Synthesis of dodecanedioic acid fromvernonia galamensis oil

Abstract Dodecanedioic acid, currently available from elaborate synthesis utilizing petrochemical feedstock, was synthesized fromVernonia galamensis oil via an efficient, relatively simple three-reaction sequence that involved the room temperature oxidation of 12,13-epoxystearic acid. The first and...
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Autor*in:	Ayorinde, Folahan O. [verfasserIn] Powers, Fiona T. Streete, Ludwig D. Shepard, Robert L. Tabi, Dorothy N.

Format:	Artikel
Sprache:	Englisch

Erschienen:	1989

Schlagwörter:	Stearic Acid Hexanoic Acid Azelaic Acid Dibasic Acid Vernolic Acid

Anmerkung:	© American Oil Chemists’ Society 1989

Übergeordnetes Werk:	Enthalten in: Journal of the American Oil Chemists’ Society - Springer-Verlag, 1947, 66(1989), 5 vom: Mai, Seite 690-692
Übergeordnetes Werk:	volume:66 ; year:1989 ; number:5 ; month:05 ; pages:690-692

Links:	Volltext

DOI / URN:	10.1007/BF02669953

Katalog-ID:	OLC2068109115

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520			\|a Abstract Dodecanedioic acid, currently available from elaborate synthesis utilizing petrochemical feedstock, was synthesized fromVernonia galamensis oil via an efficient, relatively simple three-reaction sequence that involved the room temperature oxidation of 12,13-epoxystearic acid. The first and second steps of the reaction scheme were saponification and hydrogenation, both of which were almost quantitative. The third reaction, involving chromic acid oxidation of the resulting epoxy acid, afforded greater than 50% of the theoretical yield of dodecanedioic acid (>95% purity, m.p. 123–125°C; lit. m.p. 128–130°C).
650		4	\|a Stearic Acid
650		4	\|a Hexanoic Acid
650		4	\|a Azelaic Acid
650		4	\|a Dibasic Acid
650		4	\|a Vernolic Acid
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700	1		\|a Streete, Ludwig D. \|4 aut
700	1		\|a Shepard, Robert L. \|4 aut
700	1		\|a Tabi, Dorothy N. \|4 aut
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allfields	10.1007/BF02669953 doi (DE-627)OLC2068109115 (DE-He213)BF02669953-p DE-627 ger DE-627 rakwb eng 660 VZ Ayorinde, Folahan O. verfasserin aut Synthesis of dodecanedioic acid fromvernonia galamensis oil 1989 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © American Oil Chemists’ Society 1989 Abstract Dodecanedioic acid, currently available from elaborate synthesis utilizing petrochemical feedstock, was synthesized fromVernonia galamensis oil via an efficient, relatively simple three-reaction sequence that involved the room temperature oxidation of 12,13-epoxystearic acid. The first and second steps of the reaction scheme were saponification and hydrogenation, both of which were almost quantitative. The third reaction, involving chromic acid oxidation of the resulting epoxy acid, afforded greater than 50% of the theoretical yield of dodecanedioic acid (>95% purity, m.p. 123–125°C; lit. m.p. 128–130°C). Stearic Acid Hexanoic Acid Azelaic Acid Dibasic Acid Vernolic Acid Powers, Fiona T. aut Streete, Ludwig D. aut Shepard, Robert L. aut Tabi, Dorothy N. aut Enthalten in Journal of the American Oil Chemists’ Society Springer-Verlag, 1947 66(1989), 5 vom: Mai, Seite 690-692 (DE-627)129595691 (DE-600)240684-6 (DE-576)015088715 0003-021X nnns volume:66 year:1989 number:5 month:05 pages:690-692 https://doi.org/10.1007/BF02669953 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE SSG-OLC-PHA SSG-OLC-DE-84 GBV_ILN_11 GBV_ILN_20 GBV_ILN_23 GBV_ILN_26 GBV_ILN_70 GBV_ILN_95 GBV_ILN_252 GBV_ILN_4012 GBV_ILN_4046 GBV_ILN_4219 GBV_ILN_4306 GBV_ILN_4315 AR 66 1989 5 05 690-692
spelling	10.1007/BF02669953 doi (DE-627)OLC2068109115 (DE-He213)BF02669953-p DE-627 ger DE-627 rakwb eng 660 VZ Ayorinde, Folahan O. verfasserin aut Synthesis of dodecanedioic acid fromvernonia galamensis oil 1989 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © American Oil Chemists’ Society 1989 Abstract Dodecanedioic acid, currently available from elaborate synthesis utilizing petrochemical feedstock, was synthesized fromVernonia galamensis oil via an efficient, relatively simple three-reaction sequence that involved the room temperature oxidation of 12,13-epoxystearic acid. The first and second steps of the reaction scheme were saponification and hydrogenation, both of which