Kinetic study of dehydration of calcium oxalate trihydrate
Abstract The dehydration of calcium oxalate trihydrate was studied using DSC method and open sample crucibles. The dehydration proceeds in two steps where first two molecules of water are released around 80 °C and consequently the last molecule of water is released at a temperature around 130 °C. Th...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Honcová, P. [verfasserIn] |
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| Format: |
Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2015 |
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| Schlagwörter: |
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| Anmerkung: |
© Akadémiai Kiadó, Budapest, Hungary 2015 |
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| Übergeordnetes Werk: |
Enthalten in: Journal of thermal analysis and calorimetry - Springer Netherlands, 1998, 124(2015), 1 vom: 03. Nov., Seite 151-158 |
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| Übergeordnetes Werk: |
volume:124 ; year:2015 ; number:1 ; day:03 ; month:11 ; pages:151-158 |
| Links: |
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| DOI / URN: |
10.1007/s10973-015-5110-2 |
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OLC2049844662 |
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| 520 | |a Abstract The dehydration of calcium oxalate trihydrate was studied using DSC method and open sample crucibles. The dehydration proceeds in two steps where first two molecules of water are released around 80 °C and consequently the last molecule of water is released at a temperature around 130 °C. The kinetic analysis of overlapping peaks was performed, and the apparent activation energy, pre-exponential factor, and kinetic exponents of kinetic model (reaction order model) were evaluated for both effects. | ||
| 650 | 4 | |a Calcium oxalate trihydrate | |
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| 700 | 1 | |a Beneš, L. |4 aut | |
| 700 | 1 | |a Honc, D. |4 aut | |
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10.1007/s10973-015-5110-2 doi (DE-627)OLC2049844662 (DE-He213)s10973-015-5110-2-p DE-627 ger DE-627 rakwb eng 660 VZ Honcová, P. verfasserin aut Kinetic study of dehydration of calcium oxalate trihydrate 2015 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Akadémiai Kiadó, Budapest, Hungary 2015 Abstract The dehydration of calcium oxalate trihydrate was studied using DSC method and open sample crucibles. The dehydration proceeds in two steps where first two molecules of water are released around 80 °C and consequently the last molecule of water is released at a temperature around 130 °C. The kinetic analysis of overlapping peaks was performed, and the apparent activation energy, pre-exponential factor, and kinetic exponents of kinetic model (reaction order model) were evaluated for both effects. Calcium oxalate trihydrate Dehydration Kinetics DSC Reaction order Deconvolution Svoboda, R. aut Pilný, P. aut Sádovská, G. aut Barták, J. aut Beneš, L. aut Honc, D. aut Enthalten in Journal of thermal analysis and calorimetry Springer Netherlands, 1998 124(2015), 1 vom: 03. Nov., Seite 151-158 (DE-627)244148767 (DE-600)1429493-X (DE-576)066397693 1388-6150 nnns volume:124 year:2015 number:1 day:03 month:11 pages:151-158 https://doi.org/10.1007/s10973-015-5110-2 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE GBV_ILN_70 AR 124 2015 1 03 11 151-158 |
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10.1007/s10973-015-5110-2 doi (DE-627)OLC2049844662 (DE-He213)s10973-015-5110-2-p DE-627 ger DE-627 rakwb eng 660 VZ Honcová, P. verfasserin aut Kinetic study of dehydration of calcium oxalate trihydrate 2015 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Akadémiai Kiadó, Budapest, Hungary 2015 Abstract The dehydration of calcium oxalate trihydrate was studied using DSC method and open sample crucibles. The dehydration proceeds in two steps where first two molecules of water are released around 80 °C and consequently the last molecule of water is released at a temperature around 130 °C. The kinetic analysis of overlapping peaks was performed, and the apparent activation energy, pre-exponential factor, and kinetic exponents of kinetic model (reaction order model) were evaluated for both effects. Calcium oxalate trihydrate Dehydration Kinetics DSC Reaction order Deconvolution Svoboda, R. aut Pilný, P. aut Sádovská, G. aut Barták, J. aut Beneš, L. aut Honc, D. aut Enthalten in Journal of thermal analysis and calorimetry Springer Netherlands, 1998 124(2015), 1 vom: 03. Nov., Seite 151-158 (DE-627)244148767 (DE-600)1429493-X (DE-576)066397693 1388-6150 nnns volume:124 year:2015 number:1 day:03 month:11 pages:151-158 https://doi.org/10.1007/s10973-015-5110-2 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE GBV_ILN_70 AR 124 2015 1 03 11 151-158 |
