One-Dimensional Cobalt(II) and Zinc(II) Succinato Coordination Polymers with Nicotinamide: Synthesis, Structural, Spectroscopic, Fluorescent and Thermal Properties
Abstract Cobalt(II) and zinc(II) succinato (suc) coordination polymers with nicotinamide (nia), {[Co(μ-suc)($ H_{2} $O)2(nia)2] · $ 2H_{2} $O}n (1) and {[Zn(μ-suc)($ H_{2} $O)2(nia)2] · $ 2H_{2} $O}n (2) have been synthesized and characterized by elemental analyses, magnetic moments, IR and TG-DTA....
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Demir, Selcuk [verfasserIn] |
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| Format: |
Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2009 |
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| Schlagwörter: |
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| Anmerkung: |
© Springer Science+Business Media, LLC 2009 |
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| Übergeordnetes Werk: |
Enthalten in: Journal of inorganic and organometallic polymers and materials - Springer US, 1991, 19(2009), 3 vom: 14. Apr., Seite 342-347 |
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| Übergeordnetes Werk: |
volume:19 ; year:2009 ; number:3 ; day:14 ; month:04 ; pages:342-347 |
| Links: |
|---|
| DOI / URN: |
10.1007/s10904-009-9273-9 |
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| Katalog-ID: |
OLC2061508049 |
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| 520 | |a Abstract Cobalt(II) and zinc(II) succinato (suc) coordination polymers with nicotinamide (nia), {[Co(μ-suc)($ H_{2} $O)2(nia)2] · $ 2H_{2} $O}n (1) and {[Zn(μ-suc)($ H_{2} $O)2(nia)2] · $ 2H_{2} $O}n (2) have been synthesized and characterized by elemental analyses, magnetic moments, IR and TG-DTA. Single-crystal X-ray analyses of 1 and 2 reveal that these complexes are isostructural and crystallize in triclinic space group $$ P\bar{1}.$$ Complexes 1 and 2 are 1-D coordination polymers, in which the metal(II) ions exhibit an octahedral geometry with two suc, two nia and two aqua ligands. The nia ligand is N-bonded, while the suc ligand bridges the metal centers through the carboxylate groups. The 1D chains are further assembled to form 3D networks by strong N–H···O and OW–H···O hydrogen bonds. IR spectra confirm the coordination modes of both suc and nia ligands, while TG-DTA data are in agreement with the crystal structures. Fluorescent analysis in the solid state shows that all complexes display intraligand (π–π*) emissions of nia. | ||
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| 700 | 1 | |a Yilmaz, Veysel T. |4 aut | |
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10.1007/s10904-009-9273-9 doi (DE-627)OLC2061508049 (DE-He213)s10904-009-9273-9-p DE-627 ger DE-627 rakwb eng 660 VZ Demir, Selcuk verfasserin aut One-Dimensional Cobalt(II) and Zinc(II) Succinato Coordination Polymers with Nicotinamide: Synthesis, Structural, Spectroscopic, Fluorescent and Thermal Properties 2009 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Springer Science+Business Media, LLC 2009 Abstract Cobalt(II) and zinc(II) succinato (suc) coordination polymers with nicotinamide (nia), {[Co(μ-suc)($ H_{2} $O)2(nia)2] · $ 2H_{2} $O}n (1) and {[Zn(μ-suc)($ H_{2} $O)2(nia)2] · $ 2H_{2} $O}n (2) have been synthesized and characterized by elemental analyses, magnetic moments, IR and TG-DTA. Single-crystal X-ray analyses of 1 and 2 reveal that these complexes are isostructural and crystallize in triclinic space group $$ P\bar{1}.