| 650 | 4 | |a Intercalation | |
| 650 | 4 | |a Ion exchange | |
| 650 | 4 | |a Titanates | |
| 650 | 4 | |a Tantalates | |
| 700 | 1 | |a Chislov, Mikhail |4 aut | |
| 700 | 1 | |a Burovikhina, Alena |4 aut | |
| 700 | 1 | |a Utkina, Tatyana |4 aut | |
| 700 | 1 | |a Zvereva, Irina |4 aut | |
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10.1007/s10973-012-2198-5 doi (DE-627)OLC2049814895 (DE-He213)s10973-012-2198-5-p DE-627 ger DE-627 rakwb eng 660 VZ Silyukov, Oleg verfasserin aut Thermogravimetry study of ion exchange and hydration in layered oxide materials 2012 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Akadémiai Kiadó, Budapest, Hungary 2012 Abstract The behavior in aqueous solutions of the two types of layered perovskite-like structures, $ NaLnTiO_{4} $ titanates (Ln = Nd, La) belonging to the family of Ruddlesden–Popper phases and $ ANdTa_{2} $$ O_{7} $ tantalates (A = Na, Cs, H) belonging to the family of Dion–Jacobson phases, has been studied by means of thermogravimetric analysis and powder X-ray diffraction. In the case of $ NaLnTiO_{4} $ compounds, the substitution of protons for sodium cations and the water intercalation into the interlayer space of the crystal structure were observed and proton-containing layered oxides with general formula $ H_{x} $$ Na_{1−x} $$ LnTiO_{4} $·y$ H_{2} $O (0.63 < x < 1, 0 < y < 0.74) have been obtained. Investigation on the hydration in layered tantalates $ ANdTa_{2} $$ O_{7} $ (A = H, Na, Cs) showed that $ NaNdTa_{2} $$ O_{7} $ and $ HNdTa_{2} $$ O_{7} $ form compounds intercalated by water molecules. Two steps of water intercalation were observed for $ NaNdTa_{2} $$ O_{7} $ and $ HNdTa_{2} $$ O_{7} $. Stable hydrated compounds $ HNdTa_{2} $$ O_{7} $·0.$ 84H_{2} $O, $ NaNdTa_{2} $$ O_{7} $·0.$ 60H_{2} $O, and $ NaNdTa_{2} $$ O_{7} $·1.$ 35H_{2} $O were synthesized. Thermogravimetry Intercalation Ion exchange Titanates Tantalates Chislov, Mikhail aut Burovikhina, Alena aut Utkina, Tatyana aut Zvereva, Irina aut Enthalten in Journal of thermal analysis and calorimetry Springer Netherlands, 1998 110(2012), 1 vom: 08. Feb., Seite 187-192 (DE-627)244148767 (DE-600)1429493-X (DE-576)066397693 1388-6150 nnns volume:110 year:2012 number:1 day:08 month:02 pages:187-192 https://doi.org/10.1007/s10973-012-2198-5 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE GBV_ILN_70 AR 110 2012 1 08 02 187-192 |
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10.1007/s10973-012-2198-5 doi (DE-627)OLC2049814895 (DE-He213)s10973-012-2198-5-p DE-627 ger DE-627 rakwb eng 660 VZ Silyukov, Oleg verfasserin aut Thermogravimetry study of ion exchange and hydration in layered oxide materials 2012 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Akadémiai Kiadó, Budapest, Hungary 2012 Abstract The behavior in aqueous solutions of the two types of layered perovskite-like structures, $ NaLnTiO_{4} $ titanates (Ln = Nd, La) belonging to the family of Ruddlesden–Popper phases and $ ANdTa_{2} $$ O_{7} $ tantalates (A = Na, Cs, H) belonging to the family of Dion–Jacobson phases, has been studied by means of thermogravimetric analysis and powder X-ray diffraction. In the case of $ NaLnTiO_{4} $ compounds, the substitution of protons for sodium cations and the water intercalation into the interlayer space of the crystal structure were observed and proton-containing layered oxides with general formula $ H_{x} $$ Na_{1−x} $$ LnTiO_{4} $·y$ H_{2} $O (0.63 < x < 1, 0 < y < 0.74) have been obtained. Investigation on the hydration in layered tantalates $ ANdTa_{2} $$ O_{7} $ (A = H, Na, Cs) showed that $ NaNdTa_{2} $$ O_{7} $ and $ HNdTa_{2} $$ O_{7} $ form compounds intercalated by water molecules. Two steps of water intercalation were observed for $ NaNdTa_{2} $$ O_{7} $ and $ HNdTa_{2} $$ O_{7} $. Stable hydrated compounds $ HNdTa_{2} $$ O_{7} $·0.$ 84H_{2} $O, $ NaNdTa_{2} $$ O_{7} $·0.$ 60H_{2} $O, and $ NaNdTa_{2} $$ O_{7} $·1.$ 35H_{2} $O were synthesized. Thermogravimetry Intercalation Ion exchange Titanates Tantalates Chislov, Mikhail aut Burovikhina, Alena aut Utkina, Tatyana aut Zvereva, Irina aut Enthalten in Journal of thermal analysis and calorimetry Springer Netherlands, 1998 110(2012), 1 vom: 08. Feb., Seite 187-192 (DE-627)244148767 (DE-600)1429493-X (DE-576)066397693 1388-6150 nnns volume:110 year:2012 number:1 day:08 month:02 pages:187-192 https://doi.org/10.1007/s10973-012-2198-5 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE GBV_ILN_70 AR 110 2012 1 08 02 187-192 |
