The influence of boron on the grain boundary chemistry and microstructure of ni- 16cr- 9fe- 0.03c
Abstract High-purity Ni-16Cr-9Fe-0.03C was doped with 50 wppm B in order to determine the effects of B on the grain boundary chemistry and microstructure following both high temperature anneals (1373 to 1473 K) and lower temperature heat treatments (873 to 973 K). The anneals at high temperature yie...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Kruger, R. M. [verfasserIn] |
|---|
| Format: |
Artikel |
|---|---|
| Sprache: |
Englisch |
| Erschienen: |
1988 |
|---|
| Schlagwörter: |
Scanning Transmission Electron Microscope |
|---|
| Anmerkung: |
© The Metallurgical of Society of AIME 1988 |
|---|
| Übergeordnetes Werk: |
Enthalten in: Metallurgical transactions. A, Physical metallurgy and materials science - Springer-Verlag, 1975, 19(1988), 10 vom: Okt., Seite 2555-2566 |
|---|---|
| Übergeordnetes Werk: |
volume:19 ; year:1988 ; number:10 ; month:10 ; pages:2555-2566 |
| Links: |
|---|
| DOI / URN: |
10.1007/BF02645483 |
|---|
| Katalog-ID: |
OLC2053963581 |
|---|
| LEADER | 01000caa a22002652 4500 | ||
|---|---|---|---|
| 001 | OLC2053963581 | ||
| 003 | DE-627 | ||
| 005 | 20230303053315.0 | ||
| 007 | tu | ||
| 008 | 200820s1988 xx ||||| 00| ||eng c | ||
| 024 | 7 | |a 10.1007/BF02645483 |2 doi | |
| 035 | |a (DE-627)OLC2053963581 | ||
| 035 | |a (DE-He213)BF02645483-p | ||
| 040 | |a DE-627 |b ger |c DE-627 |e rakwb | ||
| 041 | |a eng | ||
| 082 | 0 | 4 | |a 670 |a 530 |q VZ |
| 100 | 1 | |a Kruger, R. M. |e verfasserin |4 aut | |
| 245 | 1 | 0 | |a The influence of boron on the grain boundary chemistry and microstructure of ni- 16cr- 9fe- 0.03c |
| 264 | 1 | |c 1988 | |
| 336 | |a Text |b txt |2 rdacontent | ||
| 337 | |a ohne Hilfsmittel zu benutzen |b n |2 rdamedia | ||
| 338 | |a Band |b nc |2 rdacarrier | ||
| 500 | |a © The Metallurgical of Society of AIME 1988 | ||
| 520 | |a Abstract High-purity Ni-16Cr-9Fe-0.03C was doped with 50 wppm B in order to determine the effects of B on the grain boundary chemistry and microstructure following both high temperature anneals (1373 to 1473 K) and lower temperature heat treatments (873 to 973 K). The anneals at high temperature yield precipitate-free grain boundaries in the B-free material, while the addition of B results in the intergranular precipitation of B-containing $ M_{7} $$ X_{3} $ and $ M_{23} $$ X_{6} $ and a 30 to 50 Pct reduction in grain growth. The low temperature heat treatments of the B-free material result in the growth of intergranular Cr-rich $ M_{7} $$ C_{3} $, which in turn causes Cr depletion at the grain boundary. Adding B does not affect the Cr concentration at the grain boundary nor the width of the Cr-depleted zone. However, B segregation occurs, with a segregation energy of 42.6 kJ/mole. In addition, intergranular Ni + B-rich $ M_{23} $$ X_{6} $ forms. These changes in the grain boundary chemistry due to B cause a reduction in intergranular attack of up to 50 Pct as measured by the electrochemical potentiokinetic reactivation test in a solution of 0.05 M $ H_{2} $$ SO_{4} $ + 0.05 M KSCN. | ||
| 650 | 4 | |a Metallurgical Transaction | |
| 650 | 4 | |a Auger Electron Spectroscopy | |
| 650 | 4 | |a Scanning Transmission Electron Microscope | |
| 650 | 4 | |a Electron Energy Loss Spectroscopy | |
| 650 | 4 | |a Intergranular Attack | |
| 700 | 1 | |a Was, G. S. |4 aut | |
| 773 | 0 | 8 | |i Enthalten in |t Metallurgical transactions. A, Physical metallurgy and materials science |d Springer-Verlag, 1975 |g 19(1988), 10 vom: Okt., Seite 2555-2566 |w (DE-627)129429058 |w (DE-600)192156-3 |w (DE-576)01480204X |x 0026-086X |7 nnns |
| 773 | 1 | 8 | |g volume:19 |g year:1988 |g number:10 |g month:10 |g pages:2555-2566 |
| 856 | 4 | 1 | |u https://doi.org/10.1007/BF02645483 |z lizenzpflichtig |3 Volltext |
| 912 | |a GBV_USEFLAG_A | ||
| 912 | |a SYSFLAG_A | ||
| 912 | |a GBV_OLC | ||
| 912 | |a SSG-OLC-TEC | ||
| 912 | |a SSG-OLC-PHY | ||
| 912 | |a GBV_ILN_11 | ||
| 912 | |a GBV_ILN_20 | ||
| 912 | |a GBV_ILN_21 | ||
| 912 | |a GBV_ILN_23 | ||
| 912 | |a GBV_ILN_30 | ||
| 912 | |a GBV_ILN_62 | ||
| 912 | |a GBV_ILN_70 | ||
| 912 | |a GBV_ILN_602 | ||
| 912 | |a GBV_ILN_2004 | ||
| 912 | |a GBV_ILN_2015 | ||
| 912 | |a GBV_ILN_2016 | ||
| 912 | |a GBV_ILN_2020 | ||
| 912 | |a GBV_ILN_2027 | ||
| 912 | |a GBV_ILN_4035 | ||
| 912 | |a GBV_ILN_4046 | ||
| 912 | |a GBV_ILN_4082 | ||
| 912 | |a GBV_ILN_4307 | ||
| 912 | |a GBV_ILN_4313 | ||
| 912 | |a GBV_ILN_4319 | ||
| 912 | |a GBV_ILN_4323 | ||
| 951 | |a AR | ||
| 952 | |d 19 |j 1988 |e 10 |c 10 |h 2555-2566 | ||
| author_variant |
r m k rm rmk g s w gs gsw |
|---|---|
| matchkey_str |
article:0026086X:1988----::hifunefoooteribudrceitynmcot |
| hierarchy_sort_str |
1988 |
| publishDate |
1988 |
| allfields |
