Supercritical Fluid Extraction and Chromatography of Lipids in Bilberry
Abstract A supercritical fluid extraction (SFE) method has been developed for the extraction of lipids in bilberry. Experimental design was used to optimize pressure, temperature and extraction time using $ CO_{2} $ as solvent. Best SFE condition for total lipids was 450 bar, 60 °C and 45 min. The S...
Ausführliche Beschreibung
Autor*in: |
Jumaah, Firas [verfasserIn] |
---|
Format: |
Artikel |
---|---|
Sprache: |
Englisch |
Erschienen: |
2015 |
---|
Schlagwörter: |
Supercritical fluid extraction |
---|
Anmerkung: |
© The Author(s) 2015 |
---|
Übergeordnetes Werk: |
Enthalten in: Journal of the American Oil Chemists' Society - Springer Berlin Heidelberg, 1947, 92(2015), 8 vom: 11. Juli, Seite 1103-1111 |
---|---|
Übergeordnetes Werk: |
volume:92 ; year:2015 ; number:8 ; day:11 ; month:07 ; pages:1103-1111 |
Links: |
---|
DOI / URN: |
10.1007/s11746-015-2680-x |
---|
Katalog-ID: |
OLC2068164280 |
---|
LEADER | 01000caa a22002652 4500 | ||
---|---|---|---|
001 | OLC2068164280 | ||
003 | DE-627 | ||
005 | 20230518080156.0 | ||
007 | tu | ||
008 | 200819s2015 xx ||||| 00| ||eng c | ||
024 | 7 | |a 10.1007/s11746-015-2680-x |2 doi | |
035 | |a (DE-627)OLC2068164280 | ||
035 | |a (DE-He213)s11746-015-2680-x-p | ||
040 | |a DE-627 |b ger |c DE-627 |e rakwb | ||
041 | |a eng | ||
082 | 0 | 4 | |a 660 |q VZ |
100 | 1 | |a Jumaah, Firas |e verfasserin |4 aut | |
245 | 1 | 0 | |a Supercritical Fluid Extraction and Chromatography of Lipids in Bilberry |
264 | 1 | |c 2015 | |
336 | |a Text |b txt |2 rdacontent | ||
337 | |a ohne Hilfsmittel zu benutzen |b n |2 rdamedia | ||
338 | |a Band |b nc |2 rdacarrier | ||
500 | |a © The Author(s) 2015 | ||
520 | |a Abstract A supercritical fluid extraction (SFE) method has been developed for the extraction of lipids in bilberry. Experimental design was used to optimize pressure, temperature and extraction time using $ CO_{2} $ as solvent. Best SFE condition for total lipids was 450 bar, 60 °C and 45 min. The SFE method was compared to conventional Bligh & Dyer (B&D) extraction. The amount of fatty acid methyl esters (FAME) was found to be 4.84 ± 0.06 mg and 4.564 ± 0.003 mg per g of the freeze-dried bilberry sample for the developed SFE and B&D methods, respectively, while the amount of total lipids was found to be 54.40 ± 6.06 mg and 65.70 ± 0.67 mg per g of sample for SFE and B&D, respectively. This discrepancy between FAME and total lipids could be explained by the presence of wax esters, sterol esters, carotenoids and phospholipids, as determined by supercritical fluid chromatography. | ||
650 | 4 | |a Bilberry | |
650 | 4 | |a Supercritical fluid extraction | |
650 | 4 | |a Supercritical fluid chromatography | |
650 | 4 | |a GC–MS | |
650 | 4 | |a Lipids | |
650 | 4 | |a Fatty acids | |
700 | 1 | |a Sandahl, Margareta |4 aut | |
700 | 1 | |a Turner, Charlotta |4 aut | |
773 | 0 | 8 | |i Enthalten in |t Journal of the American Oil Chemists' Society |d Springer Berlin Heidelberg, 1947 |g 92(2015), 8 vom: 11. Juli, Seite 1103-1111 |w (DE-627)129595691 |w (DE-600)240684-6 |w (DE-576)015088715 |x 0003-021X |7 nnns |
773 | 1 | 8 | |g volume:92 |g year:2015 |g number:8 |g day:11 |g month:07 |g pages:1103-1111 |
856 | 4 | 1 | |u https://doi.org/10.1007/s11746-015-2680-x |z lizenzpflichtig |3 Volltext |
912 | |a GBV_USEFLAG_A | ||
912 | |a SYSFLAG_A | ||
912 | |a GBV_OLC | ||
912 | |a SSG-OLC-TEC | ||
912 | |a SSG-OLC-CHE | ||
912 | |a SSG-OLC-PHA | ||
912 | |a SSG-OLC-DE-84 | ||
912 | |a GBV_ILN_70 | ||
912 | |a GBV_ILN_183 | ||
912 | |a GBV_ILN_2018 | ||
912 | |a GBV_ILN_4012 | ||
912 | |a GBV_ILN_4219 | ||
951 | |a AR | ||
952 | |d 92 |j 2015 |e 8 |b 11 |c 07 |h 1103-1111 |
author_variant |
f j fj m s ms c t ct |
---|---|
matchkey_str |
article:0003021X:2015----::ueciiafudxrcinncrmtgah |
hierarchy_sort_str |
2015 |
publishDate |
2015 |
allfields |
