Synthesis of new aromatic polyamides containing α-amino phosphonate with high thermal stability and low heat release rate
Abstract The new aromatic polyamides containing α-amino phosphonate were synthesized from phosphorus-based dicarboxylic acid 4 and various aromatic diamines by direct polycondensation reaction. Dicarboxylic acid 4 was successfully synthesized from trimethyl phosphite, 4-aminobenzoic acid and terepht...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Hajibeygi, Mohsen [verfasserIn] |
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| Format: |
Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2019 |
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| Schlagwörter: |
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| Anmerkung: |
© Akadémiai Kiadó, Budapest, Hungary 2019 |
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| Übergeordnetes Werk: |
Enthalten in: Journal of thermal analysis and calorimetry - Springer International Publishing, 1998, 138(2019), 6 vom: 20. Mai, Seite 3949-3959 |
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| Übergeordnetes Werk: |
volume:138 ; year:2019 ; number:6 ; day:20 ; month:05 ; pages:3949-3959 |
| Links: |
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| DOI / URN: |
10.1007/s10973-019-08383-6 |
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| Katalog-ID: |
OLC2049877447 |
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| 520 | |a Abstract The new aromatic polyamides containing α-amino phosphonate were synthesized from phosphorus-based dicarboxylic acid 4 and various aromatic diamines by direct polycondensation reaction. Dicarboxylic acid 4 was successfully synthesized from trimethyl phosphite, 4-aminobenzoic acid and terephthaldehyde via a three-component reaction. The polymerization reaction produced the polyamides 6a–f with high yield and desirable inherent viscosities. The thermal properties of the all samples were investigated by thermo-gravimetric analysis (TGA). The TGA results in $ N_{2} $ exhibited the 10% mass loss temperatures (T10) in the ranges of 324–345 °C, while the T10 resulted from thermo-oxidative degradation were higher than those. The main data obtained by microscale combustion calorimetry revealed acceptable combustion properties such as very low peak of heat release rate for the synthesized polyamides 6a–f. The all of the results indicated that these polyamides can be potentially utilized as additive for improvement of thermal resistance and combustion behavior of thermoplastic materials. | ||
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| 650 | 4 | |a Thermal properties | |
| 650 | 4 | |a Combustion behavior | |
| 650 | 4 | |a α-amino phosphonate | |
| 650 | 4 | |a Polycondensation | |
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| 700 | 1 | |a Shabanian, Meisam |4 aut | |
| 700 | 1 | |a Vahabi, Henri |4 aut | |
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10.1007/s10973-019-08383-6 doi (DE-627)OLC2049877447 (DE-He213)s10973-019-08383-6-p DE-627 ger DE-627 rakwb eng 660 VZ Hajibeygi, Mohsen verfasserin (orcid)0000-0001-8085-0635 aut Synthesis of new aromatic polyamides containing α-amino phosphonate with high thermal stability and low heat release rate 2019 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Akadémiai Kiadó, Budapest, Hungary 2019 Abstract The new aromatic polyamides containing α-amino phosphonate were synthesized from phosphorus-based dicarboxylic acid 4 and various aromatic diamines by direct polycondensation reaction. Dicarboxylic acid 4 was successfully synthesized from trimethyl phosphite, 4-aminobenzoic acid and terephthaldehyde via a three-component reaction. The polymerization reaction produced the polyamides 6a–f with high yield and desirable inherent viscosities. The thermal properties of the all samples were investigated by thermo-gravimetric analysis (TGA). The TGA results in $ N_{2} $ exhibited the 10% mass loss temperatures (T10) in the ranges of 324–345 °C, while the T10 resulted from thermo-oxidative degradation were higher than those. The main data obtained by microscale combustion calorimetry revealed acceptable combustion properties such as very low peak of heat release rate for the synthesized polyamides 6a–f. The all of the results indicated that these polyamides can be potentially utilized as additive for improvement of thermal resistance and combustion behavior of thermoplastic materials. Polyamide Thermal properties Combustion behavior α-amino phosphonate Polycondensation Jafarzadeh, Hosein aut Shabanian, Meisam aut Vahabi, Henri aut Enthalten in Journal of thermal analysis and calorimetry Springer International Publishing, 1998 138(2019), 6 vom: 20. Mai, Seite 3949-3959 (DE-627)244148767 (DE-600)1429493-X (DE-576)066397693 1388-6150 nnns volume:138 year:2019 number:6 day:20 month:05 pages:3949-3959 https://doi.org/10.1007/s10973-019-08383-6 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE GBV_ILN_70 AR 138 2019 6 20 05 3949-3959 |
