Solid-state reaction of strontium oxalate with uranium oxalate
Abstract Uranyl oxalate and strontium oxalate were synthesized and characterized. Reaction of strontium oxalate with uranyl oxalate was studied by employing simultaneous TG/DTA. It has been observed that uranyl oxalate decomposes into mixture of $ U_{3} $$ O_{8} $ and $ UO_{2.13} $ with the evolutio...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Arora, Charu [verfasserIn] |
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| Format: |
Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2015 |
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| Schlagwörter: |
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| Anmerkung: |
© Akadémiai Kiadó, Budapest, Hungary 2015 |
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| Übergeordnetes Werk: |
Enthalten in: Journal of thermal analysis and calorimetry - Springer Netherlands, 1998, 124(2015), 1 vom: 16. Dez., Seite 43-49 |
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| Übergeordnetes Werk: |
volume:124 ; year:2015 ; number:1 ; day:16 ; month:12 ; pages:43-49 |
| Links: |
|---|
| DOI / URN: |
10.1007/s10973-015-5103-1 |
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OLC2049844786 |
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| 520 | |a Abstract Uranyl oxalate and strontium oxalate were synthesized and characterized. Reaction of strontium oxalate with uranyl oxalate was studied by employing simultaneous TG/DTA. It has been observed that uranyl oxalate decomposes into mixture of $ U_{3} $$ O_{8} $ and $ UO_{2.13} $ with the evolution of carbon monoxide, oxygen and carbon dioxide in the temperature range of 573–673 K, but beyond this temperature $ U_{3} $$ O_{8} $ and $ UO_{2.13} $ appeared as intermediates and the final product has been found to be $ UO_{2.12} $. Oxalates of strontium and uranium were taken in the mole ratio of 1:1 to study the solid-state reaction. The products of the reactions have been identified. In the presence of uranium oxide, strontium oxalate first decomposes to strontium carbonate followed by the reaction of the carbonate with uranium oxide at a relatively high temperature during the next step in TG. XRD characterization of the intermediates and end products indicated that $ SrUO_{4} $ is formed, which gets partially reduced to $ SrUO_{3} $ at elevated temperature. | ||
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| 700 | 1 | |a Ramarao, Gollamudi |4 aut | |
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10.1007/s10973-015-5103-1 doi (DE-627)OLC2049844786 (DE-He213)s10973-015-5103-1-p DE-627 ger DE-627 rakwb eng 660 VZ Arora, Charu verfasserin aut Solid-state reaction of strontium oxalate with uranium oxalate 2015 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Akadémiai Kiadó, Budapest, Hungary 2015 Abstract Uranyl oxalate and strontium oxalate were synthesized and characterized. Reaction of strontium oxalate with uranyl oxalate was studied by employing simultaneous TG/DTA. It has been observed that uranyl oxalate decomposes into mixture of $ U_{3} $$ O_{8} $ and $ UO_{2.13} $ with the evolution of carbon monoxide, oxygen and carbon dioxide in the temperature range of 573–673 K, but beyond this temperature $ U_{3} $$ O_{8} $ and $ UO_{2.13} $ appeared as intermediates and the final product has been found to be $ UO_{2.12} $. Oxalates of strontium and uranium were taken in the mole ratio of 1:1 to study the solid-state reaction. The products of the reactions have been identified. In the presence of uranium oxide, strontium oxalate first decomposes to strontium carbonate followed by the reaction of the carbonate with uranium oxide at a relatively high temperature during the next step in TG. XRD characterization of the intermediates and end products indicated that $ SrUO_{4} $ is formed, which gets partially reduced to $ SrUO_{3} $ at elevated temperature. Solid-state reaction Thermal decomposition Thermogravimetric analysis Sharma, Aditi aut Soni, Sanju aut Naik, Yeshwant aut Ramarao, Gollamudi aut Enthalten in Journal of thermal analysis and calorimetry Springer Netherlands, 1998 124(2015), 1 vom: 16. Dez., Seite 43-49 (DE-627)244148767 (DE-600)1429493-X (DE-576)066397693 1388-6150 nnns volume:124 year:2015 number:1 day:16 month:12 pages:43-49 https://doi.org/10.1007/s10973-015-5103-1 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE GBV_ILN_70 AR 124 2015 1 16 12 43-49 |