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10.1007/s10973-012-2198-5 doi (DE-627)OLC2049814895 (DE-He213)s10973-012-2198-5-p DE-627 ger DE-627 rakwb eng 660 VZ Silyukov, Oleg verfasserin aut Thermogravimetry study of ion exchange and hydration in layered oxide materials 2012 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Akadémiai Kiadó, Budapest, Hungary 2012 Abstract The behavior in aqueous solutions of the two types of layered perovskite-like structures, $ NaLnTiO_{4} $ titanates (Ln = Nd, La) belonging to the family of Ruddlesden–Popper phases and $ ANdTa_{2} $$ O_{7} $ tantalates (A = Na, Cs, H) belonging to the family of Dion–Jacobson phases, has been studied by means of thermogravimetric analysis and powder X-ray diffraction. In the case of $ NaLnTiO_{4} $ compounds, the substitution of protons for sodium cations and the water intercalation into the interlayer space of the crystal structure were observed and proton-containing layered oxides with general formula $ H_{x} $$ Na_{1−x} $$ LnTiO_{4} $·y$ H_{2} $O (0.63 < x < 1, 0 < y < 0.74) have been obtained. Investigation on the hydration in layered tantalates $ ANdTa_{2} $$ O_{7} $ (A = H, Na, Cs) showed that $ NaNdTa_{2} $$ O_{7} $ and $ HNdTa_{2} $$ O_{7} $ form compounds intercalated by water molecules. Two steps of water intercalation were observed for $ NaNdTa_{2} $$ O_{7} $ and $ HNdTa_{2} $$ O_{7} $. Stable hydrated compounds $ HNdTa_{2} $$ O_{7} $·0.$ 84H_{2} $O, $ NaNdTa_{2} $$ O_{7} $·0.$ 60H_{2} $O, and $ NaNdTa_{2} $$ O_{7} $·1.$ 35H_{2} $O were synthesized. Thermogravimetry Intercalation Ion exchange Titanates Tantalates Chislov, Mikhail aut Burovikhina, Alena aut Utkina, Tatyana aut Zvereva, Irina aut Enthalten in Journal of thermal analysis and calorimetry Springer Netherlands, 1998 110(2012), 1 vom: 08. Feb., Seite 187-192 (DE-627)244148767 (DE-600)1429493-X (DE-576)066397693 1388-6150 nnns volume:110 year:2012 number:1 day:08 month:02 pages:187-192 https://doi.org/10.1007/s10973-012-2198-5 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE GBV_ILN_70 AR 110 2012 1 08 02 187-192 |
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10.1007/s10973-012-2198-5 doi (DE-627)OLC2049814895 (DE-He213)s10973-012-2198-5-p DE-627 ger DE-627 rakwb eng 660 VZ Silyukov, Oleg verfasserin aut Thermogravimetry study of ion exchange and hydration in layered oxide materials 2012 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Akadémiai Kiadó, Budapest, Hungary 2012 Abstract The behavior in aqueous solutions of the two types of layered perovskite-like structures, $ NaLnTiO_{4} $ titanates (Ln = Nd, La) belonging to the family of Ruddlesden–Popper phases and $ ANdTa_{2} $$ O_{7} $ tantalates (A = Na, Cs, H) belonging to the family of Dion–Jacobson phases, has been studied by means of thermogravimetric analysis and powder X-ray diffraction. In the case of $ NaLnTiO_{4} $ compounds, the substitution of protons for sodium cations and the water intercalation into the interlayer space of the crystal structure were observed and proton-containing layered oxides with general formula $ H_{x} $$ Na_{1−x} $$ LnTiO_{4} $·y$ H_{2} $O (0.63 < x < 1, 0 < y < 0.74) have been obtained. Investigation on the hydration in layered tantalates $ ANdTa_{2} $$ O_{7} $ (A = H, Na, Cs) showed that $ NaNdTa_{2} $$ O_{7} $ and $ HNdTa_{2} $$ O_{7} $ form compounds intercalated by water molecules. Two steps of water intercalation were observed for $ NaNdTa_{2} $$ O_{7} $ and $ HNdTa_{2} $$ O_{7} $. Stable hydrated compounds $ HNdTa_{2} $$ O_{7} $·0.