Quality standardization of herbal medicines of Spondias dulcis Parkinson using analytical and microbiological analysis
Abstract The quality control is vital for the safety and efficacy of herbal medicines. However, the quality of standardization is most difficult because the studies do not cover this step. The objective of this study was quality standardization of herbal drugs of Spondias dulcis Parkinson. The leave...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Fernandes, Felipe Hugo Alencar [verfasserIn] |
|---|
| Format: |
Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2018 |
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| Schlagwörter: |
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| Anmerkung: |
© Akadémiai Kiadó, Budapest, Hungary 2018 |
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| Übergeordnetes Werk: |
Enthalten in: Journal of thermal analysis and calorimetry - Springer International Publishing, 1998, 134(2018), 3 vom: 26. Juni, Seite 1923-1928 |
|---|---|
| Übergeordnetes Werk: |
volume:134 ; year:2018 ; number:3 ; day:26 ; month:06 ; pages:1923-1928 |
| Links: |
|---|
| DOI / URN: |
10.1007/s10973-018-7486-2 |
|---|
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OLC2049866321 |
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| 520 | |a Abstract The quality control is vital for the safety and efficacy of herbal medicines. However, the quality of standardization is most difficult because the studies do not cover this step. The objective of this study was quality standardization of herbal drugs of Spondias dulcis Parkinson. The leaves were dried and ground to a powder. The plant drug was evaluated by parameters of mean particle size (417.85 μm), apparent density (0.37 ± 0.01 g $ mL^{−1} $), moisture content (7.96 ± 0.35%), loss on drying (7.33 ± 0.09%), pH (3.90 ± 0.01), total ash (12.66 ± 0.23%), acid insoluble ash (3.22 ± 0.20%) and aqueous extractives (24.00 ± 3.28%). Phytochemical screening revealed the presence of flavonoids and tannins. Microbiological analysis presented a total count within the recommended limits and the absence of pathogenic microorganisms. The infrared spectroscopy (FTIR) and thermal analysis (TG/DTA) showed that physical and chemical processes occurred. The FTIR fingerprint has been characterized by characteristic peaks. The TG curves present six steps, and DTA curve presents three events. The results provide the scientific data for the proper identification and establishment of standards for future investigations and applications. | ||
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10.1007/s10973-018-7486-2 doi (DE-627)OLC2049866321 (DE-He213)s10973-018-7486-2-p DE-627 ger DE-627 rakwb eng 660 VZ Fernandes, Felipe Hugo Alencar verfasserin (orcid)0000-0002-7210-4349 aut Quality standardization of herbal medicines of Spondias dulcis Parkinson using analytical and microbiological analysis 2018 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Akadémiai Kiadó, Budapest, Hungary 2018 Abstract The quality control is vital for the safety and efficacy of herbal medicines. However, the quality of standardization is most difficult because the studies do not cover this step. The objective of this study was quality standardization of herbal drugs of Spondias dulcis Parkinson. The leaves were dried and ground to a powder. The plant drug was evaluated by parameters of mean particle size (417.85 μm), apparent density (0.37 ± 0.01 g $ mL^{−1} $), moisture content (7.96 ± 0.35%), loss on drying (7.33 ± 0.09%), pH (3.90 ± 0.01), total ash (12.66 ± 0.23%), acid insoluble ash (3.22 ± 0.20%) and aqueous extractives (24.00 ± 3.28%). Phytochemical screening revealed the presence of flavonoids and tannins. Microbiological analysis presented a total count within the recommended limits and the absence of pathogenic microorganisms. The infrared spectroscopy (FTIR) and thermal analysis (TG/DTA) showed that physical and chemical processes occurred. The FTIR fingerprint has been characterized by characteristic peaks. The TG curves present six steps, and DTA curve presents three events. The results provide the scientific data for the proper identification and establishment of standards for future investigations and applications. Herbal drugs Thermoanalytical characterization Physicochemical characterization Boylan, Fabio aut Salgado, Hérida Regina Nunes aut Enthalten in Journal of thermal analysis and calorimetry Springer International Publishing, 1998 134(2018), 3 vom: 26. Juni, Seite 1923-1928 (DE-627)244148767 (DE-600)1429493-X (DE-576)066397693 1388-6150 nnns volume:134 year:2018 number:3 day:26 month:06 pages:1923-1928 https://doi.org/10.1007/s10973-018-7486-2 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE SSG-OLC-PHA SSG-OLC-DE-84 GBV_ILN_70 AR 134 2018 3 26 06 1923-1928 |
