Supercritical Fluid Extraction and Chromatography of Lipids in Bilberry
Abstract A supercritical fluid extraction (SFE) method has been developed for the extraction of lipids in bilberry. Experimental design was used to optimize pressure, temperature and extraction time using $ CO_{2} $ as solvent. Best SFE condition for total lipids was 450 bar, 60 °C and 45 min. The S...
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Gespeichert in:
| Autor*in: |
Jumaah, Firas [verfasserIn] |
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| Format: |
Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2015 |
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| Schlagwörter: |
Supercritical fluid extraction |
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| Anmerkung: |
© The Author(s) 2015 |
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| Übergeordnetes Werk: |
Enthalten in: Journal of the American Oil Chemists' Society - Springer Berlin Heidelberg, 1947, 92(2015), 8 vom: 11. Juli, Seite 1103-1111 |
|---|---|
| Übergeordnetes Werk: |
volume:92 ; year:2015 ; number:8 ; day:11 ; month:07 ; pages:1103-1111 |
| Links: |
|---|
| DOI / URN: |
10.1007/s11746-015-2680-x |
|---|
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OLC2068164280 |
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| 520 | |a Abstract A supercritical fluid extraction (SFE) method has been developed for the extraction of lipids in bilberry. Experimental design was used to optimize pressure, temperature and extraction time using $ CO_{2} $ as solvent. Best SFE condition for total lipids was 450 bar, 60 °C and 45 min. The SFE method was compared to conventional Bligh & Dyer (B&D) extraction. The amount of fatty acid methyl esters (FAME) was found to be 4.84 ± 0.06 mg and 4.564 ± 0.003 mg per g of the freeze-dried bilberry sample for the developed SFE and B&D methods, respectively, while the amount of total lipids was found to be 54.40 ± 6.06 mg and 65.70 ± 0.67 mg per g of sample for SFE and B&D, respectively. This discrepancy between FAME and total lipids could be explained by the presence of wax esters, sterol esters, carotenoids and phospholipids, as determined by supercritical fluid chromatography. | ||
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10.1007/s11746-015-2680-x doi (DE-627)OLC2068164280 (DE-He213)s11746-015-2680-x-p DE-627 ger DE-627 rakwb eng 660 VZ Jumaah, Firas verfasserin aut Supercritical Fluid Extraction and Chromatography of Lipids in Bilberry 2015 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © The Author(s) 2015 Abstract A supercritical fluid extraction (SFE) method has been developed for the extraction of lipids in bilberry. Experimental design was used to optimize pressure, temperature and extraction time using $ CO_{2} $ as solvent. Best SFE condition for total lipids was 450 bar, 60 °C and 45 min. The SFE method was compared to conventional Bligh & Dyer (B&D) extraction. The amount of fatty acid methyl esters (FAME) was found to be 4.84 ± 0.06 mg and 4.564 ± 0.003 mg per g of the freeze-dried bilberry sample for the developed SFE and B&D methods, respectively, while the amount of total lipids was found to be 54.40 ± 6.06 mg and 65.70 ± 0.67 mg per g of sample for SFE and B&D, respectively. This discrepancy between FAME and total lipids could be explained by the presence of wax esters, sterol esters, carotenoids and phospholipids, as determined by supercritical fluid chromatography. Bilberry Supercritical fluid extraction Supercritical fluid chromatography GC–MS Lipids Fatty acids Sandahl, Margareta aut Turner, Charlotta aut Enthalten in Journal of the American Oil Chemists' Society Springer Berlin Heidelberg, 1947 92(2015), 8 vom: 11. Juli, Seite 1103-1111 (DE-627)129595691 (DE-600)240684-6 (DE-576)015088715 0003-021X nnns volume:92 year:2015 number:8 day:11 month:07 pages:1103-1111 https://doi.org/10.1007/s11746-015-2680-x lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE SSG-OLC-PHA SSG-OLC-DE-84 GBV_ILN_70 GBV_ILN_183 GBV_ILN_2018 GBV_ILN_4012 GBV_ILN_4219 AR 92 2015 8 11 07 1103-1111 |