were almost quantitative. The third reaction, involving chromic acid oxidation of the resulting epoxy acid, afforded greater than 50% of the theoretical yield of dodecanedioic acid (>95% purity, m.p. 123–125°C; lit. m.p. 128–130°C). Stearic Acid Hexanoic Acid Azelaic Acid Dibasic Acid Vernolic Acid Powers, Fiona T. aut Streete, Ludwig D. aut Shepard, Robert L. aut Tabi, Dorothy N. aut Enthalten in Journal of the American Oil Chemists’ Society Springer-Verlag, 1947 66(1989), 5 vom: Mai, Seite 690-692 (DE-627)129595691 (DE-600)240684-6 (DE-576)015088715 0003-021X nnns volume:66 year:1989 number:5 month:05 pages:690-692 https://doi.org/10.1007/BF02669953 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE SSG-OLC-PHA SSG-OLC-DE-84 GBV_ILN_11 GBV_ILN_20 GBV_ILN_23 GBV_ILN_26 GBV_ILN_70 GBV_ILN_95 GBV_ILN_252 GBV_ILN_4012 GBV_ILN_4046 GBV_ILN_4219 GBV_ILN_4306 GBV_ILN_4315 AR 66 1989 5 05 690-692
allfields_unstemmed	10.1007/BF02669953 doi (DE-627)OLC2068109115 (DE-He213)BF02669953-p DE-627 ger DE-627 rakwb eng 660 VZ Ayorinde, Folahan O. verfasserin aut Synthesis of dodecanedioic acid fromvernonia galamensis oil 1989 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © American Oil Chemists’ Society 1989 Abstract Dodecanedioic acid, currently available from elaborate synthesis utilizing petrochemical feedstock, was synthesized fromVernonia galamensis oil via an efficient, relatively simple three-reaction sequence that involved the room temperature oxidation of 12,13-epoxystearic acid. The first and second steps of the reaction scheme were saponification and hydrogenation, both of which were almost quantitative. The third reaction, involving chromic acid oxidation of the resulting epoxy acid, afforded greater than 50% of the theoretical yield of dodecanedioic acid (>95% purity, m.p. 123–125°C; lit. m.p. 128–130°C). Stearic Acid Hexanoic Acid Azelaic Acid Dibasic Acid Vernolic Acid Powers, Fiona T. aut Streete, Ludwig D. aut Shepard, Robert L. aut Tabi, Dorothy N. aut Enthalten in Journal of the American Oil Chemists’ Society Springer-Verlag, 1947 66(1989), 5 vom: Mai, Seite 690-692 (DE-627)129595691 (DE-600)240684-6 (DE-576)015088715 0003-021X nnns volume:66 year:1989 number:5 month:05 pages:690-692 https://doi.org/10.1007/BF02669953 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE SSG-OLC-PHA SSG-OLC-DE-84 GBV_ILN_11 GBV_ILN_20 GBV_ILN_23 GBV_ILN_26 GBV_ILN_70 GBV_ILN_95 GBV_ILN_252 GBV_ILN_4012 GBV_ILN_4046 GBV_ILN_4219 GBV_ILN_4306 GBV_ILN_4315 AR 66 1989 5 05 690-692
allfieldsGer	10.1007/BF02669953 doi (DE-627)OLC2068109115 (DE-He213)BF02669953-p DE-627 ger DE-627 rakwb eng 660 VZ Ayorinde, Folahan O. verfasserin aut Synthesis of dodecanedioic acid fromvernonia galamensis oil 1989 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © American Oil Chemists’ Society 1989 Abstract Dodecanedioic acid, currently available from elaborate synthesis utilizing petrochemical feedstock, was synthesized fromVernonia galamensis oil via an efficient, relatively simple three-reaction sequence that involved the room temperature oxidation of 12,13-epoxystearic acid. The first and second steps of the reaction scheme were saponification and hydrogenation, both of which were almost quantitative. The third reaction, involving chromic acid oxidation of the resulting epoxy acid, afforded greater than 50% of the theoretical yield of dodecanedioic acid (>95% purity, m.p. 123–125°C; lit. m.p. 128–130°C). Stearic Acid Hexanoic Acid Azelaic Acid Dibasic Acid Vernolic Acid Powers, Fiona T. aut Streete, Ludwig D. aut Shepard, Robert L. aut Tabi, Dorothy N. aut Enthalten in Journal of the American Oil Chemists’ Society Springer-Verlag, 1947 66(1989), 5 vom: Mai, Seite 690-692 (DE-627)129595691 (DE-600)240684-6 (DE-576)015088715 0003-021X nnns volume:66 year:1989 number:5 month:05 pages:690-692 https://doi.org/10.1007/BF02669953 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE SSG-OLC-PHA SSG-OLC-DE-84 GBV_ILN_11 GBV_ILN_20 GBV_ILN_23 GBV_ILN_26 GBV_ILN_70 GBV_ILN_95 GBV_ILN_252 GBV_ILN_4012 GBV_ILN_4046 GBV_ILN_4219 GBV_ILN_4306 GBV_ILN_4315 AR 66 1989 5 05 690-692
