Carbon-13 NMR spectroscopic analysis of 24-methyl-$ Δ^{5,22} $-sterols in rape and mustard seed oils
Abstract 24-Methylcholesta-5,E-22-dien-3β-ol ($ C_{28} $ $ Δ^{5,22} $-sterol) was separated from the unsaponifiable matters of the following eight seed oils of Brassica species:Brassica campestris (candle I and II and torch),B. napus (tower and midas),B. juncea (brown and oriental mustards), andB. a...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Matsumoto, T. [verfasserIn] |
|---|
| Format: |
Artikel |
|---|---|
| Sprache: |
Englisch |
| Erschienen: |
1982 |
|---|
| Schlagwörter: |
|---|
| Anmerkung: |
© American Oil Chemists' Society 1982 |
|---|
| Übergeordnetes Werk: |
Enthalten in: Journal of the American Oil Chemists Society - Springer-Verlag, 1947, 59(1982), 12 vom: Dez., Seite 521-523 |
|---|---|
| Übergeordnetes Werk: |
volume:59 ; year:1982 ; number:12 ; month:12 ; pages:521-523 |
| Links: |
|---|
| DOI / URN: |
10.1007/BF02636314 |
|---|
| Katalog-ID: |
OLC2068085747 |
|---|
| LEADER | 01000caa a22002652 4500 | ||
|---|---|---|---|
| 001 | OLC2068085747 | ||
| 003 | DE-627 | ||
| 005 | 20230515203546.0 | ||
| 007 | tu | ||
| 008 | 200819s1982 xx ||||| 00| ||eng c | ||
| 024 | 7 | |a 10.1007/BF02636314 |2 doi | |
| 035 | |a (DE-627)OLC2068085747 | ||
| 035 | |a (DE-He213)BF02636314-p | ||
| 040 | |a DE-627 |b ger |c DE-627 |e rakwb | ||
| 041 | |a eng | ||
| 082 | 0 | 4 | |a 660 |q VZ |
| 100 | 1 | |a Matsumoto, T. |e verfasserin |4 aut | |
| 245 | 1 | 0 | |a Carbon-13 NMR spectroscopic analysis of 24-methyl-$ Δ^{5,22} $-sterols in rape and mustard seed oils |
| 264 | 1 | |c 1982 | |
| 336 | |a Text |b txt |2 rdacontent | ||
| 337 | |a ohne Hilfsmittel zu benutzen |b n |2 rdamedia | ||
| 338 | |a Band |b nc |2 rdacarrier | ||
| 500 | |a © American Oil Chemists' Society 1982 | ||
| 520 | |a Abstract 24-Methylcholesta-5,E-22-dien-3β-ol ($ C_{28} $ $ Δ^{5,22} $-sterol) was separated from the unsaponifiable matters of the following eight seed oils of Brassica species:Brassica campestris (candle I and II and torch),B. napus (tower and midas),B. juncea (brown and oriental mustards), andB. alba (yellow mustard). The configuration at C-24 methyl group of the respective sterols was evaluated $ by^{13} $C NMR spectroscopy. All the $ C_{28} $ $ Δ^{5,22} $-sterols in the Brassica seed oils were found to contain the C-24 epimer of brassicasterol,trans-22-dehydrocampesterol, in the range of ca. 10–30%. | ||
| 650 | 4 | |a Preparative Thin Layer Chromatography | |
| 650 | 4 | |a Winged Bean | |
| 650 | 4 | |a Bean Accession | |
| 650 | 4 | |a Yellow Mustard | |
| 650 | 4 | |a Solvent Extraction Plant | |
| 700 | 1 | |a Shimizu, N. |4 aut | |
| 700 | 1 | |a Itoh, T. |4 aut | |
| 700 | 1 | |a Iida, T. |4 aut | |
| 700 | 1 | |a Nishioka, A. |4 aut | |
| 773 | 0 | 8 | |i Enthalten in |t Journal of the American Oil Chemists Society |d Springer-Verlag, 1947 |g 59(1982), 12 vom: Dez., Seite 521-523 |w (DE-627)129595691 |w (DE-600)240684-6 |w (DE-576)015088715 |x 0003-021X |7 nnns |
| 773 | 1 | 8 | |g volume:59 |g year:1982 |g number:12 |g month:12 |g pages:521-523 |
| 856 | 4 | 1 | |u https://doi.org/10.1007/BF02636314 |z lizenzpflichtig |3 Volltext |
| 912 | |a GBV_USEFLAG_A | ||
| 912 | |a SYSFLAG_A | ||
| 912 | |a GBV_OLC | ||
| 912 | |a SSG-OLC-TEC | ||
| 912 | |a SSG-OLC-CHE | ||
| 912 | |a SSG-OLC-PHA | ||
| 912 | |a SSG-OLC-DE-84 | ||
| 912 | |a GBV_ILN_11 | ||
| 912 | |a GBV_ILN_20 | ||
| 912 | |a GBV_ILN_22 | ||
| 912 | |a GBV_ILN_23 | ||
| 912 | |a GBV_ILN_26 | ||
| 912 | |a GBV_ILN_70 | ||
| 912 | |a GBV_ILN_95 | ||
| 912 | |a GBV_ILN_252 | ||
| 912 | |a GBV_ILN_2360 | ||
| 912 | |a GBV_ILN_4012 | ||
| 912 | |a GBV_ILN_4036 | ||
| 912 | |a GBV_ILN_4046 | ||
| 912 | |a GBV_ILN_4125 | ||
| 912 | |a GBV_ILN_4219 | ||
| 912 | |a GBV_ILN_4306 | ||
| 912 | |a GBV_ILN_4315 | ||
| 951 | |a AR | ||
| 952 | |d 59 |j 1982 |e 12 |c 12 |h 521-523 | ||
| author_variant |
t m tm n s ns t i ti t i ti a n an |
|---|---|
| matchkey_str |