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10.1007/s10973-015-5110-2 doi (DE-627)OLC2049844662 (DE-He213)s10973-015-5110-2-p DE-627 ger DE-627 rakwb eng 660 VZ Honcová, P. verfasserin aut Kinetic study of dehydration of calcium oxalate trihydrate 2015 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Akadémiai Kiadó, Budapest, Hungary 2015 Abstract The dehydration of calcium oxalate trihydrate was studied using DSC method and open sample crucibles. The dehydration proceeds in two steps where first two molecules of water are released around 80 °C and consequently the last molecule of water is released at a temperature around 130 °C. The kinetic analysis of overlapping peaks was performed, and the apparent activation energy, pre-exponential factor, and kinetic exponents of kinetic model (reaction order model) were evaluated for both effects. Calcium oxalate trihydrate Dehydration Kinetics DSC Reaction order Deconvolution Svoboda, R. aut Pilný, P. aut Sádovská, G. aut Barták, J. aut Beneš, L. aut Honc, D. aut Enthalten in Journal of thermal analysis and calorimetry Springer Netherlands, 1998 124(2015), 1 vom: 03. Nov., Seite 151-158 (DE-627)244148767 (DE-600)1429493-X (DE-576)066397693 1388-6150 nnns volume:124 year:2015 number:1 day:03 month:11 pages:151-158 https://doi.org/10.1007/s10973-015-5110-2 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE GBV_ILN_70 AR 124 2015 1 03 11 151-158 |
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10.1007/s10973-015-5110-2 doi (DE-627)OLC2049844662 (DE-He213)s10973-015-5110-2-p DE-627 ger DE-627 rakwb eng 660 VZ Honcová, P. verfasserin aut Kinetic study of dehydration of calcium oxalate trihydrate 2015 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Akadémiai Kiadó, Budapest, Hungary 2015 Abstract The dehydration of calcium oxalate trihydrate was studied using DSC method and open sample crucibles. The dehydration proceeds in two steps where first two molecules of water are released around 80 °C and consequently the last molecule of water is released at a temperature around 130 °C. The kinetic analysis of overlapping peaks was performed, and the apparent activation energy, pre-exponential factor, and kinetic exponents of kinetic model (reaction order model) were evaluated for both effects. Calcium oxalate trihydrate Dehydration Kinetics DSC Reaction order Deconvolution Svoboda, R. aut Pilný, P. aut Sádovská, G. aut Barták, J. aut Beneš, L. aut Honc, D. aut Enthalten in Journal of thermal analysis and calorimetry Springer Netherlands, 1998 124(2015), 1 vom: 03. Nov., Seite 151-158 (DE-627)244148767 (DE-600)1429493-X (DE-576)066397693 1388-6150 nnns volume:124 year:2015 number:1 day:03 month:11 pages:151-158 https://doi.org/10.1007/s10973-015-5110-2 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE GBV_ILN_70 AR 124 2015 1 03 11 151-158 |
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10.1007/s10973-015-5110-2 doi (DE-627)OLC2049844662 (DE-He213)s10973-015-5110-2-p DE-627 ger DE-627 rakwb eng 660 VZ Honcová, P. verfasserin aut Kinetic study of dehydration of calcium oxalate trihydrate 2015 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Akadémiai Kiadó, Budapest, Hungary 2015 Abstract The dehydration of calcium oxalate trihydrate was studied using DSC method and open sample crucibles. The dehydration proceeds in two steps where first two molecules of water are released around 80 °C and consequently the last molecule of water is released at a temperature around 130 °C. The kinetic analysis of overlapping peaks was performed, and the apparent activation energy, pre-exponential factor, and kinetic exponents of kinetic model (reaction order model) were evaluated for both effects. Calcium oxalate trihydrate Dehydration Kinetics DSC Reaction order Deconvolution Svoboda, R. aut Pilný, P. aut Sádovská, G. aut Barták, J. aut Beneš, L. aut Honc, D. aut Enthalten in Journal of thermal analysis and calorimetry Springer Netherlands, 1998 124(2015), 1 vom: 03. Nov., Seite 151-158 (DE-627)244148767 (DE-600)1429493-X (DE-576)066397693 1388-6150 nnns volume:124 year:2015 number:1 day:03 month:11 pages:151-158 https://doi.org/10.1007/s10973-015-5110-2 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE GBV_ILN_70 AR 124 2015 1 03 11 151-158 |
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Abstract The dehydration of calcium oxalate trihydrate was studied using DSC method and open sample crucibles. The dehydration proceeds in two steps where first two molecules of water are released around 80 °C and consequently the last molecule of water is released at a temperature around 130 °C. The kinetic analysis of overlapping peaks was performed, and the apparent activation energy, pre-exponential factor, and kinetic exponents of kinetic model (reaction order model) were evaluated for both effects. © Akadémiai Kiadó, Budapest, Hungary 2015 |
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Abstract The dehydration of calcium oxalate trihydrate was studied using DSC method and open sample crucibles. The dehydration proceeds in two steps where first two molecules of water are released around 80 °C and consequently the last molecule of water is released at a temperature around 130 °C. The kinetic analysis of overlapping peaks was performed, and the apparent activation energy, pre-exponential factor, and kinetic exponents of kinetic model (reaction order model) were evaluated for both effects. © Akadémiai Kiadó, Budapest, Hungary 2015 |
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Abstract The dehydration of calcium oxalate trihydrate was studied using DSC method and open sample crucibles. The dehydration proceeds in two steps where first two molecules of water are released around 80 °C and consequently the last molecule of water is released at a temperature around 130 °C. The kinetic analysis of overlapping peaks was performed, and the apparent activation energy, pre-exponential factor, and kinetic exponents of kinetic model (reaction order model) were evaluated for both effects. © Akadémiai Kiadó, Budapest, Hungary 2015 |
