Development of a HPTLC method to profile the phytochemicals in Allanblackia parviflora (tallow tree) kernel and seed cakes
Abstract HPTLC is a useful and practical analytical tool to characterize plant compositions. This study was focused on exploring the results of high-performance thin-layer chromatography (HPTLC) analysis, particularly as a useful tool for the authentication of Allanblackia parviflora seed and kernel...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Sefah, Wilfred [verfasserIn] |
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| Format: |
Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2020 |
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| Schlagwörter: |
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| Anmerkung: |
© Akadémiai Kiadó, Budapest, Hungary 2020 |
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| Übergeordnetes Werk: |
Enthalten in: Journal of planar chromatography, modern TLC - Springer International Publishing, 1988, 33(2020), 1 vom: Feb., Seite 33-41 |
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| Übergeordnetes Werk: |
volume:33 ; year:2020 ; number:1 ; month:02 ; pages:33-41 |
| Links: |
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| DOI / URN: |
10.1007/s00764-019-00009-9 |
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OLC2051476098 |
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| 520 | |a Abstract HPTLC is a useful and practical analytical tool to characterize plant compositions. This study was focused on exploring the results of high-performance thin-layer chromatography (HPTLC) analysis, particularly as a useful tool for the authentication of Allanblackia parviflora seed and kernel cakes. Bulked samples from sixteen different Ghanaian communities were analysed by HPTLC and their fingerprints were compared. The optimum experimental conditions were established: sample weight of 2.0 g, methanol:water (80:20 v/v) as extraction solvent, 30 min extraction time and twice extraction, ethyl acetate:methanol:water (100:16.5:13.5 v/v) as mobile phase, vanillic acid as derivatisation agent and 7 min of plate heating time after derivatisation. The HPTLC profile generated from extracts across 16 communities and 157 trees was very reproducible and demonstrates the robustness of the technique in characterising the profile. | ||
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10.1007/s00764-019-00009-9 doi (DE-627)OLC2051476098 (DE-He213)s00764-019-00009-9-p DE-627 ger DE-627 rakwb eng 540 530 VZ Sefah, Wilfred verfasserin aut Development of a HPTLC method to profile the phytochemicals in Allanblackia parviflora (tallow tree) kernel and seed cakes 2020 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Akadémiai Kiadó, Budapest, Hungary 2020 Abstract HPTLC is a useful and practical analytical tool to characterize plant compositions. This study was focused on exploring the results of high-performance thin-layer chromatography (HPTLC) analysis, particularly as a useful tool for the authentication of Allanblackia parviflora seed and kernel cakes. Bulked samples from sixteen different Ghanaian communities were analysed by HPTLC and their fingerprints were compared. The optimum experimental conditions were established: sample weight of 2.0 g, methanol:water (80:20 v/v) as extraction solvent, 30 min extraction time and twice extraction, ethyl acetate:methanol:water (100:16.5:13.5 v/v) as mobile phase, vanillic acid as derivatisation agent and 7 min of plate heating time after derivatisation. The HPTLC profile generated from extracts across 16 communities and 157 trees was very reproducible and demonstrates the robustness of the technique in characterising the profile. HPTLC Fingerprint Seed cakes Kernel cakes Tallow tree Sefah, Lydia aut Ofori, Hayford aut Enthalten in Journal of planar chromatography, modern TLC Springer International Publishing, 1988 33(2020), 1 vom: Feb., Seite 33-41 (DE-627)129250651 (DE-600)59576-7 (DE-576)017944201 0933-4173 nnns volume:33 year:2020 number:1 month:02 pages:33-41 https://doi.org/10.1007/s00764-019-00009-9 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-PHY SSG-OLC-CHE GBV_ILN_70 GBV_ILN_2129 AR 33 2020 1 02 33-41 |
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10.1007/s00764-019-00009-9 doi (DE-627)OLC2051476098 (DE-He213)s00764-019-00009-9-p DE-627 ger DE-627 rakwb eng 540 530 VZ Sefah, Wilfred verfasserin aut Development of a HPTLC method to profile the phytochemicals in Allanblackia parviflora (tallow tree) kernel and seed cakes 2020 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Akadémiai Kiadó, Budapest, Hungary 2020 Abstract HPTLC is a useful and practical analytical tool to characterize plant compositions. This study was focused on exploring the results of high-performance thin-layer chromatography (HPTLC) analysis, particularly as a useful tool for the authentication of Allanblackia parviflora seed and kernel cakes. Bulked samples from sixteen different Ghanaian communities were analysed by HPTLC and their fingerprints were compared. The optimum experimental conditions were