article:0003021X:1982----::abn3msetocpcnlssf4ehl2seosna |
| hierarchy_sort_str |
1982 |
| publishDate |
1982 |
| allfields |
10.1007/BF02636314 doi (DE-627)OLC2068085747 (DE-He213)BF02636314-p DE-627 ger DE-627 rakwb eng 660 VZ Matsumoto, T. verfasserin aut Carbon-13 NMR spectroscopic analysis of 24-methyl-$ Δ^{5,22} $-sterols in rape and mustard seed oils 1982 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © American Oil Chemists' Society 1982 Abstract 24-Methylcholesta-5,E-22-dien-3β-ol ($ C_{28} $ $ Δ^{5,22} $-sterol) was separated from the unsaponifiable matters of the following eight seed oils of Brassica species:Brassica campestris (candle I and II and torch),B. napus (tower and midas),B. juncea (brown and oriental mustards), andB. alba (yellow mustard). The configuration at C-24 methyl group of the respective sterols was evaluated $ by^{13} $C NMR spectroscopy. All the $ C_{28} $ $ Δ^{5,22} $-sterols in the Brassica seed oils were found to contain the C-24 epimer of brassicasterol,trans-22-dehydrocampesterol, in the range of ca. 10–30%. Preparative Thin Layer Chromatography Winged Bean Bean Accession Yellow Mustard Solvent Extraction Plant Shimizu, N. aut Itoh, T. aut Iida, T. aut Nishioka, A. aut Enthalten in Journal of the American Oil Chemists Society Springer-Verlag, 1947 59(1982), 12 vom: Dez., Seite 521-523 (DE-627)129595691 (DE-600)240684-6 (DE-576)015088715 0003-021X nnns volume:59 year:1982 number:12 month:12 pages:521-523 https://doi.org/10.1007/BF02636314 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE SSG-OLC-PHA SSG-OLC-DE-84 GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_26 GBV_ILN_70 GBV_ILN_95 GBV_ILN_252 GBV_ILN_2360 GBV_ILN_4012 GBV_ILN_4036 GBV_ILN_4046 GBV_ILN_4125 GBV_ILN_4219 GBV_ILN_4306 GBV_ILN_4315 AR 59 1982 12 12 521-523 |
| spelling |
10.1007/BF02636314 doi (DE-627)OLC2068085747 (DE-He213)BF02636314-p DE-627 ger DE-627 rakwb eng 660 VZ Matsumoto, T. verfasserin aut Carbon-13 NMR spectroscopic analysis of 24-methyl-$ Δ^{5,22} $-sterols in rape and mustard seed oils 1982 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © American Oil Chemists' Society 1982 Abstract 24-Methylcholesta-5,E-22-dien-3β-ol ($ C_{28} $ $ Δ^{5,22} $-sterol) was separated from the unsaponifiable matters of the following eight seed oils of Brassica species:Brassica campestris (candle I and II and torch),B. napus (tower and midas),B. juncea (brown and oriental mustards), andB. alba (yellow mustard). The configuration at C-24 methyl group of the respective sterols was evaluated $ by^{13} $C NMR spectroscopy. All the $ C_{28} $ $ Δ^{5,22} $-sterols in the Brassica seed oils were found to contain the C-24 epimer of brassicasterol,trans-22-dehydrocampesterol, in the range of ca. 10–30%. Preparative Thin Layer Chromatography Winged Bean Bean Accession Yellow Mustard Solvent Extraction Plant Shimizu, N. aut Itoh, T. aut Iida, T. aut Nishioka, A. aut Enthalten in Journal of the American Oil Chemists Society Springer-Verlag, 1947 59(1982), 12 vom: Dez., Seite 521-523 (DE-627)129595691 (DE-600)240684-6 (DE-576)015088715 0003-021X nnns volume:59 year:1982 number:12 month:12 pages:521-523 https://doi.org/10.1007/BF02636314 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE SSG-OLC-PHA SSG-OLC-DE-84 GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_26 GBV_ILN_70 GBV_ILN_95 GBV_ILN_252 GBV_ILN_2360 GBV_ILN_4012 GBV_ILN_4036 GBV_ILN_4046 GBV_ILN_4125 GBV_ILN_4219 GBV_ILN_4306 GBV_ILN_4315 AR 59 1982 12 12 521-523 |
| allfields_unstemmed |