$ 84H_{2} $O, $ NaNdTa_{2} $$ O_{7} $·0.$ 60H_{2} $O, and $ NaNdTa_{2} $$ O_{7} $·1.$ 35H_{2} $O were synthesized. Thermogravimetry Intercalation Ion exchange Titanates Tantalates Chislov, Mikhail aut Burovikhina, Alena aut Utkina, Tatyana aut Zvereva, Irina aut Enthalten in Journal of thermal analysis and calorimetry Springer Netherlands, 1998 110(2012), 1 vom: 08. Feb., Seite 187-192 (DE-627)244148767 (DE-600)1429493-X (DE-576)066397693 1388-6150 nnns volume:110 year:2012 number:1 day:08 month:02 pages:187-192 https://doi.org/10.1007/s10973-012-2198-5 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE GBV_ILN_70 AR 110 2012 1 08 02 187-192 |
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10.1007/s10973-012-2198-5 doi (DE-627)OLC2049814895 (DE-He213)s10973-012-2198-5-p DE-627 ger DE-627 rakwb eng 660 VZ Silyukov, Oleg verfasserin aut Thermogravimetry study of ion exchange and hydration in layered oxide materials 2012 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Akadémiai Kiadó, Budapest, Hungary 2012 Abstract The behavior in aqueous solutions of the two types of layered perovskite-like structures, $ NaLnTiO_{4} $ titanates (Ln = Nd, La) belonging to the family of Ruddlesden–Popper phases and $ ANdTa_{2} $$ O_{7} $ tantalates (A = Na, Cs, H) belonging to the family of Dion–Jacobson phases, has been studied by means of thermogravimetric analysis and powder X-ray diffraction. In the case of $ NaLnTiO_{4} $ compounds, the substitution of protons for sodium cations and the water intercalation into the interlayer space of the crystal structure were observed and proton-containing layered oxides with general formula $ H_{x} $$ Na_{1−x} $$ LnTiO_{4} $·y$ H_{2} $O (0.63 < x < 1, 0 < y < 0.74) have been obtained. Investigation on the hydration in layered tantalates $ ANdTa_{2} $$ O_{7} $ (A = H, Na, Cs) showed that $ NaNdTa_{2} $$ O_{7} $ and $ HNdTa_{2} $$ O_{7} $ form compounds intercalated by water molecules. Two steps of water intercalation were observed for $ NaNdTa_{2} $$ O_{7} $ and $ HNdTa_{2} $$ O_{7} $. Stable hydrated compounds $ HNdTa_{2} $$ O_{7} $·0.$ 84H_{2} $O, $ NaNdTa_{2} $$ O_{7} $·0.$ 60H_{2} $O, and $ NaNdTa_{2} $$ O_{7} $·1.$ 35H_{2} $O were synthesized. Thermogravimetry Intercalation Ion exchange Titanates Tantalates Chislov, Mikhail aut Burovikhina, Alena aut Utkina, Tatyana aut Zvereva, Irina aut Enthalten in Journal of thermal analysis and calorimetry Springer Netherlands, 1998 110(2012), 1 vom: 08. Feb., Seite 187-192 (DE-627)244148767 (DE-600)1429493-X (DE-576)066397693 1388-6150 nnns volume:110 year:2012 number:1 day:08 month:02 pages:187-192 https://doi.org/10.1007/s10973-012-2198-5 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE GBV_ILN_70 AR 110 2012 1 08 02 187-192 |
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660 VZ Thermogravimetry study of ion exchange and hydration in layered oxide materials Thermogravimetry Intercalation Ion exchange Titanates Tantalates |
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Thermogravimetry study of ion exchange and hydration in layered oxide materials |
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Thermogravimetry study of ion exchange and hydration in layered oxide materials |
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Silyukov, Oleg |
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Journal of thermal analysis and calorimetry |
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2012 |
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Silyukov, Oleg Chislov, Mikhail Burovikhina, Alena Utkina, Tatyana Zvereva, Irina |
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thermogravimetry study of ion exchange and hydration in layered oxide materials |
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Thermogravimetry study of ion exchange and hydration in layered oxide materials |
