Electrospun Magnetic Zeolite/Polyacrylonitrile Nanofibers for Extraction of PAHs from Waste Water: Optimized with Central Composite Design
Abstract The present study discovered the synthesis of a novel and efficient magnetic nanofiber fabricated via electrospinning of polyacrylonitrile (PAN) and magnetic zeolite (PAN–MZeo). The synthesized nanofiber was applied as magnetic solid phase extraction (MSPE) adsorbent, for the determination...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Asadi, Marjan [verfasserIn] |
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| Format: |
Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2018 |
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| Schlagwörter: |
Magnetic solid phase extraction |
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| Anmerkung: |
© Springer Science+Business Media, LLC, part of Springer Nature 2018 |
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| Übergeordnetes Werk: |
Enthalten in: Journal of inorganic and organometallic polymers and materials - Springer US, 1991, 29(2018), 4 vom: 26. Nov., Seite 1057-1066 |
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| Übergeordnetes Werk: |
volume:29 ; year:2018 ; number:4 ; day:26 ; month:11 ; pages:1057-1066 |
| Links: |
|---|
| DOI / URN: |
10.1007/s10904-018-1027-0 |
|---|
| Katalog-ID: |
OLC2061525806 |
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| 520 | |a Abstract The present study discovered the synthesis of a novel and efficient magnetic nanofiber fabricated via electrospinning of polyacrylonitrile (PAN) and magnetic zeolite (PAN–MZeo). The synthesized nanofiber was applied as magnetic solid phase extraction (MSPE) adsorbent, for the determination of polycyclic aromatic hydrocarbons (PAHs) in water samples prior to gas chromatography flame ionization detector (GC-FID). Response surface methodology based on the central composite design was employed for the optimization of the various parameters including sorbent amount, desorption solvent volume, adsorption and desorption time on the extraction efficiency. Excellent linearity was achieved at optimized conditions, with coefficients of determination ($ R^{2} $) between 0.9948 and 0.9977. The limit of detections for PAHs was in the range of 0.14–0.21 ng $ mL^{−1} $. The repeatability and reproducibility precision (RSD%) were less than 10%. The real sample analysis showed satisfactory extraction recovery (92–113%) for the five selected PAHs in agricultural, well and mineral water samples. Therefore, the newly fabricated PAN–MZeo–MSPE is an accurate, rapid, and reliable sample-pretreatment method based on comparisons from previous studies. | ||
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10.1007/s10904-018-1027-0 doi (DE-627)OLC2061525806 (DE-He213)s10904-018-1027-0-p DE-627 ger DE-627 rakwb eng 660 VZ Asadi, Marjan verfasserin aut Electrospun Magnetic Zeolite/Polyacrylonitrile Nanofibers for Extraction of PAHs from Waste Water: Optimized with Central Composite Design 2018 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Springer Science+Business Media, LLC, part of Springer Nature 2018 Abstract The present study discovered the synthesis of a novel and efficient magnetic nanofiber fabricated via electrospinning of polyacrylonitrile (PAN) and magnetic zeolite (PAN–MZeo). The synthesized nanofiber was applied as magnetic solid phase extraction (MSPE) adsorbent, for the determination of polycyclic aromatic hydrocarbons (PAHs) in water samples prior to gas chromatography flame ionization detector (GC-FID). Response surface methodology based on the central composite design was employed for the optimization of the various parameters including sorbent amount, desorption solvent volume, adsorption and desorption time on the extraction efficiency. Excellent linearity was achieved at optimized conditions, with coefficients of determination ($ R^{2} $) between 0.9948 and 0.9977. The limit of detections for PAHs was in the range of 0.14–0.21 ng $ mL^{−1} $. The repeatability and reproducibility precision (RSD%) were less than 10%. The real