10.1007/BF02636314 doi (DE-627)OLC2068085747 (DE-He213)BF02636314-p DE-627 ger DE-627 rakwb eng 660 VZ Matsumoto, T. verfasserin aut Carbon-13 NMR spectroscopic analysis of 24-methyl-$ Δ^{5,22} $-sterols in rape and mustard seed oils 1982 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © American Oil Chemists' Society 1982 Abstract 24-Methylcholesta-5,E-22-dien-3β-ol ($ C_{28} $ $ Δ^{5,22} $-sterol) was separated from the unsaponifiable matters of the following eight seed oils of Brassica species:Brassica campestris (candle I and II and torch),B. napus (tower and midas),B. juncea (brown and oriental mustards), andB. alba (yellow mustard). The configuration at C-24 methyl group of the respective sterols was evaluated $ by^{13} $C NMR spectroscopy. All the $ C_{28} $ $ Δ^{5,22} $-sterols in the Brassica seed oils were found to contain the C-24 epimer of brassicasterol,trans-22-dehydrocampesterol, in the range of ca. 10–30%. Preparative Thin Layer Chromatography Winged Bean Bean Accession Yellow Mustard Solvent Extraction Plant Shimizu, N. aut Itoh, T. aut Iida, T. aut Nishioka, A. aut Enthalten in Journal of the American Oil Chemists Society Springer-Verlag, 1947 59(1982), 12 vom: Dez., Seite 521-523 (DE-627)129595691 (DE-600)240684-6 (DE-576)015088715 0003-021X nnns volume:59 year:1982 number:12 month:12 pages:521-523 https://doi.org/10.1007/BF02636314 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE SSG-OLC-PHA SSG-OLC-DE-84 GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_26 GBV_ILN_70 GBV_ILN_95 GBV_ILN_252 GBV_ILN_2360 GBV_ILN_4012 GBV_ILN_4036 GBV_ILN_4046 GBV_ILN_4125 GBV_ILN_4219 GBV_ILN_4306 GBV_ILN_4315 AR 59 1982 12 12 521-523 |
| allfieldsGer |
10.1007/BF02636314 doi (DE-627)OLC2068085747 (DE-He213)BF02636314-p DE-627 ger DE-627 rakwb eng 660 VZ Matsumoto, T. verfasserin aut Carbon-13 NMR spectroscopic analysis of 24-methyl-$ Δ^{5,22} $-sterols in rape and mustard seed oils 1982 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © American Oil Chemists' Society 1982 Abstract 24-Methylcholesta-5,E-22-dien-3β-ol ($ C_{28} $ $ Δ^{5,22} $-sterol) was separated from the unsaponifiable matters of the following eight seed oils of Brassica species:Brassica campestris (candle I and II and torch),B. napus (tower and midas),B. juncea (brown and oriental mustards), andB. alba (yellow mustard). The configuration at C-24 methyl group of the respective sterols was evaluated $ by^{13} $C NMR spectroscopy. All the $ C_{28} $ $ Δ^{5,22} $-sterols in the Brassica seed oils were found to contain the C-24 epimer of brassicasterol,trans-22-dehydrocampesterol, in the range of ca. 10–30%. Preparative Thin Layer Chromatography Winged Bean Bean Accession Yellow Mustard Solvent Extraction Plant Shimizu, N. aut Itoh, T. aut Iida, T. aut Nishioka, A. aut Enthalten in Journal of the American Oil Chemists Society Springer-Verlag, 1947 59(1982), 12 vom: Dez., Seite 521-523 (DE-627)129595691 (DE-600)240684-6 (DE-576)015088715 0003-021X nnns volume:59 year:1982 number:12 month:12 pages:521-523 https://doi.org/10.1007/BF02636314 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE SSG-OLC-PHA SSG-OLC-DE-84 GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_26 GBV_ILN_70 GBV_ILN_95 GBV_ILN_252 GBV_ILN_2360 GBV_ILN_4012 GBV_ILN_4036 GBV_ILN_4046 GBV_ILN_4125 GBV_ILN_4219 GBV_ILN_4306 GBV_ILN_4315 AR 59 1982 12 12 521-523 |
| allfieldsSound |
10.1007/BF02636314 doi (DE-627)OLC2068085747 (DE-He213)BF02636314-p DE-627 ger DE-627 rakwb eng 660 VZ Matsumoto, T. verfasserin aut Carbon-13 NMR spectroscopic analysis of 24-methyl-$ Δ^{5,22} $-sterols in rape and mustard seed oils 1982 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © American Oil Chemists' Society 1982 Abstract 24-Methylcholesta-5,E-22-dien-3β-ol ($ C_{28} $ $ Δ^{5,22} $-sterol) was separated from the unsaponifiable matters of the following eight seed oils of Brassica species:Brassica campestris (candle I and II and torch),B. napus (tower and midas),B. juncea (brown and oriental mustards), andB. alba (yellow mustard). The configuration at C-24 methyl group of the respective sterols was evaluated $ by^{13} $C NMR spectroscopy. All the $ C_{28} $ $ Δ^{5,22} $-sterols in the Brassica seed oils were found to contain the C-24 epimer of brassicasterol,trans-22-dehydrocampesterol, in the range of ca. 10–30%. Preparative Thin Layer Chromatography Winged Bean Bean Accession Yellow Mustard Solvent Extraction