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10.1007/s10973-018-7486-2 doi (DE-627)OLC2049866321 (DE-He213)s10973-018-7486-2-p DE-627 ger DE-627 rakwb eng 660 VZ Fernandes, Felipe Hugo Alencar verfasserin (orcid)0000-0002-7210-4349 aut Quality standardization of herbal medicines of Spondias dulcis Parkinson using analytical and microbiological analysis 2018 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Akadémiai Kiadó, Budapest, Hungary 2018 Abstract The quality control is vital for the safety and efficacy of herbal medicines. However, the quality of standardization is most difficult because the studies do not cover this step. The objective of this study was quality standardization of herbal drugs of Spondias dulcis Parkinson. The leaves were dried and ground to a powder. The plant drug was evaluated by parameters of mean particle size (417.85 μm), apparent density (0.37 ± 0.01 g $ mL^{−1} $), moisture content (7.96 ± 0.35%), loss on drying (7.33 ± 0.09%), pH (3.90 ± 0.01), total ash (12.66 ± 0.23%), acid insoluble ash (3.22 ± 0.20%) and aqueous extractives (24.00 ± 3.28%). Phytochemical screening revealed the presence of flavonoids and tannins. Microbiological analysis presented a total count within the recommended limits and the absence of pathogenic microorganisms. The infrared spectroscopy (FTIR) and thermal analysis (TG/DTA) showed that physical and chemical processes occurred. The FTIR fingerprint has been characterized by characteristic peaks. The TG curves present six steps, and DTA curve presents three events. The results provide the scientific data for the proper identification and establishment of standards for future investigations and applications. Herbal drugs Thermoanalytical characterization Physicochemical characterization Boylan, Fabio aut Salgado, Hérida Regina Nunes aut Enthalten in Journal of thermal analysis and calorimetry Springer International Publishing, 1998 134(2018), 3 vom: 26. Juni, Seite 1923-1928 (DE-627)244148767 (DE-600)1429493-X (DE-576)066397693 1388-6150 nnns volume:134 year:2018 number:3 day:26 month:06 pages:1923-1928 https://doi.org/10.1007/s10973-018-7486-2 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE SSG-OLC-PHA SSG-OLC-DE-84 GBV_ILN_70 AR 134 2018 3 26 06 1923-1928 |
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10.1007/s10973-018-7486-2 doi (DE-627)OLC2049866321 (DE-He213)s10973-018-7486-2-p DE-627 ger DE-627 rakwb eng 660 VZ Fernandes, Felipe Hugo Alencar verfasserin (orcid)0000-0002-7210-4349 aut Quality standardization of herbal medicines of Spondias dulcis Parkinson using analytical and microbiological analysis 2018 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Akadémiai Kiadó, Budapest, Hungary 2018 Abstract The quality control is vital for the safety and efficacy of herbal medicines. However, the quality of standardization is most difficult because the studies do not cover this step. The objective of this study was quality standardization of herbal drugs of Spondias dulcis Parkinson. The leaves were dried and ground to a powder. The plant drug was evaluated by parameters of mean particle size (417.85 μm), apparent density (0.37 ± 0.01 g $ mL^{−1} $), moisture content (7.96 ± 0.35%), loss on drying (7.33 ± 0.09%), pH (3.90 ± 0.01), total ash (12.66 ± 0.23%), acid insoluble ash (3.22 ± 0.20%) and aqueous extractives (24.00 ± 3.28%). Phytochemical screening revealed the presence of flavonoids and tannins. Microbiological analysis presented a total count within the recommended limits and the absence of pathogenic microorganisms. The infrared spectroscopy (FTIR) and thermal analysis (TG/DTA) showed that physical and chemical processes occurred. The FTIR fingerprint has been characterized by characteristic peaks. The TG curves present six steps, and DTA curve presents three events. The results provide the scientific data for the proper identification and establishment of standards for future investigations and applications. Herbal drugs Thermoanalytical characterization Physicochemical characterization Boylan, Fabio aut Salgado, Hérida Regina Nunes aut Enthalten in Journal of thermal analysis and calorimetry Springer International Publishing, 1998 134(2018), 3 vom: 26. Juni, Seite 1923-1928 (DE-627)244148767 (DE-600)1429493-X (DE-576)066397693 1388-6150 nnns volume:134 year:2018 number:3 day:26 month:06 pages:1923-1928 https://doi.org/10.1007/s10973-018-7486-2 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE SSG-OLC-PHA SSG-OLC-DE-84 GBV_ILN_70 AR 134 2018 3 26 06 1923-1928 |