sample analysis showed satisfactory extraction recovery (92–113%) for the five selected PAHs in agricultural, well and mineral water samples. Therefore, the newly fabricated PAN–MZeo–MSPE is an accurate, rapid, and reliable sample-pretreatment method based on comparisons from previous studies. Magnetic solid phase extraction PAN/magnetic zeolite Composite nanofibers Polycyclic aromatic hydrocarbons Central composite design Shahabuddin, Syed (orcid)0000-0001-5930-4138 aut Mollahosseini, Afsaneh aut Kaur, Jesbains aut Saidur, R. aut Enthalten in Journal of inorganic and organometallic polymers and materials Springer US, 1991 29(2018), 4 vom: 26. Nov., Seite 1057-1066 (DE-627)130968625 (DE-600)1069621-0 (DE-576)029153867 1574-1443 nnns volume:29 year:2018 number:4 day:26 month:11 pages:1057-1066 https://doi.org/10.1007/s10904-018-1027-0 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE SSG-OLC-PHA SSG-OLC-DE-84 GBV_ILN_70 AR 29 2018 4 26 11 1057-1066 |
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10.1007/s10904-018-1027-0 doi (DE-627)OLC2061525806 (DE-He213)s10904-018-1027-0-p DE-627 ger DE-627 rakwb eng 660 VZ Asadi, Marjan verfasserin aut Electrospun Magnetic Zeolite/Polyacrylonitrile Nanofibers for Extraction of PAHs from Waste Water: Optimized with Central Composite Design 2018 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Springer Science+Business Media, LLC, part of Springer Nature 2018 Abstract The present study discovered the synthesis of a novel and efficient magnetic nanofiber fabricated via electrospinning of polyacrylonitrile (PAN) and magnetic zeolite (PAN–MZeo). The synthesized nanofiber was applied as magnetic solid phase extraction (MSPE) adsorbent, for the determination of polycyclic aromatic hydrocarbons (PAHs) in water samples prior to gas chromatography flame ionization detector (GC-FID). Response surface methodology based on the central composite design was employed for the optimization of the various parameters including sorbent amount, desorption solvent volume, adsorption and desorption time on the extraction efficiency. Excellent linearity was achieved at optimized conditions, with coefficients of determination ($ R^{2} $) between 0.9948 and 0.9977. The limit of detections for PAHs was in the range of 0.14–0.21 ng $ mL^{−1} $. The repeatability and reproducibility precision (RSD%) were less than 10%. The real sample analysis showed satisfactory extraction recovery (92–113%) for the five selected PAHs in agricultural, well and mineral water samples. Therefore, the newly fabricated PAN–MZeo–MSPE is an accurate, rapid, and reliable sample-pretreatment method based on comparisons from previous studies. Magnetic solid phase extraction PAN/magnetic zeolite Composite nanofibers Polycyclic aromatic hydrocarbons Central composite design Shahabuddin, Syed (orcid)0000-0001-5930-4138 aut Mollahosseini, Afsaneh aut Kaur, Jesbains aut Saidur, R. aut Enthalten in Journal of inorganic and organometallic polymers and materials Springer US, 1991 29(2018), 4 vom: 26. Nov., Seite 1057-1066 (DE-627)130968625 (DE-600)1069621-0 (DE-576)029153867 1574-1443 nnns volume:29 year:2018 number:4 day:26 month:11 pages:1057-1066 https://doi.org/10.1007/s10904-018-1027-0 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE SSG-OLC-PHA SSG-OLC-DE-84 GBV_ILN_70 AR 29 2018 4 26 11 1057-1066 |
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10.1007/s10904-018-1027-0 doi (DE-627)OLC2061525806 (DE-He213)s10904-018-1027-0-p DE-627 ger DE-627 rakwb eng 660 VZ Asadi, Marjan verfasserin aut Electrospun Magnetic Zeolite/Polyacrylonitrile Nanofibers for Extraction of PAHs from Waste Water: Optimized with Central Composite Design 2018 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Springer Science+Business Media, LLC, part of Springer Nature 2018 Abstract The present study discovered the synthesis of a novel and efficient magnetic nanofiber fabricated via electrospinning of polyacrylonitrile (PAN) and magnetic zeolite (PAN–MZeo). The synthesized nanofiber was applied as magnetic solid phase extraction (MSPE) adsorbent, for the