Influence of the zirconia transformation on the thermal behavior of zircon–zirconia composites
Abstract During a heating–cooling cycle, zirconia ($ ZrO_{2} $) undergoes a martensitic transformation from monoclinic to tetragonal structure phases, which presents special hysteresis loop in the dilatometry curve at temperatures between 800 and 1100 °C. Monoclinic zirconia (m-$ ZrO_{2} $) particle...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Rendtorff, Nicolas M. [verfasserIn] |
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| Format: |
Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2011 |
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| Schlagwörter: |
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| Anmerkung: |
© Akadémiai Kiadó, Budapest, Hungary 2011 |
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| Übergeordnetes Werk: |
Enthalten in: Journal of thermal analysis and calorimetry - Springer Netherlands, 1998, 110(2011), 2 vom: 23. Sept., Seite 695-705 |
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| Übergeordnetes Werk: |
volume:110 ; year:2011 ; number:2 ; day:23 ; month:09 ; pages:695-705 |
| Links: |
|---|
| DOI / URN: |
10.1007/s10973-011-1906-x |
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OLC2049815522 |
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| 520 | |a Abstract During a heating–cooling cycle, zirconia ($ ZrO_{2} $) undergoes a martensitic transformation from monoclinic to tetragonal structure phases, which presents special hysteresis loop in the dilatometry curve at temperatures between 800 and 1100 °C. Monoclinic zirconia (m-$ ZrO_{2} $) particles reinforced ceramic matrix composites not always present this behavior. In order to elucidate this fact a series of zircon–zirconia ($ ZrSiO_{4} $–$ ZrO_{2} $) ceramic composites have been obtained by slip casting and characterized. The final properties were also correlated with the zirconia content (0–30 vol.%). The influence of the martensitic transformation (m–t) in well-dispersed zirconia grains ceramic composite on the thermal behavior was analyzed. Thermal behavior evaluation was carried out; the correlation between the thermal expansion coefficients with the zirconia content showed a deviation from the mixing rule applied. A hysteresis loop was observed in the reversible dilatometric curve of composites with enough zirconia grains (≥10 vol.%). Over this threshold the zirconia content is correlated with the loop area. The transformation temperatures were evaluated and correlated with the zirconia addition. When detected the m–t temperature transformation is slightly influenced by the zirconia content (due to the previously evaluated decrease in the material stiffness) and similar to the temperature reported in literature. The reverse (cooling) transformation temperature is strongly decreased by the ceramic matrix. The DTA results are consistent with the dilatometric analysis, but this technique showed more reliable results. Particularly the endothermic m–t transformation temperature showed to be easily detected even when the only m-$ ZrO_{2} $ present was the product of the slight thermal dissociation of the zircon during the processing of the pure zircon material. | ||
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10.1007/s10973-011-1906-x doi (DE-627)OLC2049815522 (DE-He213)s10973-011-1906-x-p DE-627 ger DE-627 rakwb eng 660 VZ Rendtorff, Nicolas M. verfasserin aut Influence of the zirconia transformation on the thermal behavior of zircon–zirconia composites 2011 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Akadémiai Kiadó, Budapest, Hungary 2011 Abstract During a heating–cooling cycle, zirconia ($ ZrO_{2} $) undergoes a martensitic transformation from monoclinic to tetragonal structure phases, which presents special hysteresis loop in the dilatometry curve at temperatures between 800 and 1100 °C. Monoclinic zirconia (m-$ ZrO_{2} $) particles reinforced ceramic matrix composites not always present this behavior. In order to elucidate this fact a series of zircon–zirconia ($ ZrSiO_{4} $–$ ZrO_{2} $) ceramic composites have been obtained by slip casting and characterized. The final properties were also correlated with the zirconia content (0–30 vol.%). The influence of the martensitic transformation (m–t) in well-dispersed zirconia grains ceramic composite on the thermal behavior was analyzed. Thermal behavior evaluation was carried out; the correlation between the thermal expansion coefficients with the zirconia content showed a deviation from the mixing rule applied. A hysteresis loop was observed in the reversible dilatometric curve of composites with enough zirconia grains (≥10 vol.