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10.1007/s10973-018-7486-2 doi (DE-627)OLC2049866321 (DE-He213)s10973-018-7486-2-p DE-627 ger DE-627 rakwb eng 660 VZ Fernandes, Felipe Hugo Alencar verfasserin (orcid)0000-0002-7210-4349 aut Quality standardization of herbal medicines of Spondias dulcis Parkinson using analytical and microbiological analysis 2018 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Akadémiai Kiadó, Budapest, Hungary 2018 Abstract The quality control is vital for the safety and efficacy of herbal medicines. However, the quality of standardization is most difficult because the studies do not cover this step. The objective of this study was quality standardization of herbal drugs of Spondias dulcis Parkinson. The leaves were dried and ground to a powder. The plant drug was evaluated by parameters of mean particle size (417.85 μm), apparent density (0.37 ± 0.01 g $ mL^{−1} $), moisture content (7.96 ± 0.35%), loss on drying (7.33 ± 0.09%), pH (3.90 ± 0.01), total ash (12.66 ± 0.23%), acid insoluble ash (3.22 ± 0.20%) and aqueous extractives (24.00 ± 3.28%). Phytochemical screening revealed the presence of flavonoids and tannins. Microbiological analysis presented a total count within the recommended limits and the absence of pathogenic microorganisms. The infrared spectroscopy (FTIR) and thermal analysis (TG/DTA) showed that physical and chemical processes occurred. The FTIR fingerprint has been characterized by characteristic peaks. The TG curves present six steps, and DTA curve presents three events. The results provide the scientific data for the proper identification and establishment of standards for future investigations and applications. Herbal drugs Thermoanalytical characterization Physicochemical characterization Boylan, Fabio aut Salgado, Hérida Regina Nunes aut Enthalten in Journal of thermal analysis and calorimetry Springer International Publishing, 1998 134(2018), 3 vom: 26. Juni, Seite 1923-1928 (DE-627)244148767 (DE-600)1429493-X (DE-576)066397693 1388-6150 nnns volume:134 year:2018 number:3 day:26 month:06 pages:1923-1928 https://doi.org/10.1007/s10973-018-7486-2 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE SSG-OLC-PHA SSG-OLC-DE-84 GBV_ILN_70 AR 134 2018 3 26 06 1923-1928 |
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10.1007/s10973-018-7486-2 doi (DE-627)OLC2049866321 (DE-He213)s10973-018-7486-2-p DE-627 ger DE-627 rakwb eng 660 VZ Fernandes, Felipe Hugo Alencar verfasserin (orcid)0000-0002-7210-4349 aut Quality standardization of herbal medicines of Spondias dulcis Parkinson using analytical and microbiological analysis 2018 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Akadémiai Kiadó, Budapest, Hungary 2018 Abstract The quality control is vital for the safety and efficacy of herbal medicines. However, the quality of standardization is most difficult because the studies do not cover this step. The objective of this study was quality standardization of herbal drugs of Spondias dulcis Parkinson. The leaves were dried and ground to a powder. The plant drug was evaluated by parameters of mean particle size (417.85 μm), apparent density (0.37 ± 0.01 g $ mL^{−1} $), moisture content (7.96 ± 0.35%), loss on drying (7.33 ± 0.09%), pH (3.90 ± 0.01), total ash (12.66 ± 0.23%), acid insoluble ash (3.22 ± 0.20%) and aqueous extractives (24.00 ± 3.28%). Phytochemical screening revealed the presence of flavonoids and tannins. Microbiological analysis presented a total count within the recommended limits and the absence of pathogenic microorganisms. The infrared spectroscopy (FTIR) and thermal analysis (TG/DTA) showed that physical and chemical processes occurred. The FTIR fingerprint has been characterized by characteristic peaks. The TG curves present six steps, and DTA curve presents three events. The results provide the scientific data for the proper identification and establishment of standards for future investigations and applications. Herbal drugs Thermoanalytical characterization Physicochemical characterization Boylan, Fabio aut Salgado, Hérida Regina Nunes aut Enthalten in Journal of thermal analysis and calorimetry Springer International Publishing, 1998 134(2018), 3 vom: 26. Juni, Seite 1923-1928 (DE-627)244148767 (DE-600)1429493-X (DE-576)066397693 1388-6150 nnns volume:134 year:2018 number:3 day:26 month:06 pages:1923-1928 https://doi.org/10.1007/s10973-018-7486-2 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE SSG-OLC-PHA SSG-OLC-DE-84 GBV_ILN_70 AR 134 2018 3 26 06 1923-1928 |