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10.1007/s10973-015-5103-1 doi (DE-627)OLC2049844786 (DE-He213)s10973-015-5103-1-p DE-627 ger DE-627 rakwb eng 660 VZ Arora, Charu verfasserin aut Solid-state reaction of strontium oxalate with uranium oxalate 2015 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Akadémiai Kiadó, Budapest, Hungary 2015 Abstract Uranyl oxalate and strontium oxalate were synthesized and characterized. Reaction of strontium oxalate with uranyl oxalate was studied by employing simultaneous TG/DTA. It has been observed that uranyl oxalate decomposes into mixture of $ U_{3} $$ O_{8} $ and $ UO_{2.13} $ with the evolution of carbon monoxide, oxygen and carbon dioxide in the temperature range of 573–673 K, but beyond this temperature $ U_{3} $$ O_{8} $ and $ UO_{2.13} $ appeared as intermediates and the final product has been found to be $ UO_{2.12} $. Oxalates of strontium and uranium were taken in the mole ratio of 1:1 to study the solid-state reaction. The products of the reactions have been identified. In the presence of uranium oxide, strontium oxalate first decomposes to strontium carbonate followed by the reaction of the carbonate with uranium oxide at a relatively high temperature during the next step in TG. XRD characterization of the intermediates and end products indicated that $ SrUO_{4} $ is formed, which gets partially reduced to $ SrUO_{3} $ at elevated temperature. Solid-state reaction Thermal decomposition Thermogravimetric analysis Sharma, Aditi aut Soni, Sanju aut Naik, Yeshwant aut Ramarao, Gollamudi aut Enthalten in Journal of thermal analysis and calorimetry Springer Netherlands, 1998 124(2015), 1 vom: 16. Dez., Seite 43-49 (DE-627)244148767 (DE-600)1429493-X (DE-576)066397693 1388-6150 nnns volume:124 year:2015 number:1 day:16 month:12 pages:43-49 https://doi.org/10.1007/s10973-015-5103-1 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE GBV_ILN_70 AR 124 2015 1 16 12 43-49 |
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10.1007/s10973-015-5103-1 doi (DE-627)OLC2049844786 (DE-He213)s10973-015-5103-1-p DE-627 ger DE-627 rakwb eng 660 VZ Arora, Charu verfasserin aut Solid-state reaction of strontium oxalate with uranium oxalate 2015 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Akadémiai Kiadó, Budapest, Hungary 2015 Abstract Uranyl oxalate and strontium oxalate were synthesized and characterized. Reaction of strontium oxalate with uranyl oxalate was studied by employing simultaneous TG/DTA. It has been observed that uranyl oxalate decomposes into mixture of $ U_{3} $$ O_{8} $ and $ UO_{2.13} $ with the evolution of carbon monoxide, oxygen and carbon dioxide in the temperature range of 573–673 K, but beyond this temperature $ U_{3} $$ O_{8} $ and $ UO_{2.13} $ appeared as intermediates and the final product has been found to be $ UO_{2.12} $. Oxalates of strontium and uranium were taken in the mole ratio of 1:1 to study the solid-state reaction. The products of the reactions have been identified. In the presence of uranium oxide, strontium oxalate first decomposes to strontium carbonate followed by the reaction of the carbonate with uranium oxide at a relatively high temperature during the next step in TG. XRD characterization of the intermediates and end products indicated that $ SrUO_{4} $ is formed, which gets partially reduced to $ SrUO_{3} $ at elevated temperature. Solid-state reaction Thermal decomposition Thermogravimetric analysis Sharma, Aditi aut Soni, Sanju aut Naik, Yeshwant aut Ramarao, Gollamudi aut Enthalten in Journal of thermal analysis and calorimetry Springer Netherlands, 1998 124(2015), 1 vom: 16. Dez., Seite 43-49 (DE-627)244148767 (DE-600)1429493-X (DE-576)066397693 1388-6150 nnns volume:124 year:2015 number:1 day:16 month:12 pages:43-49 https://doi.org/10.1007/s10973-015-5103-1 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE GBV_ILN_70 AR 124 2015 1 16 12 43-49 |