10.1007/BF02645483 doi (DE-627)OLC2053963581 (DE-He213)BF02645483-p DE-627 ger DE-627 rakwb eng 670 530 VZ Kruger, R. M. verfasserin aut The influence of boron on the grain boundary chemistry and microstructure of ni- 16cr- 9fe- 0.03c 1988 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © The Metallurgical of Society of AIME 1988 Abstract High-purity Ni-16Cr-9Fe-0.03C was doped with 50 wppm B in order to determine the effects of B on the grain boundary chemistry and microstructure following both high temperature anneals (1373 to 1473 K) and lower temperature heat treatments (873 to 973 K). The anneals at high temperature yield precipitate-free grain boundaries in the B-free material, while the addition of B results in the intergranular precipitation of B-containing $ M_{7} $$ X_{3} $ and $ M_{23} $$ X_{6} $ and a 30 to 50 Pct reduction in grain growth. The low temperature heat treatments of the B-free material result in the growth of intergranular Cr-rich $ M_{7} $$ C_{3} $, which in turn causes Cr depletion at the grain boundary. Adding B does not affect the Cr concentration at the grain boundary nor the width of the Cr-depleted zone. However, B segregation occurs, with a segregation energy of 42.6 kJ/mole. In addition, intergranular Ni + B-rich $ M_{23} $$ X_{6} $ forms. These changes in the grain boundary chemistry due to B cause a reduction in intergranular attack of up to 50 Pct as measured by the electrochemical potentiokinetic reactivation test in a solution of 0.05 M $ H_{2} $$ SO_{4} $ + 0.05 M KSCN. Metallurgical Transaction Auger Electron Spectroscopy Scanning Transmission Electron Microscope Electron Energy Loss Spectroscopy Intergranular Attack Was, G. S. aut Enthalten in Metallurgical transactions. A, Physical metallurgy and materials science Springer-Verlag, 1975 19(1988), 10 vom: Okt., Seite 2555-2566 (DE-627)129429058 (DE-600)192156-3 (DE-576)01480204X 0026-086X nnns volume:19 year:1988 number:10 month:10 pages:2555-2566 https://doi.org/10.1007/BF02645483 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-PHY GBV_ILN_11 GBV_ILN_20 GBV_ILN_21 GBV_ILN_23 GBV_ILN_30 GBV_ILN_62 GBV_ILN_70 GBV_ILN_602 GBV_ILN_2004 GBV_ILN_2015 GBV_ILN_2016 GBV_ILN_2020 GBV_ILN_2027 GBV_ILN_4035 GBV_ILN_4046 GBV_ILN_4082 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4319 GBV_ILN_4323 AR 19 1988 10 10 2555-2566 |
| spelling |
10.1007/BF02645483 doi (DE-627)OLC2053963581 (DE-He213)BF02645483-p DE-627 ger DE-627 rakwb eng 670 530 VZ Kruger, R. M. verfasserin aut The influence of boron on the grain boundary chemistry and microstructure of ni- 16cr- 9fe- 0.03c 1988 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © The Metallurgical of Society of AIME 1988 Abstract High-purity Ni-16Cr-9Fe-0.03C was doped with 50 wppm B in order to determine the effects of B on the grain boundary chemistry and microstructure following both high temperature anneals (1373 to 1473 K) and lower temperature heat treatments (873 to 973 K). The anneals at high temperature yield precipitate-free grain boundaries in the B-free material, while the addition of B results in the intergranular precipitation of B-containing $ M_{7} $$ X_{3} $ and $ M_{23} $$ X_{6} $ and a 30 to 50 Pct reduction in grain growth. The low temperature heat treatments of the B-free material result in the growth of intergranular Cr-rich $ M_{7} $$ C_{3} $, which in turn causes Cr depletion at the grain boundary. Adding B does not affect the Cr concentration at the grain boundary nor the width of the Cr-depleted zone. However, B segregation occurs, with a segregation energy of 42.6 kJ/mole. In addition, intergranular Ni + B-rich $ M_{23} $$ X_{6} $ forms. These changes in the grain boundary chemistry due to B cause a reduction in intergranular attack of up to 50 Pct as measured by the electrochemical potentiokinetic reactivation test in a solution of 0.05 M $ H_{2} $$ SO_{4} $ + 0.05 M KSCN. Metallurgical Transaction Auger Electron Spectroscopy Scanning Transmission Electron Microscope Electron Energy Loss Spectroscopy Intergranular Attack Was, G. S. aut Enthalten in Metallurgical transactions. A, Physical metallurgy and materials science Springer-Verlag, 1975 19(1988), 10 vom: Okt., Seite 2555-2566 (DE-627)129429058 (DE-600)192156-3 (DE-576)01480204X 0026-086X nnns volume:19 year:1988 number:10 month:10 pages:2555-2566 https://doi.org/10.1007/BF02645483 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-PHY GBV_ILN_11 GBV_ILN_20 GBV_ILN_21 GBV_ILN_23 GBV_ILN_30 GBV_ILN_62 GBV_ILN_70 GBV_ILN_602 GBV_ILN_2004 GBV_ILN_2015 GBV_ILN_2016 GBV_ILN_2020 GBV_ILN_2027 GBV_ILN_4035 GBV_ILN_4046 GBV_ILN_4082 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4319 GBV_ILN_4323 AR 19 1988 10 10 2555-2566 |
| allfields_unstemmed |