Plant Shimizu, N. aut Itoh, T. aut Iida, T. aut Nishioka, A. aut Enthalten in Journal of the American Oil Chemists Society Springer-Verlag, 1947 59(1982), 12 vom: Dez., Seite 521-523 (DE-627)129595691 (DE-600)240684-6 (DE-576)015088715 0003-021X nnns volume:59 year:1982 number:12 month:12 pages:521-523 https://doi.org/10.1007/BF02636314 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE SSG-OLC-PHA SSG-OLC-DE-84 GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_26 GBV_ILN_70 GBV_ILN_95 GBV_ILN_252 GBV_ILN_2360 GBV_ILN_4012 GBV_ILN_4036 GBV_ILN_4046 GBV_ILN_4125 GBV_ILN_4219 GBV_ILN_4306 GBV_ILN_4315 AR 59 1982 12 12 521-523 |
| language |
English |
| source |
Enthalten in Journal of the American Oil Chemists Society 59(1982), 12 vom: Dez., Seite 521-523 volume:59 year:1982 number:12 month:12 pages:521-523 |
| sourceStr |
Enthalten in Journal of the American Oil Chemists Society 59(1982), 12 vom: Dez., Seite 521-523 volume:59 year:1982 number:12 month:12 pages:521-523 |
| format_phy_str_mv |
Article |
| institution |
findex.gbv.de |
| topic_facet |
Preparative Thin Layer Chromatography Winged Bean Bean Accession Yellow Mustard Solvent Extraction Plant |
| dewey-raw |
660 |
| isfreeaccess_bool |
false |
| container_title |
Journal of the American Oil Chemists Society |
| authorswithroles_txt_mv |
Matsumoto, T. @@aut@@ Shimizu, N. @@aut@@ Itoh, T. @@aut@@ Iida, T. @@aut@@ Nishioka, A. @@aut@@ |
| publishDateDaySort_date |
1982-12-01T00:00:00Z |
| hierarchy_top_id |
129595691 |
| dewey-sort |
3660 |
| id |
OLC2068085747 |
| language_de |
englisch |
| fullrecord |
<?xml version="1.0" encoding="UTF-8"?><collection xmlns="http://www.loc.gov/MARC21/slim"><record><leader>01000caa a22002652 4500</leader><controlfield tag="001">OLC2068085747</controlfield><controlfield tag="003">DE-627</controlfield><controlfield tag="005">20230515203546.0</controlfield><controlfield tag="007">tu</controlfield><controlfield tag="008">200819s1982 xx ||||| 00| ||eng c</controlfield><datafield tag="024" ind1="7" ind2=" "><subfield code="a">10.1007/BF02636314</subfield><subfield code="2">doi</subfield></datafield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(DE-627)OLC2068085747</subfield></datafield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(DE-He213)BF02636314-p</subfield></datafield><datafield tag="040" ind1=" " ind2=" "><subfield code="a">DE-627</subfield><subfield code="b">ger</subfield><subfield code="c">DE-627</subfield><subfield code="e">rakwb</subfield></datafield><datafield tag="041" ind1=" " ind2=" "><subfield code="a">eng</subfield></datafield><datafield tag="082" ind1="0" ind2="4"><subfield code="a">660</subfield><subfield code="q">VZ</subfield></datafield><datafield tag="100" ind1="1" ind2=" "><subfield code="a">Matsumoto, T.</subfield><subfield code="e">verfasserin</subfield><subfield code="4">aut</subfield></datafield><datafield tag="245" ind1="1" ind2="0"><subfield code="a">Carbon-13 NMR spectroscopic analysis of 24-methyl-$ Δ^{5,22} $-sterols in rape and mustard seed oils</subfield></datafield><datafield tag="264" ind1=" " ind2="1"><subfield code="c">1982</subfield></datafield><datafield tag="336" ind1=" " ind2=" "><subfield code="a">Text</subfield><subfield code="b">txt</subfield><subfield code="2">rdacontent</subfield></datafield><datafield tag="337" ind1=" " ind2=" "><subfield code="a">ohne Hilfsmittel zu benutzen</subfield><subfield code="b">n</subfield><subfield code="2">rdamedia</subfield></datafield><datafield tag="338" ind1=" " ind2=" "><subfield code="a">Band</subfield><subfield code="b">nc</subfield><subfield code="2">rdacarrier</subfield></datafield><datafield tag="500" ind1=" " ind2=" "><subfield code="a">© American Oil Chemists' Society 1982</subfield></datafield><datafield tag="520" ind1=" " ind2=" "><subfield code="a">Abstract 24-Methylcholesta-5,E-22-dien-3β-ol ($ C_{28} $ $ Δ^{5,22} $-sterol) was separated from the unsaponifiable matters of the following eight seed oils of Brassica species:Brassica campestris (candle I and II and torch),B. napus (tower and midas),B. juncea (brown and oriental mustards), andB. alba (yellow mustard). The configuration at C-24 methyl group of the respective sterols was evaluated $ by^{13} $C NMR spectroscopy. All the $ C_{28} $ $ Δ^{5,22} $-sterols in the Brassica seed oils were found to contain the C-24 epimer of brassicasterol,trans-22-dehydrocampesterol, in the range of ca. 10–30%.