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10.1007/s10973-015-5103-1 doi (DE-627)OLC2049844786 (DE-He213)s10973-015-5103-1-p DE-627 ger DE-627 rakwb eng 660 VZ Arora, Charu verfasserin aut Solid-state reaction of strontium oxalate with uranium oxalate 2015 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Akadémiai Kiadó, Budapest, Hungary 2015 Abstract Uranyl oxalate and strontium oxalate were synthesized and characterized. Reaction of strontium oxalate with uranyl oxalate was studied by employing simultaneous TG/DTA. It has been observed that uranyl oxalate decomposes into mixture of $ U_{3} $$ O_{8} $ and $ UO_{2.13} $ with the evolution of carbon monoxide, oxygen and carbon dioxide in the temperature range of 573–673 K, but beyond this temperature $ U_{3} $$ O_{8} $ and $ UO_{2.13} $ appeared as intermediates and the final product has been found to be $ UO_{2.12} $. Oxalates of strontium and uranium were taken in the mole ratio of 1:1 to study the solid-state reaction. The products of the reactions have been identified. In the presence of uranium oxide, strontium oxalate first decomposes to strontium carbonate followed by the reaction of the carbonate with uranium oxide at a relatively high temperature during the next step in TG. XRD characterization of the intermediates and end products indicated that $ SrUO_{4} $ is formed, which gets partially reduced to $ SrUO_{3} $ at elevated temperature. Solid-state reaction Thermal decomposition Thermogravimetric analysis Sharma, Aditi aut Soni, Sanju aut Naik, Yeshwant aut Ramarao, Gollamudi aut Enthalten in Journal of thermal analysis and calorimetry Springer Netherlands, 1998 124(2015), 1 vom: 16. Dez., Seite 43-49 (DE-627)244148767 (DE-600)1429493-X (DE-576)066397693 1388-6150 nnns volume:124 year:2015 number:1 day:16 month:12 pages:43-49 https://doi.org/10.1007/s10973-015-5103-1 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE GBV_ILN_70 AR 124 2015 1 16 12 43-49 |
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10.1007/s10973-015-5103-1 doi (DE-627)OLC2049844786 (DE-He213)s10973-015-5103-1-p DE-627 ger DE-627 rakwb eng 660 VZ Arora, Charu verfasserin aut Solid-state reaction of strontium oxalate with uranium oxalate 2015 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Akadémiai Kiadó, Budapest, Hungary 2015 Abstract Uranyl oxalate and strontium oxalate were synthesized and characterized. Reaction of strontium oxalate with uranyl oxalate was studied by employing simultaneous TG/DTA. It has been observed that uranyl oxalate decomposes into mixture of $ U_{3} $$ O_{8} $ and $ UO_{2.13} $ with the evolution of carbon monoxide, oxygen and carbon dioxide in the temperature range of 573–673 K, but beyond this temperature $ U_{3} $$ O_{8} $ and $ UO_{2.13} $ appeared as intermediates and the final product has been found to be $ UO_{2.12} $. Oxalates of strontium and uranium were taken in the mole ratio of 1:1 to study the solid-state reaction. The products of the reactions have been identified. In the presence of uranium oxide, strontium oxalate first decomposes to strontium carbonate followed by the reaction of the carbonate with uranium oxide at a relatively high temperature during the next step in TG. XRD characterization of the intermediates and end products indicated that $ SrUO_{4} $ is formed, which gets partially reduced to $ SrUO_{3} $ at elevated temperature. Solid-state reaction Thermal decomposition Thermogravimetric analysis Sharma, Aditi aut Soni, Sanju aut Naik, Yeshwant aut Ramarao, Gollamudi aut Enthalten in Journal of thermal analysis and calorimetry Springer Netherlands, 1998 124(2015), 1 vom: 16. Dez., Seite 43-49 (DE-627)244148767 (DE-600)1429493-X (DE-576)066397693 1388-6150 nnns volume:124 year:2015 number:1 day:16 month:12 pages:43-49 https://doi.org/10.1007/s10973-015-5103-1 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE GBV_ILN_70 AR 124 2015 1 16 12 43-49 |