%). Over this threshold the zirconia content is correlated with the loop area. The transformation temperatures were evaluated and correlated with the zirconia addition. When detected the m–t temperature transformation is slightly influenced by the zirconia content (due to the previously evaluated decrease in the material stiffness) and similar to the temperature reported in literature. The reverse (cooling) transformation temperature is strongly decreased by the ceramic matrix. The DTA results are consistent with the dilatometric analysis, but this technique showed more reliable results. Particularly the endothermic m–t transformation temperature showed to be easily detected even when the only m-$ ZrO_{2} $ present was the product of the slight thermal dissociation of the zircon during the processing of the pure zircon material. Composites Zirconia Thermal behavior Suarez, Gustavo aut Sakka, Yoshio aut Aglietti, Esteban F. aut Enthalten in Journal of thermal analysis and calorimetry Springer Netherlands, 1998 110(2011), 2 vom: 23. Sept., Seite 695-705 (DE-627)244148767 (DE-600)1429493-X (DE-576)066397693 1388-6150 nnns volume:110 year:2011 number:2 day:23 month:09 pages:695-705 https://doi.org/10.1007/s10973-011-1906-x lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE GBV_ILN_70 AR 110 2011 2 23 09 695-705 |
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10.1007/s10973-011-1906-x doi (DE-627)OLC2049815522 (DE-He213)s10973-011-1906-x-p DE-627 ger DE-627 rakwb eng 660 VZ Rendtorff, Nicolas M. verfasserin aut Influence of the zirconia transformation on the thermal behavior of zircon–zirconia composites 2011 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Akadémiai Kiadó, Budapest, Hungary 2011 Abstract During a heating–cooling cycle, zirconia ($ ZrO_{2} $) undergoes a martensitic transformation from monoclinic to tetragonal structure phases, which presents special hysteresis loop in the dilatometry curve at temperatures between 800 and 1100 °C. Monoclinic zirconia (m-$ ZrO_{2} $) particles reinforced ceramic matrix composites not always present this behavior. In order to elucidate this fact a series of zircon–zirconia ($ ZrSiO_{4} $–$ ZrO_{2} $) ceramic composites have been obtained by slip casting and characterized. The final properties were also correlated with the zirconia content (0–30 vol.%). The influence of the martensitic transformation (m–t) in well-dispersed zirconia grains ceramic composite on the thermal behavior was analyzed. Thermal behavior evaluation was carried out; the correlation between the thermal expansion coefficients with the zirconia content showed a deviation from the mixing rule applied. A hysteresis loop was observed in the reversible dilatometric curve of composites with enough zirconia grains (≥10 vol.%). Over this threshold the zirconia content is correlated with the loop area. The transformation temperatures were evaluated and correlated with the zirconia addition. When detected the m–t temperature transformation is slightly influenced by the zirconia content (due to the previously evaluated decrease in the material stiffness) and similar to the temperature reported in literature. The reverse (cooling) transformation temperature is strongly decreased by the ceramic matrix. The DTA results are consistent with the dilatometric analysis, but this technique showed more reliable results. Particularly the endothermic m–t transformation temperature showed to be easily detected even when the only m-$ ZrO_{2} $ present was the product of the slight thermal dissociation of the zircon during the processing of the pure zircon material. Composites Zirconia Thermal behavior Suarez, Gustavo aut Sakka, Yoshio aut Aglietti, Esteban F. aut Enthalten in Journal of thermal analysis and calorimetry Springer Netherlands, 1998 110(2011), 2 vom: 23. Sept., Seite 695-705 (DE-627)244148767 (DE-600)1429493-X (DE-576)066397693 1388-6150 nnns volume:110 year:2011 number:2 day:23 month:09 pages:695-705 https://doi.org/10.1007/s10973-011-1906-x lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE GBV_ILN_70 AR 110 2011 2 23 09 695-705 |
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10.1007/s10973-011-1906-x doi (DE-627)OLC2049815522 (DE-He213)s10973-011-1906-x-p DE-627 ger DE-627 rakwb eng 660 VZ Rendtorff, Nicolas M. verfasserin aut Influence of the zirconia transformation on the thermal behavior of zircon–zirconia composites 2011 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Akadémiai Kiadó, Budapest, Hungary 2011 Abstract During a heating–cooling cycle, zirconia ($ ZrO_{2} $) undergoes a martensitic transformation from monoclinic to tetragonal structure phases, which presents special hysteresis loop in the dilatometry curve at temperatures between 800 and 1100 °C. Monoclinic zirconia (m-$ ZrO_{2} $) particles reinforced ceramic matrix composites not always present this behavior. In order to elucidate this fact a series of zircon–zirconia ($ ZrSiO_{4} $–$ ZrO_{2} $) ceramic composites have been obtained by slip casting and characterized. The final properties were also correlated with the zirconia content (0–30 vol.