$$ Complexes 1 and 2 are 1-D coordination polymers, in which the metal(II) ions exhibit an octahedral geometry with two suc, two nia and two aqua ligands. The nia ligand is N-bonded, while the suc ligand bridges the metal centers through the carboxylate groups. The 1D chains are further assembled to form 3D networks by strong N–H···O and OW–H···O hydrogen bonds. IR spectra confirm the coordination modes of both suc and nia ligands, while TG-DTA data are in agreement with the crystal structures. Fluorescent analysis in the solid state shows that all complexes display intraligand (π–π*) emissions of nia. Succinate Nicotinamide Coordination polymer 1D chain Crystal structure Yilmaz, Veysel T. aut Yilmaz, Fatih aut Buyukgungor, Orhan aut Enthalten in Journal of inorganic and organometallic polymers and materials Springer US, 1991 19(2009), 3 vom: 14. Apr., Seite 342-347 (DE-627)130968625 (DE-600)1069621-0 (DE-576)029153867 1574-1443 nnns volume:19 year:2009 number:3 day:14 month:04 pages:342-347 https://doi.org/10.1007/s10904-009-9273-9 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE SSG-OLC-PHA SSG-OLC-DE-84 GBV_ILN_21 GBV_ILN_70 AR 19 2009 3 14 04 342-347 |
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10.1007/s10904-009-9273-9 doi (DE-627)OLC2061508049 (DE-He213)s10904-009-9273-9-p DE-627 ger DE-627 rakwb eng 660 VZ Demir, Selcuk verfasserin aut One-Dimensional Cobalt(II) and Zinc(II) Succinato Coordination Polymers with Nicotinamide: Synthesis, Structural, Spectroscopic, Fluorescent and Thermal Properties 2009 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Springer Science+Business Media, LLC 2009 Abstract Cobalt(II) and zinc(II) succinato (suc) coordination polymers with nicotinamide (nia), {[Co(μ-suc)($ H_{2} $O)2(nia)2] · $ 2H_{2} $O}n (1) and {[Zn(μ-suc)($ H_{2} $O)2(nia)2] · $ 2H_{2} $O}n (2) have been synthesized and characterized by elemental analyses, magnetic moments, IR and TG-DTA. Single-crystal X-ray analyses of 1 and 2 reveal that these complexes are isostructural and crystallize in triclinic space group $$ P\bar{1}.$$ Complexes 1 and 2 are 1-D coordination polymers, in which the metal(II) ions exhibit an octahedral geometry with two suc, two nia and two aqua ligands. The nia ligand is N-bonded, while the suc ligand bridges the metal centers through the carboxylate groups. The 1D chains are further assembled to form 3D networks by strong N–H···O and OW–H···O hydrogen bonds. IR spectra confirm the coordination modes of both suc and nia ligands, while TG-DTA data are in agreement with the crystal structures. Fluorescent analysis in the solid state shows that all complexes display intraligand (π–π*) emissions of nia. Succinate Nicotinamide Coordination polymer 1D chain Crystal structure Yilmaz, Veysel T. aut Yilmaz, Fatih aut Buyukgungor, Orhan aut Enthalten in Journal of inorganic and organometallic polymers and materials Springer US, 1991 19(2009), 3 vom: 14. Apr., Seite 342-347 (DE-627)130968625 (DE-600)1069621-0 (DE-576)029153867 1574-1443 nnns volume:19 year:2009 number:3 day:14 month:04 pages:342-347 https://doi.org/10.1007/s10904-009-9273-9 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE SSG-OLC-PHA SSG-OLC-DE-84 GBV_ILN_21 GBV_ILN_70 AR 19 2009 3 14 04 342-347 |
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10.1007/s10904-009-9273-9 doi (DE-627)OLC2061508049 (DE-He213)s10904-009-9273-9-p DE-627 ger DE-627 rakwb eng 660 VZ Demir, Selcuk verfasserin aut One-Dimensional Cobalt(II) and Zinc(II) Succinato Coordination Polymers with Nicotinamide: Synthesis, Structural, Spectroscopic, Fluorescent and Thermal Properties 2009 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Springer Science+Business Media, LLC 2009 Abstract Cobalt(II) and zinc(II) succinato (suc) coordination polymers with nicotinamide (nia), {[Co(μ-suc)($ H_{2} $O)2(nia)2] · $ 2H_{2} $O}n (1) and {[Zn(μ-suc)($ H_{2} $O)2(nia)2] · $ 2H_{2} $O}n (2) have been synthesized and characterized by elemental analyses, magnetic moments, IR and TG-DTA. Single-crystal X-ray analyses of 1 and 2 reveal that these complexes are isostructural and crystallize in triclinic space group $$ P\bar{1}.