</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Preparative Thin Layer Chromatography</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Winged Bean</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Bean Accession</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Yellow Mustard</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Solvent Extraction Plant</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Shimizu, N.</subfield><subfield code="4">aut</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Itoh, T.</subfield><subfield code="4">aut</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Iida, T.</subfield><subfield code="4">aut</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Nishioka, A.</subfield><subfield code="4">aut</subfield></datafield><datafield tag="773" ind1="0" ind2="8"><subfield code="i">Enthalten in</subfield><subfield code="t">Journal of the American Oil Chemists Society</subfield><subfield code="d">Springer-Verlag, 1947</subfield><subfield code="g">59(1982), 12 vom: Dez., Seite 521-523</subfield><subfield code="w">(DE-627)129595691</subfield><subfield code="w">(DE-600)240684-6</subfield><subfield code="w">(DE-576)015088715</subfield><subfield code="x">0003-021X</subfield><subfield code="7">nnns</subfield></datafield><datafield tag="773" ind1="1" ind2="8"><subfield code="g">volume:59</subfield><subfield code="g">year:1982</subfield><subfield code="g">number:12</subfield><subfield code="g">month:12</subfield><subfield code="g">pages:521-523</subfield></datafield><datafield tag="856" ind1="4" ind2="1"><subfield code="u">https://doi.org/10.1007/BF02636314</subfield><subfield code="z">lizenzpflichtig</subfield><subfield code="3">Volltext</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_USEFLAG_A</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">SYSFLAG_A</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_OLC</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">SSG-OLC-TEC</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">SSG-OLC-CHE</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">SSG-OLC-PHA</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">SSG-OLC-DE-84</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_11</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_20</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_22</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_23</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_26</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_70</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_95</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_252</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2360</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4012</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4036</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4046</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4125</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4219</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4306</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4315</subfield></datafield><datafield tag="951" ind1=" " ind2=" "><subfield code="a">AR</subfield></datafield><datafield tag="952" ind1=" " ind2=" "><subfield code="d">59</subfield><subfield code="j">1982</subfield><subfield code="e">12</subfield><subfield code="c">12</subfield><subfield code="h">521-523</subfield></datafield></record></collection>
|
| author |
Matsumoto, T. |
| spellingShingle |