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10.1007/s10973-019-08383-6 doi (DE-627)OLC2049877447 (DE-He213)s10973-019-08383-6-p DE-627 ger DE-627 rakwb eng 660 VZ Hajibeygi, Mohsen verfasserin (orcid)0000-0001-8085-0635 aut Synthesis of new aromatic polyamides containing α-amino phosphonate with high thermal stability and low heat release rate 2019 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Akadémiai Kiadó, Budapest, Hungary 2019 Abstract The new aromatic polyamides containing α-amino phosphonate were synthesized from phosphorus-based dicarboxylic acid 4 and various aromatic diamines by direct polycondensation reaction. Dicarboxylic acid 4 was successfully synthesized from trimethyl phosphite, 4-aminobenzoic acid and terephthaldehyde via a three-component reaction. The polymerization reaction produced the polyamides 6a–f with high yield and desirable inherent viscosities. The thermal properties of the all samples were investigated by thermo-gravimetric analysis (TGA). The TGA results in $ N_{2} $ exhibited the 10% mass loss temperatures (T10) in the ranges of 324–345 °C, while the T10 resulted from thermo-oxidative degradation were higher than those. The main data obtained by microscale combustion calorimetry revealed acceptable combustion properties such as very low peak of heat release rate for the synthesized polyamides 6a–f. The all of the results indicated that these polyamides can be potentially utilized as additive for improvement of thermal resistance and combustion behavior of thermoplastic materials. Polyamide Thermal properties Combustion behavior α-amino phosphonate Polycondensation Jafarzadeh, Hosein aut Shabanian, Meisam aut Vahabi, Henri aut Enthalten in Journal of thermal analysis and calorimetry Springer International Publishing, 1998 138(2019), 6 vom: 20. Mai, Seite 3949-3959 (DE-627)244148767 (DE-600)1429493-X (DE-576)066397693 1388-6150 nnns volume:138 year:2019 number:6 day:20 month:05 pages:3949-3959 https://doi.org/10.1007/s10973-019-08383-6 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE GBV_ILN_70 AR 138 2019 6 20 05 3949-3959 |
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10.1007/s10973-019-08383-6 doi (DE-627)OLC2049877447 (DE-He213)s10973-019-08383-6-p DE-627 ger DE-627 rakwb eng 660 VZ Hajibeygi, Mohsen verfasserin (orcid)0000-0001-8085-0635 aut Synthesis of new aromatic polyamides containing α-amino phosphonate with high thermal stability and low heat release rate 2019 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Akadémiai Kiadó, Budapest, Hungary 2019 Abstract The new aromatic polyamides containing α-amino phosphonate were synthesized from phosphorus-based dicarboxylic acid 4 and various aromatic diamines by direct polycondensation reaction. Dicarboxylic acid 4 was successfully synthesized from trimethyl phosphite, 4-aminobenzoic acid and terephthaldehyde via a three-component reaction. The polymerization reaction produced the polyamides 6a–f with high yield and desirable inherent viscosities. The thermal properties of the all samples were investigated by thermo-gravimetric analysis (TGA). The TGA results in $ N_{2} $ exhibited the 10% mass loss temperatures (T10) in the ranges of 324–345 °C, while the T10 resulted from thermo-oxidative degradation were higher than those. The main data obtained by microscale combustion calorimetry revealed acceptable combustion properties such as very low peak of heat release rate for the synthesized polyamides 6a–f. The all of the results indicated that these polyamides can be potentially utilized as additive for improvement of thermal resistance and combustion behavior of thermoplastic materials. Polyamide Thermal properties Combustion behavior α-amino phosphonate Polycondensation Jafarzadeh, Hosein aut Shabanian, Meisam aut Vahabi, Henri aut Enthalten in Journal of thermal analysis and calorimetry Springer International Publishing, 1998 138(2019), 6 vom: 20. Mai, Seite 3949-3959 (DE-627)244148767 (DE-600)1429493-X (DE-576)066397693 1388-6150 nnns volume:138 year:2019 number:6 day:20 month:05 pages:3949-3959 https://doi.org/10.1007/s10973-019-08383-6 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE GBV_ILN_70 AR 138 2019 6 20 05 3949-3959 |