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10.1007/s11746-015-2680-x doi (DE-627)OLC2068164280 (DE-He213)s11746-015-2680-x-p DE-627 ger DE-627 rakwb eng 660 VZ Jumaah, Firas verfasserin aut Supercritical Fluid Extraction and Chromatography of Lipids in Bilberry 2015 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © The Author(s) 2015 Abstract A supercritical fluid extraction (SFE) method has been developed for the extraction of lipids in bilberry. Experimental design was used to optimize pressure, temperature and extraction time using $ CO_{2} $ as solvent. Best SFE condition for total lipids was 450 bar, 60 °C and 45 min. The SFE method was compared to conventional Bligh & Dyer (B&D) extraction. The amount of fatty acid methyl esters (FAME) was found to be 4.84 ± 0.06 mg and 4.564 ± 0.003 mg per g of the freeze-dried bilberry sample for the developed SFE and B&D methods, respectively, while the amount of total lipids was found to be 54.40 ± 6.06 mg and 65.70 ± 0.67 mg per g of sample for SFE and B&D, respectively. This discrepancy between FAME and total lipids could be explained by the presence of wax esters, sterol esters, carotenoids and phospholipids, as determined by supercritical fluid chromatography. Bilberry Supercritical fluid extraction Supercritical fluid chromatography GC–MS Lipids Fatty acids Sandahl, Margareta aut Turner, Charlotta aut Enthalten in Journal of the American Oil Chemists' Society Springer Berlin Heidelberg, 1947 92(2015), 8 vom: 11. Juli, Seite 1103-1111 (DE-627)129595691 (DE-600)240684-6 (DE-576)015088715 0003-021X nnns volume:92 year:2015 number:8 day:11 month:07 pages:1103-1111 https://doi.org/10.1007/s11746-015-2680-x lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE SSG-OLC-PHA SSG-OLC-DE-84 GBV_ILN_70 GBV_ILN_183 GBV_ILN_2018 GBV_ILN_4012 GBV_ILN_4219 AR 92 2015 8 11 07 1103-1111 |
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10.1007/s11746-015-2680-x doi (DE-627)OLC2068164280 (DE-He213)s11746-015-2680-x-p DE-627 ger DE-627 rakwb eng 660 VZ Jumaah, Firas verfasserin aut Supercritical Fluid Extraction and Chromatography of Lipids in Bilberry 2015 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © The Author(s) 2015 Abstract A supercritical fluid extraction (SFE) method has been developed for the extraction of lipids in bilberry. Experimental design was used to optimize pressure, temperature and extraction time using $ CO_{2} $ as solvent. Best SFE condition for total lipids was 450 bar, 60 °C and 45 min. The SFE method was compared to conventional Bligh & Dyer (B&D) extraction. The amount of fatty acid methyl esters (FAME) was found to be 4.84 ± 0.06 mg and 4.564 ± 0.003 mg per g of the freeze-dried bilberry sample for the developed SFE and B&D methods, respectively, while the amount of total lipids was found to be 54.40 ± 6.06 mg and 65.70 ± 0.67 mg per g of sample for SFE and B&D, respectively. This discrepancy between FAME and total lipids could be explained by the presence of wax esters, sterol esters, carotenoids and phospholipids, as determined by supercritical fluid chromatography. Bilberry Supercritical fluid extraction Supercritical fluid chromatography GC–MS Lipids Fatty acids Sandahl, Margareta aut Turner, Charlotta aut Enthalten in Journal of the American Oil Chemists' Society Springer Berlin Heidelberg, 1947 92(2015), 8 vom: 11. Juli, Seite 1103-1111 (DE-627)129595691 (DE-600)240684-6 (DE-576)015088715 0003-021X nnns volume:92 year:2015 number:8 day:11 month:07 pages:1103-1111 https://doi.org/10.1007/s11746-015-2680-x lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE SSG-OLC-PHA SSG-OLC-DE-84 GBV_ILN_70 GBV_ILN_183 GBV_ILN_2018 GBV_ILN_4012 GBV_ILN_4219 AR 92 2015 8 11 07 1103-1111 |