established: sample weight of 2.0 g, methanol:water (80:20 v/v) as extraction solvent, 30 min extraction time and twice extraction, ethyl acetate:methanol:water (100:16.5:13.5 v/v) as mobile phase, vanillic acid as derivatisation agent and 7 min of plate heating time after derivatisation. The HPTLC profile generated from extracts across 16 communities and 157 trees was very reproducible and demonstrates the robustness of the technique in characterising the profile. HPTLC Fingerprint Seed cakes Kernel cakes Tallow tree Sefah, Lydia aut Ofori, Hayford aut Enthalten in Journal of planar chromatography, modern TLC Springer International Publishing, 1988 33(2020), 1 vom: Feb., Seite 33-41 (DE-627)129250651 (DE-600)59576-7 (DE-576)017944201 0933-4173 nnns volume:33 year:2020 number:1 month:02 pages:33-41 https://doi.org/10.1007/s00764-019-00009-9 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-PHY SSG-OLC-CHE GBV_ILN_70 GBV_ILN_2129 AR 33 2020 1 02 33-41 |
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10.1007/s00764-019-00009-9 doi (DE-627)OLC2051476098 (DE-He213)s00764-019-00009-9-p DE-627 ger DE-627 rakwb eng 540 530 VZ Sefah, Wilfred verfasserin aut Development of a HPTLC method to profile the phytochemicals in Allanblackia parviflora (tallow tree) kernel and seed cakes 2020 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Akadémiai Kiadó, Budapest, Hungary 2020 Abstract HPTLC is a useful and practical analytical tool to characterize plant compositions. This study was focused on exploring the results of high-performance thin-layer chromatography (HPTLC) analysis, particularly as a useful tool for the authentication of Allanblackia parviflora seed and kernel cakes. Bulked samples from sixteen different Ghanaian communities were analysed by HPTLC and their fingerprints were compared. The optimum experimental conditions were established: sample weight of 2.0 g, methanol:water (80:20 v/v) as extraction solvent, 30 min extraction time and twice extraction, ethyl acetate:methanol:water (100:16.5:13.5 v/v) as mobile phase, vanillic acid as derivatisation agent and 7 min of plate heating time after derivatisation. The HPTLC profile generated from extracts across 16 communities and 157 trees was very reproducible and demonstrates the robustness of the technique in characterising the profile. HPTLC Fingerprint Seed cakes Kernel cakes Tallow tree Sefah, Lydia aut Ofori, Hayford aut Enthalten in Journal of planar chromatography, modern TLC Springer International Publishing, 1988 33(2020), 1 vom: Feb., Seite 33-41 (DE-627)129250651 (DE-600)59576-7 (DE-576)017944201 0933-4173 nnns volume:33 year:2020 number:1 month:02 pages:33-41 https://doi.org/10.1007/s00764-019-00009-9 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-PHY SSG-OLC-CHE GBV_ILN_70 GBV_ILN_2129 AR 33 2020 1 02 33-41 |
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10.1007/s00764-019-00009-9 doi (DE-627)OLC2051476098 (DE-He213)s00764-019-00009-9-p DE-627 ger DE-627 rakwb eng 540 530 VZ Sefah, Wilfred verfasserin aut Development of a HPTLC method to profile the phytochemicals in Allanblackia parviflora (tallow tree) kernel and seed cakes 2020 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Akadémiai Kiadó, Budapest, Hungary 2020 Abstract HPTLC is a useful and practical analytical tool to characterize plant compositions. This study was focused on exploring the results of high-performance thin-layer chromatography (HPTLC) analysis, particularly as a useful tool for the authentication of Allanblackia parviflora seed and kernel cakes. Bulked samples from sixteen different Ghanaian communities were analysed by HPTLC and their fingerprints were compared. The optimum experimental conditions were established: sample weight of 2.0 g, methanol:water (80:20 v/v) as extraction solvent, 30 min extraction time and twice extraction, ethyl acetate:methanol:water (100:16.5:13.5 v/v) as mobile phase, vanillic acid as derivatisation agent and 7 min of plate heating time after derivatisation. The HPTLC profile generated from extracts across 16 communities and 157 trees was very reproducible and demonstrates the robustness of the technique in characterising the profile. HPTLC Fingerprint Seed cakes Kernel cakes Tallow tree Sefah, Lydia aut Ofori, Hayford aut Enthalten in Journal of planar chromatography, modern TLC Springer International Publishing, 1988 33(2020), 1 vom: Feb., Seite 33-41 (DE-627)129250651 (DE-600)59576-7 (DE-576)017944201 0933-4173 nnns volume:33 year:2020 number:1 month:02 pages:33-41 https://doi.org/10.1007/s00764-019-00009-9 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-PHY SSG-OLC-CHE GBV_ILN_70 GBV_ILN_2129 AR 33 2020 1 02 33-41 |