10.1007/BF02645483 doi (DE-627)OLC2053963581 (DE-He213)BF02645483-p DE-627 ger DE-627 rakwb eng 670 530 VZ Kruger, R. M. verfasserin aut The influence of boron on the grain boundary chemistry and microstructure of ni- 16cr- 9fe- 0.03c 1988 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © The Metallurgical of Society of AIME 1988 Abstract High-purity Ni-16Cr-9Fe-0.03C was doped with 50 wppm B in order to determine the effects of B on the grain boundary chemistry and microstructure following both high temperature anneals (1373 to 1473 K) and lower temperature heat treatments (873 to 973 K). The anneals at high temperature yield precipitate-free grain boundaries in the B-free material, while the addition of B results in the intergranular precipitation of B-containing $ M_{7} $$ X_{3} $ and $ M_{23} $$ X_{6} $ and a 30 to 50 Pct reduction in grain growth. The low temperature heat treatments of the B-free material result in the growth of intergranular Cr-rich $ M_{7} $$ C_{3} $, which in turn causes Cr depletion at the grain boundary. Adding B does not affect the Cr concentration at the grain boundary nor the width of the Cr-depleted zone. However, B segregation occurs, with a segregation energy of 42.6 kJ/mole. In addition, intergranular Ni + B-rich $ M_{23} $$ X_{6} $ forms. These changes in the grain boundary chemistry due to B cause a reduction in intergranular attack of up to 50 Pct as measured by the electrochemical potentiokinetic reactivation test in a solution of 0.05 M $ H_{2} $$ SO_{4} $ + 0.05 M KSCN. Metallurgical Transaction Auger Electron Spectroscopy Scanning Transmission Electron Microscope Electron Energy Loss Spectroscopy Intergranular Attack Was, G. S. aut Enthalten in Metallurgical transactions. A, Physical metallurgy and materials science Springer-Verlag, 1975 19(1988), 10 vom: Okt., Seite 2555-2566 (DE-627)129429058 (DE-600)192156-3 (DE-576)01480204X 0026-086X nnns volume:19 year:1988 number:10 month:10 pages:2555-2566 https://doi.org/10.1007/BF02645483 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-PHY GBV_ILN_11 GBV_ILN_20 GBV_ILN_21 GBV_ILN_23 GBV_ILN_30 GBV_ILN_62 GBV_ILN_70 GBV_ILN_602 GBV_ILN_2004 GBV_ILN_2015 GBV_ILN_2016 GBV_ILN_2020 GBV_ILN_2027 GBV_ILN_4035 GBV_ILN_4046 GBV_ILN_4082 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4319 GBV_ILN_4323 AR 19 1988 10 10 2555-2566 |
| allfieldsGer |
10.1007/BF02645483 doi (DE-627)OLC2053963581 (DE-He213)BF02645483-p DE-627 ger DE-627 rakwb eng 670 530 VZ Kruger, R. M. verfasserin aut The influence of boron on the grain boundary chemistry and microstructure of ni- 16cr- 9fe- 0.03c 1988 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © The Metallurgical of Society of AIME 1988 Abstract High-purity Ni-16Cr-9Fe-0.03C was doped with 50 wppm B in order to determine the effects of B on the grain boundary chemistry and microstructure following both high temperature anneals (1373 to 1473 K) and lower temperature heat treatments (873 to 973 K). The anneals at high temperature yield precipitate-free grain boundaries in the B-free material, while the addition of B results in the intergranular precipitation of B-containing $ M_{7} $$ X_{3} $ and $ M_{23} $$ X_{6} $ and a 30 to 50 Pct reduction in grain growth. The low temperature heat treatments of the B-free material result in the growth of intergranular Cr-rich $ M_{7} $$ C_{3} $, which in turn causes Cr depletion at the grain boundary. Adding B does not affect the Cr concentration at the grain boundary nor the width of the Cr-depleted zone. However, B segregation occurs, with a segregation energy of 42.6 kJ/mole. In addition, intergranular Ni + B-rich $ M_{23} $$ X_{6} $ forms. These changes in the grain boundary chemistry due to B cause a reduction in intergranular attack of up to 50 Pct as measured by the electrochemical potentiokinetic reactivation test in a solution of 0.05 M $ H_{2} $$ SO_{4} $ + 0.05 M KSCN. Metallurgical Transaction Auger Electron Spectroscopy Scanning Transmission Electron Microscope Electron Energy Loss Spectroscopy Intergranular Attack Was, G. S. aut Enthalten in Metallurgical transactions. A, Physical metallurgy and materials science Springer-Verlag, 1975 19(1988), 10 vom: Okt., Seite 2555-2566 (DE-627)129429058 (DE-600)192156-3 (DE-576)01480204X 0026-086X nnns volume:19 year:1988 number:10 month:10 pages:2555-2566 https://doi.org/10.1007/BF02645483 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-PHY GBV_ILN_11 GBV_ILN_20 GBV_ILN_21 GBV_ILN_23 GBV_ILN_30 GBV_ILN_62 GBV_ILN_70 GBV_ILN_602 GBV_ILN_2004 GBV_ILN_2015 GBV_ILN_2016 GBV_ILN_2020 GBV_ILN_2027 GBV_ILN_4035 GBV_ILN_4046 GBV_ILN_4082 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4319 GBV_ILN_4323 AR 19 1988 10 10 2555-2566 |
| allfieldsSound |