10.1007/s11746-015-2680-x doi (DE-627)OLC2068164280 (DE-He213)s11746-015-2680-x-p DE-627 ger DE-627 rakwb eng 660 VZ Jumaah, Firas verfasserin aut Supercritical Fluid Extraction and Chromatography of Lipids in Bilberry 2015 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © The Author(s) 2015 Abstract A supercritical fluid extraction (SFE) method has been developed for the extraction of lipids in bilberry. Experimental design was used to optimize pressure, temperature and extraction time using $ CO_{2} $ as solvent. Best SFE condition for total lipids was 450 bar, 60 °C and 45 min. The SFE method was compared to conventional Bligh & Dyer (B&D) extraction. The amount of fatty acid methyl esters (FAME) was found to be 4.84 ± 0.06 mg and 4.564 ± 0.003 mg per g of the freeze-dried bilberry sample for the developed SFE and B&D methods, respectively, while the amount of total lipids was found to be 54.40 ± 6.06 mg and 65.70 ± 0.67 mg per g of sample for SFE and B&D, respectively. This discrepancy between FAME and total lipids could be explained by the presence of wax esters, sterol esters, carotenoids and phospholipids, as determined by supercritical fluid chromatography. Bilberry Supercritical fluid extraction Supercritical fluid chromatography GC–MS Lipids Fatty acids Sandahl, Margareta aut Turner, Charlotta aut Enthalten in Journal of the American Oil Chemists' Society Springer Berlin Heidelberg, 1947 92(2015), 8 vom: 11. Juli, Seite 1103-1111 (DE-627)129595691 (DE-600)240684-6 (DE-576)015088715 0003-021X nnns volume:92 year:2015 number:8 day:11 month:07 pages:1103-1111 https://doi.org/10.1007/s11746-015-2680-x lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE SSG-OLC-PHA SSG-OLC-DE-84 GBV_ILN_70 GBV_ILN_183 GBV_ILN_2018 GBV_ILN_4012 GBV_ILN_4219 AR 92 2015 8 11 07 1103-1111 |
spelling |
10.1007/s11746-015-2680-x doi (DE-627)OLC2068164280 (DE-He213)s11746-015-2680-x-p DE-627 ger DE-627 rakwb eng 660 VZ Jumaah, Firas verfasserin aut Supercritical Fluid Extraction and Chromatography of Lipids in Bilberry 2015 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © The Author(s) 2015 Abstract A supercritical fluid extraction (SFE) method has been developed for the extraction of lipids in bilberry. Experimental design was used to optimize pressure, temperature and extraction time using $ CO_{2} $ as solvent. Best SFE condition for total lipids was 450 bar, 60 °C and 45 min. The SFE method was compared to conventional Bligh & Dyer (B&D) extraction. The amount of fatty acid methyl esters (FAME) was found to be 4.84 ± 0.06 mg and 4.564 ± 0.003 mg per g of the freeze-dried bilberry sample for the developed SFE and B&D methods, respectively, while the amount of total lipids was found to be 54.40 ± 6.06 mg and 65.70 ± 0.67 mg per g of sample for SFE and B&D, respectively. This discrepancy between FAME and total lipids could be explained by the presence of wax esters, sterol esters, carotenoids and phospholipids, as determined by supercritical fluid chromatography. Bilberry Supercritical fluid extraction Supercritical fluid chromatography GC–MS Lipids Fatty acids Sandahl, Margareta aut Turner, Charlotta aut Enthalten in Journal of the American Oil Chemists' Society Springer Berlin Heidelberg, 1947 92(2015), 8 vom: 11. Juli, Seite 1103-1111 (DE-627)129595691 (DE-600)240684-6 (DE-576)015088715 0003-021X nnns volume:92 year:2015 number:8 day:11 month:07 pages:1103-1111 https://doi.org/10.1007/s11746-015-2680-x lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE SSG-OLC-PHA SSG-OLC-DE-84 GBV_ILN_70 GBV_ILN_183 GBV_ILN_2018 GBV_ILN_4012 GBV_ILN_4219 AR 92 2015 8 11 07 1103-1111 |
allfields_unstemmed |