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Solid-state reaction of strontium oxalate with uranium oxalate |
| abstract |
Abstract Uranyl oxalate and strontium oxalate were synthesized and characterized. Reaction of strontium oxalate with uranyl oxalate was studied by employing simultaneous TG/DTA. It has been observed that uranyl oxalate decomposes into mixture of $ U_{3} $$ O_{8} $ and $ UO_{2.13} $ with the evolution of carbon monoxide, oxygen and carbon dioxide in the temperature range of 573–673 K, but beyond this temperature $ U_{3} $$ O_{8} $ and $ UO_{2.13} $ appeared as intermediates and the final product has been found to be $ UO_{2.12} $. Oxalates of strontium and uranium were taken in the mole ratio of 1:1 to study the solid-state reaction. The products of the reactions have been identified. In the presence of uranium oxide, strontium oxalate first decomposes to strontium carbonate followed by the reaction of the carbonate with uranium oxide at a relatively high temperature during the next step in TG. XRD characterization of the intermediates and end products indicated that $ SrUO_{4} $ is formed, which gets partially reduced to $ SrUO_{3} $ at elevated temperature. © Akadémiai Kiadó, Budapest, Hungary 2015 |
| abstractGer |
Abstract Uranyl oxalate and strontium oxalate were synthesized and characterized. Reaction of strontium oxalate with uranyl oxalate was studied by employing simultaneous TG/DTA. It has been observed that uranyl oxalate decomposes into mixture of $ U_{3} $$ O_{8} $ and $ UO_{2.13} $ with the evolution of carbon monoxide, oxygen and carbon dioxide in the temperature range of 573–673 K, but beyond this temperature $ U_{3} $$ O_{8} $ and $ UO_{2.13} $ appeared as intermediates and the final product has been found to be $ UO_{2.12} $. Oxalates of strontium and uranium were taken in the mole ratio of 1:1 to study the solid-state reaction. The products of the reactions have been identified. In the presence of uranium oxide, strontium oxalate first decomposes to strontium carbonate followed by the reaction of the carbonate with uranium oxide at a relatively high temperature during the next step in TG. XRD characterization of the intermediates and end products indicated that $ SrUO_{4} $ is formed, which gets partially reduced to $ SrUO_{3} $ at elevated temperature. © Akadémiai Kiadó, Budapest, Hungary 2015 |
| abstract_unstemmed |
Abstract Uranyl oxalate and strontium oxalate were synthesized and characterized. Reaction of strontium oxalate with uranyl oxalate was studied by employing simultaneous TG/DTA. It has been observed that uranyl oxalate decomposes into mixture of $ U_{3} $$ O_{8} $ and $ UO_{2.13} $ with the evolution of carbon monoxide, oxygen and carbon dioxide in the temperature range of 573–673 K, but beyond this temperature $ U_{3} $$ O_{8} $ and $ UO_{2.13} $ appeared as intermediates and the final product has been found to be $ UO_{2.12} $. Oxalates of strontium and uranium were taken in the mole ratio of 1:1 to study the solid-state reaction. The products of the reactions have been identified. In the presence of uranium oxide, strontium oxalate first decomposes to strontium carbonate followed by the reaction of the carbonate with uranium oxide at a relatively high temperature during the next step in TG. XRD characterization of the intermediates and end products indicated that $ SrUO_{4} $ is formed, which gets partially reduced to $ SrUO_{3} $ at elevated temperature. © Akadémiai Kiadó, Budapest, Hungary 2015 |
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| title_short |
Solid-state reaction of strontium oxalate with uranium oxalate |
| url |
https://doi.org/10.1007/s10973-015-5103-1 |
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| author2 |
Sharma, Aditi Soni, Sanju Naik, Yeshwant Ramarao, Gollamudi |
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Sharma, Aditi Soni, Sanju Naik, Yeshwant Ramarao, Gollamudi |
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| doi_str |
10.1007/s10973-015-5103-1 |
| up_date |
2024-07-04T00:14:09.577Z |
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