10.1007/BF02645483 doi (DE-627)OLC2053963581 (DE-He213)BF02645483-p DE-627 ger DE-627 rakwb eng 670 530 VZ Kruger, R. M. verfasserin aut The influence of boron on the grain boundary chemistry and microstructure of ni- 16cr- 9fe- 0.03c 1988 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © The Metallurgical of Society of AIME 1988 Abstract High-purity Ni-16Cr-9Fe-0.03C was doped with 50 wppm B in order to determine the effects of B on the grain boundary chemistry and microstructure following both high temperature anneals (1373 to 1473 K) and lower temperature heat treatments (873 to 973 K). The anneals at high temperature yield precipitate-free grain boundaries in the B-free material, while the addition of B results in the intergranular precipitation of B-containing $ M_{7} $$ X_{3} $ and $ M_{23} $$ X_{6} $ and a 30 to 50 Pct reduction in grain growth. The low temperature heat treatments of the B-free material result in the growth of intergranular Cr-rich $ M_{7} $$ C_{3} $, which in turn causes Cr depletion at the grain boundary. Adding B does not affect the Cr concentration at the grain boundary nor the width of the Cr-depleted zone. However, B segregation occurs, with a segregation energy of 42.6 kJ/mole. In addition, intergranular Ni + B-rich $ M_{23} $$ X_{6} $ forms. These changes in the grain boundary chemistry due to B cause a reduction in intergranular attack of up to 50 Pct as measured by the electrochemical potentiokinetic reactivation test in a solution of 0.05 M $ H_{2} $$ SO_{4} $ + 0.05 M KSCN. Metallurgical Transaction Auger Electron Spectroscopy Scanning Transmission Electron Microscope Electron Energy Loss Spectroscopy Intergranular Attack Was, G. S. aut Enthalten in Metallurgical transactions. A, Physical metallurgy and materials science Springer-Verlag, 1975 19(1988), 10 vom: Okt., Seite 2555-2566 (DE-627)129429058 (DE-600)192156-3 (DE-576)01480204X 0026-086X nnns volume:19 year:1988 number:10 month:10 pages:2555-2566 https://doi.org/10.1007/BF02645483 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-PHY GBV_ILN_11 GBV_ILN_20 GBV_ILN_21 GBV_ILN_23 GBV_ILN_30 GBV_ILN_62 GBV_ILN_70 GBV_ILN_602 GBV_ILN_2004 GBV_ILN_2015 GBV_ILN_2016 GBV_ILN_2020 GBV_ILN_2027 GBV_ILN_4035 GBV_ILN_4046 GBV_ILN_4082 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4319 GBV_ILN_4323 AR 19 1988 10 10 2555-2566 |
| language |
English |
| source |
Enthalten in Metallurgical transactions. A, Physical metallurgy and materials science 19(1988), 10 vom: Okt., Seite 2555-2566 volume:19 year:1988 number:10 month:10 pages:2555-2566 |
| sourceStr |
Enthalten in Metallurgical transactions. A, Physical metallurgy and materials science 19(1988), 10 vom: Okt., Seite 2555-2566 volume:19 year:1988 number:10 month:10 pages:2555-2566 |
| format_phy_str_mv |
Article |
| institution |
findex.gbv.de |
| topic_facet |
Metallurgical Transaction Auger Electron Spectroscopy Scanning Transmission Electron Microscope Electron Energy Loss Spectroscopy Intergranular Attack |
| dewey-raw |
670 |
| isfreeaccess_bool |
false |
| container_title |
Metallurgical transactions. A, Physical metallurgy and materials science |
| authorswithroles_txt_mv |
Kruger, R. M. @@aut@@ Was, G. S. @@aut@@ |
| publishDateDaySort_date |
1988-10-01T00:00:00Z |
| hierarchy_top_id |
129429058 |
| dewey-sort |
3670 |
| id |
OLC2053963581 |
| language_de |
englisch |
| fullrecord |
<?xml version="1.0" encoding="UTF-8"?><collection xmlns="http://www.loc.gov/MARC21/slim"><record><leader>01000caa a22002652 4500</leader><controlfield tag="001">OLC2053963581</controlfield><controlfield tag="003">DE-627</controlfield><controlfield tag="005">20230303053315.0</controlfield><controlfield tag="007">tu</controlfield><controlfield tag="008">200820s1988 xx ||||| 00| ||eng c</controlfield><datafield tag="024" ind1="7" ind2=" "><subfield code="a">10.1007/BF02645483</subfield><subfield code="2">doi</subfield></datafield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(DE-627)OLC2053963581</subfield></datafield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(DE-He213)BF02645483-p</subfield></datafield><datafield tag="040" ind1=" " ind2=" "><subfield code="a">DE-627</subfield><subfield code="b">ger</subfield><subfield code="c">DE-627</subfield><subfield code="e">rakwb</subfield></datafield><datafield tag="041" ind1=" " ind2=" "><subfield code="a">eng</subfield></datafield><datafield tag="082" ind1="0" ind2="4"><subfield code="a">670</subfield><subfield code="a">530</subfield><subfield code="q">VZ</subfield></datafield><datafield tag="100" ind1="1" ind2=" "><subfield code="a">Kruger, R. M.