$$ Complexes 1 and 2 are 1-D coordination polymers, in which the metal(II) ions exhibit an octahedral geometry with two suc, two nia and two aqua ligands. The nia ligand is N-bonded, while the suc ligand bridges the metal centers through the carboxylate groups. The 1D chains are further assembled to form 3D networks by strong N–H···O and OW–H···O hydrogen bonds. IR spectra confirm the coordination modes of both suc and nia ligands, while TG-DTA data are in agreement with the crystal structures. Fluorescent analysis in the solid state shows that all complexes display intraligand (π–π*) emissions of nia. Succinate Nicotinamide Coordination polymer 1D chain Crystal structure Yilmaz, Veysel T. aut Yilmaz, Fatih aut Buyukgungor, Orhan aut Enthalten in Journal of inorganic and organometallic polymers and materials Springer US, 1991 19(2009), 3 vom: 14. Apr., Seite 342-347 (DE-627)130968625 (DE-600)1069621-0 (DE-576)029153867 1574-1443 nnns volume:19 year:2009 number:3 day:14 month:04 pages:342-347 https://doi.org/10.1007/s10904-009-9273-9 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE SSG-OLC-PHA SSG-OLC-DE-84 GBV_ILN_21 GBV_ILN_70 AR 19 2009 3 14 04 342-347 |
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10.1007/s10904-009-9273-9 doi (DE-627)OLC2061508049 (DE-He213)s10904-009-9273-9-p DE-627 ger DE-627 rakwb eng 660 VZ Demir, Selcuk verfasserin aut One-Dimensional Cobalt(II) and Zinc(II) Succinato Coordination Polymers with Nicotinamide: Synthesis, Structural, Spectroscopic, Fluorescent and Thermal Properties 2009 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Springer Science+Business Media, LLC 2009 Abstract Cobalt(II) and zinc(II) succinato (suc) coordination polymers with nicotinamide (nia), {[Co(μ-suc)($ H_{2} $O)2(nia)2] · $ 2H_{2} $O}n (1) and {[Zn(μ-suc)($ H_{2} $O)2(nia)2] · $ 2H_{2} $O}n (2) have been synthesized and characterized by elemental analyses, magnetic moments, IR and TG-DTA. Single-crystal X-ray analyses of 1 and 2 reveal that these complexes are isostructural and crystallize in triclinic space group $$ P\bar{1}.$$ Complexes 1 and 2 are 1-D coordination polymers, in which the metal(II) ions exhibit an octahedral geometry with two suc, two nia and two aqua ligands. The nia ligand is N-bonded, while the suc ligand bridges the metal centers through the carboxylate groups. The 1D chains are further assembled to form 3D networks by strong N–H···O and OW–H···O hydrogen bonds. IR spectra confirm the coordination modes of both suc and nia ligands, while TG-DTA data are in agreement with the crystal structures. Fluorescent analysis in the solid state shows that all complexes display intraligand (π–π*) emissions of nia. Succinate Nicotinamide Coordination polymer 1D chain Crystal structure Yilmaz, Veysel T. aut Yilmaz, Fatih aut Buyukgungor, Orhan aut Enthalten in Journal of inorganic and organometallic polymers and materials Springer US, 1991 19(2009), 3 vom: 14. Apr., Seite 342-347 (DE-627)130968625 (DE-600)1069621-0 (DE-576)029153867 1574-1443 nnns volume:19 year:2009 number:3 day:14 month:04 pages:342-347 https://doi.org/10.1007/s10904-009-9273-9 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE SSG-OLC-PHA SSG-OLC-DE-84 GBV_ILN_21 GBV_ILN_70 AR 19 2009 3 14 04 342-347 |