determination of polycyclic aromatic hydrocarbons (PAHs) in water samples prior to gas chromatography flame ionization detector (GC-FID). Response surface methodology based on the central composite design was employed for the optimization of the various parameters including sorbent amount, desorption solvent volume, adsorption and desorption time on the extraction efficiency. Excellent linearity was achieved at optimized conditions, with coefficients of determination ($ R^{2} $) between 0.9948 and 0.9977. The limit of detections for PAHs was in the range of 0.14–0.21 ng $ mL^{−1} $. The repeatability and reproducibility precision (RSD%) were less than 10%. The real sample analysis showed satisfactory extraction recovery (92–113%) for the five selected PAHs in agricultural, well and mineral water samples. Therefore, the newly fabricated PAN–MZeo–MSPE is an accurate, rapid, and reliable sample-pretreatment method based on comparisons from previous studies. Magnetic solid phase extraction PAN/magnetic zeolite Composite nanofibers Polycyclic aromatic hydrocarbons Central composite design Shahabuddin, Syed (orcid)0000-0001-5930-4138 aut Mollahosseini, Afsaneh aut Kaur, Jesbains aut Saidur, R. aut Enthalten in Journal of inorganic and organometallic polymers and materials Springer US, 1991 29(2018), 4 vom: 26. Nov., Seite 1057-1066 (DE-627)130968625 (DE-600)1069621-0 (DE-576)029153867 1574-1443 nnns volume:29 year:2018 number:4 day:26 month:11 pages:1057-1066 https://doi.org/10.1007/s10904-018-1027-0 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE SSG-OLC-PHA SSG-OLC-DE-84 GBV_ILN_70 AR 29 2018 4 26 11 1057-1066 |
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10.1007/s10904-018-1027-0 doi (DE-627)OLC2061525806 (DE-He213)s10904-018-1027-0-p DE-627 ger DE-627 rakwb eng 660 VZ Asadi, Marjan verfasserin aut Electrospun Magnetic Zeolite/Polyacrylonitrile Nanofibers for Extraction of PAHs from Waste Water: Optimized with Central Composite Design 2018 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Springer Science+Business Media, LLC, part of Springer Nature 2018 Abstract The present study discovered the synthesis of a novel and efficient magnetic nanofiber fabricated via electrospinning of polyacrylonitrile (PAN) and magnetic zeolite (PAN–MZeo). The synthesized nanofiber was applied as magnetic solid phase extraction (MSPE) adsorbent, for the determination of polycyclic aromatic hydrocarbons (PAHs) in water samples prior to gas chromatography flame ionization detector (GC-FID). Response surface methodology based on the central composite design was employed for the optimization of the various parameters including sorbent amount, desorption solvent volume, adsorption and desorption time on the extraction efficiency. Excellent linearity was achieved at optimized conditions, with coefficients of determination ($ R^{2} $) between 0.9948 and 0.9977. The limit of detections for PAHs was in the range of 0.14–0.21 ng $ mL^{−1} $. The repeatability and reproducibility precision (RSD%) were less than 10%. The real sample analysis showed satisfactory extraction recovery (92–113%) for the five selected PAHs in agricultural, well and mineral water samples. Therefore, the newly fabricated PAN–MZeo–MSPE is an accurate, rapid, and reliable sample-pretreatment method based on comparisons from previous studies. Magnetic solid phase extraction PAN/magnetic zeolite Composite nanofibers Polycyclic aromatic hydrocarbons Central composite design Shahabuddin, Syed (orcid)0000-0001-5930-4138 aut Mollahosseini, Afsaneh aut Kaur, Jesbains aut Saidur, R. aut Enthalten in Journal of inorganic and organometallic polymers and materials Springer US, 1991 29(2018), 4 vom: 26. Nov., Seite 1057-1066 (DE-627)130968625 (DE-600)1069621-0 (DE-576)029153867 1574-1443 nnns volume:29 year:2018 number:4 day:26 month:11 pages:1057-1066 https://doi.org/10.1007/s10904-018-1027-0 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE SSG-OLC-PHA SSG-OLC-DE-84 GBV_ILN_70 AR 29 2018 4 26 11 1057-1066 |
