Stability of the modulated structure of Ba$$\overset{\lower0.5em\hbox{$\smash{\scriptscriptstyle\smile}$}}{l} $$kal lazurite and its recrystallization at a temperature of 600°C over a wide range of sulfur dioxide fugacities
Abstract The stability of three-dimensional incommensurate modulation in cubic lazurite from the Ba$$\overset{\lower0.5em\hbox{$\smash{\scriptscriptstyle\smile}$}}{l} $$kal region is experimentally investigated at T = 600°C. It is found that the X-ray photoelectron spectra of the annealed samples ex...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Tauson, V. L. [verfasserIn] |
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| Format: |
Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2005 |
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| Schlagwörter: |
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| Anmerkung: |
© Pleiades Publishing, Inc. 2005 |
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| Übergeordnetes Werk: |
Enthalten in: Crystallography reports - Nauka/Interperiodica, 1993, 50(2005), Suppl 1 vom: Dez., Seite S1-S9 |
|---|---|
| Übergeordnetes Werk: |
volume:50 ; year:2005 ; number:Suppl 1 ; month:12 ; pages:S1-S9 |
| Links: |
|---|
| DOI / URN: |
10.1134/1.2133964 |
|---|
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OLC207024654X |
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| 245 | 1 | 0 | |a Stability of the modulated structure of Ba$$\overset{\lower0.5em\hbox{$\smash{\scriptscriptstyle\smile}$}}{l} $$kal lazurite and its recrystallization at a temperature of 600°C over a wide range of sulfur dioxide fugacities |
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| 520 | |a Abstract The stability of three-dimensional incommensurate modulation in cubic lazurite from the Ba$$\overset{\lower0.5em\hbox{$\smash{\scriptscriptstyle\smile}$}}{l} $$kal region is experimentally investigated at T = 600°C. It is found that the X-ray photoelectron spectra of the annealed samples exhibit a peak corresponding to sulfite and a split peak associated with the (Na,Ca)$ SO_{4} $ sulfate. It is assumed that the splitting is caused by the ordering of the complexes not involved in the framework. This assumption is confirmed by the presence of a similar split peak in the X-ray photoelectron spectra of triclinic lazurite. It is demonstrated that the initial modulation is retained at the fugacity $$f_{SO_2 } = 8 \times 10^{ - 3} $$ bar. The decisive factors responsible for the retention of the three-dimensional incommensurate modulation are the temperature and the fugacity of sulfur dioxide. The latter quantity should be close to the stability boundary of the basic lazurite structure. The growth and transformation mechanisms of the modulation formation are conidered. | ||
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10.1134/1.2133964 doi (DE-627)OLC207024654X (DE-He213)1.2133964-p DE-627 ger DE-627 rakwb eng 540 530 VZ Tauson, V. L. verfasserin aut Stability of the modulated structure of Ba$$\overset{\lower0.5em\hbox{$\smash{\scriptscriptstyle\smile}$}}{l} $$kal lazurite and its recrystallization at a temperature of 600°C over a wide range of sulfur dioxide fugacities 2005 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Pleiades Publishing, Inc. 2005 Abstract The stability of three-dimensional incommensurate modulation in cubic lazurite from the Ba$$\overset{\lower0.5em\hbox{$\smash{\scriptscriptstyle\smile}$}}{l} $$kal region is experimentally investigated at T = 600°C. It is found that the X-ray photoelectron spectra of the annealed samples exhibit a peak corresponding to sulfite and a split peak associated with the (Na,Ca)$ SO_{4} $ sulfate. It is assumed that the splitting is caused by the ordering of the complexes not involved in the framework. This assumption is confirmed by the presence of a similar split peak in the X-ray photoelectron spectra of triclinic lazurite. It is demonstrated that the initial modulation is retained at the fugacity $$f_{SO_2 } = 8 \times 10^{ - 3} $$ bar. The decisive factors responsible for the retention of the three-dimensional incommensurate modulation are the temperature and the fugacity of sulfur dioxide. The latter quantity should be close to the stability boundary of the basic lazurite structure. The growth and transformation mechanisms of the modulation formation are conidered. Sulfur Dioxide Recrystallization Sulfite Sulfur Dioxide Sapozhnikov, A. N. aut Enthalten in Crystallography reports Nauka/Interperiodica, 1993 50(2005), Suppl 1 vom: Dez., Seite S1-S9 (DE-627)171187822 (DE-600)1162973-3 (DE-576)038500337 1063-7745 nnns volume:50 year:2005 number:Suppl 1 month:12 pages:S1-S9 https://doi.org/10.1134/1.2133964 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-PHY SSG-OLC-CHE SSG-OLC-GEO SSG-OPC-GGO GBV_ILN_21 GBV_ILN_22 GBV_ILN_30 GBV_ILN_40 GBV_ILN_70 AR 50 2005 Suppl 1 12 S1-S9 |