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10.1007/s10973-019-08383-6 doi (DE-627)OLC2049877447 (DE-He213)s10973-019-08383-6-p DE-627 ger DE-627 rakwb eng 660 VZ Hajibeygi, Mohsen verfasserin (orcid)0000-0001-8085-0635 aut Synthesis of new aromatic polyamides containing α-amino phosphonate with high thermal stability and low heat release rate 2019 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Akadémiai Kiadó, Budapest, Hungary 2019 Abstract The new aromatic polyamides containing α-amino phosphonate were synthesized from phosphorus-based dicarboxylic acid 4 and various aromatic diamines by direct polycondensation reaction. Dicarboxylic acid 4 was successfully synthesized from trimethyl phosphite, 4-aminobenzoic acid and terephthaldehyde via a three-component reaction. The polymerization reaction produced the polyamides 6a–f with high yield and desirable inherent viscosities. The thermal properties of the all samples were investigated by thermo-gravimetric analysis (TGA). The TGA results in $ N_{2} $ exhibited the 10% mass loss temperatures (T10) in the ranges of 324–345 °C, while the T10 resulted from thermo-oxidative degradation were higher than those. The main data obtained by microscale combustion calorimetry revealed acceptable combustion properties such as very low peak of heat release rate for the synthesized polyamides 6a–f. The all of the results indicated that these polyamides can be potentially utilized as additive for improvement of thermal resistance and combustion behavior of thermoplastic materials. Polyamide Thermal properties Combustion behavior α-amino phosphonate Polycondensation Jafarzadeh, Hosein aut Shabanian, Meisam aut Vahabi, Henri aut Enthalten in Journal of thermal analysis and calorimetry Springer International Publishing, 1998 138(2019), 6 vom: 20. Mai, Seite 3949-3959 (DE-627)244148767 (DE-600)1429493-X (DE-576)066397693 1388-6150 nnns volume:138 year:2019 number:6 day:20 month:05 pages:3949-3959 https://doi.org/10.1007/s10973-019-08383-6 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE GBV_ILN_70 AR 138 2019 6 20 05 3949-3959 |
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10.1007/s10973-019-08383-6 doi (DE-627)OLC2049877447 (DE-He213)s10973-019-08383-6-p DE-627 ger DE-627 rakwb eng 660 VZ Hajibeygi, Mohsen verfasserin (orcid)0000-0001-8085-0635 aut Synthesis of new aromatic polyamides containing α-amino phosphonate with high thermal stability and low heat release rate 2019 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Akadémiai Kiadó, Budapest, Hungary 2019 Abstract The new aromatic polyamides containing α-amino phosphonate were synthesized from phosphorus-based dicarboxylic acid 4 and various aromatic diamines by direct polycondensation reaction. Dicarboxylic acid 4 was successfully synthesized from trimethyl phosphite, 4-aminobenzoic acid and terephthaldehyde via a three-component reaction. The polymerization reaction produced the polyamides 6a–f with high yield and desirable inherent viscosities. The thermal properties of the all samples were investigated by thermo-gravimetric analysis (TGA). The TGA results in $ N_{2} $ exhibited the 10% mass loss temperatures (T10) in the ranges of 324–345 °C, while the T10 resulted from thermo-oxidative degradation were higher than those. The main data obtained by microscale combustion calorimetry revealed acceptable combustion properties such as very low peak of heat release rate for the synthesized polyamides 6a–f. The all of the results indicated that these polyamides can be potentially utilized as additive for improvement of thermal resistance and combustion behavior of thermoplastic materials. Polyamide Thermal properties Combustion behavior α-amino phosphonate Polycondensation Jafarzadeh, Hosein aut Shabanian, Meisam aut Vahabi, Henri aut Enthalten in Journal of thermal analysis and calorimetry Springer International Publishing, 1998 138(2019), 6 vom: 20. Mai, Seite 3949-3959 (DE-627)244148767 (DE-600)1429493-X (DE-576)066397693 1388-6150 nnns volume:138 year:2019 number:6 day:20 month:05 pages:3949-3959 https://doi.org/10.1007/s10973-019-08383-6 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE GBV_ILN_70 AR 138 2019 6 20 05 3949-3959 |