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10.1007/s10904-009-9273-9 doi (DE-627)OLC2061508049 (DE-He213)s10904-009-9273-9-p DE-627 ger DE-627 rakwb eng 660 VZ Demir, Selcuk verfasserin aut One-Dimensional Cobalt(II) and Zinc(II) Succinato Coordination Polymers with Nicotinamide: Synthesis, Structural, Spectroscopic, Fluorescent and Thermal Properties 2009 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Springer Science+Business Media, LLC 2009 Abstract Cobalt(II) and zinc(II) succinato (suc) coordination polymers with nicotinamide (nia), {[Co(μ-suc)($ H_{2} $O)2(nia)2] · $ 2H_{2} $O}n (1) and {[Zn(μ-suc)($ H_{2} $O)2(nia)2] · $ 2H_{2} $O}n (2) have been synthesized and characterized by elemental analyses, magnetic moments, IR and TG-DTA. Single-crystal X-ray analyses of 1 and 2 reveal that these complexes are isostructural and crystallize in triclinic space group $$ P\bar{1}.$$ Complexes 1 and 2 are 1-D coordination polymers, in which the metal(II) ions exhibit an octahedral geometry with two suc, two nia and two aqua ligands. The nia ligand is N-bonded, while the suc ligand bridges the metal centers through the carboxylate groups. The 1D chains are further assembled to form 3D networks by strong N–H···O and OW–H···O hydrogen bonds. IR spectra confirm the coordination modes of both suc and nia ligands, while TG-DTA data are in agreement with the crystal structures. Fluorescent analysis in the solid state shows that all complexes display intraligand (π–π*) emissions of nia. Succinate Nicotinamide Coordination polymer 1D chain Crystal structure Yilmaz, Veysel T. aut Yilmaz, Fatih aut Buyukgungor, Orhan aut Enthalten in Journal of inorganic and organometallic polymers and materials Springer US, 1991 19(2009), 3 vom: 14. Apr., Seite 342-347 (DE-627)130968625 (DE-600)1069621-0 (DE-576)029153867 1574-1443 nnns volume:19 year:2009 number:3 day:14 month:04 pages:342-347 https://doi.org/10.1007/s10904-009-9273-9 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE SSG-OLC-PHA SSG-OLC-DE-84 GBV_ILN_21 GBV_ILN_70 AR 19 2009 3 14 04 342-347 |
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Demir, Selcuk |
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660 VZ One-Dimensional Cobalt(II) and Zinc(II) Succinato Coordination Polymers with Nicotinamide: Synthesis, Structural, Spectroscopic, Fluorescent and Thermal Properties Succinate Nicotinamide Coordination polymer 1D chain Crystal structure |
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One-Dimensional Cobalt(II) and Zinc(II) Succinato Coordination Polymers with Nicotinamide: Synthesis, Structural, Spectroscopic, Fluorescent and Thermal Properties |
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One-Dimensional Cobalt(II) and Zinc(II) Succinato Coordination Polymers with Nicotinamide: Synthesis, Structural, Spectroscopic, Fluorescent and Thermal Properties |
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Demir, Selcuk |
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Journal of inorganic and organometallic polymers and materials |
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Journal of inorganic and organometallic polymers and materials |
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2009 |
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Demir, Selcuk Yilmaz, Veysel T. Yilmaz, Fatih Buyukgungor, Orhan |
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one-dimensional cobalt(ii) and zinc(ii) succinato coordination polymers with nicotinamide: synthesis, structural, spectroscopic, fluorescent and thermal properties |
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One-Dimensional Cobalt(II) and Zinc(II) Succinato Coordination Polymers with Nicotinamide: Synthesis, Structural, Spectroscopic, Fluorescent and Thermal Properties |