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<?xml version="1.0" encoding="UTF-8"?><collection xmlns="http://www.loc.gov/MARC21/slim"><record><leader>01000caa a22002652 4500</leader><controlfield tag="001">OLC2049844662</controlfield><controlfield tag="003">DE-627</controlfield><controlfield tag="005">20230503170125.0</controlfield><controlfield tag="007">tu</controlfield><controlfield tag="008">200820s2015 xx ||||| 00| ||eng c</controlfield><datafield tag="024" ind1="7" ind2=" "><subfield code="a">10.1007/s10973-015-5110-2</subfield><subfield code="2">doi</subfield></datafield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(DE-627)OLC2049844662</subfield></datafield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(DE-He213)s10973-015-5110-2-p</subfield></datafield><datafield tag="040" ind1=" " ind2=" "><subfield code="a">DE-627</subfield><subfield code="b">ger</subfield><subfield code="c">DE-627</subfield><subfield code="e">rakwb</subfield></datafield><datafield tag="041" ind1=" " ind2=" "><subfield code="a">eng</subfield></datafield><datafield tag="082" ind1="0" ind2="4"><subfield code="a">660</subfield><subfield code="q">VZ</subfield></datafield><datafield tag="100" ind1="1" ind2=" "><subfield code="a">Honcová, P.</subfield><subfield code="e">verfasserin</subfield><subfield code="4">aut</subfield></datafield><datafield tag="245" ind1="1" ind2="0"><subfield code="a">Kinetic study of dehydration of calcium oxalate trihydrate</subfield></datafield><datafield tag="264" ind1=" " ind2="1"><subfield code="c">2015</subfield></datafield><datafield tag="336" ind1=" " ind2=" "><subfield code="a">Text</subfield><subfield code="b">txt</subfield><subfield code="2">rdacontent</subfield></datafield><datafield tag="337" ind1=" " ind2=" "><subfield code="a">ohne Hilfsmittel zu benutzen</subfield><subfield code="b">n</subfield><subfield code="2">rdamedia</subfield></datafield><datafield tag="338" ind1=" " ind2=" "><subfield code="a">Band</subfield><subfield code="b">nc</subfield><subfield code="2">rdacarrier</subfield></datafield><datafield tag="500" ind1=" " ind2=" "><subfield code="a">© Akadémiai Kiadó, Budapest, Hungary 2015</subfield></datafield><datafield tag="520" ind1=" " ind2=" "><subfield code="a">Abstract The dehydration of calcium oxalate trihydrate was studied using DSC method and open sample crucibles. The dehydration proceeds in two steps where first two molecules of water are released around 80 °C and consequently the last molecule of water is released at a temperature around 130 °C. The kinetic analysis of overlapping peaks was performed, and the apparent activation energy, pre-exponential factor, and kinetic exponents of kinetic model (reaction order model) were evaluated for both effects.</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Calcium oxalate trihydrate</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Dehydration</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Kinetics</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">DSC</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Reaction order</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Deconvolution</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Svoboda, R.</subfield><subfield code="4">aut</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Pilný, P.</subfield><subfield code="4">aut</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Sádovská, G.</subfield><subfield code="4">aut</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Barták, J.</subfield><subfield code="4">aut</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Beneš, L.</subfield><subfield code="4">aut</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Honc, D.</subfield><subfield code="4">aut</subfield></datafield><datafield tag="773" ind1="0" ind2="8"><subfield code="i">Enthalten in</subfield><subfield code="t">Journal of thermal analysis and calorimetry</subfield><subfield code="d">Springer Netherlands, 1998</subfield><subfield code="g">124(2015), 1 vom: 03. Nov., Seite 151-158</subfield><subfield code="w">(DE-627)244148767</subfield><subfield code="w">(DE-600)1429493-X</subfield><subfield code="w">(DE-576)066397693</subfield><subfield code="x">1388-6150</subfield><subfield code="7">nnns</subfield></datafield><datafield tag="773" ind1="1" ind2="8"><subfield code="g">volume:124</subfield><subfield code="g">year:2015</subfield><subfield code="g">number:1</subfield><subfield code="g">day:03</subfield><subfield code="g">month:11</subfield><subfield code="g">pages:151-158</subfield></datafield><datafield tag="856" ind1="4" ind2="1"><subfield code="u">https://doi.org/10.1007/s10973-015-5110-2</subfield><subfield code="z">lizenzpflichtig</subfield><subfield code="3">Volltext</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_USEFLAG_A</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">SYSFLAG_A</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_OLC</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">SSG-OLC-TEC</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">SSG-OLC-CHE</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_70</subfield></datafield><datafield tag="951" ind1=" " ind2=" "><subfield code="a">AR</subfield></datafield><datafield tag="952" ind1=" " ind2=" "><subfield code="d">124</subfield><subfield code="j">2015</subfield><subfield code="e">1</subfield><subfield code="b">03</subfield><subfield code="c">11</subfield><subfield code="h">151-158</subfield></datafield></record></collection>
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