10.1007/s11746-015-2680-x doi (DE-627)OLC2068164280 (DE-He213)s11746-015-2680-x-p DE-627 ger DE-627 rakwb eng 660 VZ Jumaah, Firas verfasserin aut Supercritical Fluid Extraction and Chromatography of Lipids in Bilberry 2015 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © The Author(s) 2015 Abstract A supercritical fluid extraction (SFE) method has been developed for the extraction of lipids in bilberry. Experimental design was used to optimize pressure, temperature and extraction time using $ CO_{2} $ as solvent. Best SFE condition for total lipids was 450 bar, 60 °C and 45 min. The SFE method was compared to conventional Bligh & Dyer (B&D) extraction. The amount of fatty acid methyl esters (FAME) was found to be 4.84 ± 0.06 mg and 4.564 ± 0.003 mg per g of the freeze-dried bilberry sample for the developed SFE and B&D methods, respectively, while the amount of total lipids was found to be 54.40 ± 6.06 mg and 65.70 ± 0.67 mg per g of sample for SFE and B&D, respectively. This discrepancy between FAME and total lipids could be explained by the presence of wax esters, sterol esters, carotenoids and phospholipids, as determined by supercritical fluid chromatography. Bilberry Supercritical fluid extraction Supercritical fluid chromatography GC–MS Lipids Fatty acids Sandahl, Margareta aut Turner, Charlotta aut Enthalten in Journal of the American Oil Chemists' Society Springer Berlin Heidelberg, 1947 92(2015), 8 vom: 11. Juli, Seite 1103-1111 (DE-627)129595691 (DE-600)240684-6 (DE-576)015088715 0003-021X nnns volume:92 year:2015 number:8 day:11 month:07 pages:1103-1111 https://doi.org/10.1007/s11746-015-2680-x lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE SSG-OLC-PHA SSG-OLC-DE-84 GBV_ILN_70 GBV_ILN_183 GBV_ILN_2018 GBV_ILN_4012 GBV_ILN_4219 AR 92 2015 8 11 07 1103-1111 |
allfieldsGer |
10.1007/s11746-015-2680-x doi (DE-627)OLC2068164280 (DE-He213)s11746-015-2680-x-p DE-627 ger DE-627 rakwb eng 660 VZ Jumaah, Firas verfasserin aut Supercritical Fluid Extraction and Chromatography of Lipids in Bilberry 2015 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © The Author(s) 2015 Abstract A supercritical fluid extraction (SFE) method has been developed for the extraction of lipids in bilberry. Experimental design was used to optimize pressure, temperature and extraction time using $ CO_{2} $ as solvent. Best SFE condition for total lipids was 450 bar, 60 °C and 45 min. The SFE method was compared to conventional Bligh & Dyer (B&D) extraction. The amount of fatty acid methyl esters (FAME) was found to be 4.84 ± 0.06 mg and 4.564 ± 0.003 mg per g of the freeze-dried bilberry sample for the developed SFE and B&D methods, respectively, while the amount of total lipids was found to be 54.40 ± 6.06 mg and 65.70 ± 0.67 mg per g of sample for SFE and B&D, respectively. This discrepancy between FAME and total lipids could be explained by the presence of wax esters, sterol esters, carotenoids and phospholipids, as determined by supercritical fluid chromatography. Bilberry Supercritical fluid extraction Supercritical fluid chromatography GC–MS Lipids Fatty acids Sandahl, Margareta aut Turner, Charlotta aut Enthalten in Journal of the American Oil Chemists' Society Springer Berlin Heidelberg, 1947 92(2015), 8 vom: 11. Juli, Seite 1103-1111 (DE-627)129595691 (DE-600)240684-6 (DE-576)015088715 0003-021X nnns volume:92 year:2015 number:8 day:11 month:07 pages:1103-1111 https://doi.org/10.1007/s11746-015-2680-x lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE SSG-OLC-PHA SSG-OLC-DE-84 GBV_ILN_70 GBV_ILN_183 GBV_ILN_2018 GBV_ILN_4012 GBV_ILN_4219 AR 92 2015 8 11 07 1103-1111 |
allfieldsSound |
10.1007/s11746-015-2680-x doi (DE-627)OLC2068164280 (DE-He213)s11746-015-2680-x-p DE-627 ger DE-627 rakwb eng 660 VZ Jumaah, Firas verfasserin aut Supercritical Fluid Extraction and Chromatography of Lipids in Bilberry 2015 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © The Author(s) 2015 Abstract A supercritical fluid extraction (SFE) method has been developed for the extraction of lipids in bilberry. Experimental design was used to optimize pressure, temperature and extraction time using $ CO_{2} $ as solvent. Best SFE condition for total lipids was 450 bar, 60 °C and 45 min. The SFE method was compared to conventional Bligh & Dyer (B&D) extraction. The amount of