%). The influence of the martensitic transformation (m–t) in well-dispersed zirconia grains ceramic composite on the thermal behavior was analyzed. Thermal behavior evaluation was carried out; the correlation between the thermal expansion coefficients with the zirconia content showed a deviation from the mixing rule applied. A hysteresis loop was observed in the reversible dilatometric curve of composites with enough zirconia grains (≥10 vol.%). Over this threshold the zirconia content is correlated with the loop area. The transformation temperatures were evaluated and correlated with the zirconia addition. When detected the m–t temperature transformation is slightly influenced by the zirconia content (due to the previously evaluated decrease in the material stiffness) and similar to the temperature reported in literature. The reverse (cooling) transformation temperature is strongly decreased by the ceramic matrix. The DTA results are consistent with the dilatometric analysis, but this technique showed more reliable results. Particularly the endothermic m–t transformation temperature showed to be easily detected even when the only m-$ ZrO_{2} $ present was the product of the slight thermal dissociation of the zircon during the processing of the pure zircon material. Composites Zirconia Thermal behavior Suarez, Gustavo aut Sakka, Yoshio aut Aglietti, Esteban F. aut Enthalten in Journal of thermal analysis and calorimetry Springer Netherlands, 1998 110(2011), 2 vom: 23. Sept., Seite 695-705 (DE-627)244148767 (DE-600)1429493-X (DE-576)066397693 1388-6150 nnns volume:110 year:2011 number:2 day:23 month:09 pages:695-705 https://doi.org/10.1007/s10973-011-1906-x lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE GBV_ILN_70 AR 110 2011 2 23 09 695-705 |
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10.1007/s10973-011-1906-x doi (DE-627)OLC2049815522 (DE-He213)s10973-011-1906-x-p DE-627 ger DE-627 rakwb eng 660 VZ Rendtorff, Nicolas M. verfasserin aut Influence of the zirconia transformation on the thermal behavior of zircon–zirconia composites 2011 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Akadémiai Kiadó, Budapest, Hungary 2011 Abstract During a heating–cooling cycle, zirconia ($ ZrO_{2} $) undergoes a martensitic transformation from monoclinic to tetragonal structure phases, which presents special hysteresis loop in the dilatometry curve at temperatures between 800 and 1100 °C. Monoclinic zirconia (m-$ ZrO_{2} $) particles reinforced ceramic matrix composites not always present this behavior. In order to elucidate this fact a series of zircon–zirconia ($ ZrSiO_{4} $–$ ZrO_{2} $) ceramic composites have been obtained by slip casting and characterized. The final properties were also correlated with the zirconia content (0–30 vol.%). The influence of the martensitic transformation (m–t) in well-dispersed zirconia grains ceramic composite on the thermal behavior was analyzed. Thermal behavior evaluation was carried out; the correlation between the thermal expansion coefficients with the zirconia content showed a deviation from the mixing rule applied. A hysteresis loop was observed in the reversible dilatometric curve of composites with enough zirconia grains (≥10 vol.%). Over this threshold the zirconia content is correlated with the loop area. The transformation temperatures were evaluated and correlated with the zirconia addition. When detected the m–t temperature transformation is slightly influenced by the zirconia content (due to the previously evaluated decrease in the material stiffness) and similar to the temperature reported in literature. The reverse (cooling) transformation temperature is strongly decreased by the ceramic matrix. The DTA results are consistent with the dilatometric analysis, but this technique showed more reliable results. Particularly the endothermic m–t transformation temperature showed to be easily detected even when the only m-$ ZrO_{2} $ present was the product of the slight thermal dissociation of the zircon during the processing of the pure zircon material. Composites Zirconia Thermal behavior Suarez, Gustavo aut Sakka, Yoshio aut Aglietti, Esteban F. aut Enthalten in Journal of thermal analysis and calorimetry Springer Netherlands, 1998 110(2011), 2 vom: 23. Sept., Seite 695-705 (DE-627)244148767 (DE-600)1429493-X (DE-576)066397693 1388-6150 nnns volume:110 year:2011 number:2 day:23 month:09 pages:695-705 https://doi.org/10.1007/s10973-011-1906-x lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE GBV_ILN_70 AR 110 2011 2 23 09 695-705 |