Matsumoto, T. ddc 660 misc Preparative Thin Layer Chromatography misc Winged Bean misc Bean Accession misc Yellow Mustard misc Solvent Extraction Plant Carbon-13 NMR spectroscopic analysis of 24-methyl-$ Δ^{5,22} $-sterols in rape and mustard seed oils |
| authorStr |
Matsumoto, T. |
| ppnlink_with_tag_str_mv |
@@773@@(DE-627)129595691 |
| format |
Article |
| dewey-ones |
660 - Chemical engineering |
| delete_txt_mv |
keep |
| author_role |
aut aut aut aut aut |
| collection |
OLC |
| remote_str |
false |
| illustrated |
Not Illustrated |
| issn |
0003-021X |
| topic_title |
660 VZ Carbon-13 NMR spectroscopic analysis of 24-methyl-$ Δ^{5,22} $-sterols in rape and mustard seed oils Preparative Thin Layer Chromatography Winged Bean Bean Accession Yellow Mustard Solvent Extraction Plant |
| topic |
ddc 660 misc Preparative Thin Layer Chromatography misc Winged Bean misc Bean Accession misc Yellow Mustard misc Solvent Extraction Plant |
| topic_unstemmed |
ddc 660 misc Preparative Thin Layer Chromatography misc Winged Bean misc Bean Accession misc Yellow Mustard misc Solvent Extraction Plant |
| topic_browse |
ddc 660 misc Preparative Thin Layer Chromatography misc Winged Bean misc Bean Accession misc Yellow Mustard misc Solvent Extraction Plant |
| format_facet |
Aufsätze Gedruckte Aufsätze |
| format_main_str_mv |
Text Zeitschrift/Artikel |
| carriertype_str_mv |
nc |
| hierarchy_parent_title |
Journal of the American Oil Chemists Society |
| hierarchy_parent_id |
129595691 |
| dewey-tens |
660 - Chemical engineering |
| hierarchy_top_title |
Journal of the American Oil Chemists Society |
| isfreeaccess_txt |
false |
| familylinks_str_mv |
(DE-627)129595691 (DE-600)240684-6 (DE-576)015088715 |
| title |
Carbon-13 NMR spectroscopic analysis of 24-methyl-$ Δ^{5,22} $-sterols in rape and mustard seed oils |
| ctrlnum |
(DE-627)OLC2068085747 (DE-He213)BF02636314-p |
| title_full |
Carbon-13 NMR spectroscopic analysis of 24-methyl-$ Δ^{5,22} $-sterols in rape and mustard seed oils |
| author_sort |
Matsumoto, T. |
| journal |
Journal of the American Oil Chemists Society |
| journalStr |
Journal of the American Oil Chemists Society |
| lang_code |
eng |
| isOA_bool |
false |
| dewey-hundreds |
600 - Technology |
| recordtype |
marc |
| publishDateSort |
1982 |
| contenttype_str_mv |
txt |
| container_start_page |
521 |
| author_browse |
Matsumoto, T. Shimizu, N. Itoh, T. Iida, T. Nishioka, A. |
| container_volume |
59 |
| class |
660 VZ |
| format_se |
Aufsätze |
| author-letter |
Matsumoto, T. |
| doi_str_mv |
10.1007/BF02636314 |
| dewey-full |
660 |
| title_sort |
carbon-13 nmr spectroscopic analysis of 24-methyl-$ δ^{5,22} $-sterols in rape and mustard seed oils |
| title_auth |
Carbon-13 NMR spectroscopic analysis of 24-methyl-$ Δ^{5,22} $-sterols in rape and mustard seed oils |
| abstract |
Abstract 24-Methylcholesta-5,E-22-dien-3β-ol ($ C_{28} $ $ Δ^{5,22} $-sterol) was separated from the unsaponifiable matters of the following eight seed oils of Brassica species:Brassica campestris (candle I and II and torch),B. napus (tower and midas),B. juncea (brown and oriental mustards), andB. alba (yellow mustard). The configuration at C-24 methyl group of the respective sterols was evaluated $ by^{13} $C NMR spectroscopy. All the $ C_{28} $ $ Δ^{5,22} $-sterols in the Brassica seed oils were found to contain the C-24 epimer of brassicasterol,trans-22-dehydrocampesterol, in the range of ca. 10–30%. © American Oil Chemists' Society 1982 |
| abstractGer |
Abstract 24-Methylcholesta-5,E-22-dien-3β-ol ($ C_{28} $ $ Δ^{5,22} $-sterol) was separated from the unsaponifiable matters of the following eight seed oils of Brassica species:Brassica campestris (candle I and II and torch),B. napus (tower and midas),B. juncea (brown and oriental mustards), andB. alba (yellow mustard). The configuration at C-24 methyl group of the respective sterols was evaluated $ by^{13} $C NMR spectroscopy. All the $ C_{28} $ $ Δ^{5,22} $-sterols in the Brassica seed oils were found to contain the C-24 epimer of brassicasterol,trans-22-dehydrocampesterol, in the range of ca. 10–30%. © American Oil Chemists' Society 1982 |