fatty acid methyl esters (FAME) was found to be 4.84 ± 0.06 mg and 4.564 ± 0.003 mg per g of the freeze-dried bilberry sample for the developed SFE and B&D methods, respectively, while the amount of total lipids was found to be 54.40 ± 6.06 mg and 65.70 ± 0.67 mg per g of sample for SFE and B&D, respectively. This discrepancy between FAME and total lipids could be explained by the presence of wax esters, sterol esters, carotenoids and phospholipids, as determined by supercritical fluid chromatography. Bilberry Supercritical fluid extraction Supercritical fluid chromatography GC–MS Lipids Fatty acids Sandahl, Margareta aut Turner, Charlotta aut Enthalten in Journal of the American Oil Chemists' Society Springer Berlin Heidelberg, 1947 92(2015), 8 vom: 11. Juli, Seite 1103-1111 (DE-627)129595691 (DE-600)240684-6 (DE-576)015088715 0003-021X nnns volume:92 year:2015 number:8 day:11 month:07 pages:1103-1111 https://doi.org/10.1007/s11746-015-2680-x lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE SSG-OLC-PHA SSG-OLC-DE-84 GBV_ILN_70 GBV_ILN_183 GBV_ILN_2018 GBV_ILN_4012 GBV_ILN_4219 AR 92 2015 8 11 07 1103-1111 |
language |
English |
source |
Enthalten in Journal of the American Oil Chemists' Society 92(2015), 8 vom: 11. Juli, Seite 1103-1111 volume:92 year:2015 number:8 day:11 month:07 pages:1103-1111 |
sourceStr |
Enthalten in Journal of the American Oil Chemists' Society 92(2015), 8 vom: 11. Juli, Seite 1103-1111 volume:92 year:2015 number:8 day:11 month:07 pages:1103-1111 |
format_phy_str_mv |
Article |
institution |
findex.gbv.de |
topic_facet |
Bilberry Supercritical fluid extraction Supercritical fluid chromatography GC–MS Lipids Fatty acids |
dewey-raw |
660 |
isfreeaccess_bool |
false |
container_title |
Journal of the American Oil Chemists' Society |
authorswithroles_txt_mv |
Jumaah, Firas @@aut@@ Sandahl, Margareta @@aut@@ Turner, Charlotta @@aut@@ |
publishDateDaySort_date |
2015-07-11T00:00:00Z |
hierarchy_top_id |
129595691 |
dewey-sort |
3660 |
id |
OLC2068164280 |
language_de |
englisch |
fullrecord |
<?xml version="1.0" encoding="UTF-8"?><collection xmlns="http://www.loc.gov/MARC21/slim"><record><leader>01000caa a22002652 4500</leader><controlfield tag="001">OLC2068164280</controlfield><controlfield tag="003">DE-627</controlfield><controlfield tag="005">20230518080156.0</controlfield><controlfield tag="007">tu</controlfield><controlfield tag="008">200819s2015 xx ||||| 00| ||eng c</controlfield><datafield tag="024" ind1="7" ind2=" "><subfield code="a">10.1007/s11746-015-2680-x</subfield><subfield code="2">doi</subfield></datafield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(DE-627)OLC2068164280</subfield></datafield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(DE-He213)s11746-015-2680-x-p</subfield></datafield><datafield tag="040" ind1=" " ind2=" "><subfield code="a">DE-627</subfield><subfield code="b">ger</subfield><subfield code="c">DE-627</subfield><subfield code="e">rakwb</subfield></datafield><datafield tag="041" ind1=" " ind2=" "><subfield code="a">eng</subfield></datafield><datafield tag="082" ind1="0" ind2="4"><subfield code="a">660</subfield><subfield code="q">VZ</subfield></datafield><datafield tag="100" ind1="1" ind2=" "><subfield code="a">Jumaah, Firas</subfield><subfield code="e">verfasserin</subfield><subfield code="4">aut</subfield></datafield><datafield tag="245" ind1="1" ind2="0"><subfield code="a">Supercritical Fluid Extraction and Chromatography of Lipids in Bilberry</subfield></datafield><datafield tag="264" ind1=" " ind2="1"><subfield code="c">2015</subfield></datafield><datafield tag="336" ind1=" " ind2=" "><subfield code="a">Text</subfield><subfield code="b">txt</subfield><subfield code="2">rdacontent</subfield></datafield><datafield tag="337" ind1=" " ind2=" "><subfield code="a">ohne Hilfsmittel zu benutzen</subfield><subfield code="b">n</subfield><subfield code="2">rdamedia</subfield></datafield><datafield tag="338" ind1=" " ind2=" "><subfield