allfieldsSound	10.1007/BF02669953 doi (DE-627)OLC2068109115 (DE-He213)BF02669953-p DE-627 ger DE-627 rakwb eng 660 VZ Ayorinde, Folahan O. verfasserin aut Synthesis of dodecanedioic acid fromvernonia galamensis oil 1989 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © American Oil Chemists’ Society 1989 Abstract Dodecanedioic acid, currently available from elaborate synthesis utilizing petrochemical feedstock, was synthesized fromVernonia galamensis oil via an efficient, relatively simple three-reaction sequence that involved the room temperature oxidation of 12,13-epoxystearic acid. The first and second steps of the reaction scheme were saponification and hydrogenation, both of which were almost quantitative. The third reaction, involving chromic acid oxidation of the resulting epoxy acid, afforded greater than 50% of the theoretical yield of dodecanedioic acid (>95% purity, m.p. 123–125°C; lit. m.p. 128–130°C). Stearic Acid Hexanoic Acid Azelaic Acid Dibasic Acid Vernolic Acid Powers, Fiona T. aut Streete, Ludwig D. aut Shepard, Robert L. aut Tabi, Dorothy N. aut Enthalten in Journal of the American Oil Chemists’ Society Springer-Verlag, 1947 66(1989), 5 vom: Mai, Seite 690-692 (DE-627)129595691 (DE-600)240684-6 (DE-576)015088715 0003-021X nnns volume:66 year:1989 number:5 month:05 pages:690-692 https://doi.org/10.1007/BF02669953 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE SSG-OLC-PHA SSG-OLC-DE-84 GBV_ILN_11 GBV_ILN_20 GBV_ILN_23 GBV_ILN_26 GBV_ILN_70 GBV_ILN_95 GBV_ILN_252 GBV_ILN_4012 GBV_ILN_4046 GBV_ILN_4219 GBV_ILN_4306 GBV_ILN_4315 AR 66 1989 5 05 690-692
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author	Ayorinde, Folahan O.
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title_sort	synthesis of dodecanedioic acid fromvernonia galamensis oil
title_auth	Synthesis of dodecanedioic acid fromvernonia galamensis oil
abstract	Abstract Dodecanedioic acid, currently available from elaborate synthesis utilizing petrochemical feedstock, was synthesized fromVernonia galamensis oil via an efficient, relatively simple three-reaction sequence that involved the room temperature oxidation of 12,13-epoxystearic acid. The first and second steps of the reaction scheme were saponification and hydrogenation, both of which were almost quantitative. The third reaction, involving chromic acid oxidation of the resulting epoxy acid, afforded greater than 50% of the theoretical yield of dodecanedioic acid (>95% purity, m.p. 123–125°C; lit. m.p. 128–130°C). © American Oil Chemists’ Society 1989
abstractGer	Abstract Dodecanedioic acid, currently available from elaborate synthesis utilizing petrochemical feedstock, was synthesized fromVernonia galamensis oil via an efficient, relatively simple three-reaction sequence that involved the room temperature oxidation of 12,13-epoxystearic acid. The first and second steps of the reaction scheme were saponification and hydrogenation, both of which were almost quantitative. The third reaction, involving chromic acid oxidation of the resulting epoxy acid, afforded greater than 50% of the theoretical yield of dodecanedioic acid (>95% purity, m.p. 123–125°C; lit. m.p. 128–130°C). © American Oil Chemists’ Society 1989
abstract_unstemmed	Abstract Dodecanedioic acid, currently available from elaborate synthesis utilizing petrochemical feedstock, was synthesized fromVernonia galamensis oil via an efficient, relatively simple three-reaction sequence that involved the room temperature oxidation of 12,13-epoxystearic acid. The first and second steps of the reaction scheme were saponification and hydrogenation, both of which were almost quantitative. The third reaction, involving chromic acid oxidation of the resulting epoxy acid, afforded greater than 50% of the theoretical yield of dodecanedioic acid (>95% purity, m.p. 123–125°C; lit. m.p. 128–130°C). © American Oil Chemists’ Society 1989
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container_issue	5
title_short	Synthesis of dodecanedioic acid fromvernonia galamensis oil
url	https://doi.org/10.1007/BF02669953
remote_bool	false
author2	Powers, Fiona T. Streete, Ludwig D. Shepard, Robert L. Tabi, Dorothy N.
author2Str	Powers, Fiona T. Streete, Ludwig D. Shepard, Robert L. Tabi, Dorothy N.
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doi_str	10.1007/BF02669953
up_date	2024-07-03T17:36:55.259Z
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Synthesis of dodecanedioic acid fromvernonia galamensis oil

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