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10.1007/s10973-011-1906-x doi (DE-627)OLC2049815522 (DE-He213)s10973-011-1906-x-p DE-627 ger DE-627 rakwb eng 660 VZ Rendtorff, Nicolas M. verfasserin aut Influence of the zirconia transformation on the thermal behavior of zircon–zirconia composites 2011 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Akadémiai Kiadó, Budapest, Hungary 2011 Abstract During a heating–cooling cycle, zirconia ($ ZrO_{2} $) undergoes a martensitic transformation from monoclinic to tetragonal structure phases, which presents special hysteresis loop in the dilatometry curve at temperatures between 800 and 1100 °C. Monoclinic zirconia (m-$ ZrO_{2} $) particles reinforced ceramic matrix composites not always present this behavior. In order to elucidate this fact a series of zircon–zirconia ($ ZrSiO_{4} $–$ ZrO_{2} $) ceramic composites have been obtained by slip casting and characterized. The final properties were also correlated with the zirconia content (0–30 vol.%). The influence of the martensitic transformation (m–t) in well-dispersed zirconia grains ceramic composite on the thermal behavior was analyzed. Thermal behavior evaluation was carried out; the correlation between the thermal expansion coefficients with the zirconia content showed a deviation from the mixing rule applied. A hysteresis loop was observed in the reversible dilatometric curve of composites with enough zirconia grains (≥10 vol.%). Over this threshold the zirconia content is correlated with the loop area. The transformation temperatures were evaluated and correlated with the zirconia addition. When detected the m–t temperature transformation is slightly influenced by the zirconia content (due to the previously evaluated decrease in the material stiffness) and similar to the temperature reported in literature. The reverse (cooling) transformation temperature is strongly decreased by the ceramic matrix. The DTA results are consistent with the dilatometric analysis, but this technique showed more reliable results. Particularly the endothermic m–t transformation temperature showed to be easily detected even when the only m-$ ZrO_{2} $ present was the product of the slight thermal dissociation of the zircon during the processing of the pure zircon material. Composites Zirconia Thermal behavior Suarez, Gustavo aut Sakka, Yoshio aut Aglietti, Esteban F. aut Enthalten in Journal of thermal analysis and calorimetry Springer Netherlands, 1998 110(2011), 2 vom: 23. Sept., Seite 695-705 (DE-627)244148767 (DE-600)1429493-X (DE-576)066397693 1388-6150 nnns volume:110 year:2011 number:2 day:23 month:09 pages:695-705 https://doi.org/10.1007/s10973-011-1906-x lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE GBV_ILN_70 AR 110 2011 2 23 09 695-705 |
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Influence of the zirconia transformation on the thermal behavior of zircon–zirconia composites |
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Influence of the zirconia transformation on the thermal behavior of zircon–zirconia composites |
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Rendtorff, Nicolas M. |
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Journal of thermal analysis and calorimetry |
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2011 |
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Rendtorff, Nicolas M. Suarez, Gustavo Sakka, Yoshio Aglietti, Esteban F. |
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Rendtorff, Nicolas M. |
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10.1007/s10973-011-1906-x |
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660 |
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influence of the zirconia transformation on the thermal behavior of zircon–zirconia composites |
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Influence of the zirconia transformation on the thermal behavior of zircon–zirconia composites |
| abstract |
Abstract During a heating–cooling cycle, zirconia ($ ZrO_{2} $) undergoes a martensitic transformation from monoclinic to tetragonal structure phases, which presents special hysteresis loop in the dilatometry curve at temperatures between 800 and 1100 °C. Monoclinic zirconia (m-$ ZrO_{2} $) particles reinforced ceramic matrix composites not always present this behavior. In order to elucidate this fact a series of zircon–zirconia ($ ZrSiO_{4} $–$ ZrO_{2} $) ceramic composites have been obtained by slip casting and characterized. The final properties were also correlated with the zirconia content (0–30 vol.%). The influence of the martensitic transformation (m–t) in well-dispersed zirconia grains ceramic composite on the thermal behavior was analyzed. Thermal behavior evaluation was carried out; the correlation between the thermal expansion coefficients with the zirconia content showed a deviation from the mixing rule applied. A hysteresis loop was observed in the reversible dilatometric curve of composites with enough zirconia grains (≥10 vol.%). Over this threshold the zirconia content is correlated with the loop area. The transformation temperatures were evaluated and correlated with the zirconia addition. When detected the m–t temperature transformation is slightly influenced by the zirconia content (due to the previously evaluated decrease in the material stiffness) and similar to the temperature reported in literature. The reverse (cooling) transformation temperature is strongly decreased by the ceramic matrix. The DTA results are consistent with the dilatometric analysis, but this technique showed more reliable results. Particularly the endothermic m–t transformation temperature showed to be easily detected even when the only m-$ ZrO_{2} $ present was the product of the slight thermal dissociation of the zircon during the processing of the pure zircon material. © Akadémiai Kiadó, Budapest, Hungary 2011 |