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Abstract The behavior in aqueous solutions of the two types of layered perovskite-like structures, $ NaLnTiO_{4} $ titanates (Ln = Nd, La) belonging to the family of Ruddlesden–Popper phases and $ ANdTa_{2} $$ O_{7} $ tantalates (A = Na, Cs, H) belonging to the family of Dion–Jacobson phases, has been studied by means of thermogravimetric analysis and powder X-ray diffraction. In the case of $ NaLnTiO_{4} $ compounds, the substitution of protons for sodium cations and the water intercalation into the interlayer space of the crystal structure were observed and proton-containing layered oxides with general formula $ H_{x} $$ Na_{1−x} $$ LnTiO_{4} $·y$ H_{2} $O (0.63 < x < 1, 0 < y < 0.74) have been obtained. Investigation on the hydration in layered tantalates $ ANdTa_{2} $$ O_{7} $ (A = H, Na, Cs) showed that $ NaNdTa_{2} $$ O_{7} $ and $ HNdTa_{2} $$ O_{7} $ form compounds intercalated by water molecules. Two steps of water intercalation were observed for $ NaNdTa_{2} $$ O_{7} $ and $ HNdTa_{2} $$ O_{7} $. Stable hydrated compounds $ HNdTa_{2} $$ O_{7} $·0.$ 84H_{2} $O, $ NaNdTa_{2} $$ O_{7} $·0.$ 60H_{2} $O, and $ NaNdTa_{2} $$ O_{7} $·1.$ 35H_{2} $O were synthesized. © Akadémiai Kiadó, Budapest, Hungary 2012 |
| abstractGer |
Abstract The behavior in aqueous solutions of the two types of layered perovskite-like structures, $ NaLnTiO_{4} $ titanates (Ln = Nd, La) belonging to the family of Ruddlesden–Popper phases and $ ANdTa_{2} $$ O_{7} $ tantalates (A = Na, Cs, H) belonging to the family of Dion–Jacobson phases, has been studied by means of thermogravimetric analysis and powder X-ray diffraction. In the case of $ NaLnTiO_{4} $ compounds, the substitution of protons for sodium cations and the water intercalation into the interlayer space of the crystal structure were observed and proton-containing layered oxides with general formula $ H_{x} $$ Na_{1−x} $$ LnTiO_{4} $·y$ H_{2} $O (0.63 < x < 1, 0 < y < 0.74) have been obtained. Investigation on the hydration in layered tantalates $ ANdTa_{2} $$ O_{7} $ (A = H, Na, Cs) showed that $ NaNdTa_{2} $$ O_{7} $ and $ HNdTa_{2} $$ O_{7} $ form compounds intercalated by water molecules. Two steps of water intercalation were observed for $ NaNdTa_{2} $$ O_{7} $ and $ HNdTa_{2} $$ O_{7} $. Stable hydrated compounds $ HNdTa_{2} $$ O_{7} $·0.$ 84H_{2} $O, $ NaNdTa_{2} $$ O_{7} $·0.$ 60H_{2} $O, and $ NaNdTa_{2} $$ O_{7} $·1.$ 35H_{2} $O were synthesized. © Akadémiai Kiadó, Budapest, Hungary 2012 |
| abstract_unstemmed |
Abstract The behavior in aqueous solutions of the two types of layered perovskite-like structures, $ NaLnTiO_{4} $ titanates (Ln = Nd, La) belonging to the family of Ruddlesden–Popper phases and $ ANdTa_{2} $$ O_{7} $ tantalates (A = Na, Cs, H) belonging to the family of Dion–Jacobson phases, has been studied by means of thermogravimetric analysis and powder X-ray diffraction. In the case of $ NaLnTiO_{4} $ compounds, the substitution of protons for sodium cations and the water intercalation into the interlayer space of the crystal structure were observed and proton-containing layered oxides with general formula $ H_{x} $$ Na_{1−x} $$ LnTiO_{4} $·y$ H_{2} $O (0.63 < x < 1, 0 < y < 0.74) have been obtained. Investigation on the hydration in layered tantalates $ ANdTa_{2} $$ O_{7} $ (A = H, Na, Cs) showed that $ NaNdTa_{2} $$ O_{7} $ and $ HNdTa_{2} $$ O_{7} $ form compounds intercalated by water molecules. Two steps of water intercalation were observed for $ NaNdTa_{2} $$ O_{7} $ and $ HNdTa_{2} $$ O_{7} $. Stable hydrated compounds $ HNdTa_{2} $$ O_{7} $·0.$ 84H_{2} $O, $ NaNdTa_{2} $$ O_{7} $·0.$ 60H_{2} $O, and $ NaNdTa_{2} $$ O_{7} $·1.$ 35H_{2} $O were synthesized. © Akadémiai Kiadó, Budapest, Hungary 2012 |
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Thermogravimetry study of ion exchange and hydration in layered oxide materials |
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Chislov, Mikhail Burovikhina, Alena Utkina, Tatyana Zvereva, Irina |
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