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10.1007/s11746-015-2680-x doi (DE-627)OLC2068164280 (DE-He213)s11746-015-2680-x-p DE-627 ger DE-627 rakwb eng 660 VZ Jumaah, Firas verfasserin aut Supercritical Fluid Extraction and Chromatography of Lipids in Bilberry 2015 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © The Author(s) 2015 Abstract A supercritical fluid extraction (SFE) method has been developed for the extraction of lipids in bilberry. Experimental design was used to optimize pressure, temperature and extraction time using $ CO_{2} $ as solvent. Best SFE condition for total lipids was 450 bar, 60 °C and 45 min. The SFE method was compared to conventional Bligh & Dyer (B&D) extraction. The amount of fatty acid methyl esters (FAME) was found to be 4.84 ± 0.06 mg and 4.564 ± 0.003 mg per g of the freeze-dried bilberry sample for the developed SFE and B&D methods, respectively, while the amount of total lipids was found to be 54.40 ± 6.06 mg and 65.70 ± 0.67 mg per g of sample for SFE and B&D, respectively. This discrepancy between FAME and total lipids could be explained by the presence of wax esters, sterol esters, carotenoids and phospholipids, as determined by supercritical fluid chromatography. Bilberry Supercritical fluid extraction Supercritical fluid chromatography GC–MS Lipids Fatty acids Sandahl, Margareta aut Turner, Charlotta aut Enthalten in Journal of the American Oil Chemists' Society Springer Berlin Heidelberg, 1947 92(2015), 8 vom: 11. Juli, Seite 1103-1111 (DE-627)129595691 (DE-600)240684-6 (DE-576)015088715 0003-021X nnns volume:92 year:2015 number:8 day:11 month:07 pages:1103-1111 https://doi.org/10.1007/s11746-015-2680-x lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE SSG-OLC-PHA SSG-OLC-DE-84 GBV_ILN_70 GBV_ILN_183 GBV_ILN_2018 GBV_ILN_4012 GBV_ILN_4219 AR 92 2015 8 11 07 1103-1111 |
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10.1007/s11746-015-2680-x doi (DE-627)OLC2068164280 (DE-He213)s11746-015-2680-x-p DE-627 ger DE-627 rakwb eng 660 VZ Jumaah, Firas verfasserin aut Supercritical Fluid Extraction and Chromatography of Lipids in Bilberry 2015 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © The Author(s) 2015 Abstract A supercritical fluid extraction (SFE) method has been developed for the extraction of lipids in bilberry. Experimental design was used to optimize pressure, temperature and extraction time using $ CO_{2} $ as solvent. Best SFE condition for total lipids was 450 bar, 60 °C and 45 min. The SFE method was compared to conventional Bligh & Dyer (B&D) extraction. The amount of fatty acid methyl esters (FAME) was found to be 4.84 ± 0.06 mg and 4.564 ± 0.003 mg per g of the freeze-dried bilberry sample for the developed SFE and B&D methods, respectively, while the amount of total lipids was found to be 54.40 ± 6.06 mg and 65.70 ± 0.67 mg per g of sample for SFE and B&D, respectively. This discrepancy between FAME and total lipids could be explained by the presence of wax esters, sterol esters, carotenoids and phospholipids, as determined by supercritical fluid chromatography. Bilberry Supercritical fluid extraction Supercritical fluid chromatography GC–MS Lipids Fatty acids Sandahl, Margareta aut Turner, Charlotta aut Enthalten in Journal of the American Oil Chemists' Society Springer Berlin Heidelberg, 1947 92(2015), 8 vom: 11. Juli, Seite 1103-1111 (DE-627)129595691 (DE-600)240684-6 (DE-576)015088715 0003-021X nnns volume:92 year:2015 number:8 day:11 month:07 pages:1103-1111 https://doi.org/10.1007/s11746-015-2680-x lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE SSG-OLC-PHA SSG-OLC-DE-84 GBV_ILN_70 GBV_ILN_183 GBV_ILN_2018 GBV_ILN_4012 GBV_ILN_4219 AR 92 2015 8 11 07 1103-1111 |