| abstractGer |
Abstract During a heating–cooling cycle, zirconia ($ ZrO_{2} $) undergoes a martensitic transformation from monoclinic to tetragonal structure phases, which presents special hysteresis loop in the dilatometry curve at temperatures between 800 and 1100 °C. Monoclinic zirconia (m-$ ZrO_{2} $) particles reinforced ceramic matrix composites not always present this behavior. In order to elucidate this fact a series of zircon–zirconia ($ ZrSiO_{4} $–$ ZrO_{2} $) ceramic composites have been obtained by slip casting and characterized. The final properties were also correlated with the zirconia content (0–30 vol.%). The influence of the martensitic transformation (m–t) in well-dispersed zirconia grains ceramic composite on the thermal behavior was analyzed. Thermal behavior evaluation was carried out; the correlation between the thermal expansion coefficients with the zirconia content showed a deviation from the mixing rule applied. A hysteresis loop was observed in the reversible dilatometric curve of composites with enough zirconia grains (≥10 vol.%). Over this threshold the zirconia content is correlated with the loop area. The transformation temperatures were evaluated and correlated with the zirconia addition. When detected the m–t temperature transformation is slightly influenced by the zirconia content (due to the previously evaluated decrease in the material stiffness) and similar to the temperature reported in literature. The reverse (cooling) transformation temperature is strongly decreased by the ceramic matrix. The DTA results are consistent with the dilatometric analysis, but this technique showed more reliable results. Particularly the endothermic m–t transformation temperature showed to be easily detected even when the only m-$ ZrO_{2} $ present was the product of the slight thermal dissociation of the zircon during the processing of the pure zircon material. © Akadémiai Kiadó, Budapest, Hungary 2011 |
| abstract_unstemmed |
Abstract During a heating–cooling cycle, zirconia ($ ZrO_{2} $) undergoes a martensitic transformation from monoclinic to tetragonal structure phases, which presents special hysteresis loop in the dilatometry curve at temperatures between 800 and 1100 °C. Monoclinic zirconia (m-$ ZrO_{2} $) particles reinforced ceramic matrix composites not always present this behavior. In order to elucidate this fact a series of zircon–zirconia ($ ZrSiO_{4} $–$ ZrO_{2} $) ceramic composites have been obtained by slip casting and characterized. The final properties were also correlated with the zirconia content (0–30 vol.%). The influence of the martensitic transformation (m–t) in well-dispersed zirconia grains ceramic composite on the thermal behavior was analyzed. Thermal behavior evaluation was carried out; the correlation between the thermal expansion coefficients with the zirconia content showed a deviation from the mixing rule applied. A hysteresis loop was observed in the reversible dilatometric curve of composites with enough zirconia grains (≥10 vol.%). Over this threshold the zirconia content is correlated with the loop area. The transformation temperatures were evaluated and correlated with the zirconia addition. When detected the m–t temperature transformation is slightly influenced by the zirconia content (due to the previously evaluated decrease in the material stiffness) and similar to the temperature reported in literature. The reverse (cooling) transformation temperature is strongly decreased by the ceramic matrix. The DTA results are consistent with the dilatometric analysis, but this technique showed more reliable results. Particularly the endothermic m–t transformation temperature showed to be easily detected even when the only m-$ ZrO_{2} $ present was the product of the slight thermal dissociation of the zircon during the processing of the pure zircon material. © Akadémiai Kiadó, Budapest, Hungary 2011 |
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Influence of the zirconia transformation on the thermal behavior of zircon–zirconia composites |
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Suarez, Gustavo Sakka, Yoshio Aglietti, Esteban F. |
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