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10.1134/1.2133964 doi (DE-627)OLC207024654X (DE-He213)1.2133964-p DE-627 ger DE-627 rakwb eng 540 530 VZ Tauson, V. L. verfasserin aut Stability of the modulated structure of Ba$$\overset{\lower0.5em\hbox{$\smash{\scriptscriptstyle\smile}$}}{l} $$kal lazurite and its recrystallization at a temperature of 600°C over a wide range of sulfur dioxide fugacities 2005 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Pleiades Publishing, Inc. 2005 Abstract The stability of three-dimensional incommensurate modulation in cubic lazurite from the Ba$$\overset{\lower0.5em\hbox{$\smash{\scriptscriptstyle\smile}$}}{l} $$kal region is experimentally investigated at T = 600°C. It is found that the X-ray photoelectron spectra of the annealed samples exhibit a peak corresponding to sulfite and a split peak associated with the (Na,Ca)$ SO_{4} $ sulfate. It is assumed that the splitting is caused by the ordering of the complexes not involved in the framework. This assumption is confirmed by the presence of a similar split peak in the X-ray photoelectron spectra of triclinic lazurite. It is demonstrated that the initial modulation is retained at the fugacity $$f_{SO_2 } = 8 \times 10^{ - 3} $$ bar. The decisive factors responsible for the retention of the three-dimensional incommensurate modulation are the temperature and the fugacity of sulfur dioxide. The latter quantity should be close to the stability boundary of the basic lazurite structure. The growth and transformation mechanisms of the modulation formation are conidered. Sulfur Dioxide Recrystallization Sulfite Sulfur Dioxide Sapozhnikov, A. N. aut Enthalten in Crystallography reports Nauka/Interperiodica, 1993 50(2005), Suppl 1 vom: Dez., Seite S1-S9 (DE-627)171187822 (DE-600)1162973-3 (DE-576)038500337 1063-7745 nnns volume:50 year:2005 number:Suppl 1 month:12 pages:S1-S9 https://doi.org/10.1134/1.2133964 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-PHY SSG-OLC-CHE SSG-OLC-GEO SSG-OPC-GGO GBV_ILN_21 GBV_ILN_22 GBV_ILN_30 GBV_ILN_40 GBV_ILN_70 AR 50 2005 Suppl 1 12 S1-S9 |
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10.1134/1.2133964 doi (DE-627)OLC207024654X (DE-He213)1.2133964-p DE-627 ger DE-627 rakwb eng 540 530 VZ Tauson, V. L. verfasserin aut Stability of the modulated structure of Ba$$\overset{\lower0.5em\hbox{$\smash{\scriptscriptstyle\smile}$}}{l} $$kal lazurite and its recrystallization at a temperature of 600°C over a wide range of sulfur dioxide fugacities 2005 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Pleiades Publishing, Inc. 2005 Abstract The stability of three-dimensional incommensurate modulation in cubic lazurite from the Ba$$\overset{\lower0.5em\hbox{$\smash{\scriptscriptstyle\smile}$}}{l} $$kal region is experimentally investigated at T = 600°C. It is found that the X-ray photoelectron spectra of the annealed samples exhibit a peak corresponding to sulfite and a split peak associated with the (Na,Ca)$ SO_{4} $ sulfate. It is assumed that the splitting is caused by the ordering of the complexes not involved in the framework. This assumption is confirmed by the presence of a similar split peak in the X-ray photoelectron spectra of triclinic lazurite. It is demonstrated that the initial modulation is retained at the fugacity $$f_{SO_2 } = 8 \times 10^{ - 3} $$ bar. The decisive factors responsible for the retention of the three-dimensional incommensurate modulation are the temperature and the fugacity of sulfur dioxide. The latter quantity should be close to the stability boundary of the basic lazurite structure. The growth and transformation mechanisms of the modulation formation are conidered. Sulfur Dioxide Recrystallization Sulfite Sulfur Dioxide Sapozhnikov, A. N. aut Enthalten in Crystallography reports Nauka/Interperiodica, 1993 50(2005), Suppl 1 vom: Dez., Seite S1-S9 (DE-627)171187822 (DE-600)1162973-3 (DE-576)038500337 1063-7745 nnns volume:50 year:2005 number:Suppl 1 month:12 pages:S1-S9 https://doi.org/10.1134/1.2133964 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-PHY SSG-OLC-CHE SSG-OLC-GEO SSG-OPC-GGO GBV_ILN_21 GBV_ILN_22 GBV_ILN_30 GBV_ILN_40 GBV_ILN_70 AR 50 2005 Suppl 1 12 S1-S9 |