code="a">Band</subfield><subfield code="b">nc</subfield><subfield code="2">rdacarrier</subfield></datafield><datafield tag="500" ind1=" " ind2=" "><subfield code="a">© The Author(s) 2015</subfield></datafield><datafield tag="520" ind1=" " ind2=" "><subfield code="a">Abstract A supercritical fluid extraction (SFE) method has been developed for the extraction of lipids in bilberry. Experimental design was used to optimize pressure, temperature and extraction time using $ CO_{2} $ as solvent. Best SFE condition for total lipids was 450 bar, 60 °C and 45 min. The SFE method was compared to conventional Bligh & Dyer (B&D) extraction. The amount of fatty acid methyl esters (FAME) was found to be 4.84 ± 0.06 mg and 4.564 ± 0.003 mg per g of the freeze-dried bilberry sample for the developed SFE and B&D methods, respectively, while the amount of total lipids was found to be 54.40 ± 6.06 mg and 65.70 ± 0.67 mg per g of sample for SFE and B&D, respectively. This discrepancy between FAME and total lipids could be explained by the presence of wax esters, sterol esters, carotenoids and phospholipids, as determined by supercritical fluid chromatography.</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Bilberry</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Supercritical fluid extraction</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Supercritical fluid chromatography</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">GC–MS</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Lipids</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Fatty acids</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Sandahl, Margareta</subfield><subfield code="4">aut</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Turner, Charlotta</subfield><subfield code="4">aut</subfield></datafield><datafield tag="773" ind1="0" ind2="8"><subfield code="i">Enthalten in</subfield><subfield code="t">Journal of the American Oil Chemists' Society</subfield><subfield code="d">Springer Berlin Heidelberg, 1947</subfield><subfield code="g">92(2015), 8 vom: 11. Juli, Seite 1103-1111</subfield><subfield code="w">(DE-627)129595691</subfield><subfield code="w">(DE-600)240684-6</subfield><subfield code="w">(DE-576)015088715</subfield><subfield code="x">0003-021X</subfield><subfield code="7">nnns</subfield></datafield><datafield tag="773" ind1="1" ind2="8"><subfield code="g">volume:92</subfield><subfield code="g">year:2015</subfield><subfield code="g">number:8</subfield><subfield code="g">day:11</subfield><subfield code="g">month:07</subfield><subfield code="g">pages:1103-1111</subfield></datafield><datafield tag="856" ind1="4" ind2="1"><subfield code="u">https://doi.org/10.1007/s11746-015-2680-x</subfield><subfield code="z">lizenzpflichtig</subfield><subfield code="3">Volltext</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_USEFLAG_A</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">SYSFLAG_A</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_OLC</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">SSG-OLC-TEC</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">SSG-OLC-CHE</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">SSG-OLC-PHA</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">SSG-OLC-DE-84</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_70</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_183</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2018</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4012</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4219</subfield></datafield><datafield tag="951" ind1=" " ind2=" "><subfield code="a">AR</subfield></datafield><datafield tag="952" ind1=" " ind2=" "><subfield code="d">92</subfield><subfield code="j">2015</subfield><subfield code="e">8</subfield><subfield code="b">11</subfield><subfield code="c">07</subfield><subfield code="h">1103-1111</subfield></datafield></record></collection>
|
author |
Jumaah, Firas |
spellingShingle |