</subfield><subfield code="e">verfasserin</subfield><subfield code="4">aut</subfield></datafield><datafield tag="245" ind1="1" ind2="0"><subfield code="a">The influence of boron on the grain boundary chemistry and microstructure of ni- 16cr- 9fe- 0.03c</subfield></datafield><datafield tag="264" ind1=" " ind2="1"><subfield code="c">1988</subfield></datafield><datafield tag="336" ind1=" " ind2=" "><subfield code="a">Text</subfield><subfield code="b">txt</subfield><subfield code="2">rdacontent</subfield></datafield><datafield tag="337" ind1=" " ind2=" "><subfield code="a">ohne Hilfsmittel zu benutzen</subfield><subfield code="b">n</subfield><subfield code="2">rdamedia</subfield></datafield><datafield tag="338" ind1=" " ind2=" "><subfield code="a">Band</subfield><subfield code="b">nc</subfield><subfield code="2">rdacarrier</subfield></datafield><datafield tag="500" ind1=" " ind2=" "><subfield code="a">© The Metallurgical of Society of AIME 1988</subfield></datafield><datafield tag="520" ind1=" " ind2=" "><subfield code="a">Abstract High-purity Ni-16Cr-9Fe-0.03C was doped with 50 wppm B in order to determine the effects of B on the grain boundary chemistry and microstructure following both high temperature anneals (1373 to 1473 K) and lower temperature heat treatments (873 to 973 K). The anneals at high temperature yield precipitate-free grain boundaries in the B-free material, while the addition of B results in the intergranular precipitation of B-containing $ M_{7} $$ X_{3} $ and $ M_{23} $$ X_{6} $ and a 30 to 50 Pct reduction in grain growth. The low temperature heat treatments of the B-free material result in the growth of intergranular Cr-rich $ M_{7} $$ C_{3} $, which in turn causes Cr depletion at the grain boundary. Adding B does not affect the Cr concentration at the grain boundary nor the width of the Cr-depleted zone. However, B segregation occurs, with a segregation energy of 42.6 kJ/mole. In addition, intergranular Ni + B-rich $ M_{23} $$ X_{6} $ forms. These changes in the grain boundary chemistry due to B cause a reduction in intergranular attack of up to 50 Pct as measured by the electrochemical potentiokinetic reactivation test in a solution of 0.05 M $ H_{2} $$ SO_{4} $ + 0.05 M KSCN.</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Metallurgical Transaction</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Auger Electron Spectroscopy</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Scanning Transmission Electron Microscope</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Electron Energy Loss Spectroscopy</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Intergranular Attack</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Was, G. S.</subfield><subfield code="4">aut</subfield></datafield><datafield tag="773" ind1="0" ind2="8"><subfield code="i">Enthalten in</subfield><subfield code="t">Metallurgical transactions. A, Physical metallurgy and materials science</subfield><subfield code="d">Springer-Verlag, 1975</subfield><subfield code="g">19(1988), 10 vom: Okt., Seite 2555-2566</subfield><subfield code="w">(DE-627)129429058</subfield><subfield code="w">(DE-600)192156-3</subfield><subfield code="w">(DE-576)01480204X</subfield><subfield code="x">0026-086X</subfield><subfield code="7">nnns</subfield></datafield><datafield tag="773" ind1="1" ind2="8"><subfield code="g">volume:19</subfield><subfield code="g">year:1988</subfield><subfield code="g">number:10</subfield><subfield code="g">month:10</subfield><subfield code="g">pages:2555-2566</subfield></datafield><datafield tag="856" ind1="4" ind2="1"><subfield code="u">https://doi.org/10.1007/BF02645483</subfield><subfield code="z">lizenzpflichtig</subfield><subfield code="3">Volltext</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_USEFLAG_A</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">SYSFLAG_A</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_OLC</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">SSG-OLC-TEC</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">SSG-OLC-PHY</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_11</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_20</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_21</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_23</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_30</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_62</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_70</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_602</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2004</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2015</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2016</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2020</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2027</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4035</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4046</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4082</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4307</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4313</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4319</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4323</subfield></datafield><datafield tag="951" ind1=" " ind2=" "><subfield code="a">AR</subfield></datafield><datafield tag="952" ind1=" " ind2=" "><subfield code="d">19</subfield><subfield code="j">1988</subfield><subfield code="e">10</subfield><subfield code="c">10</subfield><subfield code="h">2555-2566</subfield></datafield></record></collection>