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Synthesis of new aromatic polyamides containing α-amino phosphonate with high thermal stability and low heat release rate |
| abstract |
Abstract The new aromatic polyamides containing α-amino phosphonate were synthesized from phosphorus-based dicarboxylic acid 4 and various aromatic diamines by direct polycondensation reaction. Dicarboxylic acid 4 was successfully synthesized from trimethyl phosphite, 4-aminobenzoic acid and terephthaldehyde via a three-component reaction. The polymerization reaction produced the polyamides 6a–f with high yield and desirable inherent viscosities. The thermal properties of the all samples were investigated by thermo-gravimetric analysis (TGA). The TGA results in $ N_{2} $ exhibited the 10% mass loss temperatures (T10) in the ranges of 324–345 °C, while the T10 resulted from thermo-oxidative degradation were higher than those. The main data obtained by microscale combustion calorimetry revealed acceptable combustion properties such as very low peak of heat release rate for the synthesized polyamides 6a–f. The all of the results indicated that these polyamides can be potentially utilized as additive for improvement of thermal resistance and combustion behavior of thermoplastic materials. © Akadémiai Kiadó, Budapest, Hungary 2019 |
| abstractGer |
Abstract The new aromatic polyamides containing α-amino phosphonate were synthesized from phosphorus-based dicarboxylic acid 4 and various aromatic diamines by direct polycondensation reaction. Dicarboxylic acid 4 was successfully synthesized from trimethyl phosphite, 4-aminobenzoic acid and terephthaldehyde via a three-component reaction. The polymerization reaction produced the polyamides 6a–f with high yield and desirable inherent viscosities. The thermal properties of the all samples were investigated by thermo-gravimetric analysis (TGA). The TGA results in $ N_{2} $ exhibited the 10% mass loss temperatures (T10) in the ranges of 324–345 °C, while the T10 resulted from thermo-oxidative degradation were higher than those. The main data obtained by microscale combustion calorimetry revealed acceptable combustion properties such as very low peak of heat release rate for the synthesized polyamides 6a–f. The all of the results indicated that these polyamides can be potentially utilized as additive for improvement of thermal resistance and combustion behavior of thermoplastic materials. © Akadémiai Kiadó, Budapest, Hungary 2019 |
| abstract_unstemmed |
Abstract The new aromatic polyamides containing α-amino phosphonate were synthesized from phosphorus-based dicarboxylic acid 4 and various aromatic diamines by direct polycondensation reaction. Dicarboxylic acid 4 was successfully synthesized from trimethyl phosphite, 4-aminobenzoic acid and terephthaldehyde via a three-component reaction. The polymerization reaction produced the polyamides 6a–f with high yield and desirable inherent viscosities. The thermal properties of the all samples were investigated by thermo-gravimetric analysis (TGA). The TGA results in $ N_{2} $ exhibited the 10% mass loss temperatures (T10) in the ranges of 324–345 °C, while the T10 resulted from thermo-oxidative degradation were higher than those. The main data obtained by microscale combustion calorimetry revealed acceptable combustion properties such as very low peak of heat release rate for the synthesized polyamides 6a–f. The all of the results indicated that these polyamides can be potentially utilized as additive for improvement of thermal resistance and combustion behavior of thermoplastic materials. © Akadémiai Kiadó, Budapest, Hungary 2019 |
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| title_short |
Synthesis of new aromatic polyamides containing α-amino phosphonate with high thermal stability and low heat release rate |
| url |
https://doi.org/10.1007/s10973-019-08383-6 |
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| author2 |
Jafarzadeh, Hosein Shabanian, Meisam Vahabi, Henri |
| author2Str |
Jafarzadeh, Hosein Shabanian, Meisam Vahabi, Henri |
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| doi_str |
10.1007/s10973-019-08383-6 |
| up_date |
2024-07-04T00:21:55.535Z |
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