Jumaah, Firas ddc 660 misc Bilberry misc Supercritical fluid extraction misc Supercritical fluid chromatography misc GC–MS misc Lipids misc Fatty acids Supercritical Fluid Extraction and Chromatography of Lipids in Bilberry |
authorStr |
Jumaah, Firas |
ppnlink_with_tag_str_mv |
@@773@@(DE-627)129595691 |
format |
Article |
dewey-ones |
660 - Chemical engineering |
delete_txt_mv |
keep |
author_role |
aut aut aut |
collection |
OLC |
remote_str |
false |
illustrated |
Not Illustrated |
issn |
0003-021X |
topic_title |
660 VZ Supercritical Fluid Extraction and Chromatography of Lipids in Bilberry Bilberry Supercritical fluid extraction Supercritical fluid chromatography GC–MS Lipids Fatty acids |
topic |
ddc 660 misc Bilberry misc Supercritical fluid extraction misc Supercritical fluid chromatography misc GC–MS misc Lipids misc Fatty acids |
topic_unstemmed |
ddc 660 misc Bilberry misc Supercritical fluid extraction misc Supercritical fluid chromatography misc GC–MS misc Lipids misc Fatty acids |
topic_browse |
ddc 660 misc Bilberry misc Supercritical fluid extraction misc Supercritical fluid chromatography misc GC–MS misc Lipids misc Fatty acids |
format_facet |
Aufsätze Gedruckte Aufsätze |
format_main_str_mv |
Text Zeitschrift/Artikel |
carriertype_str_mv |
nc |
hierarchy_parent_title |
Journal of the American Oil Chemists' Society |
hierarchy_parent_id |
129595691 |
dewey-tens |
660 - Chemical engineering |
hierarchy_top_title |
Journal of the American Oil Chemists' Society |
isfreeaccess_txt |
false |
familylinks_str_mv |
(DE-627)129595691 (DE-600)240684-6 (DE-576)015088715 |
title |
Supercritical Fluid Extraction and Chromatography of Lipids in Bilberry |
ctrlnum |
(DE-627)OLC2068164280 (DE-He213)s11746-015-2680-x-p |
title_full |
Supercritical Fluid Extraction and Chromatography of Lipids in Bilberry |
author_sort |
Jumaah, Firas |
journal |
Journal of the American Oil Chemists' Society |
journalStr |
Journal of the American Oil Chemists' Society |
lang_code |
eng |
isOA_bool |
false |
dewey-hundreds |
600 - Technology |
recordtype |
marc |
publishDateSort |
2015 |
contenttype_str_mv |
txt |
container_start_page |
1103 |
author_browse |
Jumaah, Firas Sandahl, Margareta Turner, Charlotta |
container_volume |
92 |
class |
660 VZ |
format_se |
Aufsätze |
author-letter |
Jumaah, Firas |
doi_str_mv |
10.1007/s11746-015-2680-x |
dewey-full |
660 |
title_sort |
supercritical fluid extraction and chromatography of lipids in bilberry |
title_auth |
Supercritical Fluid Extraction and Chromatography of Lipids in Bilberry |
abstract |
Abstract A supercritical fluid extraction (SFE) method has been developed for the extraction of lipids in bilberry. Experimental design was used to optimize pressure, temperature and extraction time using $ CO_{2} $ as solvent. Best SFE condition for total lipids was 450 bar, 60 °C and 45 min. The SFE method was compared to conventional Bligh & Dyer (B&D) extraction. The amount of fatty acid methyl esters (FAME) was found to be 4.84 ± 0.06 mg and 4.564 ± 0.003 mg per g of the freeze-dried bilberry sample for the developed SFE and B&D methods, respectively, while the amount of total lipids was found to be 54.40 ± 6.06 mg and 65.70 ± 0.67 mg per g of sample for SFE and B&D, respectively. This discrepancy between FAME and total lipids could be explained by the presence of wax esters, sterol esters, carotenoids and phospholipids, as determined by supercritical fluid chromatography. © The Author(s) 2015 |
abstractGer |
Abstract A supercritical fluid extraction (SFE) method has been developed for the extraction of lipids in bilberry. Experimental design was used to optimize pressure, temperature and extraction time using $ CO_{2} $ as solvent. Best SFE condition for total lipids was 450 bar, 60 °C and 45 min. The SFE method was compared to conventional Bligh & Dyer (B&D) extraction. The amount of fatty acid methyl esters (FAME) was found to be 4.84 ± 0.06 mg and 4.564 ± 0.003 mg per g of the freeze-dried bilberry sample for the developed SFE and B&D methods, respectively, while the amount of total lipids was found to be 54.40 ± 6.06 mg and 65.70 ± 0.67 mg per g of sample for SFE and B&D, respectively. This discrepancy between FAME and total lipids could be explained by the presence of wax esters, sterol esters, carotenoids and phospholipids, as determined by supercritical fluid chromatography. © The Author(s) 2015 |