|
| author |
Kruger, R. M. |
| spellingShingle |
Kruger, R. M. ddc 670 misc Metallurgical Transaction misc Auger Electron Spectroscopy misc Scanning Transmission Electron Microscope misc Electron Energy Loss Spectroscopy misc Intergranular Attack The influence of boron on the grain boundary chemistry and microstructure of ni- 16cr- 9fe- 0.03c |
| authorStr |
Kruger, R. M. |
| ppnlink_with_tag_str_mv |
@@773@@(DE-627)129429058 |
| format |
Article |
| dewey-ones |
670 - Manufacturing 530 - Physics |
| delete_txt_mv |
keep |
| author_role |
aut aut |
| collection |
OLC |
| remote_str |
false |
| illustrated |
Not Illustrated |
| issn |
0026-086X |
| topic_title |
670 530 VZ The influence of boron on the grain boundary chemistry and microstructure of ni- 16cr- 9fe- 0.03c Metallurgical Transaction Auger Electron Spectroscopy Scanning Transmission Electron Microscope Electron Energy Loss Spectroscopy Intergranular Attack |
| topic |
ddc 670 misc Metallurgical Transaction misc Auger Electron Spectroscopy misc Scanning Transmission Electron Microscope misc Electron Energy Loss Spectroscopy misc Intergranular Attack |
| topic_unstemmed |
ddc 670 misc Metallurgical Transaction misc Auger Electron Spectroscopy misc Scanning Transmission Electron Microscope misc Electron Energy Loss Spectroscopy misc Intergranular Attack |
| topic_browse |
ddc 670 misc Metallurgical Transaction misc Auger Electron Spectroscopy misc Scanning Transmission Electron Microscope misc Electron Energy Loss Spectroscopy misc Intergranular Attack |
| format_facet |
Aufsätze Gedruckte Aufsätze |
| format_main_str_mv |
Text Zeitschrift/Artikel |
| carriertype_str_mv |
nc |
| hierarchy_parent_title |
Metallurgical transactions. A, Physical metallurgy and materials science |
| hierarchy_parent_id |
129429058 |
| dewey-tens |
670 - Manufacturing 530 - Physics |
| hierarchy_top_title |
Metallurgical transactions. A, Physical metallurgy and materials science |
| isfreeaccess_txt |
false |
| familylinks_str_mv |
(DE-627)129429058 (DE-600)192156-3 (DE-576)01480204X |
| title |
The influence of boron on the grain boundary chemistry and microstructure of ni- 16cr- 9fe- 0.03c |
| ctrlnum |
(DE-627)OLC2053963581 (DE-He213)BF02645483-p |
| title_full |
The influence of boron on the grain boundary chemistry and microstructure of ni- 16cr- 9fe- 0.03c |
| author_sort |
Kruger, R. M. |
| journal |
Metallurgical transactions. A, Physical metallurgy and materials science |
| journalStr |
Metallurgical transactions. A, Physical metallurgy and materials science |
| lang_code |
eng |
| isOA_bool |
false |
| dewey-hundreds |
600 - Technology 500 - Science |
| recordtype |
marc |
| publishDateSort |
1988 |
| contenttype_str_mv |
txt |
| container_start_page |
2555 |
| author_browse |
Kruger, R. M. Was, G. S. |
| container_volume |
19 |
| class |
670 530 VZ |
| format_se |
Aufsätze |
| author-letter |
Kruger, R. M. |
| doi_str_mv |
10.1007/BF02645483 |
| dewey-full |
670 530 |
| title_sort |
the influence of boron on the grain boundary chemistry and microstructure of ni- 16cr- 9fe- 0.03c |
| title_auth |
The influence of boron on the grain boundary chemistry and microstructure of ni- 16cr- 9fe- 0.03c |
| abstract |
Abstract High-purity Ni-16Cr-9Fe-0.03C was doped with 50 wppm B in order to determine the effects of B on the grain boundary chemistry and microstructure following both high temperature anneals (1373 to 1473 K) and lower temperature heat treatments (873 to 973 K). The anneals at high temperature yield precipitate-free grain boundaries in the B-free material, while the addition of B results in the intergranular precipitation of B-containing $ M_{7} $$ X_{3} $ and $ M_{23} $$ X_{6} $ and a 30 to 50 Pct reduction in grain growth. The low temperature heat treatments of the B-free material result in the growth of intergranular Cr-rich $ M_{7} $$ C_{3} $, which in turn causes Cr depletion at the grain boundary. Adding B does not affect the Cr concentration at the grain boundary nor the width of the Cr-depleted zone. However, B segregation occurs, with a segregation energy of 42.6 kJ/mole. In addition, intergranular Ni + B-rich $ M_{23} $$ X_{6} $ forms. These changes in the grain boundary chemistry due to B cause a reduction in intergranular attack of up to 50 Pct as measured by the electrochemical potentiokinetic reactivation test in a solution of 0.05 M $ H_{2} $$ SO_{4} $ + 0.05 M KSCN. © The Metallurgical of Society of AIME 1988 |
| abstractGer |