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10.1007/s10904-018-1027-0 doi (DE-627)OLC2061525806 (DE-He213)s10904-018-1027-0-p DE-627 ger DE-627 rakwb eng 660 VZ Asadi, Marjan verfasserin aut Electrospun Magnetic Zeolite/Polyacrylonitrile Nanofibers for Extraction of PAHs from Waste Water: Optimized with Central Composite Design 2018 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Springer Science+Business Media, LLC, part of Springer Nature 2018 Abstract The present study discovered the synthesis of a novel and efficient magnetic nanofiber fabricated via electrospinning of polyacrylonitrile (PAN) and magnetic zeolite (PAN–MZeo). The synthesized nanofiber was applied as magnetic solid phase extraction (MSPE) adsorbent, for the determination of polycyclic aromatic hydrocarbons (PAHs) in water samples prior to gas chromatography flame ionization detector (GC-FID). Response surface methodology based on the central composite design was employed for the optimization of the various parameters including sorbent amount, desorption solvent volume, adsorption and desorption time on the extraction efficiency. Excellent linearity was achieved at optimized conditions, with coefficients of determination ($ R^{2} $) between 0.9948 and 0.9977. The limit of detections for PAHs was in the range of 0.14–0.21 ng $ mL^{−1} $. The repeatability and reproducibility precision (RSD%) were less than 10%. The real sample analysis showed satisfactory extraction recovery (92–113%) for the five selected PAHs in agricultural, well and mineral water samples. Therefore, the newly fabricated PAN–MZeo–MSPE is an accurate, rapid, and reliable sample-pretreatment method based on comparisons from previous studies. Magnetic solid phase extraction PAN/magnetic zeolite Composite nanofibers Polycyclic aromatic hydrocarbons Central composite design Shahabuddin, Syed (orcid)0000-0001-5930-4138 aut Mollahosseini, Afsaneh aut Kaur, Jesbains aut Saidur, R. aut Enthalten in Journal of inorganic and organometallic polymers and materials Springer US, 1991 29(2018), 4 vom: 26. Nov., Seite 1057-1066 (DE-627)130968625 (DE-600)1069621-0 (DE-576)029153867 1574-1443 nnns volume:29 year:2018 number:4 day:26 month:11 pages:1057-1066 https://doi.org/10.1007/s10904-018-1027-0 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE SSG-OLC-PHA SSG-OLC-DE-84 GBV_ILN_70 AR 29 2018 4 26 11 1057-1066 |
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Journal of inorganic and organometallic polymers and materials |
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Electrospun Magnetic Zeolite/Polyacrylonitrile Nanofibers for Extraction of PAHs from Waste Water: Optimized with Central Composite Design |
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Electrospun Magnetic Zeolite/Polyacrylonitrile Nanofibers for Extraction of PAHs from Waste Water: Optimized with Central Composite Design |
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Asadi, Marjan |
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Journal of inorganic and organometallic polymers and materials |
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Journal of inorganic and organometallic polymers and materials |
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2018 |
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Asadi, Marjan Shahabuddin, Syed Mollahosseini, Afsaneh Kaur, Jesbains Saidur, R. |
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Asadi, Marjan |
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electrospun magnetic zeolite/polyacrylonitrile nanofibers for extraction of pahs from waste water: optimized with central composite design |
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Electrospun Magnetic Zeolite/Polyacrylonitrile Nanofibers for Extraction of PAHs from Waste Water: Optimized with Central Composite Design |