abstract_unstemmed |
Abstract A supercritical fluid extraction (SFE) method has been developed for the extraction of lipids in bilberry. Experimental design was used to optimize pressure, temperature and extraction time using $ CO_{2} $ as solvent. Best SFE condition for total lipids was 450 bar, 60 °C and 45 min. The SFE method was compared to conventional Bligh & Dyer (B&D) extraction. The amount of fatty acid methyl esters (FAME) was found to be 4.84 ± 0.06 mg and 4.564 ± 0.003 mg per g of the freeze-dried bilberry sample for the developed SFE and B&D methods, respectively, while the amount of total lipids was found to be 54.40 ± 6.06 mg and 65.70 ± 0.67 mg per g of sample for SFE and B&D, respectively. This discrepancy between FAME and total lipids could be explained by the presence of wax esters, sterol esters, carotenoids and phospholipids, as determined by supercritical fluid chromatography. © The Author(s) 2015 |
collection_details |
GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-CHE SSG-OLC-PHA SSG-OLC-DE-84 GBV_ILN_70 GBV_ILN_183 GBV_ILN_2018 GBV_ILN_4012 GBV_ILN_4219 |
container_issue |
8 |
title_short |
Supercritical Fluid Extraction and Chromatography of Lipids in Bilberry |
url |
https://doi.org/10.1007/s11746-015-2680-x |
remote_bool |
false |
author2 |
Sandahl, Margareta Turner, Charlotta |
author2Str |
Sandahl, Margareta Turner, Charlotta |
ppnlink |
129595691 |
mediatype_str_mv |
n |
isOA_txt |
false |
hochschulschrift_bool |
false |
doi_str |
10.1007/s11746-015-2680-x |
up_date |
2024-07-03T17:50:35.788Z |
_version_ |
1803581166228340737 |
fullrecord_marcxml |
<?xml version="1.0" encoding="UTF-8"?><collection xmlns="http://www.loc.gov/MARC21/slim"><record><leader>01000caa a22002652 4500</leader><controlfield tag="001">OLC2068164280</controlfield><controlfield tag="003">DE-627</controlfield><controlfield tag="005">20230518080156.0</controlfield><controlfield tag="007">tu</controlfield><controlfield tag="008">200819s2015 xx ||||| 00| ||eng c</controlfield><datafield tag="024" ind1="7" ind2=" "><subfield code="a">10.1007/s11746-015-2680-x</subfield><subfield code="2">doi</subfield></datafield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(DE-627)OLC2068164280</subfield></datafield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(DE-He213)s11746-015-2680-x-p</subfield></datafield><datafield tag="040" ind1=" " ind2=" "><subfield code="a">DE-627</subfield><subfield code="b">ger</subfield><subfield code="c">DE-627</subfield><subfield code="e">rakwb</subfield></datafield><datafield tag="041" ind1=" " ind2=" "><subfield code="a">eng</subfield></datafield><datafield tag="082" ind1="0" ind2="4"><subfield code="a">660</subfield><subfield code="q">VZ</subfield></datafield><datafield tag="100" ind1="1" ind2=" "><subfield code="a">Jumaah, Firas</subfield><subfield code="e">verfasserin</subfield><subfield code="4">aut</subfield></datafield><datafield tag="245" ind1="1" ind2="0"><subfield code="a">Supercritical Fluid Extraction and Chromatography of Lipids in Bilberry</subfield></datafield><datafield tag="264" ind1=" " ind2="1"><subfield code="c">2015</subfield></datafield><datafield tag="336" ind1=" " ind2=" "><subfield code="a">Text</subfield><subfield code="b">txt</subfield><subfield code="2">rdacontent</subfield></datafield><datafield tag="337" ind1=" " ind2=" "><subfield code="a">ohne Hilfsmittel zu benutzen</subfield><subfield code="b">n</subfield><subfield code="2">rdamedia</subfield></datafield><datafield tag="338" ind1=" " ind2=" "><subfield