| abstract_unstemmed |
Abstract 24-Methylcholesta-5,E-22-dien-3β-ol ($ C_{28} $ $ Δ^{5,22} $-sterol) was separated from the unsaponifiable matters of the following eight seed oils of Brassica species:Brassica campestris (candle I and II and torch),B. napus (tower and midas),B. juncea (brown and oriental mustards), andB. alba (yellow mustard). The configuration at C-24 methyl group of the respective sterols was evaluated $ by^{13} $C NMR spectroscopy. All the $ C_{28} $ $ Δ^{5,22} $-sterols in the Brassica seed oils were found to contain the C-24 epimer of brassicasterol,trans-22-dehydrocampesterol, in the range of ca. 10–30%. © American Oil Chemists' Society 1982 |
| collection_details |
GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE SSG-OLC-PHA SSG-OLC-DE-84 GBV_ILN_11 GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_26 GBV_ILN_70 GBV_ILN_95 GBV_ILN_252 GBV_ILN_2360 GBV_ILN_4012 GBV_ILN_4036 GBV_ILN_4046 GBV_ILN_4125 GBV_ILN_4219 GBV_ILN_4306 GBV_ILN_4315 |
| container_issue |
12 |
| title_short |
Carbon-13 NMR spectroscopic analysis of 24-methyl-$ Δ^{5,22} $-sterols in rape and mustard seed oils |
| url |
https://doi.org/10.1007/BF02636314 |
| remote_bool |
false |
| author2 |
Shimizu, N. Itoh, T. Iida, T. Nishioka, A. |
| author2Str |
Shimizu, N. Itoh, T. Iida, T. Nishioka, A. |
| ppnlink |
129595691 |
| mediatype_str_mv |
n |
| isOA_txt |
false |
| hochschulschrift_bool |
false |
| doi_str |
10.1007/BF02636314 |
| up_date |
2024-07-03T17:32:44.453Z |
| _version_ |
1803580042857414656 |
| fullrecord_marcxml |
<?xml version="1.0" encoding="UTF-8"?><collection xmlns="http://www.loc.gov/MARC21/slim"><record><leader>01000caa a22002652 4500</leader><controlfield tag="001">OLC2068085747</controlfield><controlfield tag="003">DE-627</controlfield><controlfield tag="005">20230515203546.0</controlfield><controlfield tag="007">tu</controlfield><controlfield tag="008">200819s1982 xx ||||| 00| ||eng c</controlfield><datafield tag="024" ind1="7" ind2=" "><subfield code="a">10.1007/BF02636314</subfield><subfield code="2">doi</subfield></datafield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(DE-627)OLC2068085747</subfield></datafield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(DE-He213)BF02636314-p</subfield></datafield><datafield tag="040" ind1=" " ind2=" "><subfield code="a">DE-627</subfield><subfield code="b">ger</subfield><subfield code="c">DE-627</subfield><subfield code="e">rakwb</subfield></datafield><datafield tag="041" ind1=" " ind2=" "><subfield code="a">eng</subfield></datafield><datafield tag="082" ind1="0" ind2="4"><subfield code="a">660</subfield><subfield code="q">VZ</subfield></datafield><datafield tag="100" ind1="1" ind2=" "><subfield code="a">Matsumoto, T.</subfield><subfield code="e">verfasserin</subfield><subfield code="4">aut</subfield></datafield><datafield tag="245" ind1="1" ind2="0"><subfield code="a">Carbon-13 NMR spectroscopic analysis of 24-methyl-$ Δ^{5,22} $-sterols in rape and mustard seed oils</subfield></datafield><datafield tag="264" ind1=" " ind2="1"><subfield code="c">1982</subfield></datafield><datafield tag="336" ind1=" " ind2=" "><subfield code="a">Text</subfield><subfield code="b">txt</subfield><subfield code="2">rdacontent</subfield></datafield><datafield tag="337" ind1=" " ind2=" "><subfield code="a">ohne Hilfsmittel zu benutzen</subfield><subfield code="b">n</subfield><subfield code="2">rdamedia</subfield></datafield><datafield tag="338" ind1=" " ind2=" "><subfield code="a">Band</subfield><subfield code="b">nc</subfield><subfield code="2">rdacarrier</subfield></datafield><datafield tag="500" ind1=" " ind2=" "><subfield code="a">© American Oil Chemists' Society 1982</subfield></datafield><datafield tag="520" ind1=" " ind2=" "><subfield code="a">Abstract 24-Methylcholesta-5,E-22-dien-3β-ol ($ C_{28} $ $ Δ^{5,22} $-sterol) was separated from the unsaponifiable matters of the following eight seed oils of Brassica species:Brassica campestris (candle I and II and torch),B. napus (tower and midas),B. juncea (brown and oriental mustards), andB. alba (yellow mustard). The configuration at C-24 methyl group of the respective sterols was evaluated $ by^{13} $C NMR spectroscopy. All the $ C_{28} $ $ Δ^{5,22} $-sterols in the Brassica seed oils were found to contain the C-24 epimer of brassicasterol,trans-22-dehydrocampesterol, in the range of ca. 10–30%.