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10.1134/1.2133964 doi (DE-627)OLC207024654X (DE-He213)1.2133964-p DE-627 ger DE-627 rakwb eng 540 530 VZ Tauson, V. L. verfasserin aut Stability of the modulated structure of Ba$$\overset{\lower0.5em\hbox{$\smash{\scriptscriptstyle\smile}$}}{l} $$kal lazurite and its recrystallization at a temperature of 600°C over a wide range of sulfur dioxide fugacities 2005 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Pleiades Publishing, Inc. 2005 Abstract The stability of three-dimensional incommensurate modulation in cubic lazurite from the Ba$$\overset{\lower0.5em\hbox{$\smash{\scriptscriptstyle\smile}$}}{l} $$kal region is experimentally investigated at T = 600°C. It is found that the X-ray photoelectron spectra of the annealed samples exhibit a peak corresponding to sulfite and a split peak associated with the (Na,Ca)$ SO_{4} $ sulfate. It is assumed that the splitting is caused by the ordering of the complexes not involved in the framework. This assumption is confirmed by the presence of a similar split peak in the X-ray photoelectron spectra of triclinic lazurite. It is demonstrated that the initial modulation is retained at the fugacity $$f_{SO_2 } = 8 \times 10^{ - 3} $$ bar. The decisive factors responsible for the retention of the three-dimensional incommensurate modulation are the temperature and the fugacity of sulfur dioxide. The latter quantity should be close to the stability boundary of the basic lazurite structure. The growth and transformation mechanisms of the modulation formation are conidered. Sulfur Dioxide Recrystallization Sulfite Sulfur Dioxide Sapozhnikov, A. N. aut Enthalten in Crystallography reports Nauka/Interperiodica, 1993 50(2005), Suppl 1 vom: Dez., Seite S1-S9 (DE-627)171187822 (DE-600)1162973-3 (DE-576)038500337 1063-7745 nnns volume:50 year:2005 number:Suppl 1 month:12 pages:S1-S9 https://doi.org/10.1134/1.2133964 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-PHY SSG-OLC-CHE SSG-OLC-GEO SSG-OPC-GGO GBV_ILN_21 GBV_ILN_22 GBV_ILN_30 GBV_ILN_40 GBV_ILN_70 AR 50 2005 Suppl 1 12 S1-S9 |
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10.1134/1.2133964 doi (DE-627)OLC207024654X (DE-He213)1.2133964-p DE-627 ger DE-627 rakwb eng 540 530 VZ Tauson, V. L. verfasserin aut Stability of the modulated structure of Ba$$\overset{\lower0.5em\hbox{$\smash{\scriptscriptstyle\smile}$}}{l} $$kal lazurite and its recrystallization at a temperature of 600°C over a wide range of sulfur dioxide fugacities 2005 Text txt rdacontent ohne Hilfsmittel zu benutzen n rdamedia Band nc rdacarrier © Pleiades Publishing, Inc. 2005 Abstract The stability of three-dimensional incommensurate modulation in cubic lazurite from the Ba$$\overset{\lower0.5em\hbox{$\smash{\scriptscriptstyle\smile}$}}{l} $$kal region is experimentally investigated at T = 600°C. It is found that the X-ray photoelectron spectra of the annealed samples exhibit a peak corresponding to sulfite and a split peak associated with the (Na,Ca)$ SO_{4} $ sulfate. It is assumed that the splitting is caused by the ordering of the complexes not involved in the framework. This assumption is confirmed by the presence of a similar split peak in the X-ray photoelectron spectra of triclinic lazurite. It is demonstrated that the initial modulation is retained at the fugacity $$f_{SO_2 } = 8 \times 10^{ - 3} $$ bar. The decisive factors responsible for the retention of the three-dimensional incommensurate modulation are the temperature and the fugacity of sulfur dioxide. The latter quantity should be close to the stability boundary of the basic lazurite structure. The growth and transformation mechanisms of the modulation formation are conidered. Sulfur Dioxide Recrystallization Sulfite Sulfur Dioxide Sapozhnikov, A. N. aut Enthalten in Crystallography reports Nauka/Interperiodica, 1993 50(2005), Suppl 1 vom: Dez., Seite S1-S9 (DE-627)171187822 (DE-600)1162973-3 (DE-576)038500337 1063-7745 nnns volume:50 year:2005 number:Suppl 1 month:12 pages:S1-S9 https://doi.org/10.1134/1.2133964 lizenzpflichtig Volltext GBV_USEFLAG_A SYSFLAG_A GBV_OLC SSG-OLC-TEC SSG-OLC-PHY SSG-OLC-CHE SSG-OLC-GEO SSG-OPC-GGO GBV_ILN_21 GBV_ILN_22 GBV_ILN_30 GBV_ILN_40 GBV_ILN_70 AR 50 2005 Suppl 1 12 S1-S9 |
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Stability of the modulated structure of Ba$$\overset{\lower0.5em\hbox{$\smash{\scriptscriptstyle\smile}$}}{l} $$kal lazurite and its recrystallization at a temperature of 600°C over a wide range of sulfur dioxide fugacities |
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| title_full |
Stability of the modulated structure of Ba$$\overset{\lower0.5em\hbox{$\smash{\scriptscriptstyle\smile}$}}{l} $$kal lazurite and its recrystallization at a temperature of 600°C over a wide range of sulfur dioxide fugacities |
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Tauson, V. L. |
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Crystallography reports |