Abstract High-purity Ni-16Cr-9Fe-0.03C was doped with 50 wppm B in order to determine the effects of B on the grain boundary chemistry and microstructure following both high temperature anneals (1373 to 1473 K) and lower temperature heat treatments (873 to 973 K). The anneals at high temperature yield precipitate-free grain boundaries in the B-free material, while the addition of B results in the intergranular precipitation of B-containing $ M_{7} $$ X_{3} $ and $ M_{23} $$ X_{6} $ and a 30 to 50 Pct reduction in grain growth. The low temperature heat treatments of the B-free material result in the growth of intergranular Cr-rich $ M_{7} $$ C_{3} $, which in turn causes Cr depletion at the grain boundary. Adding B does not affect the Cr concentration at the grain boundary nor the width of the Cr-depleted zone. However, B segregation occurs, with a segregation energy of 42.6 kJ/mole. In addition, intergranular Ni + B-rich $ M_{23} $$ X_{6} $ forms. These changes in the grain boundary chemistry due to B cause a reduction in intergranular attack of up to 50 Pct as measured by the electrochemical potentiokinetic reactivation test in a solution of 0.05 M $ H_{2} $$ SO_{4} $ + 0.05 M KSCN. © The Metallurgical of Society of AIME 1988 |
| abstract_unstemmed |
Abstract High-purity Ni-16Cr-9Fe-0.03C was doped with 50 wppm B in order to determine the effects of B on the grain boundary chemistry and microstructure following both high temperature anneals (1373 to 1473 K) and lower temperature heat treatments (873 to 973 K). The anneals at high temperature yield precipitate-free grain boundaries in the B-free material, while the addition of B results in the intergranular precipitation of B-containing $ M_{7} $$ X_{3} $ and $ M_{23} $$ X_{6} $ and a 30 to 50 Pct reduction in grain growth. The low temperature heat treatments of the B-free material result in the growth of intergranular Cr-rich $ M_{7} $$ C_{3} $, which in turn causes Cr depletion at the grain boundary. Adding B does not affect the Cr concentration at the grain boundary nor the width of the Cr-depleted zone. However, B segregation occurs, with a segregation energy of 42.6 kJ/mole. In addition, intergranular Ni + B-rich $ M_{23} $$ X_{6} $ forms. These changes in the grain boundary chemistry due to B cause a reduction in intergranular attack of up to 50 Pct as measured by the electrochemical potentiokinetic reactivation test in a solution of 0.05 M $ H_{2} $$ SO_{4} $ + 0.05 M KSCN. © The Metallurgical of Society of AIME 1988 |
| collection_details |
GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-PHY GBV_ILN_11 GBV_ILN_20 GBV_ILN_21 GBV_ILN_23 GBV_ILN_30 GBV_ILN_62 GBV_ILN_70 GBV_ILN_602 GBV_ILN_2004 GBV_ILN_2015 GBV_ILN_2016 GBV_ILN_2020 GBV_ILN_2027 GBV_ILN_4035 GBV_ILN_4046 GBV_ILN_4082 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4319 GBV_ILN_4323 |
| container_issue |
10 |
| title_short |
The influence of boron on the grain boundary chemistry and microstructure of ni- 16cr- 9fe- 0.03c |
| url |
https://doi.org/10.1007/BF02645483 |
| remote_bool |
false |
| author2 |
Was, G. S. |
| author2Str |
Was, G. S. |
| ppnlink |
129429058 |
| mediatype_str_mv |
n |
| isOA_txt |
false |
| hochschulschrift_bool |
false |
| doi_str |
10.1007/BF02645483 |
| up_date |
2024-07-03T21:23:10.933Z |
| _version_ |
1803594540970409985 |
| fullrecord_marcxml |
<?xml version="1.0" encoding="UTF-8"?><collection xmlns="http://www.loc.gov/MARC21/slim"><record><leader>01000caa a22002652 4500</leader><controlfield tag="001">OLC2053963581</controlfield><controlfield tag="003">DE-627</controlfield><controlfield tag="005">20230303053315.0</controlfield><controlfield tag="007">tu</controlfield><controlfield tag="008">200820s1988 xx ||||| 00| ||eng c</controlfield><datafield tag="024" ind1="7" ind2=" "><subfield code="a">10.1007/BF02645483</subfield><subfield code="2">doi</subfield></datafield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(DE-627)OLC2053963581</subfield></datafield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(DE-He213)BF02645483-p</subfield></datafield><datafield tag="040" ind1=" " ind2=" "><subfield code="a">DE-627</subfield><subfield code="b">ger</subfield><subfield code="c">DE-627</subfield><subfield code="e">rakwb</subfield></datafield><datafield tag="041" ind1=" " ind2=" "><subfield code="a">eng</subfield></datafield><datafield tag="082" ind1="0" ind2="4"><subfield code="a">670</subfield><subfield code="a">530</subfield><subfield code="q">VZ</subfield></datafield><datafield tag="100" ind1="1" ind2=" "><subfield code="a">Kruger, R. M.