</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Preparative Thin Layer Chromatography</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Winged Bean</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Bean Accession</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Yellow Mustard</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Solvent Extraction Plant</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Shimizu, N.</subfield><subfield code="4">aut</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Itoh, T.</subfield><subfield code="4">aut</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Iida, T.</subfield><subfield code="4">aut</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Nishioka, A.</subfield><subfield code="4">aut</subfield></datafield><datafield tag="773" ind1="0" ind2="8"><subfield code="i">Enthalten in</subfield><subfield code="t">Journal of the American Oil Chemists Society</subfield><subfield code="d">Springer-Verlag, 1947</subfield><subfield code="g">59(1982), 12 vom: Dez., Seite 521-523</subfield><subfield code="w">(DE-627)129595691</subfield><subfield code="w">(DE-600)240684-6</subfield><subfield code="w">(DE-576)015088715</subfield><subfield code="x">0003-021X</subfield><subfield code="7">nnns</subfield></datafield><datafield tag="773" ind1="1" ind2="8"><subfield code="g">volume:59</subfield><subfield code="g">year:1982</subfield><subfield code="g">number:12</subfield><subfield code="g">month:12</subfield><subfield code="g">pages:521-523</subfield></datafield><datafield tag="856" ind1="4" ind2="1"><subfield code="u">https://doi.org/10.1007/BF02636314</subfield><subfield code="z">lizenzpflichtig</subfield><subfield code="3">Volltext</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_USEFLAG_A</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">SYSFLAG_A</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_OLC</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">SSG-OLC-TEC</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">SSG-OLC-CHE</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">SSG-OLC-PHA</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">SSG-OLC-DE-84</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_11</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_20</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_22</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_23</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_26</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_70</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_95</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_252</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2360</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4012</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4036</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4046</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4125</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4219</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4306</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4315</subfield></datafield><datafield tag="951" ind1=" " ind2=" "><subfield code="a">AR</subfield></datafield><datafield tag="952" ind1=" " ind2=" "><subfield code="d">59</subfield><subfield code="j">1982</subfield><subfield code="e">12</subfield><subfield code="c">12</subfield><subfield code="h">521-523</subfield></datafield></record></collection>
|
| score |
7.401458 |