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Crystallography reports |
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500 - Science |
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2005 |
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Tauson, V. L. Sapozhnikov, A. N. |
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Tauson, V. L. |
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10.1134/1.2133964 |
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540 530 |
| title_sort |
stability of the modulated structure of ba$$\overset{\lower0.5em\hbox{$\smash{\scriptscriptstyle\smile}$}}{l} $$kal lazurite and its recrystallization at a temperature of 600°c over a wide range of sulfur dioxide fugacities |
| title_auth |
Stability of the modulated structure of Ba$$\overset{\lower0.5em\hbox{$\smash{\scriptscriptstyle\smile}$}}{l} $$kal lazurite and its recrystallization at a temperature of 600°C over a wide range of sulfur dioxide fugacities |
| abstract |
Abstract The stability of three-dimensional incommensurate modulation in cubic lazurite from the Ba$$\overset{\lower0.5em\hbox{$\smash{\scriptscriptstyle\smile}$}}{l} $$kal region is experimentally investigated at T = 600°C. It is found that the X-ray photoelectron spectra of the annealed samples exhibit a peak corresponding to sulfite and a split peak associated with the (Na,Ca)$ SO_{4} $ sulfate. It is assumed that the splitting is caused by the ordering of the complexes not involved in the framework. This assumption is confirmed by the presence of a similar split peak in the X-ray photoelectron spectra of triclinic lazurite. It is demonstrated that the initial modulation is retained at the fugacity $$f_{SO_2 } = 8 \times 10^{ - 3} $$ bar. The decisive factors responsible for the retention of the three-dimensional incommensurate modulation are the temperature and the fugacity of sulfur dioxide. The latter quantity should be close to the stability boundary of the basic lazurite structure. The growth and transformation mechanisms of the modulation formation are conidered. © Pleiades Publishing, Inc. 2005 |
| abstractGer |
Abstract The stability of three-dimensional incommensurate modulation in cubic lazurite from the Ba$$\overset{\lower0.5em\hbox{$\smash{\scriptscriptstyle\smile}$}}{l} $$kal region is experimentally investigated at T = 600°C. It is found that the X-ray photoelectron spectra of the annealed samples exhibit a peak corresponding to sulfite and a split peak associated with the (Na,Ca)$ SO_{4} $ sulfate. It is assumed that the splitting is caused by the ordering of the complexes not involved in the framework. This assumption is confirmed by the presence of a similar split peak in the X-ray photoelectron spectra of triclinic lazurite. It is demonstrated that the initial modulation is retained at the fugacity $$f_{SO_2 } = 8 \times 10^{ - 3} $$ bar. The decisive factors responsible for the retention of the three-dimensional incommensurate modulation are the temperature and the fugacity of sulfur dioxide. The latter quantity should be close to the stability boundary of the basic lazurite structure. The growth and transformation mechanisms of the modulation formation are conidered. © Pleiades Publishing, Inc. 2005 |
| abstract_unstemmed |
Abstract The stability of three-dimensional incommensurate modulation in cubic lazurite from the Ba$$\overset{\lower0.5em\hbox{$\smash{\scriptscriptstyle\smile}$}}{l} $$kal region is experimentally investigated at T = 600°C. It is found that the X-ray photoelectron spectra of the annealed samples exhibit a peak corresponding to sulfite and a split peak associated with the (Na,Ca)$ SO_{4} $ sulfate. It is assumed that the splitting is caused by the ordering of the complexes not involved in the framework. This assumption is confirmed by the presence of a similar split peak in the X-ray photoelectron spectra of triclinic lazurite. It is demonstrated that the initial modulation is retained at the fugacity $$f_{SO_2 } = 8 \times 10^{ - 3} $$ bar. The decisive factors responsible for the retention of the three-dimensional incommensurate modulation are the temperature and the fugacity of sulfur dioxide. The latter quantity should be close to the stability boundary of the basic lazurite structure. The growth and transformation mechanisms of the modulation formation are conidered. © Pleiades Publishing, Inc. 2005 |
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Stability of the modulated structure of Ba$$\overset{\lower0.5em\hbox{$\smash{\scriptscriptstyle\smile}$}}{l} $$kal lazurite and its recrystallization at a temperature of 600°C over a wide range of sulfur dioxide fugacities |
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