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quality standardization of herbal medicines of spondias dulcis parkinson using analytical and microbiological analysis |
| title_auth |
Quality standardization of herbal medicines of Spondias dulcis Parkinson using analytical and microbiological analysis |
| abstract |
Abstract The quality control is vital for the safety and efficacy of herbal medicines. However, the quality of standardization is most difficult because the studies do not cover this step. The objective of this study was quality standardization of herbal drugs of Spondias dulcis Parkinson. The leaves were dried and ground to a powder. The plant drug was evaluated by parameters of mean particle size (417.85 μm), apparent density (0.37 ± 0.01 g $ mL^{−1} $), moisture content (7.96 ± 0.35%), loss on drying (7.33 ± 0.09%), pH (3.90 ± 0.01), total ash (12.66 ± 0.23%), acid insoluble ash (3.22 ± 0.20%) and aqueous extractives (24.00 ± 3.28%). Phytochemical screening revealed the presence of flavonoids and tannins. Microbiological analysis presented a total count within the recommended limits and the absence of pathogenic microorganisms. The infrared spectroscopy (FTIR) and thermal analysis (TG/DTA) showed that physical and chemical processes occurred. The FTIR fingerprint has been characterized by characteristic peaks. The TG curves present six steps, and DTA curve presents three events. The results provide the scientific data for the proper identification and establishment of standards for future investigations and applications. © Akadémiai Kiadó, Budapest, Hungary 2018 |
| abstractGer |
Abstract The quality control is vital for the safety and efficacy of herbal medicines. However, the quality of standardization is most difficult because the studies do not cover this step. The objective of this study was quality standardization of herbal drugs of Spondias dulcis Parkinson. The leaves were dried and ground to a powder. The plant drug was evaluated by parameters of mean particle size (417.85 μm), apparent density (0.37 ± 0.01 g $ mL^{−1} $), moisture content (7.96 ± 0.35%), loss on drying (7.33 ± 0.09%), pH (3.90 ± 0.01), total ash (12.66 ± 0.23%), acid insoluble ash (3.22 ± 0.20%) and aqueous extractives (24.00 ± 3.28%). Phytochemical screening revealed the presence of flavonoids and tannins. Microbiological analysis presented a total count within the recommended limits and the absence of pathogenic microorganisms. The infrared spectroscopy (FTIR) and thermal analysis (TG/DTA) showed that physical and chemical processes occurred. The FTIR fingerprint has been characterized by characteristic peaks. The TG curves present six steps, and DTA curve presents three events. The results provide the scientific data for the proper identification and establishment of standards for future investigations and applications. © Akadémiai Kiadó, Budapest, Hungary 2018 |
| abstract_unstemmed |
Abstract The quality control is vital for the safety and efficacy of herbal medicines. However, the quality of standardization is most difficult because the studies do not cover this step. The objective of this study was quality standardization of herbal drugs of Spondias dulcis Parkinson. The leaves were dried and ground to a powder. The plant drug was evaluated by parameters of mean particle size (417.85 μm), apparent density (0.37 ± 0.01 g $ mL^{−1} $), moisture content (7.96 ± 0.35%), loss on drying (7.33 ± 0.09%), pH (3.90 ± 0.01), total ash (12.66 ± 0.23%), acid insoluble ash (3.22 ± 0.20%) and aqueous extractives (24.00 ± 3.28%). Phytochemical screening revealed the presence of flavonoids and tannins. Microbiological analysis presented a total count within the recommended limits and the absence of pathogenic microorganisms. The infrared spectroscopy (FTIR) and thermal analysis (TG/DTA) showed that physical and chemical processes occurred. The FTIR fingerprint has been characterized by characteristic peaks. The TG curves present six steps, and DTA curve presents three events. The results provide the scientific data for the proper identification and establishment of standards for future investigations and applications. © Akadémiai Kiadó, Budapest, Hungary 2018 |
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| title_short |
Quality standardization of herbal medicines of Spondias dulcis Parkinson using analytical and microbiological analysis |
| url |
https://doi.org/10.1007/s10973-018-7486-2 |
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Boylan, Fabio Salgado, Hérida Regina Nunes |
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