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Abstract The present study discovered the synthesis of a novel and efficient magnetic nanofiber fabricated via electrospinning of polyacrylonitrile (PAN) and magnetic zeolite (PAN–MZeo). The synthesized nanofiber was applied as magnetic solid phase extraction (MSPE) adsorbent, for the determination of polycyclic aromatic hydrocarbons (PAHs) in water samples prior to gas chromatography flame ionization detector (GC-FID). Response surface methodology based on the central composite design was employed for the optimization of the various parameters including sorbent amount, desorption solvent volume, adsorption and desorption time on the extraction efficiency. Excellent linearity was achieved at optimized conditions, with coefficients of determination ($ R^{2} $) between 0.9948 and 0.9977. The limit of detections for PAHs was in the range of 0.14–0.21 ng $ mL^{−1} $. The repeatability and reproducibility precision (RSD%) were less than 10%. The real sample analysis showed satisfactory extraction recovery (92–113%) for the five selected PAHs in agricultural, well and mineral water samples. Therefore, the newly fabricated PAN–MZeo–MSPE is an accurate, rapid, and reliable sample-pretreatment method based on comparisons from previous studies. © Springer Science+Business Media, LLC, part of Springer Nature 2018 |
| abstractGer |
Abstract The present study discovered the synthesis of a novel and efficient magnetic nanofiber fabricated via electrospinning of polyacrylonitrile (PAN) and magnetic zeolite (PAN–MZeo). The synthesized nanofiber was applied as magnetic solid phase extraction (MSPE) adsorbent, for the determination of polycyclic aromatic hydrocarbons (PAHs) in water samples prior to gas chromatography flame ionization detector (GC-FID). Response surface methodology based on the central composite design was employed for the optimization of the various parameters including sorbent amount, desorption solvent volume, adsorption and desorption time on the extraction efficiency. Excellent linearity was achieved at optimized conditions, with coefficients of determination ($ R^{2} $) between 0.9948 and 0.9977. The limit of detections for PAHs was in the range of 0.14–0.21 ng $ mL^{−1} $. The repeatability and reproducibility precision (RSD%) were less than 10%. The real sample analysis showed satisfactory extraction recovery (92–113%) for the five selected PAHs in agricultural, well and mineral water samples. Therefore, the newly fabricated PAN–MZeo–MSPE is an accurate, rapid, and reliable sample-pretreatment method based on comparisons from previous studies. © Springer Science+Business Media, LLC, part of Springer Nature 2018 |
| abstract_unstemmed |
Abstract The present study discovered the synthesis of a novel and efficient magnetic nanofiber fabricated via electrospinning of polyacrylonitrile (PAN) and magnetic zeolite (PAN–MZeo). The synthesized nanofiber was applied as magnetic solid phase extraction (MSPE) adsorbent, for the determination of polycyclic aromatic hydrocarbons (PAHs) in water samples prior to gas chromatography flame ionization detector (GC-FID). Response surface methodology based on the central composite design was employed for the optimization of the various parameters including sorbent amount, desorption solvent volume, adsorption and desorption time on the extraction efficiency. Excellent linearity was achieved at optimized conditions, with coefficients of determination ($ R^{2} $) between 0.9948 and 0.9977. The limit of detections for PAHs was in the range of 0.14–0.21 ng $ mL^{−1} $. The repeatability and reproducibility precision (RSD%) were less than 10%. The real sample analysis showed satisfactory extraction recovery (92–113%) for the five selected PAHs in agricultural, well and mineral water samples. Therefore, the newly fabricated PAN–MZeo–MSPE is an accurate, rapid, and reliable sample-pretreatment method based on comparisons from previous studies. © Springer Science+Business Media, LLC, part of Springer Nature 2018 |
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Electrospun Magnetic Zeolite/Polyacrylonitrile Nanofibers for Extraction of PAHs from Waste Water: Optimized with Central Composite Design |
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Shahabuddin, Syed Mollahosseini, Afsaneh Kaur, Jesbains Saidur, R. |
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