code="a">Band</subfield><subfield code="b">nc</subfield><subfield code="2">rdacarrier</subfield></datafield><datafield tag="500" ind1=" " ind2=" "><subfield code="a">© The Author(s) 2015</subfield></datafield><datafield tag="520" ind1=" " ind2=" "><subfield code="a">Abstract A supercritical fluid extraction (SFE) method has been developed for the extraction of lipids in bilberry. Experimental design was used to optimize pressure, temperature and extraction time using $ CO_{2} $ as solvent. Best SFE condition for total lipids was 450 bar, 60 °C and 45 min. The SFE method was compared to conventional Bligh & Dyer (B&D) extraction. The amount of fatty acid methyl esters (FAME) was found to be 4.84 ± 0.06 mg and 4.564 ± 0.003 mg per g of the freeze-dried bilberry sample for the developed SFE and B&D methods, respectively, while the amount of total lipids was found to be 54.40 ± 6.06 mg and 65.70 ± 0.67 mg per g of sample for SFE and B&D, respectively. This discrepancy between FAME and total lipids could be explained by the presence of wax esters, sterol esters, carotenoids and phospholipids, as determined by supercritical fluid chromatography.</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Bilberry</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Supercritical fluid extraction</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Supercritical fluid chromatography</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">GC–MS</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Lipids</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Fatty acids</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Sandahl, Margareta</subfield><subfield code="4">aut</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Turner, Charlotta</subfield><subfield code="4">aut</subfield></datafield><datafield tag="773" ind1="0" ind2="8"><subfield code="i">Enthalten in</subfield><subfield code="t">Journal of the American Oil Chemists' Society</subfield><subfield code="d">Springer Berlin Heidelberg, 1947</subfield><subfield code="g">92(2015), 8 vom: 11. Juli, Seite 1103-1111</subfield><subfield code="w">(DE-627)129595691</subfield><subfield code="w">(DE-600)240684-6</subfield><subfield code="w">(DE-576)015088715</subfield><subfield code="x">0003-021X</subfield><subfield code="7">nnns</subfield></datafield><datafield tag="773" ind1="1" ind2="8"><subfield code="g">volume:92</subfield><subfield code="g">year:2015</subfield><subfield code="g">number:8</subfield><subfield code="g">day:11</subfield><subfield code="g">month:07</subfield><subfield code="g">pages:1103-1111</subfield></datafield><datafield tag="856" ind1="4" ind2="1"><subfield code="u">https://doi.org/10.1007/s11746-015-2680-x</subfield><subfield code="z">lizenzpflichtig</subfield><subfield code="3">Volltext</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_USEFLAG_A</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">SYSFLAG_A</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_OLC</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">SSG-OLC-TEC</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">SSG-OLC-CHE</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">SSG-OLC-PHA</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">SSG-OLC-DE-84</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_70</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_183</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_2018</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4012</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ILN_4219</subfield></datafield><datafield tag="951" ind1=" " ind2=" "><subfield code="a">AR</subfield></datafield><datafield tag="952" ind1=" " ind2=" "><subfield code="d">92</subfield><subfield code="j">2015</subfield><subfield code="e">8</subfield><subfield code="b">11</subfield><subfield code="c">07</subfield><subfield code="h">1103-1111</subfield></datafield></record></collection>
|
score |
7.398122 |