</subfield><subfield code="e">verfasserin</subfield><subfield code="4">aut</subfield></datafield><datafield tag="245" ind1="1" ind2="0"><subfield code="a">The influence of boron on the grain boundary chemistry and microstructure of ni- 16cr- 9fe- 0.03c</subfield></datafield><datafield tag="264" ind1=" " ind2="1"><subfield code="c">1988</subfield></datafield><datafield tag="336" ind1=" " ind2=" "><subfield code="a">Text</subfield><subfield code="b">txt</subfield><subfield code="2">rdacontent</subfield></datafield><datafield tag="337" ind1=" " ind2=" "><subfield code="a">ohne Hilfsmittel zu benutzen</subfield><subfield code="b">n</subfield><subfield code="2">rdamedia</subfield></datafield><datafield tag="338" ind1=" " ind2=" "><subfield code="a">Band</subfield><subfield code="b">nc</subfield><subfield code="2">rdacarrier</subfield></datafield><datafield tag="500" ind1=" " ind2=" "><subfield code="a">© The Metallurgical of Society of AIME 1988</subfield></datafield><datafield tag="520" ind1=" " ind2=" "><subfield code="a">Abstract High-purity Ni-16Cr-9Fe-0.03C was doped with 50 wppm B in order to determine the effects of B on the grain boundary chemistry and microstructure following both high temperature anneals (1373 to 1473 K) and lower temperature heat treatments (873 to 973 K). The anneals at high temperature yield precipitate-free grain boundaries in the B-free material, while the addition of B results in the intergranular precipitation of B-containing $ M_{7} $$ X_{3} $ and $ M_{23} $$ X_{6} $ and a 30 to 50 Pct reduction in grain growth. The low temperature heat treatments of the B-free material result in the growth of intergranular Cr-rich $ M_{7} $$ C_{3} $, which in turn causes Cr depletion at the grain boundary. Adding B does not affect the Cr concentration at the grain boundary nor the width of the Cr-depleted zone. However, B segregation occurs, with a segregation energy of 42.6 kJ/mole. In addition, intergranular Ni + B-rich $ M_{23} $$ X_{6} $ forms. These changes in the grain boundary chemistry due to B cause a reduction in intergranular attack of up to 50 Pct as measured by the electrochemical potentiokinetic reactivation test in a solution of 0.05 M $ H_{2} $$ SO_{4} $ + 0.05 M KSCN.</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Metallurgical Transaction</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Auger Electron Spectroscopy</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Scanning Transmission Electron Microscope</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Electron Energy Loss Spectroscopy</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Intergranular Attack</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Was, G. S.</subfield><subfield code="4">aut</subfield></datafield><datafield tag="773" ind1="0" ind2="8"><subfield code="i">Enthalten in</subfield><subfield code="t">Metallurgical transactions. A, Physical metallurgy and materials science</subfield><subfield code="d">Springer-Verlag, 1975</subfield><subfield code="g">19(1988), 10 vom: Okt., Seite 2555-2566</subfield><subfield code="w">(DE-627)129429058</subfield><subfield code="w">(DE-600)192156-3</subfield><subfield code="w">(DE-576)01480204X</subfield><subfield code="x">0026-086X</subfield><subfield code="7">nnns</subfield></datafield><datafield tag="773" ind1="1" ind2="8"><subfield code="g">volume:19</subfield><subfield code="g">year:1988</subfield><subfield code="g">number:10</subfield><subfield code="g">month:10</subfield><subfield code="g">pages:2555-2566</subfield></datafield><datafield tag="856" ind1="4" ind2="1"><subfield code="u">https://doi.org/10.1007/BF02645483</subfield><subfield code="z">lizenzpflichtig</subfield><subfield code="3">Volltext</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_USEFLAG_A</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">SYSFLAG_A</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_OLC</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">SSG-OLC-TEC</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">SSG-OLC-PHY</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_11</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_20</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_21</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_23</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_30</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_62</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_70</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_602</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2004</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2015</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2016</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2020</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2027</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4035</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4046</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4082</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4307</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4313</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4319</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4323</subfield></datafield><datafield tag="951" ind1=" " ind2=" "><subfield code="a">AR</subfield></datafield><datafield tag="952" ind1=" " ind2=" "><subfield code="d">19</subfield><subfield code="j">1988</subfield><subfield code="e">10</subfield><subfield code="c">10</subfield><subfield code="h">2555-2566</subfield></datafield></record></collection>
|
| score |
7.401025 |