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Supercritical Fluid Extraction and Chromatography of Lipids in Bilberry |
| abstract |
Abstract A supercritical fluid extraction (SFE) method has been developed for the extraction of lipids in bilberry. Experimental design was used to optimize pressure, temperature and extraction time using $ CO_{2} $ as solvent. Best SFE condition for total lipids was 450 bar, 60 °C and 45 min. The SFE method was compared to conventional Bligh & Dyer (B&D) extraction. The amount of fatty acid methyl esters (FAME) was found to be 4.84 ± 0.06 mg and 4.564 ± 0.003 mg per g of the freeze-dried bilberry sample for the developed SFE and B&D methods, respectively, while the amount of total lipids was found to be 54.40 ± 6.06 mg and 65.70 ± 0.67 mg per g of sample for SFE and B&D, respectively. This discrepancy between FAME and total lipids could be explained by the presence of wax esters, sterol esters, carotenoids and phospholipids, as determined by supercritical fluid chromatography. © The Author(s) 2015 |
| abstractGer |
Abstract A supercritical fluid extraction (SFE) method has been developed for the extraction of lipids in bilberry. Experimental design was used to optimize pressure, temperature and extraction time using $ CO_{2} $ as solvent. Best SFE condition for total lipids was 450 bar, 60 °C and 45 min. The SFE method was compared to conventional Bligh & Dyer (B&D) extraction. The amount of fatty acid methyl esters (FAME) was found to be 4.84 ± 0.06 mg and 4.564 ± 0.003 mg per g of the freeze-dried bilberry sample for the developed SFE and B&D methods, respectively, while the amount of total lipids was found to be 54.40 ± 6.06 mg and 65.70 ± 0.67 mg per g of sample for SFE and B&D, respectively. This discrepancy between FAME and total lipids could be explained by the presence of wax esters, sterol esters, carotenoids and phospholipids, as determined by supercritical fluid chromatography. © The Author(s) 2015 |
| abstract_unstemmed |
Abstract A supercritical fluid extraction (SFE) method has been developed for the extraction of lipids in bilberry. Experimental design was used to optimize pressure, temperature and extraction time using $ CO_{2} $ as solvent. Best SFE condition for total lipids was 450 bar, 60 °C and 45 min. The SFE method was compared to conventional Bligh & Dyer (B&D) extraction. The amount of fatty acid methyl esters (FAME) was found to be 4.84 ± 0.06 mg and 4.564 ± 0.003 mg per g of the freeze-dried bilberry sample for the developed SFE and B&D methods, respectively, while the amount of total lipids was found to be 54.40 ± 6.06 mg and 65.70 ± 0.67 mg per g of sample for SFE and B&D, respectively. This discrepancy between FAME and total lipids could be explained by the presence of wax esters, sterol esters, carotenoids and phospholipids, as determined by supercritical fluid chromatography. © The Author(s) 2015 |
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| container_issue |
8 |
| title_short |
Supercritical Fluid Extraction and Chromatography of Lipids in Bilberry |
| url |
https://doi.org/10.1007/s11746-015-2680-x |
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false |
| author2 |
Sandahl, Margareta Turner, Charlotta |
| author2Str |
Sandahl, Margareta Turner, Charlotta |
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| doi_str |
10.1007/s11746-015-2680-x |
| up_date |
2024-07-03T17:50:35.788Z |
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