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10.1007/s00764-019-00009-9 doi (DE-627)OLC2051476098 (DE-He213)s00764-019-00009-9-p DE-627 ger DE-627 rakwb eng 540 530 VZ Sefah, Wilfred verfasserin aut Development of a HPTLC method to profile the phytochemicals in Allanblackia parviflora (tallow tree) kernel and seed cakes 2020 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Akadémiai Kiadó, Budapest, Hungary 2020 Abstract HPTLC is a useful and practical analytical tool to characterize plant compositions. This study was focused on exploring the results of high-performance thin-layer chromatography (HPTLC) analysis, particularly as a useful tool for the authentication of Allanblackia parviflora seed and kernel cakes. Bulked samples from sixteen different Ghanaian communities were analysed by HPTLC and their fingerprints were compared. The optimum experimental conditions were established: sample weight of 2.0 g, methanol:water (80:20 v/v) as extraction solvent, 30 min extraction time and twice extraction, ethyl acetate:methanol:water (100:16.5:13.5 v/v) as mobile phase, vanillic acid as derivatisation agent and 7 min of plate heating time after derivatisation. The HPTLC profile generated from extracts across 16 communities and 157 trees was very reproducible and demonstrates the robustness of the technique in characterising the profile. HPTLC Fingerprint Seed cakes Kernel cakes Tallow tree Sefah, Lydia aut Ofori, Hayford aut Enthalten in Journal of planar chromatography, modern TLC Springer International Publishing, 1988 33(2020), 1 vom: Feb., Seite 33-41 (DE-627)129250651 (DE-600)59576-7 (DE-576)017944201 0933-4173 nnns volume:33 year:2020 number:1 month:02 pages:33-41 https://doi.org/10.1007/s00764-019-00009-9 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-PHY SSG-OLC-CHE GBV_ILN_70 GBV_ILN_2129 AR 33 2020 1 02 33-41 |
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Development of a HPTLC method to profile the phytochemicals in Allanblackia parviflora (tallow tree) kernel and seed cakes |
| abstract |
Abstract HPTLC is a useful and practical analytical tool to characterize plant compositions. This study was focused on exploring the results of high-performance thin-layer chromatography (HPTLC) analysis, particularly as a useful tool for the authentication of Allanblackia parviflora seed and kernel cakes. Bulked samples from sixteen different Ghanaian communities were analysed by HPTLC and their fingerprints were compared. The optimum experimental conditions were established: sample weight of 2.0 g, methanol:water (80:20 v/v) as extraction solvent, 30 min extraction time and twice extraction, ethyl acetate:methanol:water (100:16.5:13.5 v/v) as mobile phase, vanillic acid as derivatisation agent and 7 min of plate heating time after derivatisation. The HPTLC profile generated from extracts across 16 communities and 157 trees was very reproducible and demonstrates the robustness of the technique in characterising the profile. © Akadémiai Kiadó, Budapest, Hungary 2020 |
| abstractGer |
Abstract HPTLC is a useful and practical analytical tool to characterize plant compositions. This study was focused on exploring the results of high-performance thin-layer chromatography (HPTLC) analysis, particularly as a useful tool for the authentication of Allanblackia parviflora seed and kernel cakes. Bulked samples from sixteen different Ghanaian communities were analysed by HPTLC and their fingerprints were compared. The optimum experimental conditions were established: sample weight of 2.0 g, methanol:water (80:20 v/v) as extraction solvent, 30 min extraction time and twice extraction, ethyl acetate:methanol:water (100:16.5:13.5 v/v) as mobile phase, vanillic acid as derivatisation agent and 7 min of plate heating time after derivatisation. The HPTLC profile generated from extracts across 16 communities and 157 trees was very reproducible and demonstrates the robustness of the technique in characterising the profile. © Akadémiai Kiadó, Budapest, Hungary 2020 |
| abstract_unstemmed |
Abstract HPTLC is a useful and practical analytical tool to characterize plant compositions. This study was focused on exploring the results of high-performance thin-layer chromatography (HPTLC) analysis, particularly as a useful tool for the authentication of Allanblackia parviflora seed and kernel cakes. Bulked samples from sixteen different Ghanaian communities were analysed by HPTLC and their fingerprints were compared. The optimum experimental conditions were established: sample weight of 2.0 g, methanol:water (80:20 v/v) as extraction solvent, 30 min extraction time and twice extraction, ethyl acetate:methanol:water (100:16.5:13.5 v/v) as mobile phase, vanillic acid as derivatisation agent and 7 min of plate heating time after derivatisation. The HPTLC profile generated from extracts across 16 communities and 157 trees was very reproducible and demonstrates the robustness of the technique in characterising the profile. © Akadémiai Kiadó, Budapest, Hungary 2020 |
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Development of a HPTLC method to profile the phytochemicals in Allanblackia parviflora (tallow tree) kernel and seed cakes |
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https://doi.org/10.1007/s00764-019-00009-9 |
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Sefah, Lydia Ofori, Hayford |
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10.1007/s00764-019-00009-9 |
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