| abstract |
Abstract Cobalt(II) and zinc(II) succinato (suc) coordination polymers with nicotinamide (nia), {[Co(μ-suc)($ H_{2} $O)2(nia)2] · $ 2H_{2} $O}n (1) and {[Zn(μ-suc)($ H_{2} $O)2(nia)2] · $ 2H_{2} $O}n (2) have been synthesized and characterized by elemental analyses, magnetic moments, IR and TG-DTA. Single-crystal X-ray analyses of 1 and 2 reveal that these complexes are isostructural and crystallize in triclinic space group $$ P\bar{1}.$$ Complexes 1 and 2 are 1-D coordination polymers, in which the metal(II) ions exhibit an octahedral geometry with two suc, two nia and two aqua ligands. The nia ligand is N-bonded, while the suc ligand bridges the metal centers through the carboxylate groups. The 1D chains are further assembled to form 3D networks by strong N–H···O and OW–H···O hydrogen bonds. IR spectra confirm the coordination modes of both suc and nia ligands, while TG-DTA data are in agreement with the crystal structures. Fluorescent analysis in the solid state shows that all complexes display intraligand (π–π*) emissions of nia. © Springer Science+Business Media, LLC 2009 |
| abstractGer |
Abstract Cobalt(II) and zinc(II) succinato (suc) coordination polymers with nicotinamide (nia), {[Co(μ-suc)($ H_{2} $O)2(nia)2] · $ 2H_{2} $O}n (1) and {[Zn(μ-suc)($ H_{2} $O)2(nia)2] · $ 2H_{2} $O}n (2) have been synthesized and characterized by elemental analyses, magnetic moments, IR and TG-DTA. Single-crystal X-ray analyses of 1 and 2 reveal that these complexes are isostructural and crystallize in triclinic space group $$ P\bar{1}.$$ Complexes 1 and 2 are 1-D coordination polymers, in which the metal(II) ions exhibit an octahedral geometry with two suc, two nia and two aqua ligands. The nia ligand is N-bonded, while the suc ligand bridges the metal centers through the carboxylate groups. The 1D chains are further assembled to form 3D networks by strong N–H···O and OW–H···O hydrogen bonds. IR spectra confirm the coordination modes of both suc and nia ligands, while TG-DTA data are in agreement with the crystal structures. Fluorescent analysis in the solid state shows that all complexes display intraligand (π–π*) emissions of nia. © Springer Science+Business Media, LLC 2009 |
| abstract_unstemmed |
Abstract Cobalt(II) and zinc(II) succinato (suc) coordination polymers with nicotinamide (nia), {[Co(μ-suc)($ H_{2} $O)2(nia)2] · $ 2H_{2} $O}n (1) and {[Zn(μ-suc)($ H_{2} $O)2(nia)2] · $ 2H_{2} $O}n (2) have been synthesized and characterized by elemental analyses, magnetic moments, IR and TG-DTA. Single-crystal X-ray analyses of 1 and 2 reveal that these complexes are isostructural and crystallize in triclinic space group $$ P\bar{1}.$$ Complexes 1 and 2 are 1-D coordination polymers, in which the metal(II) ions exhibit an octahedral geometry with two suc, two nia and two aqua ligands. The nia ligand is N-bonded, while the suc ligand bridges the metal centers through the carboxylate groups. The 1D chains are further assembled to form 3D networks by strong N–H···O and OW–H···O hydrogen bonds. IR spectra confirm the coordination modes of both suc and nia ligands, while TG-DTA data are in agreement with the crystal structures. Fluorescent analysis in the solid state shows that all complexes display intraligand (π–π*) emissions of nia. © Springer Science+Business Media, LLC 2009 |
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One-Dimensional Cobalt(II) and Zinc(II) Succinato Coordination Polymers with Nicotinamide: Synthesis, Structural, Spectroscopic, Fluorescent and Thermal Properties |
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